SPME Applications Guide - Labicom

SUPELCO 

Bulletin 925E 

SPME Applications Guide 

The SPME Applications Guide is a bibliographic resource of published technical articles about solid phase microextraction. With the 

continued growth of SPME, and its expansion into environmental, food, forensic, and other fields, we recognize the need for an organized 

bibliography. This guide should serve a useful purpose in your SPME research and analyses. 

This guide is for general information only. We have made every attempt to make the information as complete and accurate as possible. 

Where entries are missing, information was not available at the time of printing. 

NOTE: Because of copyright restrictions, Supelco cannot provide copies of the articles listed. If you desire copies, please refer to the 

publications cited. 

Using This Guide 

This guide is organized in an easy-to-use format. The references are 

grouped into application areas (see the Table of Contents) with the 

over 600 new references placed at the end of each area in bold. The 

Analyte/Matrix column identifies the class of analytes and the 

sample matrix. The Literature Reference column provides the title of 

the article, journal reference, and authors. The next column describes 

the SPME fiber and conditions used in the sample extraction. 

The last column indicates the instrument used in the analysis. 

Key to Abbreviations 

Abbrev. Description 

AED atomic emission detection 

DVB divinylbenzene 

ECD electron capture detection 

FID flame ionization detection 

FPD flame photometric detection 

FTD flame thermonic detection 

GC gas chromatography 

HPLC high pressure liquid chromatography 

ICP inductive coupled plasma 

MS mass spectrometry 

MSD mass selective detection 

NPD nitrogen/phosphorus detection 

PAD photodiode-array detection 

PDMS polydimethylsiloxane 

PICI positive ion chemical ionization 

SIM selective ion monitoring 

TCD thermionic-selective detection 

TED thermal energy detection 

VIS visible spectrophotometry 

sigma-aldrich.com/supelco 

Table of Contents 

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email: supelco@sial.com 


Bulletin 925E 

Application Area 

Books .................................................................... 2 

Foods .................................................................... 2 

Polymers and Coatings .......................................... 48 

Natural Products .................................................... 51 

Pharmaceuticals .................................................... 65 

Biological Matrices ................................................. 67 

Toxicology ............................................................. 78 

Forensics ............................................................... 94 

Environmental ....................................................... 99 

Water .......................................................... 102 

Pesticides ..................................................... 138 

Soil .............................................................. 149 

Air ............................................................... 157 

Theory and Technique ......................................... 163 

Supelco SPME Literature ...................................... 181 

SPME Products .................................................... 182 

1

Books 

Foods 

SPME Application Guide 6th Edition 

(New references added to the 6th edition are in bold) SPME Fiber / 

Analyte / Extraction 

Matrix Literature Reference Conditions Instrument 

Techniques for Analyzing Food Aroma, Supelco Cat. # 26589-u 

Marcel Decker ISBN: 0-8247-9788-4, Marsili, R. 

Solid Phase Microextraction: A Practical Guide Supelco Cat. # 26610-u 

Edited by SueAnn Scheppers Wercinski 

Marcel Decker 15BN: 0-8247-7058-7 

Solid Phase Microextraction: Theory and Practice Supelco Cat. # 26591-u 

Edited by Janusz Pawliszyn 

VCH, New York, 275pp (1997) 

Applications of Solid Phase Microextraction Supelco Cat. # 26611-u 


RSC Chromatography Monographs ISBN 0-85404-525-2 

Royal Society of Chemistry 1999 

Applied SPME, 1999, 364-371 Royal Society of 

Chemistry, Cambridge, UK Coden: 67TUA8 

Talon, R, Montel, M. 

601 Aroma compounds Developments in extraction techniques and their Review article GC 

in food application to analysis of volatiles in foods 

Trends-Anal-Chem, May 2000, 19(5), 322-329 

Sides, S., Robards, K., Helliwell, S. 

602 Contaminants Application of SPME in Food Analysis Review article GC, LC, MS 

in Food J. Chromatogr. A (2000), 880(1+2), 35-62 

Kataok, H., Lord, H., Pawliszyn, J. 

784 Catechins, cafeine Automated in-tube solid phase microextraction coupled polypyrrole capillary LC-ES-MS 

in tes with HPLC-ES-MS for the determination of catechins 

and caffeine in tea 

Analyst (Cambridge, U. K.) (2000) 125(12), 2216-2222 

Wu, J. C.; Xie, W.; Pawliszyn, J. 

834 Caffeine Caffeine determination in beverages by SPME and GC-MS 

in beverages Ind. Bevande (2000) 29(170) 595-597, 605 

Guidotti, Maurizio; Panzironi, Laura 

8 Caffeine and flavors Solventless Determination of Caffeine in uncoated fiber GC-MS 

in coffee/tea/cola Beverages Using SPME with Fused Silica Fibers 

J. Chromatogr. 603: 185-191 (1992) 

Hawthorne, S., Miller, D., Arthur, C., Pawliszyn, J. 

5 min 

32 Flavors in Solid Phase Microextraction for Flavor Analysis 100µm PDMS GC/GC-MS 

coffee/fruit juice/ J. Agric. Food Chem, 42: 1925-1930 (1994) 10 min 

vegetable oil Peppard, T., Yang, X. 

603 Volatiles Analysis of volatile contaminants in vegetable oils by 75µm Carboxen/PDMS GC-MS 

in vegetable oil headspace SPME with Carboxen-based fibers. 30-45 min @ 100°C 

J. Chromatogr. 873 (2000): 79-94 

Page, B., Lacroix, G. 

headspace 

39 Halogenated volatiles Application of SPME to the Headspace GC Analysis of GC 

in food Halogenated Volatiles in Selected Foods 

J. Chromatogr. 648 (1): 199-211 (1993) 

Page, B., Lacroix, G. 

Ambient temperature, unless otherwise indicated. 2




41 Fatty acids C2-C10 Determination of Fatty Acids Using SPME 85µm polyacrylate GC/GC-MS 

in water Anal. Chem: 67(23): 4396-4403 (1995) Low pH, salt 

Pan, L., Adams, M., Pawliszyn, J. derivative: 1-pyrenediazomethane 

42 Flavors in Measuring Flavors Using SPME 100µm PDMS GC-MS 

corn oil Food Quality January/February 1995, pp40-41 

Mindrup, R. 

40°C, 45 min 

925 Flavors, off-flavors Sample preparation for the analysis of flavors and Review article 

in food off-flavors in foods 

J. Chromatogr A, 2000, 873(1), 3-11 

Wilkes, J., Conte, E., Kim, Y., Holcomb, M., Sutherland, J. 

Miller, D. 

883 Flavors in Recent application of SPME for monitoring flavor 75µm Carboxen/PDMS GC-MS 

food components in foods 

Food Testing & Analysis Feb./March 2000, 17-20 

Mindrup, R. 

65µm DVB/PDMS 

181 Flavors in SPME Associated with Microwave Assisted 100µm PDMS SIM GC-MS 

coffee, potato chips Extraction of Food Products pH 2, salt 

J. High Res. Chromatogr. 20 (4): 213-216 (1997) headspace 

Wang, Y., Bonella, M., Khaled, M., McNair, H. 10 min 

60 Sulfur volatiles in Headspace SPME Analysis of Volatile Organic Sulfur 

truffle aroma Compounds in Black and White Truffle Aroma 

J. Agric. Food Chem, 43 (8): 2138-2143 (1995) 

Pelusio, F., Nilsson, T., Tino, R., Larsen, B., Montnarell, L. 

830 Sulfur compounds Changes of aroma in shell eggs 

from egg shell Czech J. Food Sci (2000) 18, 231-233 

Adamiec, J.; Dolezal, M.; Mikova, K.; Davidek, J 

831 Sulfur compounds Limitations to the use of SPME for quantitation 

of mixtures of volatile organic sulfur compounds 

Anal. Chem (2001) 73(7) 1646-1649 

Murray, R. A. 

604 Aroma compounds Determination of major aroma impact compounds in 75µm Carboxen/PDMS GC-MS 

in fermented fermented cucumbers by SPME-GC-MS- 20min @50°C 

cucumbers Olfactometry detection 

J. Chromatogr. Sci. (2000), 38(7), 307-314 

Marsili, R., Miller, N. 

NaCl added 

61 Flavors in SPME of Flavor Compounds -- A Comparison of Two Fiber 100µm PDMS, GC-FID 

cinnamon bark Coatings and Discussion of the Rules of Thumb for Adsorption 85µm polyacrylate 

LC-GC 13 (11): 882-886 (1995) 120°C 

Yang, X., Peppard, T. headspace 

62 Flavors in SPME and Chiral Gas Chromatography Separations 100µm PDMS GC-FID 

apple essence, LC-GC 13 (9): 734-740 (1995) 30°C or 40°C 

seeds, candy Mani, V., Woolley, C. headspace 

772 Volatiles in Analysis of volatile constituents of mustard paste by GC/MS 100µm PDMS GC-MS 

mustard paste w/SPME and simultaneous distillation and extraction 

Fenxi Huaxue (2000) 28(12) 1489-1492 

30min @ 70°C 

Liu, B. in Chinese 





854 Volatiles in Analysis of the volatile components in vanilla extracts and 85µm polyacrylate GC-MS 

vanilla extracts flavourings by SPME and gas chromatography 

J Ag Food Chem (2000) 48(12), 5802-5807 

Sostaric, T.; Boyce, M. C.; Spickett, E. E. 

40min @20°C 

829 Volatiles of Analysis of headspace compounds of distillers grains using 75µm Carboxen/PDMS GC-MS 

distillers grains SPME in conjunction with GC/MS and TGA. 60min 

J Cereal Sci. (2001) 33(2), 223-229 

Staff, C., Biswas, S. 

headspace 

878 Essential oils in SPME of hop volatiles Potential use for determination and 100µm PDMS GC-MS 

hops verification of hop varieties 30min @ 70°C 

J. Chromatogr A 918 (2001) 159-167 

Kovacevic, M., Kac, M. 

headspace 

63 Essential oils in Determination of Essential Oils in Hops by Headspace SPME 100µm PDMS GC-FID 

hops J. Agric. Food. Chem, 44: 1768-1772 (1996) 

Field, J., Nickerson, G., James, D. Heider, C. 

50°C, 4 hr 

605 Essential oils Production of Yarrow (Achillea millefolium L.) in Norway: 100µm PDMS GC-MS 

in yarrow Essential Oil Content and Quality 40min @ 50°C 

J. Agric. Food Chem, (2000) 48 No,12, 6205-6209 

Rohloff, J., Skagen, E., Steen, A., Iversen, T. 

headspace 

221 Essential oils in A Comparison of Selected Analytical Approaches to the 100µm PDMS GC-MS 

Virginia cedar oil Analysis of an Essential Oil 10-120 sec 

Flavour and Fragrance Journal 12 (1): 1-8, (1997) 

Coleman, W., Lawrence, B. 

headspace 

396 Essential oils in Automatic Injection SPME-Chiral-GC-MSD Analysis of 7µm PDMS GC-MS 

Virginia cedar oil Essential Oils 6 sec 

J.Chromatographic Sci., Vol. 36, Dec. 1998, 575-578 headspace 

Coleman, W., Perfetti, T., Lawrence, B. stirring 

444 Volatiles in Identification of Volatile Compounds in Sunflower Oil 100µm PDMS GC-MS 

sunflower oil by Headspace SPME and Ion-Trap GC/MS 

J. High Resolut. Chromatgr. (1998), 46(7), 2744-2747 

Keszler, A., Heberger, K., Gude M. 

841 Volatiles in Mechanism of volatile compound production during storage 100µm PDMS GC-MS 

sunflower oil of sunflower oil 40 min @ 25°C 

J Ag Food Chem. (2000) 48(12), 5981-5985 

Keszler, A., Kiska, T. Nemeth, A.. 

headspace 

569 12 Aldehydes Influence of extraction parameters and medium on 100µm PDMS GC-MS 

in sunflower oil/water efficiency of SPME sampling in analysis of aliphatic aldehydes 30 min @ 40°C 

J-Chromatogram-A. 11 Jun 1999; 845(1-2): 337-347 

Keszler,-A; Heberger,-K 

headspace 

447 Xylene Determination of trace xylene in contaminated palm 100µm PDMS GC-FID 

in palm oil oil by SPME and capillary GC 1 min. 60°C 

Fenxi Huaxue (1999), 27(6), 676-678 headspace 

Chen, W., Guo, C., Hu, C. 

803 Volatiles Volatile compounds of virgin olive oil evaluated by SPME 

in olive oil An application in the discrimination of virgin olive oils 

according to the cultivar and area 

Proceedings of the Phytochemical Society of Europe 

(2000) Vol. 46, 211-220 

Servili, M; Montedoro, G; Selvaggini, R; Taticchi, A 

577 Dimetyl disulfide & Volatile reduced sulfur compounds in butter by SPME 85µm polyacrylate GC-EID 

methanethiol J-Dairy-Res. Feb 1999; 66(1): 115-123 10 min. @ 30-35°C 

in butter Shooter,-D; Jayatissa,-N; Renner,-N 





338 Benzene, toluene Determination of benzene & toluene in vegetable HPLC 

in vegetable oil oil by SPME/HPLC headspace 

J. Commod. Sci. (1999), 38(1), 3-14 

Giuffrida, R., Clasadonte, M., Zerbo, A. 

606 Volatiles Headspace SPME use for the Characterization of volatile Carboxen/DVB/PDMS GC-FID 

in vegetable oil compounds in vegetable oils of different sensory quality 20-60°C 

J. Agric Food Chem, (2000), 48(6), 2360-2367 headspace 

Jelen, H., Obuchowska, M., Zawirska-Wojtasiak, R. 

885 Steroisomers Different stereoselectivity in the reduction of pulegone GC-MS 

Pulegone enantiomers by Mentha species 

Planta Medica (2001) 67(3) 260-262 

Mosandl, A.; Beck, T.; Fuchs, S. 

106 Flavors in Characterization of Beer Samples Using SPME-GC Analysis 100µm PDMS GC-FID 

beer Supelco Reporter Vol. 16, #4, pg. 7 

Vas, G. 

10 min 

607 Sulfur compounds Determination of sulfur compounds in beer using headspace 65µm Carboxen/PDMS GC-FPD 

in beer SPME and GC analysis with pulsed FPD detector 32min @45°C 

J. Chromatogr. A. (2000), 872(1+2), 203-213 

Hill, P., Smith, R. 

headspace 

100 Flavors Characterization of Commercial Vodkas by SPME-GC/MS 100µm PDMS GC-MS 

in vodka J. Sci. Food Agric. 70: 380-388 (1996) 

Ng, L., Hupe, M., Harnois, J., Moccia, D. 

1 hr 

202 Methylcyclopendienyl Determination of Methylcyclopendienyl Manganese Tricarbonyl 

manganese in Beverages by SPME 

tricarbonyl Food Addit. Contam. 14 (3): 301-307 (1997) 

in beverages Forsyth, D., Dusseault, L. 

395 Aroma volatiles Determination of Fresh Onion (Allium Cepa L) Volatiles 100µm PDMS GC-MS 

in onion by SPME Combined with GC/MS 1 min 

Z Lebedsm Unters Forsch A (1998) 207: 39-43 

Jarvedpaa, E., Zhung, Z., Huopalahti, R., King, J. 

headspace 

799 Aroma volatiles Possible advantage of various sample transfer techniques 100µm PDMS, GC-MS 

in onion for fast GC-MS analysis of true onion volatiles polyacrylate 

J. Chromatogr. A. (2000), 896(1+2), 117-124 2min, headspace 

Arnault, I.; Mondy, N.; Cadoux, F.; Auger, J. 

954 Fatty acids, Analysis of free fatty acids in whey products by SPME 30µm PDMS GC-FID 

in whey products J Agric Food Chem, 2001, 49, 3993-3998 40 min @ 110°C 

Tomaino, R., Parker, J., Larick, D. headspace 

816 Fatty acids, lactones Determination of free fatty acids and lactones in cheese 

in cheese by solid phase microextraction (SPME) 

Aust. J. Dairy Technol.,(1998), 53(2), 140 

Wijesundera, C., Drury, L., Walsh, T. 

101 Flavors SPME for Cheese Volatile Compound Analysis 100µm PDMS, GC, GC-MS 

in cheese J. Food Sci. 61: 1118-1129 (1996) polyacrylate 

Chin, H., Bernhard, R., Rosenberg, M. 60°C, 20 min 

788 Volatilse Solid-Phase Microextraction-Mass Spectrometry: A New GC-MS 

in cheese Approach to the Rapid Characterization of Cheeses 

Anal. Chem (2001) 73(5), 1030-1036 

Peres, Christophe; Viallon, Christine; Berdague, Jean-Louis 

826 Volatiles in Use of preconcentration techniques applied to a Mass GC-MS 

Emmital cheese Spectrometer based "Electronic Nose". 

Analusis (2000) 28(8), 743-749 

Bosset, J.; Escher, F.; Schaller, E.; Zenhausern, S.; Zesiger, T. 





380 Aroma volatiles Pattern Recognition of Swiss Cheese Aroma Compounds by 85µm polyacrylate GC-FID 

in cheese SPME/GC and an Electronic Nose 40°C, 30 min 

Milchwissenscaft (1998) 53 (5) 259-263 

Jou, K., Harper, W. 

headspace 

449 Aroma volatiles Cryo-trapping/SPME/GC analysis of cheese aroma 100µm PDMS GC-FID, EMS 

in cheese Talanta (1999) 48(4), 747-753 4 min @ 20°C 

Jaillais, B., Bertrand, V., Auger, J. headspace 

187 Volatiles in A Study of Volatile "Trapping" in Spray-Dried Whey Protein GC-MS 

whey protein Concentrate by Crushing and/or Vacuuming and Detection 

by SPME/GC-MS 

Food Res. Int. 29: 495-504 (1996) 

Stevenson, R., Chen, X. 

379 Volatiles in Use of SPME of Volatile Compounds in Whey Protein 85µm polyacrylate GC-MS 

whey protein Concentrates 40°C, 30 min 

Milchwissenschaft (1998) 53 (4) 209-212 

Yang, J., Li, W., Harper, W. 

headspace, stirring 

450 Volatiles in Headspace sampling of whey protein concentrate GC-MS 

whey protein solutions using SPME headspace 

Food Res. Int. (1999), 31(5), 371-379 

Le Quanch, M., Chen, X., Stevenson, R. 

422 Flavors in Isolation of Flavor Compounds from Protein Material 

protein ACS Symp. Ser. (1998), 705 (Flavor Analysis), 107-115 

Mills, O., Broome, A. 

102 Flavors in Qualitative and Quantitative Analysis of Flavor Carbowax/DVB GC-MS 

tobacco Additives on Tobacco Products Using SPME-GC-MS 95°C, 15 min 

J. Agric. Food Chem. 45: 844-849 (1997) 

Clark, J., Bunch, J. 

headspace 

137 Phenols in Quantitative Determination of Phenols in Mainstream Smoke Polyacrylate GC-MS 

tobacco smoke with SPME-GC Selected Ion Monitoring MS 

J. Chromatogr. Sci. 34: 272-275 (1996) 


Buffer, 1 hr 

608 Acetates Quantitative analysis of acetates in cigarette tobacco 75µm Carboxen/PDMS GC-MS 

in Cigarette tobacco using SPME and GC-MS 


Watxon, C., Ashley, D. 

5min. Headspace 

369 Carboxylic acid esters Derivatization of SPME GC-MS Determination of 85µm polyacrylate GC-MS 

in tobacco Organic Acids in Tobacco 15 min, stirring 

J. Chromatographic Science, Vol. 35, (1997) 209-212 


MeOH-HCl derivatives 

822 Alkenylbenzenes SPME of alkenylbenzenes and other flavor-related 65µm Carbowax/DVB GC-MS 

flavor compounds compounds from tobacco for analysis by selected ion 2min @ 95°C 

in tobacco monitoring GC-MS 

J. Chromatogr.A, 858 (1999) 79-89 

Stanfill, S., Ashley, D. 

931 Pesticide residues SPME applied to the analysis of pesticide residues 100µm PDMS, GC-ECD 

in honey in honey using GC with ECD 60min @ 70°C 

J. Chromatogr. A (1998), 829(1-2), 269-277 immersed 

Jiméniz, J., Bernal, J., del Nozal, G., Martin, M., Mayorga, A. agitated 





431 Phenols in Application of SPME in Determination of Phenol in Honey 

honey Riv. Sci. Aliment, (1997) 26(3/4), 97-102 

Conte, L., Botolomeazzi, R., Moret, S., Sibaini, A., 

Marcazzan, G. 

433 Volatile organics Identification of Volatile Organic Compounds Present GC-MS 

in honey in Different Honeys Through SPME and GC/MS 

Ind. Alimenti., (1998), 37(368), 351-356 

Guidotti, M., Vitali, M. 

109 Aroma volatiles in Comparison of Dynamic Headspace Concentration 100µm PDMS, GC-MS 

carbonated cola on Tenax with SPME for Analysis of Aroma Volatiles 85µm polyacrylate 

beverages J. Agric. Food Chem. 45: 2638-2641 (1997) 60°C, 30 min 

Elmore, S., Erbahdir, M., Mottram, D. headspace 

349 Aroma volatiles in SPME Applications in Gas Chromatography Olfactometry 100µm, 30µm, 7µm PDMS GC-FID 

brewed coffee Dilution Analysis 1-90 min 

J. Agric. Food Chem. 1999, 47, 1616-1618 

Deibler, K., Acree, T., Lavin, E. 


119 Aroma in Solid Phase Microextraction: A Valuable Problem Solver various fibers & 

food products Food Product Design December 1996, pp 73-77 

Marsili, R. 

extraction conditions 

128 Flavor volatiles in Analysis of Flavor Volatiles Using Headspace SPME 85µm polyacrylate GC-FID 

fruit juice J. Agric. Food Chem. 44: 2187 (1997) 60 min, salt added 

Steffen, A., Pawliszyn, J. headspace, stirring 

609 Aroma compounds Screening of Brazilian fruit aromas using SPME-GC-MS various fibers GC-MS 

in Brazilian fruit J. Chromatogr. A.,873(1), 117-127 headspace 

Augusto, F., Valenta, A., dosSantos, T., Rivellino, S. 

425 Volatiles Analysis of Volatile Fruit Components by Headspace 100µm PDMS GC-MS 

in fruit Solid Phase Microextraction 30 min @ 30°C 

Food Chem. (1998), 63(2), 281-286 

Ibanez, E., Lopez-Sebastian, S., Ramos, E., Tabera, J. 

Reglero, G. 

headspace 

872 Phenolics Sample preparation in the determination of phenolic review article 

in fruits compounds in fruits 

Analyst (Cambridge, U. K.) (2000) 125(5) 989-1009 

Antolovich, M.; Prenzler, P.; Robards, K.; Ryan, D. 

130 Flavor volatiles in Flavor Volatiles in Fruit Beverage with Automated SPME 100µm PDMS, GC-FID 

fruit beverage Food Test. Anal, 2(3), pp16-18 (1996) 85µm polyacrylate 

Penton, Z. 20 min, headspace 

424 Oxidative byproducts Changes in Citrus Hystrix Oil During Autoxidation 

in citrus hystrix oil Dev. Food Sci. (1998), 40 (Food Flavors: Formation, 

Analysis and Packaging Influences), 707-718 

Pudil, F., Wijaya, H., Janda, V., Volfova, J., Valentova, H., 

Porkorny, J. 

893 Monoterpenes Degradation of monoterpenes in orange juice 100µm PDMS GC-MSD 

in orange juice by gamma radiation 60°C, 20 min 

J. Ag Food Chem. (2001) 49(5) 2422-2426 

Fan, Xuetong; Gates, Robert A 


358 Flavor compounds Optimization of SPME Analysis for Headspace 100µm PDMS GC-FID 

in orange juice Flavor Compounds of Orange Juice 60°C, 20 min 


Jia, M., Zhang, H., Min, D. 






451 Flavor compounds Pulsed electric field processing effects on flavor 

in orange juice compounds and microorganism of orange juice 

Food Chem (1999), 65(4), 445-451 

Jia, M., Zhang, Q, Min, D. 

561 Flavor compounds Volatiles from Unpasteurized and Excessively 75µm Carboxen/PDMS GC-MS 

in orange juice heated orange juice with SPME and 30 min Headspace 

GC Olfactometry 40°C 

J. Food Science, Vol.64, N0.5, 1999, 800-803 

Bazemore, R., Goodner, K. Rouseff, R. 

359 Flavors in Comparison of Gas-Sampled and SPME-Sampled Static 65µm PDMS/DVB GC-MS 

fruit juices Headspace for the Determination of Volatile Flavor Compounds 40°C, 30 min 

Anal. Chem. Vol. 71, No. 1, January 1, 1999, pg 23-27 

Miller, M., Stuart, J. 

headspace 

131 Flavor volatiles Solid Phase Microextraction for Quantitative 100µm PDMS GC-MS 

in apples Headspace Sampling of Apple Volatiles 30 min 

Anal. Chem. 68: 4114 (1996) 

Matich, A., Rowan, D., Banks, N. 

headspace 

203 Flavor volatiles Rapid Analysis of Volatile Flavor Compounds in 100µm PDMS GC-FID 

In apples Apple Fruit Using SPME & GC-Time-of-Flight Mass Spec 2-8 min 


Song, J., Gardner, B., Holand, J., Beaudry, R. 

headspace 

433 Volatiles in Volatile Production and Fruit Quality During Development 

red delicious apples of Superficial Scald in Red Delicious Apples 

Food Res. Int. (1997), 30(2), 95-103 

Paliyath, G., Whiting, M., Stasiak, M., Murr, D., Clegg, G. 

899 Aroma compounds Influence of packaging on the aroma stability of strawberry 100µm PDMS GC-FID 

in strawberries syrup during shelf life 60 min @ 50°C 

J. Agric. Food Chem. 49(5): 2290-2297 (2001) headspace 

Ducruet, V Feigenbaum, A; Fournier, N; Guichard, E; Saillard, P. agitated 

383 Flavor volatiles in Application of SPME and GC/Time-o-Flight Mass 65µm PDMS/DVB GC-MS 

tomato, strawberry Spectrometry for Rapid Analysis of Flavor Volatiles 23°C, 12 min 

in Tomato and Strawberry Fruits 


Song, J., Fan, L., Beaudry, R. 

headspace 

452 Flavor volatiles in A new concept for the measurement of total 

tomato, strawberry, volatile compounds of food 

raspberries, apples Z. Lebenam. Unters, Forsch A, 1999, 208(4), 254-258 

Azodanlou, R., Darbellay, c., Luisier, J., 

Villettaz,J., Amode, R. 

387 Flavor volatiles Comparison of Three Sample Preparation Techniques for the 100µm PDMS GC-MS 

in tomato Determination of Fresh Tomato Aroma Volatiles 30°C, 10 min 

Book: Flavor Science: Recent Developments, Buttery & headspace 

Shadhidi, Washington, DC, 1998 p. 289-292 

Krumbein, A., Ulrich, D. 

salt added 

766 Volatiles Volatile emissions of tomato 

in tomato Mededelingen Faculteit Landbouwkundige en Toegepaste 

Biologische Wetenschappen Universiteit Gent 

(1999) 64(4), 159-161 

Maes, K; Debergh, P; Sandra, P; Vercammen, J 

headspace 





933 Volatiles Critical aspects for the reliable headspace analysis of plants 

in tomato cultivated in vitro 

Phytochemical Analysis (2001) 12(3), 153-158 

Maes, K; Debergh, P; Sandra, P; Vercammen, J 

Pham-Tuan, Hai 

headspace 

400 Flavor volatiles Effect of Thermal Treatment in the Headspace Volatile 65µm Carbowax/DVB GC-MS 

in tomato juice Compounds of Tomato Juice 35°C, 30 min 

Istituto di Indstrie Agrarie, University of Perugi, via S. 

Costnazo I-06126, Pergia-Italy 

Servili, M., Selvaggini, R., Begliomini, A., Montedoro, G. 

CaCl added 

780 Flavor volatiles Relationships between the volatile compounds evaluated by 65µm Carbowax/DVB GC-EIMS 

in tomato juice SPME and the thermal treatment of tomato juice: 

optimization of the blanching parameters 

Food Chemistry (2000) 71(3), 407-415 

Servili, M.; Selvaggini, R.; Taticchi, A.; 

Begliomini, A. L.; Montedoro, G. 

29°C, 15 min 

214 Strawberries & apples Solid-Phase Microextraction: Artifact Formation and Its 85µm polyacrylate GC-MS 

in fruit homogenate Avoidance 30 sec 

Chromatographia 46: 63-66 (1997) 

Verhoeven, H., Beuerle, T., Schwab, W. 

immersion 

132 Aroma volatiles Analysis of Strawberry Aroma by SPME 

in strawberry Dtsch. Lebesm - Rundsch. 91: 349 (1995) 

Ulrich, D., Eunert, S., Hober, E., Rapp, E. 

590 Aroma volatiles A new concept for the measurement of total volatile PDMS, CW/DVB, PDMS/DVB GC-FID 

in strawberries compounds of food. polyacrylate 

Z-Lebensm-Unters-Forsch-A. Apr 1999; 208(4): 254-258 30 min @ 25°C 

Azodanlou-R; Darbellay,C; Luisier,JL; Villettaz,JC; Amado,R headspace 

133 Aroma volatiles Evaluation of the Solid Phase Microextraction of 

in banana Aroma Compounds in Banana 

Collog.-Inst. Nat. Rech. Agron. 75 (Bioflavour 95) 117 (1995) 

Picque, D., Normand, A., Corrieu, G. 

750 Flavor volatiles Identification of volatile coumpounds in cantaloupe at 100µm PDMS GC-MS 

in cantaloupe various developmental stages using SPME 12.5 min headspace 

J Agric Food Chem 2001, 49(3), 1345-1352 

Beaulieu, J., Grimm, C. 

sat. salt, agitated 

150 Pyrazines SPME of Pyrazines in Model Reaction Systems 

J. Sci. Food Agric. 72: 91 (1996) 

Ibanez, E., Bernhard, R. 

934 Pyrazines Solid-phase microextraction with aqueous immersion for 

analysis of Maillard-generated pyrazines in model reaction 

system 

Diss. Abstr. Int., B 2000, 61(5), 2287 

Cai, Yanxuan 

356 Menthol SPME-GC-Mass Selective Detection Analysis of Selected 65µm Carboxen/PDMS GC-MS 

(natural) Sources of Menthol 50°C, 20 sec 

J. Chromatogr. Sci. (1998), 36(8) 401-405 

Coleman, W., Lawson, S. 

headspace 

453 Menthol, menthone Determination of menthol and menthone in food and ethoxy dimethylsiloxane GC-FID 

food/pharmaceutical pharmaceutical products by SPME-GC 15 min @ 30°C 

J. Chromatogr., A 1999, 847 (1+2), 161-169 

Ligor, M., Buszewski, B. 

immersed 





610 Aroma Measurement of gas-liquid partition coefficient and 7µm PDMS GC-MS 

in perfume headspace concentration profiles of perfume materials 10 min headspace 

by SPME and capillary GC-MS 


Liu, Z. Wene, M. 

611 Flavor compounds Contribution of volatiles to the flavor of oatmeal 100µm PDMS GC-MS 

in oatmeal J. Sci Food Agric.1/15/2000, 80(2);, 247-254 water solution @ 100°C 

Zhou, M, Robards, K., Helliwell, S., Glennie-Hommes, M. headspace 

894 Flavor compounds Changes in the volatile profile of oats induced by processing 100µm PDMS GC-MS 

in oats J. Agric. Food Chem. 49 (5): 2125-2130 (2001) 30SEC @ 25°c 

Robards, Kevin; An, Min; Helliwell, Stuart; Sides, Alasdair headspace 

309 Flavors in SPME for the Analysis of Flavors various fibers 

food products Techniques for Analyzing Food Aroma, pp81-112, 

Food Sci. Technol., New York (1997) 

Harmon, A. 

& conditions 

388 Volatiles in Analysis of Volatile Fragrance and Flavor Compounds by 100µm PDMS GC-MS 

consumer products Headspace SPME Combined with Gas Chromatography/ 30 min 

Mass Spectrometry 

J. Chem. Educ. 1999, 76(2), 245-248 

Galipo, R., Canhoto, A., Walla, M., Morgan, S. 

headspace 

760 Flavor volatiles Solid Phase Microextraction for the enantiometric analysis of 85µm Polyacrylate GC-MS 

in beverages Flavors in Beverages 60 min., headspace 

J. AOAC Intl, Vol. 84, No. 2, 2001, 479-485 

Ebeler, S., Sun, G., Datta, M., Stremple, P., Vicker, A. 

salt added 

891 Volatile carbonyls Comparison of extraction techniques for GC GC-ECD 

in alcoholS determination of volatile carbonyl compounds in alcohols. 

Fresenius' J.Anal Chem. (2001) 369(7-8) 661-665 

Wardencki, W; Namiesnik, J; Orlita, J. PFBHA derivatives 

903 Carbonyls Determination of carbonyl compounds in water by GC 

in water derivatization SPME and GC analysis 

J. Chromatography A 1998, 809, 1-2, 75-87 

Bao,M., Pantani,F.,Griffini,O.,Burrini,D.,Santianni, D., Barbieri, K. 

454 Organic content Research on alcoholic beverages at Alko's control Lab GC-MS 

in alcoholic Kem.-Kemi, 1999, 26(2), 95-97 

beverage Lehtonen, P. Finnish 

455 Alcohols, esters, free Analysis of free fatty acids, higher alcohols and 

fatty acids esters in sake by headspace-SPME 

in Sake Nippon Jozo Kyokaishi (1999), 94(3), 252-257 Japanese 

Utsunomiya, H. 

312 Flavor volatiles in Headspace Gas Chromatography Profiles of Fruit-Flavored 100µm PDMS GD-FID 

malt beverages Malt Beverages, Using SPME 45°C, 45-60 min 

J. Am. Soc. Brew. Chem. 55 (3): 112-118 (1997) 

Constant, M., Collier, J. 

headspace 

313 Alcohols, esters Solid Phase Microextraction for the Analysis of Some 85µm polyacrylate GC-FID 

in beer Alcohols and Esters in Beer: Comparison with Static 50°C, 30 min 

Headspace Method headspace 

J. Agric. Food Chem. 46 (4): 1469-1473 (1998) 

Wasowicz, E., Kaminski, E., Jelen, H., Wlazly, K. 

salt added 

456 Dimethyl sulfide Headspace SPME for the analysis of dimethyl 65µm Carboxen/PDMS GC-FPD 

in beer sulfide from beer 15 min @ 30°C 

J. Agric. Food Chem. 1999, 47(7), 2505-2508 headspace 

Scarlata, C. Ebeler, S. 1.5gm NaCl 





612 Volatiles in Characterization of whiskIes using SPME with GC-MS 85µm polyacrylate GC-MS 

whiskies J.Chromatogr. A (2000) 896, 351-359 35 min 

Fitzgerald, G., James, K., MacNamara, K., Stack, M. headspace 

953 Volatiles A headspace SPME method for the determination of some 85µm polyacrylate GC-FID 

in sugar cane spirits secondary compounds of Brazilian sugar cane spirits by GC 25 min @ 60°C 

J Agric Food Chem, 2001, 49, 3533-3539 headspace 

Nonato, E., Carazza, F., Silva, C. Carvalho, C., Cardeal, Z. 2.5g NaCl 

595 Aroma volatiles Changes in odor of Bartlett pear brandy influenced by 100µm PDMS GC-EIMS 

in Brandy sunlight irradiation. 15 min @ 40°C 

Chemosphere. Mar 1999; 38(6): 1299-1303 

Kralj-Cigic,-I; Zupancic-Kralj,-L 

613 Aroma compounds Analysis of brandy aroma by SPME and liquid-liquid extraction 100µm PDMS GC-FID 

in brandy J. Sci. Food Agric. Apr 2000, 80(5), 625-630 30 min @ 50°C 

Ebeler, S., Terrien, M., Butzka, C. Headspace 

827 Aroma volatiles Optimization of headspace SPME for analysis of wine 

in wine aroma compounds 

Am Journal Enology and Viticul (2000) 51(4), 379-382 headspace 

Zoecklein, B. W.; Whiton, R. S 

901 Aroma volatiles Discrimination of wine aroma using an array of conducting 

in wine polymer sensors in conjunction with SPME technique 

Sens Actuators, B Chem (2001) 77(1-2), 401-408 

De Saja, J.A.; Fernandez, J.A.; Guadarrama, A.; Iniguez, M.; Souto, J 

896 Aroma volatiles Effect of cultural practices and environmental factors on GC-MS 

in wine fruit and wine quality 

Agriculturae Conspectus Scientificus 2001 66(1) 13-20 

Bravdo, Ben Ami 

135 Aroma volatiles Systematic Optimization of the Analysis of Wine Bouquet 85µm polyacrylate GC-FID 

in wine Components by SPME 15 min 

J. High Res. Chromatogr. 19: 257-262( 1996) immersion, stirring 

Garcia, D., Magnaghi, S., Danzer, K. pH 4, salt added 

798 trans-ResverAtrol Gas-phase post-derivatization following SPME for rapid GC-MS 

in wine determination of trans -resveratrol in wine by GC-MS 22°C 

Analytica Chimica Acta (2000) 424(1), 19-25 headspace 

Luan, T. G.; Li, G. K.; Zhang, Z. X. silyl derivative 

201 Procymidone residue Comparison of Two Recent Solventless Methods for the 100µm PDMS GC-MS 

in wine Determination of Procymidone Residues in Wines: 30 min 

Solid-Phase Microextraction-GC-MS and ELISA Tests immersion 


Urruty, L., Montury, M., Braci, M., Fournier, J., Dournel, J. 

stirring 

936 Aroma volatiles Qualitative and quantitative analyses of volatile organic 

in wine compounds in wines using SPME-GC 

Chem. Anal. (Warsaw, Pol.) (2001) 46(2) 215-224 

Buszewski, B; Ligor, M. 

314 Aroma volatiles Investigation of Wine Bouquet Components by SPME- 85µm polyacrylate GC-FID 

in wine Capillary GC, Using Different Fibers 30 min 

J. High Resolut. Chromatogr. 20 (12): 665-668 (1997) immersion 

De La Calle Garcia, D., Feller, K., Reichbacher, M., 

Danzer, K., Hurlbeck, C., Bartzech, C. 

stirring 

428 Aroma volatiles Analysis of Wine Bouquet Components Using Headspace 85µm polyacrylate GC-MS 

in wine SPME-Capillary Gas Chromatography 60 min 

J. High Resolut. Chromatogr. (1998), 21(7), 373-377 headspace 

De La Calle Garcia, D., Feller, K., Reichbacher, M., Danzer, K., stirring 

Hurlbeck, C., Bartzech, C. salt added 





824 Aroma volatiles Classification of wine samples according to origin and 85µm polyacrylate GC-MS 

in wine grape varieties on the basis of inorganic and organic 60 min 

trace analysis headspace 

American Lab, Oct. 1999, Vol. 31(20) 26-33 stirring 

Danzier, K., De La Calle Garcia, D., Thiel, G., Reichbacher, M., salt added 

94 Trichloroanisole Analysis of Cork Taint in Wine and Cork Material at 100µm PDMS SIM-GC-MS 

in wine Olfactory Sub-Threshold Levels by SPME 20°C, 30 min 


Fisher, C., Fischer, U. 

salt added 

385 Trichloroanisole Detection of Cork Taint in Wine Using Automated SPME in 100µm PDMS, GC-MS-SIM 

in wine Combination with GC-MS-SIM 85µm polyacrylate 

Book chapter 15: ACS Symposium Series 1999, Oxford 45°C, 25 min 

University Press, "Flavor Analysis Development in 

Isolation and Characterization" 

Butzke, C., Evans, T., Ebeler, S. 

headspace 

377 Sulfides, disulfides Headspace SPME Analysis of Volatile Sulfides and 100µm PDMS, GC-FPD 

in wine Disulfides in Wine Aroma 85µm polyacrylate 

J. Chromatogr. A 808 (1998) 211-218 30°C, 15 min, salt 

Mestres, M., Busto, O., Guasch, J. headspace 

406 Sulfides, disulfides Headspace SPME of Sulfides and Disulfides Using 75µm Carboxen/PDMS GC-FPD 

in wine Carboxen/PDMS Fibers in the Analysis of Wine Aroma 25°C, 30 min 

J. Chromatogr. A, 835 (1999) 137-144 headspace 

Mestres, M., Sala, C., Marit, M., Busto, O., Guasch, J. stirring, salt added 

614 Benzothiazoles Analysis of benzothiazole in Italian wines using 65µm Carbowax/DVB GC-MS 

in wine SPME-GC-MS 15min @ 50°C 

J. Agric. Food Chem. (2000), 48(4), 1239-1242 headspace 

Bellavia, V., Natangelo, M., Fanelli, R., Rotilio, D. 

363 Aroma volatiles Similarities in the Aroma Chemistry of Gewurztraminer 100µm PDMS GC-MS 

in wine Variety of Wines and Lychee (Litchi chinesis Sonn.) Fruit 15 min 

J. Agri. Food Chem. 1999, 47, 665-670 

Ong, P., Acrees, T. 

headspace 

427 Volatiles Fast Screening Method for Wine Headspace Compounds headspace 

in wine Using SPME and Capillary GC Technique 

Am. J. Enol. Vitic. (1998), 49(1), 100-104 

Vas, G., Koteleky, K., Farkas, M., Ddobo, A., Vekey, K. 

397 Aroma volatiles Determination of Volatile Aroma Compounds of 100µm PDMS GC-MS 

in wine Blaufrankisch Wines Extracted by SPME 10 min (headspace) 

J. Chromatographic Sci., Vol. 36, Oct. 1998, 505-510 

Vas, G., Gal, L., Harangi, J., Dobo, A., Vekey, K. 

1 hr (immersion) 

457 Flavor volatiles Classification of wine samples according to origin 85µm polyacrylate GC-FID 

in wine and grape varieties on the basis of inorganic and 60-90 min 

organic trace analysis headspace 

Am. Laboratory, Oct. 1999, Vol. 31, No. 20, 26-34 Satr.salt 

Danzier, K, DeLaCalle Garcia, D, Thiel, G., 

Reichenbacher, M 

458 Aroma volatiles Examination of aroma production kinetics of 100µm PDMS GC-FID 

in wine different commercial wine yeast in fermenting 10 min 

muscat ottonel wines with the help of SPME 

headspace sampling and fast GC analysis 

Acta Aliment, (1999), 28(2), 133-140 

Vaes, W., Blechschmidt, I., Kovacs, T., Vekey, K. 

headspace 





582 Aroma volatiles Improvement of the chemometric variety characterization of 85µm polyacrylate GC-EMIS 

in wine wines by improving the detection limit for aroma compound 3 hr. , headspace 

J-High-Resolut-Chromatogr. Jun 1999; 22(6): 322-326 

Weber,-J; Beeg,-M; Bartzsch,-C; Feller,-K-H; 

De-la-Calle-Garcia,-D; Reichenbaecher,-M; Danzer,-M 

NaCl added 

459 Aroma volatiles Determination of volatiles from red wines made 100µm PDMS GC-EIMS 

in wine by carbonic maceration using SPME technique 

Acta Aliment, 1999, 28(1), 95-101 

Vas, G., Loerincz, G. 

10 min headspace 

559 Aroma volatiles Monitoring Toasting Intensity of Barrels by 100µm PDMS GC-FID 

from toasted oak Chromatographic Analysis of Volatile 30 min @ 22°C 

compounds from Toasted Oak Wood 

J. Agric. Food Chem, 1999, 47, 4310-4318 headspace 

Chatonnet, P., Cutzach, I., Pons, M., Dubourdieu, D. 

460 Polyphenolics Assembly tests of "Nero d'Avola" with wines GC-MS 

in red wine derived from an allocthonous cultivar: headspace 

study of polyphenolic and aromatic profiles. Italian 

Ind. Bevande (1999), 28(160), 119-126 

Papucci, A, Monte, L., D'Agostino, S, 

Aozzino, P., Avellone, G 

775 Esters Monitoring ester formation in grape juice fermentations 100µm PDMS GC-MS 

in grape juice using SPME coupled with GC-MS 1 hr. 

J. Agric. Food Chem (2001) 49(2), 589-595 headspace 

Vianna, E; Ebeler, S. 

315 Styrene Determination of Styrene in Wine by SPME and GC-MS GC-MS 

in wine Mitt. Klosterneuburg 47 (4): 117-123 (1997) 

Flak, W., Tscheik, G. 

311 Methylisocyanate SPME Analysis of Methyl Isothiocyanate in Wine 65µm Carbowax/DVB GC-FID, NPD 

in wine J. Agric. Food Chem. 45 (8): 3092-3094 (1997) 30 min 

Gandini, N., Riguzzi, R. headspace 

salt added 

366 Diacetyl Analysis of Diacetyl in Wine Using SPME -GC-MS 60µm Carbowax/DVB GC-MS 

in wine J. Agric Food Chem. 1999, 47, 612-617 24°C, 5 min 

Hayasaka, Y., Bartowsky, E. headspace 

salt added 

316 Pesticides Determination of Pesticide Residues in Wine by SPME and GC-MS 

in Wine GC/MS for Consumer Risk Assessment 

Food Addit. Contam. 15 (3): 280-287 (1998) 

Vitali, M., Guidotti, M., Giovinazao, R., Cendrone, O. 

615 Pesticide residue Applications of SPME to the Analysis of 100µm PDMS, GC-ECD 

on vegetables Pesticide Residues in Vegetables 60µm Carbowax/DVB GC-NPD 

Pest. Manag Sci 56: 618-636 (2000) 

Volante, M.,Pontello, M., Volante, L. Cattaneo, M., Bianchi, M., 

Bianchi, M., Colzani, L. 

50 min 

774 Pesticide residue Study on the method of SPME coupled to GC for 

on vegetables determination of organophosphorus pesticide residue 

in vegetables. 

Ziran Kexueban (2000) 39(4), 509-515 

Chen, W; Hou, X; Zhang, L; Lin, H; Pan, Ji (in Chinese) 

432 Pesticides in Some Applications of SPME in the Analysis of 

food Pesticide Residues in Food 

J. Environ. Sci. Health, Part B (1998), B33 (3), 279-292 

Volante, M.,Cattaneo, M., Bianchi, M., Zoccola, G. 





461 Pesticides SPME of pesticide residues from strawberries 100µm PDMS 

on strawberries Food Addit. Contam. (1999), 16(3), 111-117 45 min @ 25°C 

Hut, R., Henniont, B., Urrutyt, L., Monturyt, M. 

783 Pesticides SPME coupled with HPLC: a complementry technique to SPME 60µm PDMS/DVB LC-UV 

on strawberries GC for the analysis of pesticide residues in strawberries 45 min @ 25°C 

Food Addit. Contam. (2000), 17(11), 915-923 headspace 

Wang, Z.; Hennion, B.; Urruty, L.; Montury, M. 

462 Organophosphorus Validation of a SPME method for the 100µm PDMS GC-FPD 

pesticides in determination of organophosphorus pesticides 3 min 

fruit/fruit juices in fruits and fruit juice immersed 

J. Chromatogr. A (1999), 843(1), 35-42 

Simplicio, A, Vilas Boas, L. 

929 Organophosphorus Determination of organophosphorus pesticides in honeybees 85µm Polyacrylate GC-NPD 

pesticides in after solid phase microextraction 45min @ 25°C 

honeybees J. Chromatogr. A (2001), 922(1-2) 257-265 immersed 

Fernandez, M., Padron, C., Marconi, L., Colombo, R. Ghinie, S. stirred 

Sabatini, A, Girotti, S. 

463 Organochlorine & A Systematic Approach to Optimize SPME 

organophosphorus determination of Pesticides in Ethanol/Water 

in water/ethanol mixtures used as Food Simulates 

Anal. Chem. (1999), 71(13), 2417-2422 

Batlle, R, Sanchez, C., Nerin, C. 

616 Volatiles Evidence for selectivity of absorption of volatile organics 30µm PDMS GC-MS 

in water compounds by PDMS SPME fiber 60min 

J. Chromatogr. A,(2000) 885, 457-464 

Niedziella, S., Rudkin, S., Cooke, M. 

headspace 

317 Aroma volatiles Analysis of Aroma Release During Microwave Heating 60µm Carbowax/DVB GC-FID 

in water traps J. Agric. Food Chem. 45 (11): 4388-4392 (1997) 10 min 

Roberts, D., Pollien, R. immersion, stirring 

435 Aroma volatiles SPME Associated with Microwave Assisted Extraction of 

in food products Food Products 

J. High Resolut. Chromatogr. (1997), 20(4), 213-216 

Wang, Y., Bonilla, M., McNari, H., Khaled, M. 

318 N-nitrosamines Rapid Semi-Quantitative Estimation of N-Nitrosodibulylamine 85µm polyacrylate GC-thermal 

in smoked hams and N-Nitrosodibenzylamine in Smoked Hams by SPME 10 min energy or MS 

Followed by GC-Thermal Energy Analysis headspace 

J. Chromatogr. A 788(1+2): 131-140 (1997) stirring 

Sen, N., Seaman, S., Page, B. salt added 

348 Flavor volatiles Application of SPME to the Analysis of Warmed 100µm PDMS GC-MS 

in beef Over Flavor in Beef 35°C, 10 min 

Poster Paper, IFT 1999 

Gruen, I., Fernando, L., Mobley, S. 

headspace 

890 Atrazine in Ethanol-modified subcritical water extraction combined 60µm Carbowax/DVB GC-MS 

beef with SPME for determining atrazine in beef kidney. 

J.Ag Food Chem (2001) 49(5) 2175-2180 

Curren, Meredith S. S.; King, Jerry 

30MIN @ 25°c 

617 Aroma compounds Two-fiber SPME combined with GC-MS for the analysis of Carboxen/PDMS. GC-MS 

in cooked pork volatile aroma compounds in cooked pork Carboxen/DVB/PDMS 

J. Chromatogr. A 905(2000), 233-240 

Elmore, J. Mottram, D., Hierro, E. 

30 min @ 60°C 

618 Hexanal, pentanal A comparison of SPME fibers for measurement of hexanal Carboxen/DVB/PDMS GC-FID 

in cooked turkey and pentanal in cooked turkey 

Food Chem Feb. 2000, 68(3), 339-345 

Brunton, N., Cronin, D, Durcan, R., Monahan, F. 

20 min, headspace @ 40°C 





924 Volatiles SPME as a tool for studying volatile compounds in frog skin 

in frog skin Chemistry and Ecology 2000 

Smith, B, Zini, C., Pawliszyn, J. Tyler, M., Hayasaka, Y, 

Williams, B., Caramao, E. 

423 Volatiles Comparison of Volatile Analysis of Lipid-Containing and 

in meat Meat Matrices by SPME and SFE 

ACS Symp. Ser. (1998), 705 (Flavor Analysis), 107-115 

Snyder, J., King, J., Zhang, Z. 

786 Volaitle amines New method for the rapid determination of volatile GC-FID, NPD 

in fish substances: The SPME-direct method. Part II. Determination 

of the freshness of fish headspace 

Sens Actuators, B Chem (2001) 72(3), 204-207 

Bene, A.; Hayman, A.; Luisier, J.L.; Reynard, E.; Villettaz, J 

619 Volatiles from SPME/GC of Salmonella-Infected Beef 75µm Carboxen/PDMS GC-FID 

salmonellas infected J Agric Food Chem, 2000, 48, 2253-2259 10 min 

beef Ogihara, H., Horimoto, Y., Hai, Z., Skura, B., Nakai, S. 25% NaCl 

393 Volatiles from Use of Digital Aroma Technology and SPME GC-MS to 100µm PDMS GC-MS 

processed poultry compare Volatile compounds Produced by Bacteria 30 min @ 37°C 

isolated from Processed Poultry headspace 

J. Sci. food Agric. 1998, 78, 343-348 

Arnold, J., Senter, S. 

stirred 

862 Allyl isothiocyanate Formation of allyl isothiocyanate from sinigrin in the GC-MS 

in rats digestive tract of rats monoassociated with a human colonic 

strain of Bacteroides thetaiotaomicron 

FEMS Microbiology Letters (2001) 197(1) 99-103 

Rabot, S; Duguay, A; Elfoul, L; Khelifa, N; Quinsac,A; Rimbault, A 

headspace 

253 Putrescine, An Electrodeposition Device for the Determination of carbon fibers HPLC 

cadaverine in Putrescine and Cadaverine by High-Resolution GC 0-60 min, immersion (C18 column) 

borate buffer solution J. High Resolut. Chromatogr. 19 (5): 294-297 (1996) stirring 

Conte, E., Miller, D. pH 8 

620 Hexanal, pentanal Shelf-life prediction of processed milk by SPME -MS and 75µm Carboxen/PDMS GC-MS 

metabolites in milk multivariate analysis 20min. @ 50°C 

J. Agric Food chem (2000), 48(8), 3470-3475 

Marsili, R. 

headspace 

386 Oxidative byproducts Comparison of SPME and Dynamic Headspace Methods for 75µm Carboxen/PDMS GC-MS 

in milk the GC-MS Analysis of Lighted Induced Lipid Oxidation 45°C, 15 min 

Products in Milk headspace 

J. Chromatogr. Sci. 1999, 37, 17-23 

Marsili, R. 

salt added 

372 Off-flavors SPME-MS-MVA as an Electronic Nose for the Study of 75µm Carboxen/PDMS GC-MS 

in milk Off-Flavors in Milk 45°C, 12 min 


Marsili, R. 

headspace 

621 Chlorinated organics Application of SPME for the rapid analysis of chlorinated GC-ECD 

in breast milk organics in breast milk 

Fresenius, J. Anal.Chem, Jan 2000, 366(1), 106-111 

Rohrig, L., Meisch, H. 

749 Acetaldehyde Flavor threshold for acetaldehyde in milk, chocolate milk, and 75µm Carboxen/PDMS GC-FID 

in milk & water spring water using SPME-GC for quantification 45°C, 15 min 

J.Agric.FoodChem 2001, 49(3), 1377-1381 headspace 

vanAardt, M., Duncan, S., Bourne, D., Marcy, J., Long, T., 

Hackney, C., Heisey, C., 

salt added 





364 Off-flavors Off Flavor and Malodors in Food: Mechanism of Formation various fibers GC 

in food and Analytical Techniques 

Book-Techniques for Analyzing Food Aroma, 

Marcel Decker ISBN: 0-8247-9788-4 

Marsili, R. 

and conditions 

376 Volatile metabolites Evaluation of SPME for Analysis of Volatile Metabolites 85µm polyacrylate GC-FID 

in water Produced by Staphylococci 80°C, 15 min 


Vergnais, L., Masson, F., Montel, M., Berdague, J., Talon, R. 


365 Volatiles Determination of Volatile Organic Compounds in Tea 100µm PDMS GC-MS 

in tea Industrie de la Bevande XXVI (1997) febbralo, 19-22 50°C, 15 min 

Guidotti, M. headspace 

622 Polyphenols Comparative Study and Partial characterization of Azorean 

in green tea green Tea Polyphenols 

J. Food Compos. Anal. (1999), 12(4), 273-287 

Baptista, J., da P Tavares, J., Carvalho, R. 

319 Caffeine Quantitative Determination of Caffeine in Beverages, bare fiber GC-MS 

in tea, coffee Using a Combined SPME-GC-MS Method 

J. Chem. Educ. 74 (9): 1130-1132 (1997) 

Yang, M., Orton, M., Pawliszyn, J. 

381 Aroma volatiles Characterization of Roasted Coffee and Coffee Beverages 100µm PDMS, GC-MS 

in coffee by SPME-GC and Principal Component Analysis 7µm PDMS 

J. Agric. Food Chem. 1997, 45: 4680-4686 60°C, 5 min 

Bicchi, C., Panero, O., Pellegrino, G., Vanni, A. headspace 

302 Volatile aroma Obtention of a Brewed Coffee Aroma Extract by an 100µm PDMS GC-MS 

in brewed coffee Optimized Supercritical CO2-Based Process 60°C, 10 min 


Ramos, E., Valero, E., Ibanez, E., Reglero, G., Tabera, J. 

headspace 

623 Aroma volatiles SPME Method Development for Headspace analysis of PDMS/DVB GC-MS 

in coffee volatile flavor compounds 60 min headspace 

J. Agri. Food Chem 2000, 48, (6) 2430-2437 

Roberts, D., Pollien, P., Milo, C. 

pH 2 

624 2-Acetyl-1-pyrroline Screening for 2-Acetyl-1-pyrroline in the Headspace of Rice 80µm Carboxen/DVB/PDMS GC-MS 

in rice using SPME/GC-MS 80°C, 15 min 

J. Agric. Food Chem 2001, 49, 245-249 headspace 

Grimm, C, Bergman, jC., Delgado, J., Bryant, R. .75gm in 100µl H20 

464 2-MIB, geosmin Microwave mediated distillation with SPME 100µm PDMS GC-MS 

in water determination off-flavors, geosmin and 25 min 

methylisoborneol, in catfish tissue immersed 

J. Chromatogr. A (1999), 833(2), 223-230 salt added 

Zhu, M., Aviles, F., Conte, E., Miller, D., 

Perschbacher, P. 

625 2-MIB, geosmin Microwave Distillation-SPME-GC Analysis of 80µm Carboxen/DVB/PDMS GC-IC-MS 

in water 2-methylisoboreneol and Geosmin in Catfish 60°C, 20 min 

Am-Lab Feb 2000: 32(3), 40-48 

Lloyd, S., Grimm, C. 

heaspace 

2-MIB, geosmin Analysis of 2-Methylisoboreneol and Geosmin in Catfish 100µm PDMS GC-MS 

in water by Microwave Distillation-SPME 40°C, 15 min 

J. Agri. Food Chem., 47, No. 1, pg. 164-169, 1999 saturated salt 

Lloyd, S., Grimm, C. stirring 





362 MIB & geosmin Determination of Geosmin and 2-Methylisoboreneol in Water Carboxen/DVB/PDMS GC-MS 

in water Using SPME and GC-Chemical Ionization/Electron Impact 60°C, 30 min 

Ionization Ion Trap MS headspace 

Analyst (Cambridge, U.K.) (1998), 123 (10), 2155-2160 stirring 

McCallum, R., Pendleton, P., Scumann, R., Trinh, M. salt added 

465 C2-C10 acid, Evaluating Peats for their capacities to remove 85µm polyacrylate GC-MS 

aldehydes, phenols odorous compounds from liquid swine manure 20 min @ 72°C 

in swine manure using headspace SPME headspace, pH 2 

J. Environ. Sci.Health, B34(4), 709-748 (1999) 

Rizzuti, A., Cohen, A., Hunt, P., Vanotti, M. 

966 Esters in wine Analysis of esters in wines Various GC 

J.Chromatogr. A (2002) 963(1-2), 213-223 

Rodriguez-Bencomo, J.J.; Conde, J.E.; Rodriguez-Delgado, M.A.; Garcia- 

Montelongo, F.; Perez-Trujillo, J.P. 

967 Aroma in onions Flavor and odor differences between fresh and preserved onions Polyacrylate GC-MS 

J.Chromatogr. A (2002) 963(1-2), 89-93 

Mondy, N.; Duplat, D.; Christides, J.P.; Arnault, L.; Auger, J. 

968 Volatiles in olive oil Influence of crushing technique on composition of volatiles in olive oil. 65 um Carbowax/DVB GC-MS 

969 

970 

992 

996 

997 

999 

European Journal of Lipid Science and Technology (2002) 104(8), 483-489 30 mins. 

Servili, M.; Piacquadio, P.; de Stefano, G.; Taticchi, A.; Sciancalepore, V. 

Volatiles in dry-cured 

ham Monitoring volatile compounds during the dry-cured ham ripening process 

J.Chromatogr. A (2002) 963(1-2), 83-88 

Andres, A.I.; Cava, R.; Ruiz, J. 

Bisphenol in food 

packaging 

Odour compounds in 

food packaging 

materials 

Photooxidative quality 

changes of havarti 

cheese. 

Volatile compounds 

from scallops 

1007 Insecticides in fruit 

Bisphenol type contaminants from food packaging materials in aqueous 

foods. HPLC 

J.Chromatogr. A (2002) 963(1-2), 375-380 

Nerin, C.; Philo, M.R.; Salafranca, J.; Castle, L. 

Development of headspace SPME, GC-MS method for the identification of 

odour causing volatile compounds in packaging materials. 75 um carboxen/PDMS GC-MS 

J.Chromatogr. A (2002) 963(1-2), 381-392 

Ezquerro, O.; Pons, B.; Tena, M.T. 

Response surface models used for prediction of photooxidative quality 

changes of havarti cheese. GC-MS 

European Food Research and Technology (2003) 216 (2), 93-98. 

Stapelfeldt, Henrik; Mortensen, Grith; Sorensen, John. 

Solid phase micro-extraction technique and its applications in medical 

analysis. 

Yaoxue Xuebao (2003) 38 (2), 153-158. 

Liu Zhen-ling; Wu Cai-ying. 

Volatile compounds recovered by solid-phase microextraction from fresh 

adductor muscle and total lipids from sea scallop ( Placopecten 

magellanicus ) from Georges Bank (Nova Scotia). PDMS/DVB GC-MS 

Journal of Food Science (2002) 67 (6), 2032-2037. 250 C, 2 minutes 

Linder, M.; Ackman, R. G. 

Headspace solid-phase microextraction in combination with gas 

chromatography-mass spectrometry for the rapid screening of 

organophosphorus insecticide residues in strawberries and cherries GC-MS 

J.Chromatogr. A (2003) 993(1-2), 197-203. 

Albanis, Triantafyllos A.; Lambropoulou, Dimitra A. 





1012 Mercury in fish 

1016 Volatiles in flowers 

1017 

1018 

Volatile byproducts in 

wine 

Terpenoids from 

hemlock 

1027 Volatiles from meats 

1044 

1052 

Volatiles and semivolatile 

in cigarettes. 

Oxidation of infant 

formula 

1053 Aroma compounds 

1055 

1063 

1064 


from tea leaves. 


from kimchi. 

Solid phase microextraction capillary gas chromatography combined with 

furnace atomization plasma emission spectrometry for speciation of 

mercury in fish tissues GC-FAPES 

Spectrochmica Acta - Part B Atomic Spectroscopy (2003) 58 (3), 427-441. 

Campos, Reinaldo C.; Grinberg, Patricia; Mester, Zoltan; Sturgeon, Ralph E. 

Volatile constituents of the leaves and flowers of Hypericum triquetrifolium 

Turrat GC-MS 

Flavour and Fragrance Journal (2003) 18 (2), 91-94. 

Bertoli, Alessandra; Mazzetti, Michele; Menichini, Francesco; Morelli, Ivano; 

Spinelli, Guido 

Evolution of volatile byproducts during wine fermentations using 

immobilized cells on grape skins. 

Journal of Agricultural and Food Chemistry (2003) 51 (8), 2402-2408. 

Komaitis, Michael; Kanellaki, Maria; Koutinas, Athanasios; Mallouchos, 

Athanasios 

Analysis of terpenoids from hemlock (Tsuga) species by solid-phase 

microextraction/gas chromatography/ion-trap mass spectrometry. GC-MS 


Lagalante, Anthony F.; Montgomery, Michael E. 

Volatile components associated with freshly cooked and oxidized offflavours 

in turkey breast meat. GC-MS 

Flavour and Fragrance Journal 2002) 17 (5), 327-334. 

Brunton, N. P.; Cronin, D. A.*; Monahan, F. J. 

Analysis of volatile and semivolatile composition in cut tobacco and total 

particulate matter of cigarettes with SPME-GC-MS. 85 um Polyacrylate GC-MS 

Fenxi Shiyanshi (2002) 21 (5), 31-35. 

Li, R.; Wang, L.; Li, Q.; Tong, X. D. 

Comparison of mass spectrometry-based electronic nose and solid phase 

microextraction gas chromatography-mass spectrometry technique to 

assess infant formula oxidation. GC-MS 


Guy, Philippe A.; Fenaille, Francois; Fumeaux, Rene; Milo, Christian; Visani, 

Piero 

Formation of aroma compounds from ribose and cysteine during the 

maillard reaction. GC-MS 


Cerny, Christoph; Davidek, Tomas 

Solid-phase microextraction for studies on the enantiomeric composition of 

filbertone in hazelnut oils. 


Ruiz del Castillo, M. L.; Blanch, G. P.; Flores, G.; Herraiz, M. 

Changes in lipoxygenase activity and volatile compounds of fresh tea leaves 

during early growing season. GC-MS 

Agricultural Chemistry and Biotechnology (2003) 46 (1), 23-27. 

Park, Seung-Kook; Kim, Hyun-Jeong; Lee, Sang-Jun; Roh, Jin-Chul; Ryu, 

Sung-Kwon 

Optimization of solid-phase microextraction for the analysis of the 

headspace volatile compounds in kimchi, a traditional Korean fermented 

vegetable product. 100 um PDMS 

Journal of Food Science (2003) 68 (3), 844-848. 

Min, D. B.; Kang, J. H.; Lee, J. H. 





1077 Volatile phenols in wine. 

1065 

1066 

1067 

1080 

1081 

Chloroanisoles from 

cork. 

Volatile free fatty acids 

in ewe cheese. 

Pyrimethanil and 

kresoxim-methyl in 

green groceries. 

Optimisation of headspace solid-phase microextraction for the analysis of 

volatile phenols in wine Carbowax/DVB 

Journal of Chromatography A (2003) 995 (1-2), 11-20. 

Castro Mejias, Remedios; Garcia Barroso, Carmelo; Garcia Moreno, Ma. De 

Valme; Natera Marin, Ramon 

Optimization of headspace sampling using solid-phase microextraction for 

chloroanisoles in cork stoppers and gas chromatography-ion-trap tandem 

mass spectrometric analysis. 

Journal of Separation Science (2003) 26 (5), 369-375. 

Musci, Marilena; Bianchi, Federica; Careri, Maria; Mangia, Alessandro 

75 um Carboxen/PDMS GC-MS-MS 

Solid-phase microextraction in combination with GC-MS for quantification of 

the major volatile free fatty acids in ewe cheese. 

Analytical Chemistry (2002) 74 (20), 5199-5204. 

Pinho, O.; Ferreira, I. M. P. L. V. O.*; Ferreira, M. A. 

85 um polyacrylate GC-MS 

Determination of pyrimethanil and kresoxim-methyl in green groceries by 

headspace solid-phase microextraction and gas chromatography-mass 

spectrometry. 

Journal of Chromatography, A (2002) 975 (2), 355-360. 

Navalon, A.; Prieto, A.; Araujo, L.; Vilchez, J. L.* 


Aroma compounds in 

mango. Distribution of aroma volatile compounds in different parts of mango fruit. GC-MS 

Odors from overripe 

mango. 

Journal of Horticultural Science & Biotechnology (2003) 78 (2), 131-138. 

Singh, Zora; Lalel, H. J. D.; Tan, S. C. 

Identification of odors from overripe mango that attract vinegar flies, 

Drosophila melanogaster. GC-EAD 

Journal of Chemical Ecol (2003) 29 (4), 899-909. 

Zhu, Junwei; Baker, Thomas C.; Park, Kye-Chung 

1083 Methyl jasmonate Prediction correlation of vapor pressure for methyl jasmonate 

Journal of Food Engineering (2003) 59 (4), 431-433. 

Acevedo, C.; Sanchez, E.; Simpson, R.; Young, M.E. 

GC-MS 

1085 


from cilantro 

1086 Ethanol in Tequila 

1087 

1088 

Butyltin compounds in 

alcoholic beverages 

Ethanediol and diethyl 

disulfide in wine. 

Changes in volatile compounds of small gamma -irradiated fresh cilantro 

leaves during cold storage. GC-MS 


Fan, X. T.; Sokorai, K. J. B. 

Tequila authenticity assessment by headspace SPME-HRGC-IRMS analysis 

of carbon-13/carbon-12 and oxygen-18/oxygen-16 ratios of ethanol. GC-MS 


Aguilar-Cisneros, B. O.; Lopez, M. G.; Richling, E.; Heckel, F.; Schreier, P. * 

Survey on the presence of butyltin compounds in Chinese alcoholic 

beverages, determined by using headspace solid-phase microextraction 

coupled with gas chromatography-flame photometric detection. GC-MS 


Liu, J. Y.; Jiang, G. B.* 

Synthesis and stable isotope dilution assay of ethanethiol and diethyl 

disulfide in wine using solid phase microextraction. Effect of aging on their 

levels in wine. GC-MS 


Majcenovic, A. B.; Schneider, R.; Lepoutre, J. -P.; Lempereur, V.; Baumes, 

R. * 


1089 




Aroma compounds from 

tomatoes. 

1090 Volatile fraction of milk 

1091 VOC's from eucalyptus. 

1105 Volatiles in mango 

1106 Methylmercury in fish. 

1127 

1128 

Alcohols, acetates in 

sweet wines. 

2,4,6-trichloroanisole in 

wine. 

1129 VOC's in fruit 

1130 

1131 

1132 

Differential effects of tomato ( Lycopersicon esculentum Mill) matrix on the 

volatility of important aroma compounds. 


Bezman, Y.; Mayer, F.; Takeoka, G. R.; Buttery, R. G.; Ben-Oliel, G.; 

Rabinowitch, H. D.; Naim, M. 

Volatile fraction of milk: comparison between purge and trap and solid 

phase microextraction techniques. 


Contarini, G.; Povolo, M. 

SPME applied to the study of volatile organic compounds emitted by three 

species of Eucalyptus in situ. 65 um PDMS/DVB GC-MS 


Zini, C. A.; Augusto, F.; Christensen, E.; Caramao, E. B.; Pawliszyn, J. * 

Headspace solid-phase microextraction and gas chromatography-mass 

spectrometry analysis of free volatile compounds in Mango. 

Chromatographia (2002) 55(11-12), 737-741 

Shang, C. Q.; Deng, C. H.; Zhang, X. Y.; Chen, Z. F.; Hu, Y. M. 

GC-MS 

Determination of methylmercury in fish tissues by isotope dilution SPME-GC- 

ICP-MS 

Journal of Analytical Atomic Spectrometry (2003) 18 (5), 431-436. 

Mester, Zoltan; Sturgeon, Ralph E.; Yang, Lu 

PDMS GC-ICP-MS 

Determination of major compounds in sweet wines by headspace solidphase 

microextraction and gas chromatography. GC 


Rodriguez-Bencomo, J. J.; Conde, J. E.; Garcia-Montelongo, F.; Perez- 

Trujillo, J. P.* 

Determination of 2,4,6-trichloroanisole in wines by headspace solid-phase 

microextraction and gas chromatography-electron-capture detection. GC-ECD 


Riu, M.; Mestres, M.; Busto, O. *; Guasch, J. 

Analysis of volatile compounds of tapereba ( Spondias mombin L.) and caja 

( Spondias mombin L.) by simultaneous distillation and extraction (SDE) and 

solid phase microextraction (SPME). DVB/CAR/PDMS 


Ceva-Antunes, P. M. N.; Bizzo, H. R.; Alves, S. M.; Antunes, O. A. C.* 

Volatile compounds in 

goat's milk cheese. Study of light-induced volatile compounds in goat apostrophe s milk cheese. GC-MS 


parmesan cheese. 

Volatile from virgin olive 

oil. 


Kim, G. Y.; Lee, J. H.; Min, D. B.* 

Optimization of solid phase microextraction analysis for the headspace 

volatile compounds of Parmesan cheese. 


Lee, J. H.; Diono, R.; Kim, G. Y.; Min, D. B.* 

Volatiles from leaves, fruits, and virgin oil from Olea europaea cv. Olivastra 

Seggianese from Italy. 


Flamini, G.; Cioni, P. L.; Morelli, I. 





1140 Hexanal from pork. 

1145 

Aroma compounds from 

pepper. 

1146 Flavours from milk 

1147 

1160 

1161 

1174 

1178 

1179 

1180 

1185 

1190 

Volatile flavor 

compounds 


bread crumb 

2,4,6-trichloroanisole in 

wine. 

Halogenated fungicides 

in wine. 

Flavor characteristics in 

apple cider. 

Trans-resveratrol in 

wine. 

2-acetyl-1-pyrroline in 

bread flowers. 


ground coffee. 

2-pentylfuran and 2pentenylfuran 

in 

soybean oil. 

Quantitation of hexanal by automated SPME for studying dietary influences 

on the oxidation of pork. Carboxen/PDMS GC 

Journal of Food Composition and Analysis (2003) 16 (2), 179-188. 

Grun, Ingolf U.; Berg, Eric P.; Fernando, Lakdas N. 

Aroma compound analysis of Piper nigrum and Piper guineense essential 

oils from Cameroon using solid-phase microextraction-gas chromatography, 

solid-phase microextraction-gas chromatography-mass spectrometry and 

olfactometry. GC-MS 

Journal of Chromatography, A (2002) 976 (1-2), 265-275. 

Jirovetz, L.; Buchbauer, G.; Ngassoum, M. B.; Geissler, M. 

Experimental and modelling studies showing the effect of lipid type and level 

on flavour release from milk-based liquid emulsions. GC-MS 


Roberts, D. D.; Pollien, P.; Watzke, B. 

Headspace solid-phase microextraction method for the study of the volatility 

of selected flavour compounds. GC-MS 


Jung, D. M.; Ebeler, S. E.* 

Solid-phase microextraction method for headspace analysis of volatile 

compounds in bread crumb. Carboxen/PDMS 

Cereal Chemistry (2003) 80 (3), 255-259. 

Ruiz, J. A.; Guasch, J.; Mestres, M.; Quilez, J. 

Accurate determination of 2,4,6-trichloroanisole in wines at low parts per 

trillion by solid-phase microextraction followed by GC-ECD. PDMS GC-MS 


Alzaga, Roberto; Bayona, Josep Maria; Marco, M.-Pilar; Ortiz, Laura; 

Sanchez-Baeza, Francisco 

Coupling solid-phase microextraction and high-performance liquid 

chromatography for direct and sensitive determination of halogenated 

fungicides in wine. PDMS/DVB HPLC-DAD 


Barrio, R. J.; Goicolea, M. A.; Millan, S.; Rodriguez, E.; Sampedro, M. C.; 

Unceta, N. 

Effects of processing treatment and sorbate addition on the flavor 

characteristics of apple cider. 


Boylston, T. D.; Wang, H.; Reitmeier, C. A.; Glatz, B. A. 

Solid-phase microextraction long dash on-fibre derivatization with 

comprehensive two-dimensional gas chromatography analysis of trans - 

resveratrol in wine. GC 

Chromatographia (2003) 51 (Supp), S349-S353. 

Shao, Y.; Marriott, P. *; Hugel, H. 

Identification and quantification of the rice aroma compound, 2-acetyl-1pyrroline, 

in bread flowers ( Vallaris glabra Ktze). GC-FID 


Wongpornchai, S.; Sriseadka, T.; Choonvisase, S. 

Analysis of volatile compounds released during the grinding of roasted 

coffee beans using solid-phase microextraction. PDMS/DVB GC-MS 


Akiyama, M.; Murakami, K.; Ohtani, N.; Iwatsuki, K.; Sotoyama, K.; Wada, 

A.; Tokuno, K.; Iwabuchi, H.; Tanaka, K. 

Singlet oxygen oxidation for 2-pentylfuran and 2-pentenylfuran formation in 

soybean oil. GC-MS 

Journal of Food Science (2003) 68 (4), 1175-1178. 

Min, D. B.; Callison, A. L.; Lee, H. O. 


1191 

1197 




Organo-selenium in 

garlic SPME for on-line volatile organo-selenium speciation. 

Journal of Analytical Atomic Spectrometry (2003), 18 (5), 467-473. 

Dietz, C.; Camara, C.; Madrid-Albarran, Y.; Perez-Corona, T. 

PDMS ICP-MS 


wine. 

Aroma compounds of an Italian wine ( Ruche ) by HS-SPME analysis 

coupled with GC-ion trap MS. 

Food Chemistry (2003) 80 (1), 125-133. 

Bonino, M.; Schellino, R.; Rizzi, C.; Aigotti, R.; Delfini, C.; Baiocchi, C. * 

Various GC-MS 

1208 Dairy products. The electronic nose applied to dairy products: A review 

Sensors and Actuators, B: Chemical (2003) 94 (1), 1-12. 

Ampuero, Silvia; Bosset, J.O. 

1215 Flavor analysis in wine. 

1216 Volatiles in malt whisky. 

1217 

1218 

1224 

Volatile fractions in 

butter. 

Volatile components in 

virgin olive oil. 

Flavour analysis of Greek white wine by solid-phase microextractioncapillary 

gas chromatography-mass spectrometry. 


Demyttenaere, J. C. R.; Dagher, C.; Sandra, P.; Kallithraka, S.; Verhe, R.; 

de Kimpe, N. 

Various GC-MS 

Analysis of volatiles of malt whisky by solid-phase microextraction and stir 

bar sorptive extraction. Various compared 


Demyttenaere, J. C. R.; Sanchez Martinez, J. I.; Verhe, R.; Sandra, P.; de 

Kimpe, N. 

Comparison of solid-phase microextraction and purge-and-trap methods for 

the analysis of the volatile fraction of butter. 


Povolo, M.; Contarini, G. * 

Analysis of virgin olive oil volatile compounds by headspace solid-phase 

microextraction coupled to gas chromatography with mass spectrometric 

and flame ionization detection. 


Vichi, S.; Castellote, A. I.; Pizzale, L.; Conte, L. S.; Buxaderas, S.; Lopez- 

Tamames, E. * 

DVB/carboxen/PDMS GC-MS 

Peppermint flavor in 

tablets. A SPME-GC procedure for monitoring peppermint flavour in tablets. 

Journal of Pharmaceutical and Biomedical Analysis 2003) 30 (5), 1469- 

1477. 

Yeung, D. Y. H.; Lee, T.; Grant, G.; Ma, M. H.; Kwong, E. * 

GC 

1226 Limonene in castor oil 

1231 

1232 


from pork loins. 

Determination of the disproportionation products of limonene used for the 

catalytic hydrogenation of castor oil. GC-MS 


Schneider, R. C. S.; Baldissarelli, V. Z.; Martinelli, M.; von Holleben, M. L. 

A.; Caramao, E. B.* 

Effect of Penicillium chryso genum and Debaryomyces hansenii on the 

volatile compounds during controlled ripening of pork loins. GC-MS 

International Journal of Food Microbiology (2003) 84 (3), 327-338. 

Cordoba, Juan J.; Aranda, Emilio; Asensio, Miguel A.; Benito, Maria J.; 

Martin, Alberto 

Limonene from Release of limonene from polysaccharide matrices: Viscosity and synergy 

polysaccharide matrices. effect. 


Grisel, Michel; Decroix, Bernard; Malhiac, Catherine; Secouard, Sebastien 





1236 Walnut oils Oxidative stability of walnut oils extracted with supercritical carbon dioxide 

1237 

Volatile carbonyl 

compounds from spirits. 

Journal of the American Oil Chemists' Society (2003) 80 (6), 575-578. 

Crowe, Tammy D.; White, Pamela J. 

Evaluation of headspace solid-phase microextraction for the analysis of 

volatile carbonyl compounds in spirits and alcoholic beverages. GC-ECD 


Wardencki, W.; Sowinski, P.; Curylo, J. 

1238 Truffle aroma Truffle aroma analysis by headspace solid phase microextraction. GC-MS 

1246 Methanol in aspartame 

1248 


Diaz, P.; Senorans, F. J.; Reglero, G.; Ibanez, E. * 

Headspace solid-phase micro-extraction gas chromatography method for 

the determination of methanol in aspartame sweeteners. 

Food Additives and Contaminants 92003) 20 (6), 519-523. 

de Lourdes Cardeal, Z.; Sales, J. A. 

85 um polyacrylate. GC-FID 

Limonene oxidation 

products Determination of limonene oxidation products using SPME and GC-MS. 

Journal of Chromatographic Science (2003) 41 (1), 31-35. 

Marine, S. S.; Clemons, J. 

7 um PDMS 

1249 Geosmin in red beet. Biosynthetic origin of geosmin in red beets ( Beta vulgaris L.). GC-MS 

1250 Geosmin in red beet. 

1251 Acidic pesticides in fruit. 


Lu, G. P.; Edwards, C. G.; Fellman, J. K.; Mattinson, D. S.; Navazio, J. 

Quantitative determination of geosmin in red beets ( Beta vulgaris L.) using 

headspace solid-phase microextraction. GC 


Lu, G. P.; Fellman, J. K.; Edwards, C. G.; Mattinson, D. S.; Navazio, J. 

Off-line solid-phase microextraction and capillary electrophoresis mass 

spectrometry to determine acidic pesticides in fruits. CE-MS 


Rodriguez, R.; Manes, J.; Pico, Y. * 

1252 

Application of solid-phase microextraction for the determination of pyrethroid 

Pyrethroid in vegetables. residues in vegetable samples by GC-MS. 

Analytical and Bioanalytical Chemistry (2003) 376 (4), 502-511. 

Beltran, J.; Peruga, A.; Pitarch, E.; Lopez, F. J.; Hernandez, F. 

GC-MS 

1253 

Daidzein and genistein 

in soybean foods. 

1266 Volatiles from honey 

1271 Aroma from truffles 

Determination of daidzein and genistein in soybean foods by automated online 

in-tube solid-phase microextraction coupled to high-performance liquid 

chromatography. HPLC 


Mitani, K.; Narimatsu, S.; Kataoka, H. * 

Analysis of volatile composition of honey by solid phase microextraction and 

gas chromatography-mass spectrometry GC-MS 

Journal of Separation Science (2002) 26 (9-10), 793-801. 

Martinez-Castro, Isabel; Sanz, Jesus; Soria, Ana Cristina 

Rebuttal on truffle aroma analysis by headspace solid phase 

microextraction (wrong information or wrong interpretation?). 

Journal of Agricultural and Food Chemistry (2003) 51 (15), 4484. 

Ibanez, Elena; Diaz, Paloma; Reglero, Guillermo; Senorans, F. Javier 





1272 Hexanal from chicken 

1275 

1282 

1283 

1284 

1285 

Phenolic compounds in 

smoked herring. 

Solid phase microextraction-gas chromatography for quantifying headspace 

hexanal above freeze-dried chicken myofibrils. GC-MS 


Goodridge, Carolyn F.; Beaudry, Randolph M.; Pestka, James J.; Smith, 

Denise M. 

Optimization of solid-phase microextraction coupled to gas chromatography 

for determination of phenolic compounds in smoked herring. 85 um polyacrylate, 50 C, 55 minutes. 


Serot, T.; Lafficher, C. 

Aromatic components in 

bananas. Changes in aromatic components of banana during ripening and air-drying. 

Lebensmittel-Wissenschaft & Technologie (2003) 36 (6), 633-642. 

Bonazzi, C.; Boudhrioua, N.; Giampaoli, P. 

GC-MS 

Selenium in roasted 

coffee. Studies of selenium-containing volatiles in roasted coffee. GC/ICP-MS 


soybeans. 

Chiral compounds in 

orange juice. 

1289 Methylketone in cognac. 

1290 

1291 

Volatile (flavour) 

compounds in Raclette 

cheese. 

Volatiles from tomato 

shoots. 


Caruso, Joseph A.; Bryson, Joshua M.; Meija, Juris; Montes-Bayon, Maria; 

Vonderheide, Anne P. 

Identification of volatile compounds in soybean at various developmental 

stages using solid phase microextraction. GC-MS 


Boue, Stephen M.; Carter-Wientjes, Carol H.; Cleveland, Thomas E.; Shih, 

Betty Y. 

Enantiomeric distribution of chiral compounds in orange juices according to 

their geographical origins. GC-MS 

Journal of Food Protection (2003) 66 (8), 1448-1454. 

Herraiz, M.; Blanch, G. P.; Caja, M. M.; Ruiz del Castillo, M. L. 

Analysis of microvolatiles in brandy: Relationship between methylketone 

concentration and Cognac age. 

Journal of the Science of Food and Agriculture (2003) 83 (11), 1143-1149. 

Watts, Vivian A.; Butzke, Christian E. 

Distribution of the volatile (flavour) compounds in Raclette cheese produced 

with different staphylococci in the smear. 

Mitteilungen aus Lebensmitteluntersuchung und Hygiene (2003) 94 (3), 192- 

211. 

Bosset, Jacques Olivier; Imhof, Miroslava; Place, Raymond B.; Teuber, 

Michael 

Volatiles emitted from in vitro grown tomato shoots during abiotic and biotic 

stress. 

Plant Cell Tissue and Organ Culture (2003) 75 (1), 73-78. 

Debergh, Pierre C.; Maes, Katrien 

1292 Ethylene in mango fruit. The role of ethylene in mango fruit aroma volatiles biosynthesis. GC-MS 

1295 

Postharvest fungicides 

in fruits. 

Journal of Horticultural Science & Biotechnology (2003) 78 (4), 485-496. 

Singh, Zora; Lalel, H. J. D.; Tan, S. C. 

Solid-phase microextraction liquid chromatography-tandem mass 

spectrometry to determine postharvest fungicides in fruits. 


Blasco, C.; Font, G.; Manes, J.; Pico, Y. * 

50 um carbowax/template resin LC-MS-MS 


1296 




Volatile components in 

cheese. Volatile components of Grana Parmigiano-Reggiano type hard cheese. 


Bellesia, F.; Pinetti, A. *; Pagnoni, U. M.; Rinaldi, R.; Zucchi, C.; Caglioti, L.; 

Palyi, G. 

GC-MS 

1306 PCBs in milk. 

1307 

1315 

Application of Strategically Designed Sample Composition to the Rapid 

Analytical Screening of Milk Samples for Polychlorinated Biphenyls 

Journal of AOAC International (2003) 86 (4), 846-855. 

Carro, Antonia M.; Cela, Rafael; Llompart, Maria; Martinez, Elena; Pazos, 

Manuel 

Polyphenols in 

grapes/wine. Mass spectrometry in grape and wine chemistry. Part I: Polyphenols 

Mass Spectrometry Reviews (2003) 22 (4), 218-250. 

Flamini, Riccardo 

LC-MS 

Ochratoxin A, 

cyclopiasonic acid in 

cornflakes. 

1319 Iberian ham 

1323 

Organochlorine 

pesticides in Chinese 

teas. 

Simultaneous determination of ochratoxin A and cyclopiazonic, 

mycophenolic, and tenuazonic acids in cornflakes by solid-phase 

microextraction coupled to high-performance liquid chromatography. PDMS/DVB LC-UV/DAD 


Palmisano, Francesco; Aresta, Antonella; Cioffi, Nicola; Zambonin, Carlo 

G. 

Challenges and prospects of Iberian pork products: Verification of the 

sensorial and nutritional quality of Iberian ham. 

Alimentaria (2003) 40 (345), 45-58. 

Ventanas, S.; Ventanas, J.; Petron, M. J.; Jurado, A.; Carrapiso, A. 

Application of polyphenylmethylsiloxane coated fiber for solid-phase 

microextraction combined with microwave-assisted extraction for the 

determination of organochlorine pesticides in Chinese teas polyphenylmethylsiloxane GC-ECD 


Cai, Lingshuang; Dong, Li; Wu, Caiying; Xing, Jun 

1325 Pesticides in foods Analyses of pesticides and their metabolites in foods and drinks. LC-MS 

Trends in Analytical Chemistry (2002) 20(11), 649-661 

Ahmed, Farid E. 

1330 

1338 

Oil aroma compounds in 

Ocimem species. 


ewe cheese. 

1339 Methylmercury in fish. 

1347 


coffee 

Chemotaxonomical analysis of the essential oil aroma compounds of four 

different Ocimum species from southern India. GC-MS 

European Food Research and Technology (2003) 217 (2), 120-124. 

Jirovetz, Leopold; Buchbauer, Gerhard; Kaniampady, Molikutty M.; Shafi, 

Mohamed 

Solid-phase microextraction of volatile compounds in left dbl quote 

Terrincho right dbl quote ewe cheese: comparison of different fibres. CAR-PDMS GC-MS 


Pinho, O.; Peres, C.; Ferreira, I. M. P. L. V. O.* 

Application of isotope dilution to the determination of methylmercury in fish 

tissue by solid-phase microextraction gas chromatography-mass 

spectrometry. 


Yang, L.; Colombini, V.; Maxwell, P.; Mester, Z.; Sturgeon, R. E. 

PDMS GC-MS 

Comparison of two SPME fibres for differentiation of coffee by analysis of 

volatile compounds. 

Chromatographia (2001) 54(9-10), 647-652. 

Costa Freitas, A. M.; Parreira, C.; Vilas-Boas, L. 

Carbowax/DVB, PDMS GC-MS 





1348 Fungicides in wine 

1356 Volatiles in wines 

1362 

1367 

1368 

Cyclopiazonic acid in 

cheese. 

Off flavours in orange 

juice. 

Flavour compounds in 

wine. 

Solid-phase microextraction-gas chromatographic-mass spectrometric 

method for the determination of the fungicides cyprodinil and fludioxonil in 

white wines. 

Journal of Chromatography A (2002) 942(1-2), 41-52 

Simal Gandara, J.; Cancho Grande, B.; Rial Otero, R.; Yague Ruiz, C. 

Classification of Nebbiolo-based wines from Piedmont (Italy) by means of 

solid-phase microextraction-gas chromatography-mass spectrometry of 

volatile compounds. 

Journal of Chromatography A (2002) 943(1), 123-137 

Aceto, Maurizio; Marengo, Emilio; Maurino, Valter 

50/30um DVB/Carboxen PDMS GC-MS 

GC-MS 

Determination of cyclopiazonic acid in cheese samples using solid-phase 

microextraction with high performance liquid chromatography. 

Food Chemistry (2001) 75(2), 249-254. 

Zambonin, C. G.; Monaci, L.; Aresta, A. * 

Carbowax/TPR HPLC 

2-Methyl-3-furanthiol and methional are possible off-flavours in stored 

orange juice: aroma-similarity, NIF/SNIF GC-Olfactometry, and GC 

analyses. GC-O 

Journal of Agricultural and Food Chemistry (2001) 49(11), 5425-5432. 

Bezman, Y.; Rouseff, R. L.; Naim, M. * 

Headspace solid phase microextraction ( SPME ) analysis of flavour 

compounds in wines. Effect of the matrix volatile composition in the relative 

response factors in a wine model. GC 


Rocha, S.; Ramalheira, V.; Barros, A.; Delgadillo, I.; Coimbra, M. A. 

1370 Volatiles in solid foods. New device for direct extraction of volatiles in solid samples using SPME GC-MS 

1372 Coffee aroma 


Ruiz, J.; Ventanas, J.; Cava, R. 

The use of an electronic aroma-sensing device to assess coffee 

differentiation. Comparison with SPME gas chromatography-mass 

spectrometry aroma patterns. 100 um PDMS GC-MS 

Journal of Food Composition and Analysis (2001) 14(5), 513-522. 

Costa Freitas, A. M.; Parreira, C.; Vilas-Boas, L. 

1377 PAH in rice. Dynamics analysis for the distribution of PAH in rice. 

Journal of Health Science (2001) 47(5), 446-451. 

Liu, X. X.; Korenaga, T. 

GC-MS 

1378 Fatty acids in milk. 

1382 

1387 

Volatile flavour 

compounds. 

Cucumber flavour 

compounds 

Quantitative determination of short-chain free fatty acids in milk using solidphase 

microextraction and gas chromatography. Polyacrylate GC 


Gonzalez-Cordova, A. F.; Vallejo-Cordoba, B. * 

Comparison of simultaneous distillation extraction and solid-phase 

microextraction for the determination of volatile flavour components. GC-MS 

Journal of Chromatography, A (2001) 930(1-2), 1-7. 

Cai, J. B.; Liu, B. Z.; Su, Q. D.* 

Solid-phase microextraction ( SPME ) technique for measurement of 

generation of fresh cucumber flavour compounds. 


Palma-Harris, C.; McFeeters, R. F.*; Fleming, H. P. 

PDMS GC 





1389 Scotch whiskies 

1390 Volatiles in potato tubers 

1399 PCBs in food. 

1401 Aroma from wine must. 

1402 

Headspace congeners of blended scotch whiskies of different product 

categories from SPME analysis. 

Journal of the Institute of Brewing (2001) 107(5), 315-332. 

Lee, K. -Y. M.; Paterson, A. *; Birkmyre, L.; Piggott, J. R 

PDMS, polyacrylate GC-FID 

Volatile fingerprinting (SPME-GC-FID) to detect and discriminate diseases 

of potato tubers. 

Plant Disease (2002) 86(2), 131-137 

Kushalappa, A. C.; Chen, C. R.; Lee, B.; Lui, L. H. 

Fast extraction, clean-up and detection methods for the rapid analysis and 

screening of seven indicator PCBs in food matrices. 


Anklam, E.; von Holst, Christoph; Bjorklund, E. 

Optimization of solid phase microextraction analysis of aroma compounds in 

a Portuguese muscatel wine must. 85 um polyacrylate 

Journal of Microcolumn Separations (2001) 13(6), 236-242. 

Relva, A. M.; Freire, Luis M. T. Vaz; Freitas, A. M. Costa 

GC-FID 

Lipid degeneration 

products in oils Monitoring of lipid degradation products by solid-phase microextraction 100 um PDMS GC-FID 


1403 Volatiles in bananas 

1414 Volatiles from fruit. 

1415 Off-flavors from milk 

1418 

1420 

1421 

1422 

Volatiles in soybean and 

corn oils 


wine. 

Pesticides in 

strawberries. 


from oranges. 

Doleschall, Fruzsina; Kemeny, Zsolt; Kovari, Katalin; Recseg, Katalin 

Optimization of solid-phase microextraction analysis for studying change of 

headspace flavor compounds of banana during ripening. 

Journal of Agricultural and Food Chemistry (2002) 50(4), 653-657 

Liu, Tai-Ti; Yang, Tsung-Shi 

Solid phase microextraction and gas chromatography-olfactometry analysis 

of internal volatiles from intact citrus fruits and their aroma activity GC-O 

Abstracts of Papers American Chemical Society (2001) 222(1-2), AGFD142. 

Rouseff, Russell L.; Lin, Jianming 

SPME GC-MS-based testing for monitoring off-flavor development in 

processed milk. 

Abstracts of Papers American Chemical Society (2001) 222(1-2), AGFD27. 

Marsili, Ray T. 

Solid phase microextraction of volatile soybean oil and corn oil compounds. 

Journal of Food Science (2002) 67(1), 71-76 

Min, D. B.; Lee, J. H.; Steenson, D. F. 

Various fibers compared GC-MS 

Polydimethylsiloxane solid-phase microextraction-gas chromatography 

method for the analysis of volatile compounds in wines. Its application to the 

characterization of varietal wines. PDMS GC 

Journal of Chromatography A (2001) 922(1-2), 267-275. 

Polo, M. C.; Martin-Alvarez, P. J.; Pozo-Bayon, M. A.; Pueyo, E. 

Determination of organochlorine pesticides and chlorobenzenes in 

strawberries by using accelerated solvent extraction combined with sorptive 

enrichment and gas chromatography/mass spectrometry. 

Journal of AOAC International (2001) 84(4), 1194-1201. 

Wennrich, Luise; Breuste, Juergen; Koeller, Gabor; Popp, Peter 

Analysis of volatile compounds released from embryogenic cultures and 

somatic embryos of sweet oranges by head space SPME GC-MS 

Plant Cell Tissue and Organ Culture (2001) 66(1), 31-34. 

Del Bosco, S. Fatta; Alonzo, G.; Saiano, F.; Tusa, N. 


1423 

1424 

1426 




Volatiles from turkey 

breast. 

Volatiles of gourd 

flowers. 

The effects of temperature and pressure on the performance of 

Carboxen/PDMS fibres during solid phase microextraction ( SPME ) of 

headspace volatiles from cooked and raw turkey breast. Carboxen/PDMS 

Flavour and Fragrance Journal (2001) 16(4), 294-302. 

Cronin, D. A.; Brunton, N. P.; Monahan, F. J. 

Headspace-SPME analysis of volatiles of the ridge gourd (Luffa acutangula) 

and bitter gourd (Momordica charantia) flowers. GC-MS 


Grun, I. U.; Fernando, L. N. 

Aroma of strawberry 

drink. Changes in the aroma of a strawberry drink during storage. 


Siegmund, Barbara; Derler, Karin; Pfannhauser, Werner 

1440 Truffle aroma Truffle aroma characterization by headspace solid-phase microextraction 


Diaz, P.; Ibanez, E.; Reglero, G.; Senorans, F.J 

1441 Propionic acid in feed 

1442 

1448 

Volatiles in Italian 

Vinegars 

Garlic flavor 

components 

1451 Volatiles in Olive Oil 

1452 Volatiles in Olive Oil 

1453 

Free fatty acids in ewe 

cheese 

1454 Aroma volatiles in beef 

Analysis of total propionic acid in feed using headspace solid-phase 

microextraction and gas chromatography 


Ibanez, Carlos 

Quantitative analysis of 2-furfural and 5-methylfurfural in different Italian 

vinegars by headspace solid-phase microextraction coupled to gas 

chromatography-mass spectrometry using isotope dilution 


Calabrese, Roberto; Davoli, Enrico; Giordano, Lucia; Rotilio, Domenic 

Comparative study of extraction techniques for determination of garlic 

flavour components by gas chromatography-mass spectrometry. 

Analytical and Bioanalytical Chemistry (2003) 377(4), 749-756 

Lee, S. N.; Kim, N. S.; Lee, D. S. 

Solid-phase microextraction in the analysis of virgin olive oil volatile fraction: 

Characterization of virgin olive oils from two distinct geographical areas of 

northern Italy. 


Lopez-Tamames, Elvira; Buxaderas, Susana; Conte, Lanfranco S.; Pizzale, 

Lorena; Vichi, Stefania 

Solid-phase microextraction in the analysis of virgin olive oil volatile fraction: 

Modifications induced by oxidation and suitable markers of oxidative status. 


Lopez-Tamames, Elvira; Buxaderas, Susana; Conte, Lanfranco S.; Pizzale, 

Lorena; Vichi, Stefania 

Quantification of short-chain free fatty acids in "Terrincho" ewe cheese: 

Intravarietal comparison. 

Journal of Dairy Science (2003) 86(10), 3102-3109 

Ferreira, I. M. P. L. V. O.; Ferreira, M. A.; Pinho, O. 

Evaluation of two commercial solid-phase microextraction fibres for the 

analysis of target aroma compounds in cooked beef meat 

Talanta (2003) 61(4), 529-537 

Istasse, Louis; Machiels, David 

Ambient temperature, unless otherwise indicated. 28 

50/30um DVB/Carboxen PDMS 

headspace 13.6 mins. 

GC-MS 

85um Polyacrylate headspace GC-FID, GC-MS 


headspace 

50/30um DVB/Carboxen PDMS, 

headspace 

85um Polyacrylate 65 degrees 

C, 45 mins. Headspace 


Carboxen PDMS, headspace 

GC-MS 

GC-MS 

GC-FID, GC-MS 

GC-FID, GC-MS 

GC-FID 

GC-MS




1457 Volatiles in wine Volatile compounds by SPME-GC as age markers of sparkling wines. GC-MS 

1463 

Long chain alcohols 

from 

food-borne bacteria 

1465 Thymol in honey 

1471 VOCs in Riseling wine 

1472 

Volatiles in dry-cured 

ham 

1473 Carvone in dill seeds 

1474 

1481 

1482 

1496 

1499 

Volatiles from soybean 

leaves 

2-pentyl pyridine binding 

to soy proteins 


Vinegar 

Mycophenolic acid in 

cheese 

Characterization of 

flavors in coffee 

American Journal of Enology and Viticulture (2003) 54(3), 158-162 

Buxaderas, Susana; Francioli, Sonia; Lopez-Tamames, Elvira; Riu- 

Aumatell, Montserrat; Torrens, Jordi 

Comparison of long-chain alcohols and other volatile compounds emitted 

from food-borne and related Gram positive and Gram negative bacteria. 

Journal of Basic Microbiology (2002) 42(6), 373-380 

Hamilton-Kemp, T. R.; Archbold, D. D.; Collins, R. W.; Elgaali, Hesham; 

Newman, M. C.; Yu, Keshun 

Application of solid phase microextraction to evaluate traces of thymol in 

honey. 

Apidologie (2002) 33(6), 545-552 

Conte, Lanfranco S.; Bogdanov, Stefan; Gracco, Luisa; Piasenzotto, Lara 

Analysis of Riesling wine volatiles by a novel headspace solid-phase 

microextraction gas chromatography method. 

American Journal of Enology and Viticulture (2002) 53(3), 251A 

Wang, X. D.; Reynolds, A. G.; Mattinson, D. S.; Fellman, J. K.; Edwards, C. 

G.; Bohlscheid, J. C 

Optimisation of solid phase microextraction ( SPME ) for the analysis of 

volatile compounds in dry-cured ham. 

Journal of the Science of Food and Agriculture (2002) 82(14), 1703-1709 

Flores, Monica; Gianelli, Maria Pia; Toldra, Fidel 

Estimation of the main dill seeds odorant carvone by solid-phase 

microextraction and gas chromatography. 

Nahrung (2002) 46(5), 357-359 

Zawirska-Wojtasiak, Renata; Wasowicz, Erwin 

Clean recovery and HRGC-MS/HRGC-FTIR identification of volatiles from 

soybean (Glycine max). 

Italian Journal of Food Science (2002) 12(2), 175-182 

Damiani, P.; Bin, F.; Castellini, M.; Cossignani, L. 

Binding properties of 2-pentyl pyridine to soy protein as measured by solid 

phase microextraction 


Boatright, W. L.; Johnson, L. A.; Reuber, M.; Zhou, A. 

Headspace solid-phase microextraction analysis of aroma compounds in 

vinegar. Validation study. 


Castro Mejias, Remedios; Garcia Barroso, Carmelo; Garcia Moreno, Ma. de 

Valme; Garcia Rowe, Fernando; Natera Marin, Ramon 

Solid-phase microextraction-high performance liquid chromatography and 

diode array detection for the determination of mycophenolic acid in cheese. 

Food Chemistry (2002) 78(2), 249-254 

Zambonin, C. G.; Aresta, A.; Monaci, L. 

Characterization of flavor compounds during grinding of roasted coffee 

beans. 

Abstracts of Papers American Chemical Society (2002) 224(1-2), AGFD 68 

Sotoyama, Kazuyoshi; Ohtani, Noboru; Murakami, Kazuya; Iwatsuki, Keiji; 

Akiyama, Masayuki; Iwabuchi, Hisakatsu; Tanaka, Kiyofumi; Tokuno, 

Katsuya; Wada, Akira 



85um Polyacrylate, 100um 

PDMS 

75um Carboxen/PDMS 

GC-MS 

GC-FID 

GC-MS 

50um Carbowax TPR HPLC-PAD




1500 Volatiles in orange juice Variables affecting SPME headspace analysis of orange juice volatiles 

1516 Voltiles in pineapple 

1517 


wine 

1520 Volatiles in smoked fish 

1521 

1525 

1526 

Aroma volatiles in 

cantaloupe 

Fatty acid ethyl ethers in 

rum 

Volatiles in alcoholic 

fermentation of grapes 

1534 Butyltin in wines 

1535 Ethylphenol in wine 


Goodrich, Renee M.; Bryan, Charles R.; Braddock, Robert J. 

Volatile compounds in hydrolyzed pineapple (Ananas comosus L. Merryl) 

perola variety and clarified pasteurized juices obtained by solid-phase 

microextraction 

Alimentaria (2002) 39(333), 129-132 

de Carvalho, Lucia Maria Jaeger; da Silva, Carlos Alberto Bento; de Oliveira 

Godoy, Ronoel Luiz; Abadio, Fernanda Dias Bartolomeu; Figueira, Jose 

Americo A. 

Headspace solid-phase microextraction gas chromatography/mass 

spectrometry in the analysis of the aroma constituents of 'Cannonau of 

Jerzu' wine. 

Rapid Communications in Mass Spectrometry (2002) 16(11), 1086-1091 

Podda, Gianni; Begala, Michela; Corda, Luciana; Fedrigo, Maria Anna; 

Traldi, Pietro 

Volatile components of raw and smoked black bream (Brama raii) and 

rainbow trout (Oncorhynchus mykiss) studied by means of solid phase 

microextraction and gas chromatography/mass spectrometry. 

Journal of the Science of Food and Agriculture (2002) 82(9), 945-952 

Guillen, Maria D.; Errecalde, Maria C. 

Effect of storage on some volatile aroma compounds in fresh-cut 

cantaloupe melon. 


Lamikanra, Olusola; Richard, Olga A. 

Headspace solid-phase microextraction of higher fatty acid ethyl esters in 

white rum aroma. 


Guasch, J.; Busto, O.; Marti, M. P.; Mestres, M.; Perez, J.; Pino, J. 

Investigation of volatiles evolution during the alcoholic fermentation of grape 

must using free and immobilized cells with the help of solid phase 

microextraction ( SPME ) headspace sampling. 


Komaitis, Michael; Kanellaki, Maria; Koutinas, Athanasios; Mallouchos, 

Athanasios 


Ducruet, Violette; Feigenbaum, Alexandre; Gratadoux, Jean Jacques; 

Jouquand, Celine; Lecanu, Laurent 

Headspace solid-phase micro-extraction gas chromatography-mass 

detection method for the determination of butyltin compounds in wines. 

Analytica Chimica Acta (2002) 458(1), 231-239 

Azenha, Manuel; Vasconcelos, Maria Teresa 

Determination of ethylphenol compounds in wine by headspace solid-phase 

microextraction in conjunction with gas chromatography and flame 

ionization detection. 


Nepveu, Francoise; Gastine, Valerie; Monje, Marie-Carmen; Privat, 

Christelle 


65um PDMS DVB GC-MS 

GC-MS 

headspace GC-MS 


85um Polyacrylate, NaCl added, 

40mins. 

GC-FID




1537 Ethyl carbamate in wine 

1539 

1541 

1542 

1546 

1555 

3-alkyl-2methoxypyrazines 

in 

wine 

Butyltin in Portuguese 

wines 

Volatiles in Spanish 

honey 

Short-chain fatty acids in 

cane and beet sugars 

Sulfur compounds in 

wines 

Determination of ethyl carbamate in wine by solid-phase microextraction 

and gas chromatography/mass spectrometry. 

American Journal of Enology and Viticulture (2002) 53(1), 60-63 

Zoecklein, B. W.; Whiton, R. S. 

Headspace solid-phase microextraction analysis of 3-alkyl-2methoxypyrazines 

in wines. 


Guasch, J.; Busto, O.; Marti, M. P.; Mestres, M.; Sala, C. 

65um Carbowax DVB, 30mins, 

headspace 

GC-MS 

Butyltin compounds in Portuguese wines. GC-MS 


Azenha, Manuel; Vasconcelos, Maria Teresa 

Analysis of volatiles from Spanish honeys by solid-phase microextraction 

and gas chromatography-mass spectrometry. 


Tadeo, Jose L.; Calvo, Rosa M.; Perez, Rosa A.; Sanchez-Brunete, 

Consuelo 

Semiquantitative determination of short-chain fatty acids in cane and beet 

sugars. 

Journal of Chromatographic Science (2002) 40(3), 127-132 

Grimm, Casey C.; Batista, Rebecca B.; Godshall, Mary An 

Application of headspace solid-phase microextraction to the determination 

of sulphur compounds with low volatility in wines. 


Mestres, M.; Busto, O.; Guasch, J. 

75um Carboxen PDMS, 70 

degrees C, 30mins. 

GC-MS 

50/30um DVB/Carboxen PDMS GC-MS 

1196 Analysis of chemical constituents of capsicol by GC-MS. 

Fenxi Ceshi Xuebao (2003) 22 (1), 67-70. 

Zhu, X. L.; Liu, B. Z.; Zong, R. W.; Yun, G. O. 

GC-MS 

1211 

1243 Nicotine in cigarettes 

1274 

1314 

Identification of 2-bromo-3,4,5,6-tetrachloroaniline and its quantification in 

the color additives D&C Red Nos. 27 and 28 (phloxine B) using solid-phase 

microextraction and gas chromatography-mass spectrometry GC-MS 


Andrzejewski, Denis; Weisz, Adrian 

Determination of nicotine and other minor alkaloids in international 

cigarettes by solid-phase microextraction and gas chromatography/mass 

spectrometry. GC-MS 


Wu, W. J.; Ashley, D. L.; Watson, C. H.* 

Determination of the volatile constituents of Chinese Coriandrum sativum L. 

by gas chromatography-mass spectrometry with solid-phase 

microextraction. 100 um PDMS, 250 C, 3 minutes GC-MS 

Chromatographia (2003) 57 (5-6), 357-361. 

Deng, C. H.; Song, G. X.; Hu, Y. M.*; Zhang, X. M. 

Aroma dilution method using GC injector split ratio for volatile compounds 

extracted by headspace solid phase microextraction. GC-O 


Lee, Hyong Joo; Kim, Kyoung Heon; Kim, Tae Hwan; Kim, Young-Suk; Lee, 

Sang Mi; Oh, Sangsuk 


1409 




Disulfide flavors from 

proteins 

Flavor-protein binding: Disulfide interchange reactions between ovalbumin 

and volatile disulfides. 

Journal of Agricultural and Food Chemistry (2001), 49(9), 4333-4336. 

Mottram, Donald S.; Adams, Rachel L.; Brown, Helen M.; Parker, Jane K. 

1559 Esters Analysis of esters in wines Various GC 

in wine J.Chromatogr. A (2002) 963(1-2), 213-223 

Rodriguez-Bencomo, J.; Conde, J.; Rodriguez-Delgado, M.A.; 

Garcia-Montelongo, F.; Perez-Trujillo, J.P. 

1560 Dimethyl Contribution of dimethyl sulfide to the aroma of Syrah and headspace GC-MS 

sulfide in Grenache Noir wines and estimation of its potential in grapes 

wine of these varieties 

J Agr Food Chem, 52, #23, 7084-7093 

Segurel, M.; Razungles, A.; Riou, C; Salles, M; Baumes, R 

1561 Volaitles in Hydrolysis of glycosidically bound volatiles from apple leaves headspace GC-MS 

apple leaves (cv. Anna) by Aspergillus niger beta-glucosidase affects 

the behavior of codling moth (Cydia pomonella L.) 

J Agril and Food Chem, 52, #26, 6212-6216 

Wei, Shu; Reuveny, Haim; Bravdo, Ben-Ami; Shoseyov, Oded 

1562 Volaitles in Monitoring seasonal variation in apple fruit volatile in situ GC 

apples emissions in situ using SPME 

Phytochemical Analysis, 14, No 4, 232-240 

Hern, Alan; Dorn, Silvia 

1563 Esters in Ester variability in apple varieties as determined PDMS fiber GC-MS 

apples by SPME-GC-MS Headspace 

J Agril and Food Chem, 52, #26, 8086-8093 

Young, J. C.; Chu, C. L. G.; Lu, X. W.; Zhu, H. H. 

1564 Volaitles in Potential of SPME-GC and chemometrics to detect Headspace GC-FID 

stawberry vs adulteration of soft fruit purees. GC-MS 

a puree J Agr Food Chem, 52, #3, 421-427 

Reid, L.; Oapostrophe Donnell, C.; Downey, G. 

1565 Solvents in Development of headspace SPME-GC method for the various fibers GC-FID 

edible oils, determination of solvent residues in edible oils headspace GC-ECD 

pharmaceutics and pharmaceuticals 

J. Chromatogr. A, 1071, #1-2, 119-124 

Michulec, M.; Wardencki, W. 

1566 Volatiles in Identification of volatile compounds in structured lipid of headspace GC-MS 

safflower oil safflower oil using electronic nose and SPME-GC-MS 

Agr Chem&Biotechnogy, 46, #4, 152-155 

Shin, Jung-Ah; Lee, Jong-Ho; Lee, Ki-Teak 

1567 Volatiles in Comparative study on volatile analysis of extra virgin 100µm PDMS GC-MS-TOF 

olive oils olive oil by dynamic headspace and SPME 65µm PDMS-DVB 

Food Chemistry, 90, #1-2, 69-79 headspace 

Kanavouras, A.; Kiritsakis, A.; Hernandez, R. J. 

1568 Volatiles in Application of SPME in the analysis of volatile oils. 100µm PDMS GC 

olive oils compounds in virgin olive oils. 15 min @ 45°C 

J Chromatogr A, 1028, #2, 321-324 headspace 

Jimenez, A.; Beltran, G.; Aguilera, M. P. 

1569 Volatiles in Analysis of virgin olive oil volatiles by a novel electronic headspace SAW 

olive oils nose based on a miniaturized SAW sensor array GC 

coupled with SPME enhanced headspace enrichment 

J AgriFood Chem, 52, #25, 7475-7479 

Garcia-Gonzalez, D.; Barie, N; Rapp, M; Aparicio, R 

1570 Terpenes A chemical investigation by headspace SPME and headspace GC-MS 

in olibanum GC-MS of volatile and semi-volatile terpenes in 

various olibanum samples 

Phytochemistry (Amsterdam), 66, #12,1499-1514 

Hamm, S; Bleton, J; Connan, J; Tchapla, A 





1571 Terpenes & Characterization of three Agave species by GC headspace GC, GC-MS 

fatty acids in and SPME-GC-MS steam distillation 

plants J Chromatogr A, 1027, #1-2, 131-136 

Pena-Alvarez, A.; Diaz, L.; Medina, A.; Labastida, C.; 

Capella, S.; Vera,L.. 

1572 Volatiles Analysis of volatile secondary metabolites headspace GC-MS 

in fruit from Colombian Xylopia ronatica (Lamarck) by 

different extraction and headspace methods and GC 

J Chromatogr A, 1025, #1, 105-113 

Stashenko, E.; Jaramillo, B.; Martinez, J 

1573 Volatiles Comparison of volatile compounds of corn oil and headspace GC-MS 

in corn oil modified corn oil by electronic nose and SPME-GC-MS 

Agri Chem and Biotechnology, 47, #3, 153-156 

Vu, Phuong-Lan; Shin, Jung-Ah; Lee, Ki-Teak 

1574 Review Application of the SPME and in food analysis 100µm PDMS GC-MS 

Polish J Food and Nutrition Sci, 13, #4, 355-361 85µm polyacrylate 

Ligor, Magdalena; Wojcik, Jan; Buszewski, Boguslaw headspace 

1575 Volatiles from Steam distillation-SPME for the detection of headspace GC-MS 

essential oils Ephedra sinica in herbal preparations 

J Chromatogr A, 1025, #1, 51-56 

Tellez, M.; Khan, I.; Schaneberg, B.; Crockett, S.; 

Rimando, A.; Kobaisy,M 

1576 Volatiles from Testing of microencapsulated flavours by electronic headspace GC-MS 

essential oils nose and SPME-GC 

Food Chem, 92, #1, 45-54 

Baranauskiene, R; Venskutonis, P, Galdikas,A., 

Senuliene, Daiva; Setkus, Arunas 

1577 Organo- SPME-GC-MS a fast and simple screening method headspace GC-MS 

phosphorus for the assessment of organophosphorus 

pesticides pesticides residues in wine and fruit juices. 

in wine/juice Food Chemistry, 86,#2, 269-274 

Zamabonin, C; Quinto, M; deVietro, N; Palmisano, F 

1578 Volatiles Metabolites of lesser grain borer in grains. headspace GC-MS 

from wheat J Agrl Food Chem, 52, #4, 898-908 0-240min @ 20°-40°C 

Seitz, L. M.; Ram, M. S. 

1579 Volatiles of Headspace SPME-GC-Mass spectrometric headspace GC-MS 

essential oils analysis of the essential oils of two traditional 

Chinese medicines, Angelica pubescens and 

Angelica sinensis. 

Chromatographia, 59, #5-6, 343-349 

Song, G. X.; Deng, C. H.; Wu, D.; Hu, Y. M.* 

1580 Organo- SPME-multicapillary GC coupled to different headspace ICP-MS, MIP-AES, 

selenium in detection systems and applied to volatile AFS 

yeast organo-selenium speciation in yeast. 

J Analytical Atomic Spectrometry, 19, #2, 260-266 

Dietz, C.; Sanz Landaluze, J.; Ximenez-Embun, P.; Madrid-Albarran, Y.; 

Camara, C. 

1581 Organo- Volatile organoselenium monitoring in production and gastric headspace MIP-AES 

selenium in digestion processes of selenized yeast by SPME-multicapillary 

yeast GC coupled microwave-induced plasma atomic 

emission spectrometry 

Appl. Organomet. Chem., 18, #12, 606-613 

Camara, C.; Dietz, C.; Madrid, Y.; Sanz Landaluze, J. 

1582 Sulfur compd Production of volatile organic sulfur compounds (VOSCs) headspace GC-MS 

in yeast by basidiomycetous yeasts 

FEMS Yeast Research, 5, #4-5, 379-385 

Buzzini, Pietro; Romano, Sergio; Turchetti, Benedetta; 

Vaughan, Ann; Pagnoni, Ugo Maria; Davoli, Paolo 





1583 Methyl Direct coupling of SPME and quartz tube-atomic 65µm PDMS-DVB GC-MS, AA 

mercury in absortpion spectrometry for selective and sensitive bare silica fiber 

seafood determination of methylmercury in seafood: An headspace 

assessment of chloride & hydride generation chloride derivative. 

J Analytical Atomic Spectrometry, 19, #2, 220-254 

Fragueiro, S; Lavilla, I; Bendicho, C. 

1584 Flavor volatiles Volatile profile, sensory attributes, and quality of headspace GC-MS 

in cantaloupe freshcut cantaloupe is maturity-at-cutting dependent 

Hortscience, 38, #5, 833 

Beaulieu, John C.; Bett, Karen L. 

1585 Fatty acids Fatty acid composition of tomato affects fruit and GC-MS 

in tomatos leaf biosynthesis of C6 aldehydes and alcohols. 


Canoles, M; Li, C; Howe, Gg; Beaudry, R 

1586 C6 aldehydes Rapid determination of C6-aldehydes in tomato plant emission 65µm PDMS-DVB GC-MS 

in tomatos by GC-MS and SPME with on-fiber derivatization 5 min @ 25ºC 

J Sep Science, 28, #2, 172-176 PFBHA derivatives 

Deng, Chunhui; Li, Ning; Zhu, Weimin; Qian, Ji; headspace 

Yang, Xiaofeng; Zhang, Xiangmin 

1587 Sulfur aroma The measurement of sulfur-containing aroma compounds in headspace GC-FPD 

from Beer samples from production-scale brewery operations 

JAm Society of Brewing Chemists, 63, #3, 129-134 

Miracle, R. E.; Ebeler, S. E.; Bamforth, C. W. 

1588 Aldehydes in Determination of C3-C10 aliphatic aldehydes using PFBHA PFBHA derivatives GC 

beer derivatization and SPME.Application to the analysis of beer 20min @ 20°C 

Chemia Analityczna, 49, #6, 869-880 headspace 

Jelen, H.; Dabrowska, A.; Klensporf, D.; Nawrocki, J.; Wasowicz,E. 

1589 Volatiles from Volatile compounds of Aspergillus strains with different headspace @ GC 

wheat grain abilities to produce ochratoxin A 20° to 27°C 

J Agri Food Chem, 53, #5, 1678-1683 

Jelen, Henryk H.; Grabarkiewicz-Szczesna, Jadwiga 

1590 Volatiles from Comparison of methodologies for the identification of aroma headspace GC-MS 

strawberries compounds in strawberry 

Turk. J. Agric. For., 29, #5, 383-390 

Bar, E; Kafkas, E; Kafkas, S; Koch-Dean, M.Larkov, O; Lavid, N 

Lewinsohn, Efraim; Ravid, Uzi; Schwab, Wilfried 

1591 Volatiles from Analysis of strawberry volatiles using comprehensive two- headspace GC-GC 

strawberries dimensional gas chromatography with headspace SPME 

J Chromatogr, B:817, # 1, 97-107 

Williams, A.; Ryan, D.; Guasca, A.; Marriott, P.; Pang, E. 

1592 Off-odour in Main compounds responsible for off-odour of strawberries headspace GC-olfactometry 

strawberries infected by Phytophthora cactorum 

Letters in Applied Microbiology, 40, #4, 255-259 

Jelen, H. ; Krawczyk, J.; Larsen, T. ; Jarosz, A.; Golebniak, B. 

1593 Volatiles from Volatile compounds as markers for coliforms 15 min headspace GC 

strawberries inoculated on strawberry fruit. 


Yu, K; Elgaali, H; Hamilton-Kemp, T; Newman, M; 

Collins, R; Archbold,D. 

1594 Sulfur volatiles SPME-GC-MS analysis of garlic oil obtained various fibers GC-MS 

from garlic by hydrodistillation headspace 

J. Chromatogr. A, 1036, #1, 91-93 

Calvo-Gomez, O.; Lopez, M.; Morales-Lopez, J. 

1595 Garlic flavor Comparative study of extraction techniques for 50/30µm DVB/CAR GC-MS 

components determination of garlic flavor components by GC-MS headspace 

Anal. Bioanal. Chem., 377, #4, 749-756 

Kim, Nam-Sun; Lee, Dong-Sun; Lee, Sun-Neo 





1596 Volatiles from SPME and GC-MS of volatile compounds from headspace GC-MS 

avocado avocado puree after microwave processing 30sec microwave 

J. Chromatogr. A, 1036, #1, 87-90 pH 5.5 

Dorantes, A.; Guzman, G; Lopez, M. 

1597 Oxidative Synergistic Effect of BSA on Antioxidant Activities in GC+G742 

byproducts in Model Food Emulsions 

sunflower oil J Am Oil Chem Soc, 81, #3, 275-280 

Almajano, M. Pilar; Gordon, Michael H. 

1598 Oxidative Study of both sunflower oil and its headspace throughout the headspace @ 70°C GC-MS 

byproducts in oxidation process. Occurrence in the headsapce of 

sunflower oil toxic oxygenated aldehydes 

J Agr& Food Chemistry, 53, #4, 1093-1101 

Guillen, Maria D.; Cabo, Nerea; Ibargoitia, Maria L.; Ruiz, A 

1599 Permethrin SPME of permethrin residues from cucumber using 75µm Carboxen/PDMS GC 

on cucumbers a silica-bonded phase-coated stainless steel fibre. 100µm PDMS 

Food Additives & Contaminants, 21, #3. 222-231 headspace 

Noroozian, E.; Kazemipour, M.; Tehrani, M.; Mahmoudian, M. 

1600 Volatiles in Application of headspace SPME and comprehensive headspace GC-GC 

herbal mixture two-dimensional gas chromatography (GC x GC) for the 

chemical profiling of volatile oils in complex herbal mixtures 

J. Sep. Sci., 27, #5-6, 451-458 

Di, Xin; Huie, C.; Marriott, P.; Shellie, R. 

1601 Solvents in Determination of residual solvents content headspace GC-FID 

plant oil (hexane residue) in plant oil by headspace SPME 

Fenxi Shiyanshi, 23, #4, 70-72 

Lan, F.; Xie, L. Q.; Yang, Z.; Pan, K. Y.; Wu, C. 

1602 Fungus Early detection of fungal growth in bakery products by use headspace GC/MS 

backery of an electronic nose based on mass spectrometry 

products J Agr Food Chem, 52, #20, 6068-6074 

Vinaixa, M.; Marin, S.; Brezmes, J.; Llobet, E.; 

Vilanova, X.; Correig, X.; Ramos, A.; Sanchis, V. 

1603 Odors from Investigation of the interaction of active packaging headspace GC-MS 

packaging material with food aroma compounds 

Sens Actuators, B Chem, 106, #1, 83-87 

Pastorelli, S.; Simoneau, C.; Strathmann, S. 

1604 N-nitrosamines A method for the determination of volatile N -nitrosamines 65µm PDMS-DVB GC-TEA 

in sausage in food by HS-SPME-GC-TEA. 85µm polyacrylate 

Food Chemistry, 91, #1, 173-179 headspace 

Andrade, R.; Reyes, F. G. R.; Rath, S. 

1605 Flavor SPME-GC-MS analysis of volatile organic compounds in GC-MS 

Volatiles honey from Basilicata. Evidence for the presence of 

from honey pollutants from anthropogenic activities 

Intl J Food Sci & Tech; 39, #10, 1079-1086 

Bentivenga, G; D'Auria, M; Fedeli, P; Mauriello, G; 

Racioppi, R 

1606 Monoterpenes SPME-GC-MS determination of monoterpenes in honey 100µm PDMS GC-MS 

in honey J. Sep. Sci.,27, #17-18, 1540-1544 15min @ 20°C 

Pena, Rosa M.; Barciela, Julia; Herrero, C; Garcia-Martin, S agitated, 25% salt 

1607 Aroma Evaluation of four isolation techniques for honey headspace GC 

Volatiles aroma compounds. 

from honey J Sci of Food and Agriculture, 85, #1,91-97 

Alissandrakis, E.; Tarantilis, P. A.; Harizanis, P.; Polissiou, M. 

1608 Aroma Characterization of Spanish unifloral honeys by SPME-GC-MS headspace GC-MS 

Volatiles J. Sep. Sci., 28, #9-10, 1093-1100 

from honey de la Fuente, Esther; Martinez-Castro, Isabel; Sanz, Jesus 





1609 Aroma Estimation of the honeydew ratio in honey samples from headspace GC-MS 

Volatiles their physicochemical data and from their volatile composition 

from honey obtained by SPME and GC-M 

J Sci of Food and Agriculture, 85, #817-824 

Soria,A; Gonzalez, M; deLorenzo, C; MartinezCastro,I; Sanz, J 

1610 Flavors in Profiling flavor compounds of potato crisps during storage 65µm PDMS-DVB GC-MS 

potato crisps using SPME 20min @ 70°C 

J Chromatogra, A, 1064, #2, 239-245 headspace 

Sanches-Silva, A; Lopez-Hernandez, J; Paseiro-Losada, P 

1611 Rancidity in Fast detection of rancidity in potato crisps using e-noses headspace GC-MS 

potato crisps based on mass spectrometry or gas sensors 


Badia, C.; Brezmes, J.; Correig, X.; Duran, C.; Llobet, E.; 

Vergara, A.; Vilanova, X.; Vinaixa, M. 

1612 Rancidity in A fuzzy ARTMAP- and PLS-based MS e-nose for the headspace GC-MS 

potato crisps qualitative and quantitative assessment of rancidity of crisps 


Brezmes, J.; Correig, X.; Llobet, E.; Vilanova, X.; Vinaixa, M. 

1613 PAHs in Headspace SPME as a tool to estimate the contamination 85µm polacrylate GC-MS 

smoked of smoked cheeses by polycyclic aromatic hydrocarbons 60min @ 70°C 

cheese J of Dairy Science, 88, #1, 13-20 headspace 

Guillen, M. D.; Sopelana, P. 

1614 Terpenes Application of artificial neural network on mono-and headspace GC-MS 

from cheese sequiterpenes compounds determined by headspace 

SPME-GC-MS for the Piedmont ricotta cheese traceability 

J Chromatogra, A, 1071, #1-2, 247-253 

Giuseppe, Z; Manuela, G; Marta, Bo; Vincenzo, G 

1615 Review of Calibration of gas chromatography inlet splitting for GC GC 

technique olfactometry dilution analysis 

Flavour Fragrance J., 19, #6, 518-521 

Acree, T.; Deibler, K.; Lavin, E.; Llesca, F. 

1616 Volatile free Volatile free fatty acids as ripening indicators for Serra headspace GC 

fatty acids in da Estrela cheese 

cheese J Dairy Sci, 87, #12, 4064-4072 

Tavaria, F. K.; Ferreira, A. C. Silva; Malcata, F. 

1617 Aroma of Composition and aroma compounds of Ragusano headspace GC 

cheese cheese: Native pasture and total mixed rations. 

J Dairy Sci, 87, #4, 816-830 

Carpino, S.; Mallia, S.; LaTerra, S.; Melilli, C.; Licitra, G.; 

Acree, T.; Barbano, D.; VanSoest, P. 

1618 Aroma of Comparison of purge and trap and SPME techniques for headspace GC 

cheese studying the volatile aroma compounds of three European 

PDO hard cheeses 

International Dairy Journal, 15, #6-9, 741-758 

Mallia, S.; Fernandez-Garcia, E.; Bosset, J. Olivier 

1619 Aroma of Characterization of "Provola dei Nebrodi", a typical Sicilian headspace GC-MS 

cheese cheese, by volatiles analysis using SPME-GC/MS 

International Dairy Journal, 15, #6-9, 585-593 

Ziino, M.; Condurso, C.; Romeo, V.; Giuffrida, D.; Verzera, A. 

1620 Aroma of SPME and GC-MS for rapid characterisation of headspace GC-MS 

cheese semi-hard cheeses 

Anal. Bioanal. Chem., 380, #7-8, 930-936 

Condurso, C.; Romeo, V.; Verzera, A.; Zappala, M.; Ziino, M. 

1621 Sulfur compd Volatile sulfur compounds in Cheddar cheese determined 75µm Carboxen GC-PFPD 

in cheese by headspace SPME and GC-pulsed FPD headspace 

J Chromatogr A, 1066, #1-2, 149-157 

Burbank, Helen M.; Qian, Michael C. 





1622 Aroma of Analysis of volatile aroma compounds of fresh chilli headspace GC-MS 

chilli (Capsicum annuum) during stages of maturity using SPME 30min @ 60°C 

J Food Composition & Analysis, 18, #5, 427-437 

Mazida, M. M.; Salleh, M. M.; Osman, H. 

1623 Volaitles from SPME Ccmbined with GC and olfactometry-MS 75µm Carboxen GC-MS 

cheese for characterization of cheese aroma compounds. headspace GC-olfactometry 

Lebensmittel-Wissenschaft & Technologie, 37, #2, 139-154 9-16hr extract 

Frank, D.; Owen, C.; Patterson, J. 

1624 Flavors from Improved determination of flavour compounds in headspace GC-GC-TOFMS 

butter butter by SPME & comprehensive two-dimensional GC GC-FID 

J. Chromatogr. A 1086, #1-2, 99-106 

Adahchour, M., Brinkman, U.; Verdel, R., 

Vreuls, R.; Wiewel, J. 

1625 Aroma Effect of thickeners and sweeteners on the release headspace GC 

compounds of blended aroma compounds in fat-free stirred 

in yoghurt yoghurt during shear conditions 

Intl Dairy Journal, 14, #9, 783-789 

Decourcelle, N.; Lubbers, S.; Vallet, N.; Rondeau, P.; 

Guichard, E. 

1626 Volaitles from Optimization of SPME for the analysis of volatile headspace GC 

milk compounds in milk. 

Journal of Dairy Science, 86, Supplement 1, 294 

Clarkson, H.; Duncan, S.; O'Keefe, S. 

1627 Volaitles from Volatile compounds and chemical changes in headspace @ 5°C GC-MS 

milk ultrapasteurized milk packaged in polyethylene 

terephthalate containers 

J of Food Science, 70. #6, C407-C412 

Solano-Lopez, C.; Ji, T.; Alvarez, V. 

1628 Phthalate Development of a headspace SPME method combined 60min @ 90°C. GC-MS 

esters in w/ GC-MS for the determination of phthalate esters headspace 

cow milk in cow milk NaCl added 

Analytica Chimica Acta, 538, #1-2, 41-48 

Feng, Yong-Lai; Zhu, Jiping; Sensenstein, R. 

1629 Aromatic SPME coupled with HPLC for the analysis 50µm CW-TPR LC-diode array 

amines of heterocyclic aromatic amines. methanolic NaOH 

in food J Chromatogr A, 1030, #1-2, 87-93 

Cardenes, L.; Ayala, J.; Afonso, A.; Gonzalez, V. 

1630 Isothiocynates SPME-GC-MS analysis of horseradish (Armoracia rusticana) GC-MS 

in horseradish Italian J Food Sci, 16, #4,487-490 

D'Auria, M.; Mauriello, G.; Racioppi, R. 

1631 Volatiles from Volatile compounds in different cultivars of Apium headspace GC-MS 

cultivars graveolens L. 

Italian J Food Sci, 16, #4, 477-482 

Tirillini, B.; Pellegrino, R.; Pagiotti, R.; 

Pocceschi, N.; Menghini, L. 

1632 Volatiles in Tequila volatile characterization and ethyl ester determination 100µm PDMS GC-MS 

tequila by SPME-GC-MS analysis 60min @ 40°C 

J Agri and Food Chem, 52, #18, 5567-5571 immersed 

Vallejo-Cordoba, B.; Gonzalez-Cordova, A.; . 

del Carmen Estrada-Montoya, M. 

1633 Volatile aroma Rapid determination of volatile compounds in grapes by 65µm DVB-PDMS GC 

compounds HS-SPME coupled with GC-MS 20 min @ 70°C 

in grapes Talanta, 66, #5, 1152-1157 headspace 

Sanchez-Palomo, E.; Diaz-Maroto, A. ; Perez-Coello, A. 





1634 Fermentation Stable isotope dilution analysis of wine fermentation products headspace GC-MS 

products of by HS-SPME-GC salt addition 

wines Anal. Bioanal. Chem., 381, #4, 937-947 

Capone, D.; Herderich, M.; Neuwohner, C.; Pardon, K.; 

Pollnitz, A.; Sefton, M; Skouroumounis, G.; 

Smyth, H.; Siebert, T. 

1635 Monoter- Comparison of ultrasound-assisted extraction and direct immersion GC-MS 

penoids in immersion SPME method for the analysis of monoterpenoids 

wine in wine 

Talanta, 67, #1, 129-135 

Barciela, J.; Garcia-Martin, S.; Herrero, C.; Pena, R. 

1636 Volatiles in Analytical method for determination of some 50/30µm DVB/CAR GC 

white wine aroma compounds on white wines by SPME-GC Headspace 

J of Food Sci, 68, #9, 2817-2820 

Ferreira, A.; Guedes de Pinho, P. 

1637 Methoxy- Analysis of methoxypyrazines in wine using Headspace GC-GC-NPD 

pyrazine headspace SPME with isotope dilution and GC-GC-TOFMS 

in wine comprehensive two dimensional GC 

J. Sep. Sci., 28, #9-10, 1075-1082 

Allen, M.; Marriott, P.; Ryan, D.; Smith, J.; Watkins, P. 

1638 Volatiles in GC profile of volatiles in cheese induced by headspace GC 

cheese different fat globule surface coatings. 

J of Dairy Science, 86, Supplement 1, 43 

Everett, D. ; Crownshaw, J.; Ginestet, A.; 

Leus, M.; Dufour, J.. 

1639 Flavors in Flavor stability of skim and whole milk powder. GC 

milk products J of Dairy Science, 86, Supplement 1, 40 

Whetstine, M.; Drake, M..; Karagul-Yuceer, Y.; Avsar, Y. 

1640 Methyl GC-MS with SPME method for determination of 100µm PDMS GC-MS 

salicylate in methyl salicylate and other volatile compounds in Headspace 

tomato leaves leaves of Lycopersicon esculentum. 


Deng, C; Zhang, X; Zhu, W; Qian, J 

1641 Flavors in SPME for flavor analysis in Harari Khat 100µm PDMS GC-MS 

Harari Khat (Catha edulis) stimulant. 30min @ 20°C 

stimulant J. Zhejiang Univ: Sci, 5, #4, 428-431 

Abdulsalam, Al-Flahi; Yin, Xue-Feng; Zou, Jian-Kai 

1642 Nonvolatiles Interactions between volatile and nonvolatile coffee headspace GC 

from brewed components. Screening of nonvolatile components 

coffee J Agr Food Chem., 53, #11, 4417-4425 

Charles-Bernard, M.; Kraehenbuehl, K.; 

Rytz, A.; Roberts, D. 

1643 Volatiles in Comprehensive multidimensional GC for the headspace GC-GC 

coffee beans characterization of roasted coffee beans 

J. Sep. Sci., 27, #5-6, 442-450 

Casilli, A., Costa, R.; Dugo, G., Dugo, P.; Festa, S.; 

Mondello, L.; Tranchida, P. 

1644 Volatiles in Analysis of roasted coffee bean volatiles by using headspace GC-GC-TOF-MS 

coffee beans comprehensive two-dimensional GC-TOF-MS 

J. Chromatogr. A, 1054, #1-2, 57-65 

Casilli, A.; Marriott, P.; Mondello, L.; Ryan, D.; 

Shellie, R.; Tranchida, P. 

1645 Volatiles in Reliable characterization of coffee bean aroma headspace GC-MS 

coffee beans profiles by automated headspace SPME-GC-MS with 

the support of a dual-filter mass a dual-filter spectra library 

J. Sep. Sci., 28, #9-10, 1101-1109 

Casilli, A, Costa, R; Dugo, G, Dugo, P; Festa, S; 

Mondello, L; Tranchida, P. 





1646 Furan in Determination of furan levels in coffee using headspace GC-MS 

coffee automated SPME-GC-MS 

JAOAC Intl, 88, #2,574-576 

Ho, I-Pin; Yoo, Seong-Jae; Tefera, Sebhat 

1647 Volatiles in SPME-GC-MS and multivariate analysis headspace GC-MS 

roasted for the characterization of roasted coffees 

coffee Talanta, 66, #1, 261-265 

Zambonin, C.; Balest, L.; De Benedetto, G.; Palmisano, F. 

1648 Essential oils A direct liquid, non-equilibrium SPME application 100µm PDMS fiber GC-MS 

from leaves for analysing chemical variation of single peltate immersed 

trichomes on leaves of Salvia officinalis. 

Phytochemical Analysis, 15, #3, 198-203 

Grassi, P.; Novak, J.; Steinlesberger, H.; Franz, C. 

1649 Aroma from GC-olfactometric characterization of aroma active Headspace GC-FID 

Tarhana compounds in sun-dried and vacuum-dried tarhana 

European Food Res &Tech, 218, #6, 573-578 

Goemen, D; Gurbuz, O; Rouseff, R; Smoot, J.; Dagdelen, A 

1650 Aroma from Lactic acid fermentation of Brassica rapa: headspace GC-FID 

fermentation chemical and microbial evaluation of a typical 

process Italian product (brovada) 

European Food Res &Tech, 218, #5, 469-473 

Maifreni, Michela; Marino, Marilena; Conte, L 

1651 2,4,6-trichloro Relationship between sensory and instrumental Headspace GC-ECD 

anisole in analysis of 2,4,6-trichloroanisole in wine and cork 

wine/cork stoppers 

Anal. Chim. Acta, 513, #1, 291-297 

Antico, E.; Garcia Regueiro, J.A.; Guerrero, L.; Insa, S.; . 

Juanola, R.; Salvado, V.; Subira, D 

1652 Chlloro- Assay of stability, free and total concentration of headspace GC 

hexidine in chlorhexidine in saliva by solid phasemicroextraction 

saliva J Pharma and Biomed Analysis, 37, #5, 1015-1024 

Musteata, Florin Marcel; Pawliszyn, Janusz 

1653 Pyrazines Improving headspace-SPME of 3-isobutyl-2- headspace GC-MS 

in wine methoxypyrazine by experimental design with regard saturated salt 

to stable isotope dilution GC-MS analysis of wine 

Anal. Chim. Acta, 513, #1, 223-227 

Lucchese, Y.; Nepveu, F.; Prouteau, C.; Renard, R.; 

Schneider, R.;Vaca-Garcia, C. 

1654 Terpenes in Optimization of SPME methods for GC-MS 100µm PDMS GC-MS 

wine determination of terpenes in wine 15min @ 20°C 

J Sci of Food and Agr, 85, #7, 1227-1234 immersed 

Pena, R.; B, Julia; Herrero, C; Garcia-Martin, S. 25% NaCl 

1655 Volatiles in Characterization of the aroma profile of Madeira wine headspace GC-MS 

red wine by sorptive extraction techniques 

Anal. Chim. Acta, 546, #1, 11-21 

Alves, R.F.; Nascimento, A.M.D.; Nogueira, J.M.F. 

1656 Flavors from Varietal flavour compounds of four grape varieties dynamic headspace GC-MS 

Madeira wine producing Madeira wines 

Analytica Chimica Acta, 513, #1, 203-207 

Camara, J.; Herbert, P.; Marques, J.; Alves, M. 

1657 Volatiles in Elimination of matrix effects for headspace SPME of 65µm PDMS-DVB, GC 

red wine important volatile compounds in red wine using a novel coating 85µm polyacrylate 

Anal. Chim. Acta, 540, #2, 341-353 100µm PDMS 

Liu, Mingming; Tian, Yun; Zeng, Zhaorui headspace 

1658 Sulfur Sensitive quantification of sulfur compounds in wine by headspace GC-FPD 

compounds headspace solid-phase microextraction technique 

in wine J. Chromatogr. A, 1080, #-2, 177-185 

Fang, Yu; Qian, Michael C. 





1659 Fungicides Screening of grapes and wine for azoxystrobin, headspace GC-MS 

on grapes kresoxim-methyl and trifloxystrobin fungicides 

by HPLC with diode array detection 

Food Additives and Contaminants, 22, #6, 549-566 

Abreu, S.; Correia, M.; Herbert, P.; 

Santos, L.; Alves, A. 

1660 Tribromo- Determination of 2,4,6-tribromoaniline in the color additives headspace GC-MS 

aniline in D&C Red Nos. 21 and 22 (Eosin Y) using SPME-GC-MS 

color additives J. Chromatogr. A, 1057, #1--2, 185-191 

Andrzejewski, Denis; Rasooly, Irit R.; Weisz, Adrian 

1661 Ochratoxin A Determination of Ochratoxin A in foods: State-of-the-art LC-FLD 

in foods and analytical challenges 


Monaci, Linda; Palmisano, Francesco 

1662 Volatiles in Comparative analysis of volatile compounds of headspace GC-MS 

sherry wine "fino" sherry wine by rotatory and continuous liquidliquid 

extraction and SPME in conjunction w/GC-MS 

Anal. Chim. Acta, 513, #1, 141-150 

Barroso, C.G.; Benitez, P.; Castro, R.; Natera, R. 

1663 Volatiles in Application of a wavelet-based algorithm on headspace GC-MS 

vinegars headspace SPME-GC signals for the classification 

of balsamic vinegars. 

Chemometrics and Intelligent Lab Systems, 71, #2, 129-140 

Cocchi, M.; Durante, C.; Foca, G.; Manzini, D.;. 

Marchetti, A.; Ulrici, A. 

1664 Flavors from Flavour release and rheology behaviour of headspace @ 10°C GC 

yogurt strawberry fat-free stirred yogurt during storage. stirred 

J Agri and Food Chemistry, 52, #10, 3077-3082 

Lubbers, S.; Decourcelle, N.; Vallet, N.; Guichard, E. 

1665 Aroma of Solid-phase aroma concentrate extraction (SPACE): headspace GC-MS 

coffee beans a new headspace technique for more sensitive 

analysis of volatiles 

Flavour & Fragrance Journal, 19, #3, 183-187 

Ishikawa, M.; Ito, O.; Ishizaki, S.; 

Kurobayashi, Y.; Fujita, A. 

1666 Volatiles from Comparison of volatile compounds formed by 40°C headspace GC-MS 

cod liver oil autoxidation and photosensitized oxidation of cod ferrous chloride added GC-FID 

liver oil in emulsion systems foil lined sample vial 

Fisheries Science (Tokyo), 71, #3, 639-647 

Pan, Xiang-Qing; Ushio, Hideki; Ohshima, Toshiak 

1667 2,4,6- Detection of 2,4,6-trichloroanisole in microorganism- 50/30µm DVB/CAR GC-MS 

trichloroanisole free irradiated raisins by SPME-GC-MS headspace 

in raisins J Stored Products Res, 40, #4, 451-459 

Aung, L. H.; Jenner, J. F. 

1668 Anisoles in Simultaneous separation, clean-up and analysis headspace GC-MS-MS 

wines of musty odorous compounds in wines by on-line 

coupling of a pervaporation unit to GC- tandem MS 

Anal. Chim. Acta, 516, #1-2, 165-170 

Garcia-Barrera, T.; Gomez-Ariza, J.L.; Lorenzo, F. 

1669 Anisoles in Optimisation of a two-dimensional on-line coupling headspace GC-ECD-ICP-MS 

wines for the determination of anisoles in wineusing ECD 

and ICP-MS after SPME-GC separation 

Jof AnalyAtomic Spectrometry, 20, #9, 883-888 

Gomez-Ariza, J. L.; Garcia-Barrera, T.; Lorenzo, F. 

1670 Aroma volatile Aroma profile of strawberry juice cocktail produced 100µm PDMS GC-FID and GC-MS 

from in industrial conditions headspace 

stawberry Kem Ind, 54, #3, 135-141 

juice Cosic, B.; Ganic, K. Kovacevic; Komes, D.; Lovric, T. 





1671 Aroma Assessment of strawberry aroma through SPME- headspace GC-MS 

volatiles from GC and artificial neuron network methods. Variety 

stawberry Classification versus growing years. 

J Agri Food Chemistry, 52, #9, 2472-2478 

deBoishebert, V.; Urruty, L.; Giraudel, J.; Montury, M. 

1672 Triazine Hollow fiber membrane-protected SPME of triazine 65µm PDMS-DVB GC-MS 

herbicides in herbicides in bovine milk and sewage sludge samples 

milk/ sludge J. Chromatogr. A, 1047, #2, 189-194 

Basheer, Chanbasha; Lee, Hian Kee 

1673 Acrylamide Silylation of acrylamide for analysis by SPME-GC 100µm PDMS GC-MS 

in cereals ion-trap mass spectrometry BSTFA derivative 

J Agri and Food Chem, 52, #12, 3744-3748 headspace 

Lagalante, Anthony F.; Felter, Matthew A. 

1674 Quinoxyfen Influence of quinoxyfen residues on Saccharomyces GC 

pesticide in cerevisiae fermentation of grape musts 

grape musts Food Tech and Biotechnology, 42, #2, 89-97 

Lopez, C; Boselli, E; Piva, A; Ndaghijimana, M; 

Paparella, A; Antonello; S; Mastrocola, D 

1675 Pyrazine in Influence of vine training and sunlight exposure headspace GC 

musts/wines on the 3-alkyl-2-methoxypyrazines content in 

musts and wines from Vitis vinifera variety 

cabernet sauvignon 


Sala, C; Busto, O; Guasch, J; Zamora, Fernando 

1676 Volatiles from The effects of sample preparation and GC injection headspace GC-MS 

oak in wine techniques on the accuracy of measuring quaiacol, 

4-methylguaiacol and other volatile oak compounds 

in oak extracts by stable isotope dilution analyses 


Pollnitz, A.; Pardon, K.; Sykes, M; Sefton, M. 

1677 Volatiles Analysis of oak volatiles by GC-MS after ozone sanitization headspace GC-MS 

from Oak American J Enology & Viticulture, 56, #1, 46-51 5, 10, 15min sampling 

Marko, S.; Dormedy, E.; Fugelsang, K.; Dormedy, D.; 82°C 

Gump, B.; Wample, Robert 

1678 Volatiles Fast screening method for volatile compounds of oak wood 50/30µm DVB/CAR GC-MS (SIM) 

from Oak used for aging wines by headspace SPME-GC-MS (SIM) 40min @ 70°C 

wood J Agri and Food Chemistry, 52, #23, 6857-6861 Headspace 

Diaz-Maroto, M.; Sanchez-Palomo, Eva; Perez-Coello, M. 

1679 Volatiles in Rapid analysis of flavor volatiles in apple wine 75µm Carboxen GC-MS 

apple wine using headspace SPME Headspace 

J Institute of Brewing, 110, #1, 57-65 

Wang, L.; Xu, Y.; Zhao, G.; Li, J. 

1680 Volatiles from Markers for irradiated food headspace GC 

irradiated Chem. World, 2, #2, 20 

food Down, Steve 

1681 Volatiles from Development of SPME methodology for analysis 50/30µm DVB/CAR GC 

Beef of headspace volatile compounds in 60min @ 60°C 

extract simulated beef flavour. headspace 

Food Chemistry, 88, #1, 141-149 

Moon, S. Y.; Li-Chan, E. C. Y.* 

1682 Volatiles from Identification of radiolytic marker compounds in the headspace @ 30°C GC 

Beef irradiated beef extract powder by volatile analysis 

extract Microchemical Journal, 80. #2, 127-137 

Kim, Hun; Cho, Woo-; Ahn, Jun-; Cho, Dooe; Cha, Yong- 

1683 Volatiles from Characterization of volatile compounds of fruit juices headspace GC/MS 

fruit juices and nectars by headspace SPMEand GC-MS. 


Riu-Aumatell, M.; Castellari, M.; Lopez-Tamames, E.; 

Galassi, S.; Buxaderas, S. * 





1684 Volatiles from Effect of fat nature and aroma compound hydrophobicity headspace GC-MS 

food emulsions on flavor release from complex food emulsions 

J Agr and Food Chem, 52, #20, 6257-6263 

Relkin, Perla; Fabre, Marjorie; Guichard, Elisabeth 

1685 Volatiles from Characterization of volatile compounds of French headspace GC-RI and GC-MS, 

olive oil and Spanish virgin olive oils by HS-SPME: I. 

identification of quality-freshness markers 


Cavalli, J; Fernandez, X.; Lizzani-Cuvelier, L; Loiseau, A 

1686 Oxidative Oxidation of lipids in food headspace GC 

byproducts Polish JFood and Nutrition Sci, 13, #1, 87-100 

from lipids Wasowicz, E; Gramza, A; Hes, M; Jelen, H;Korczak,J; 

Malecka, M; Mildner-Szkudlarz, S; Rudzinska, M; 

Samotyja, U; Zawirska-Wojtasiak, R 

1687 Volatiles from Photo-oxidation of lipids impregnated on the surface headspace @ 45°C GC-FID and GC-MS 

sea weed of dried seaweed (porphyra yezoensis ueda). 

Characterization of volatiles 

JAOCS, 81, #8, 773-781 

Ohshima, Toshiaki; Pan, Xiangqing; Ushio, Hideki 

1688 Oxidation Lipid oxidation in high-pressure processed chicken 10min @ 80°C GC-MS 

byproducts breast during chill storage andsubsequent heat headspace 

from chicken treatment: effect of working pressure, packaging 

atmosphere and storage time 

European Food Res and Tech, 219, #2, 167-170 

Wiggers, S.; Kroeger-Ohlsen, M.; Skibsted, L. 

1689 Volatiles in Determination of organic volatile impurities in citric acid GC-MS 

Citric acid by SPME-GC 


Li, L. H.; Zheng, L.; Guo, W. 

1690 Hexanal in Determination of hexanal as indicator of the lipidic headspace GC-MS 

potato crisps oxidation state in potato crisps using GC and HPLC 2,4-dinitrophenyl- HPLC 

J. Chromatogr. A, 1046, #1-2, 75-81 hydrazone derivative. 

Lopez-Hernandez, J.; Paseiro-Losada, P.; Rodriguez- 

Bernaldo De Quiros, A.; Sanches-Silva, A. 

1691 Volatile thiol Variation in 4-mercapto-4-methyl-pentan-2-one release headspace GC-AED 

from wine by Saccharomyces cerevisiae commercial wine strains 

FEMS Microbiology Letters, 240, #2, 125-129 

Howell, K.; Swiegers, J.; Elsey, Go.; Siebert, T.; 

Bartowsky, E.; Fleet, G.; Pretorius, I.; Lopes, M. 

1692 Volatiles Determination of volatile compounds in wine by headspace GC-FID 

in wine automated SPME-GC 


Cabredo-Pinillos, S.; Cedron-Fernandez, T.; 

Parra-Manzanares, A.; Saenz-Barrio, C. 

1693 Off taste of Evaluation of the antimicrobial activity of citrus headspace GC-MS 

soft drink essences on Saccharomyces cerevisiae 

J Agrl and Food Chemis, 52. #23, 6932-6938 

Belletti, Nicoletta; Ndagijimana, Maurice; Sisto, C 

Guerzoni, Maria E.; Lanciotti, Rosalba; Gardini, F. 

1694 Methyloxime Phenylacetaldehyde O-methyloxime: A volatile oxime methyl ether GC-MS 

in grapefruit compound produced by grapefruit leaves infected derivatives 

leaves with the citrus canker pathogen, Xanthomonas headspace 

axonopodis pv. citri 

J Agrl and Food Chemis, 53. #13, 5134-5137 

Zhang, Aijun; Hartung, John S. 

1695 Aroma Analysis and characterization of aroma-active compounds headspace GC-MS 

of leaves of Schizandra chinensis (omija) leaves. 

J Sci of Food and Agriculture, 85, #1, 161-166 

Zheng, C. H.; Kim, K. H.; Kim, T. H.; Lee, H. J.* 





1696 Essential oils Comparison of three different SPME fibres for analysis of 100µm PDMS GC-FID 

from yacon essential oils in yacon (Smallanthus sonchifolius) leaves 65µm PDMS-DVB 

leaves J. Chromatogr. A, 1084, #1-2, 2-6 50/30µm DVB/CAR 

Adam, M.; Bajer, T.; Eisner, A.; Juklova, M.; Ventura, K. headspace 

1697 Essential oils Comparison of essential oil composition of Artemisia headspace GC-MS 

from argyi argyi leaves at different collection times by 

leaves headspace SPME-GC-MS 


Zheng, X. H.; Deng, C. H.; Song, G. X.; Hu, Y. M.* 

1698 Essential oils A SPME method to fingerprint dissolved organic 100µm PDMS GC 

from carbon released from Eucalyptus camaldulensis 15min @ 40°C, pH 2 

Eucalyptus Dehnh (River Red Gum) leaves saturated salt 

leaves Analytica Chimica Acta, 530, #2, 325-333 rapid stirring 

Zander, Alek; Bishop, Andrea G.; Prenzler, Paul D. 

1699 Off flavors Instrumental versus sensory detection of off- headspace GC-MS 

in catfish flavors in farm-raised channel catfish 

Aquaculture, 236, #1-4, 309-319 

Grimm, Casey; Lloyd, Steven; Zimba, Paul 

1700 Volaitiles from Composition of the essential oils and in vivo emission headspace GC-MS 

essential oils of volatiles of four Lamium species from Italy: L. 

purpureum, L hybridum , L bifidum & L.amplexicaule. 


Flamini, G.; Cioni, P. L.; Morelli, I. 

1701 Volatiles from The use of a non-equilibrated SPME method to headspace GC/SIM-MS 

essential oils quantitativelydetermine the off-notes in mint and 

other essential oil 

J Sci Food & Agri, 84, #10, 1223-1228 

Coleman, W. M., III.; Lawrence, B. M.; Craven, S. H. 

1702 Volatiles in Effect of gamma-irradiation on color, pungency, and headspace GC-MS 

red pepper volatiles of Korean red pepper powder 

Journal of Food Science, 69, #8, C585-C592 

Lee, J. H.; Sung, T. H.; Lee, K. T.; Kim, M. R. 

1703 Isothiocyanate Analysis of the isothiocyanates present in cabbage headspace GC-MS 

in cabbage leaves extract and their potential application 

leaves to controlAlternaria rot in bell peppers 

Food Res Intl., 38, #6, 701-708 

Troncoso, R.; Espinoza, C.; Sanchez-Estrada, A.;S. 

Tiznado, M. E.; Garcia, Hugo S. 

1704 Organo- New approach for the detection of organophosphorus headspace GC 

phosphate pesticide in cabbage using SPME/SnO2 gas sensor: 

in cabbage Principle and preliminary experiment 


Huang, Xingjiu; Liu, Jinhuai; Meng, Fanli; Sun, Yufeng 

1705 Off flavor Determination of off-flavour compounds in apple juice caused headspace GC-MS 

in apple juice by microorganisms using headspace SPME-GC-MS 

Anal. Chim. Acta, 520, #1-2, 3-11 

Pfannhauser, W.; Siegmund, B.; Zierler, B. 

1706 Volatiles from Study of the effect of different fiber coatings and 75µm Carboxen GC 

cured ham extraction condition on dry cured ham volatile 50/30µm DVB/CAR 

compounds extracted by SPME 15, 30, 60min extraction 

Talanta, 64, #2, 458-466 headspace 

Ansorena, D.; Astiasaran, I.; Garcia-Esteban, M.; Ruiz, J. saturated NaCl 

1707 Volatiles in Comparison of simultaneous distillation extraction and SPME 75µm Carboxen GC-MS 

cured ham for the analysis of volatile compounds in dry-cured ham. headspace 

J Sci Food and Agri, 84, #11, 1364-1370 

Garcia-Esteban, M.; Ansorena, D.; Astiasaran, I.; 

Martin, D.; Ruiz, J. * 





1708 Volatiles from Characterization of French and Spanish dry-cured hams: headspace GC 

hams influence of the volatiles from the muscles and the 

subcutaneous fat quantified by SPME-GC 

Meat Science, 69, #4, 635-645 

Sanchez-Pena, C.; Luna, G; Garcia-Gonzalez, D.; Aparicio, R 

1709 Chloroanisoles Optimisation of a headspace SPME method for the direct headspace GC-ECD 

in wine determination of chloroanisoles related to cork taint in red wine 

J. Chromatogr. A, 1056, #1-2, 49-56 

Gonzalez-Saiz, J.; Martinez-Urunuela, A.; Pizarro, C. 

1710 Chlorophenols Multiple SPME in a non-equilibrium situation: Application in headspace GC-MS 

in wine quantitativeanalysis of chlorophenols and chloroanisoles 

related to cork taint in wine 

J. Chromatogr. A, 1089, #1-2, 31-38 

Gonzalez-Saiz, J.; Martinez-Urunuela, A.; Pizarro, C. 

1711 Chlorophenols Development of solid-phase extraction and SPME 100µm PDMS GC-ECD 

in cork/wine methods for the determination of chlorophenols Acetylation derivative 

in cork macerate and wine samples headspace 

J. Chromatogr. A, 1047, #1, 15-20 

Antico, E.; Insa, S.; Salvado, V. 

1712 2,4,6-Trichloro- Migration of 2,4,6-trichloroanisole from cork stoppers to wine headspace GC-ECD 

anisole European Food Research and Tech, 220, #3-4,347-352 

in wine Juanola, R.; Subira, D.; Salvado, V.; Regueiro, J.; Antico, E. 

1713 Volatile esters Inhibition of the decline of volatile esters and terpenols headspace GC-MS 

in wine during oxidative storage of Muscat-white and Xinomavro- 20°C heated sample 

red wine by caffeic acid and N-acetyl-cysteine 

Food Chemistry, 93. #3, 485-492 

Roussis, I.; Lambropoulos, I; Papadopoulou, D 

1714 Volatiles in Volatile compounds of red and white wines by headspace 50/30µm DVB/CAR GC 

wine SPME using different fibres. 40min @ 35°C 

J of Chromatographic Sci, 42, #6, 310-316 headspace 

Torrens, J.; Riu-Aumatell, M.; Lopez-Tamames, E.; 

Buxaderas, S. * 

1715 Haloanisoles Optimisation of a two-dimensional on-line coupling for headspace GC-ICP-MS 

in wine the determination of anisoles in wine using ECD GC-ECD 

and ICP-MS after SPME-GC separation 

J Anal At Spectrom, 20, #9, .883-888 

Garcia-Barrera, T.; Gomez-Ariza, J.L.; Lorenzo, F. 

1716 Impurities A review of theoretical and practical aspects of SPME headspace GC 

constituents in food analysis 

additives IntL J Food Sci & Technology, 39, #7, 703-717 

flavours Wardencki, Waldemar; Michulec, Magdalena; Curylo, J. 

1717 Flavour from Relationship between procyanidin and flavour contents headspace HPLC-UV 

cocoa liqours of cocoa liquors from different origins. 


Counet, C.; Ouwerx, C.; Rosoux, D.; Collin, S. 

1718 Methylpyrazine Cocoa quality and processing: A study by SPME and GC headspace GC-MS 

in cocoa analysis of methylpyrazines 

Food Bioprod. Process., 82, #4C, 291-297 

Cavicchioli, M.; Del Borghi, M.; Fabiano, B.; Perego, P. 

1719 Chlorophenol Optimisation of the derivatisation reaction and headspace GC 

in red wine subsequent headspace SPMEmethod for the direct acetylated derivaties 

determination of chlorophenols in red wine 

J. Chromatogr. A, 1048, #2, 141-151 

Gonzalez-Saiz, J; Martinez-Urunuela, A; Pizarro, C. 

1720 Volatiles Headspace SPME-GC-MS analysis of the volatile 50/30µm DVB/CAR GC-MS 

from dried compounds of Evodia species fruits 18min @ 80°C 

fruit J. Chromatogr. A, 1087, #1-2, 265-273 headspace 

Benvenuti, S; Bertelli, D; Pellati, F; Rossi, M; Yoshizaki, F. 





1721 Volatiles Comparison of SPME, SFE, steam distillation, and solvent headspace GC-MS 

from dried extraction techniques for analysis of volatile consituents 

ripe fruit in Fructus amomi 

J AOAC Intl, 88, #2, 418-423 

Shen, S; Sha, Y; Deng, C; Fu, D; Chen, ; Zhang, Xian 

1722 Volatiles Rapid analysis of essential oil from Fructus Amomi by headspace GC-MS 

from dried pressurized hot water extraction followed by SPME-GC-MS 15min @ 80°C 

ripe fruit J Pharma& Biomedical Analysis, 38, #2, 326-331 

Deng, C; Wang, A; Shen, S; Fu, D; Chen, J; Zhang, X 

1723 Volatiles Sensory and instrumental evaluation of sweet marjoram headspace GC 

from sweet (Origanum majorana L.) aroma 

marjoram Flavour Fragrance J., 20, #5, 492-500 

Baranauskiene, R.; Demyttenaere, J.C.R.; Venskutonis, P. 

1724 Arom Trehalose improves flavour retention in dehydrated headspace GC-FID 

compouonds apricot puree GC-MS 

apricot puree Intl J Food Science & Tech, 40, #4, 425-435 

Komes, D; Lovric, T; Kovacevic G, Karin; 

Gajdos Kljusuric, Jasenka; Banovic, Mara 

1725 Volatiles from Volatile components of truffle species collected in Basilicata headspace GC-MS 

truffles Micologia Italiana, 30, #3, 11-29 

Mauriello, G.; Marino, R.; D'Auria, M.; Cerone, G.; Rana, G. L. 

1726 Volatiles from Sensitive detection of volatile organic compounds headspace GC-MS 

mould (MVOC) produced by mould by means of SPME-GC-MS 

Naunyn-Schmiedeberg's Archives of Pharmacology 

369, Suppl 1, R145 

Schuetz, E. 

1727 Phenylurea Application of SPME for determining phenylurea herbicides 85µm polyacrylate GC-NPD 

herbicides on and their homologous anilines from vegetables. headspace GC-MS-SIM 

vegetables J Chromatogr, A, 1042, #1-2, 9-14 14% salt, pH 11 

Berrada, H.; Font, G.; Molto, J. C.* 

1728 Volatiles in GC-mass Spectrometry coupled with SPME for 100µm PDMS GC-MS 

ginger determination of volatile constituents of chinese ginger headspace 

Fudan Xuebao Zirankexueban, 42, #6, 939-949 

Song Guo-xin; Deng Chun-hui; Wu Dan; Hu Yao-ming 

1729 MIBP in red Yield effects on 2-methoxy-3-isobutylpyrazine 50/30µm DVB/CAR GC-MS 

wine concentration in Cabernet Sauvignon using a SPME-GC-MS 30min @ 40°C 

J of Agri Food Chemistry, 52, #17, 5431-5435 30% NaCl 

Chapman, D. M.; Thorngate, J. H.; Matthews, M. A.; immersed sampling 

Guinard, J. -X.; Ebeler, S. E.* 

1730 Essential oils Volatile constituents of micropropagated plants of headspace GC and GC-MS 

from plants Bupleurum fruticosum L 

Plant Science (Oxford), 167, #4, 807-810 

Bertoli, Alessandra; Pistelli, Luisa; Morelli, lvano; 

Fraternale, Daniele; Giamperi, Laura; Ricci, Donata 

1731 Volatiles from Analysis of volatiles in porcine liver pates with added sage headspace GC-MS 

liver pates and rosemary essential oils by using SPME-GC-MS 


Estevez, Mario; Ventanas, Sonia; Ramirez, R; Cava, R 

1732 Volatiles in Determination of volatile compounds in antioxidant 50/30µm DVB/CAR GC-MS, GC-FID 

rosemary rosemary extracts by SPME-GC Preheat 15min @ 70C 

Analytical Letters, 38, #7, 1193-1212 Extract 60min @ 20C 

Carrillo, Jose David; Tena, Maria Teresa headspace 

1733 Volatiles from Kinetin enhanced linalool production by in vitro plantlets headspace GC 

plantlets of Lippia alba 

J. Essent. Oil Res., 16, #5, 405-408 

Bizzo, Humberto R.; Lage, Celso L.S.; Leitao, Suzana G.; 

Lopes, Daise; Tavares, Eliana S. 





1734 Volatiles in Optimization of wine headspace analysis by SPME 50/30µm DVB/CAR 

wine capillary GC-w/MS & FID headspace GC-MS 


Tat, L.; Comuzzo, P.; Stolfo, I.; Battistutta, F. 

1735 Chloroanisole Determination of chloroanisole compounds in red wine by headspace GC-MS 

in red wine headspace SPME AND GC-mass spectrometry 

J. Chromatogr. A, 1052, #1-2, 145-149 

Belsue, V; Gonzalez-Penas, E; Irigoyen, A; Lizarraga, E 

1736 Flavor volatiles Volatile flavour components of mandarin wine obtained headspace & GC-MS 

in madarin from clementines (Citrus reticula Blanco) extracted by SPME immersion sampling 

wine Flavour and Fragrance Journal. 19, #5, 413-416 

Selli, S.; Kurkcuoglu, M.; Kafkas, E.; Cabaroglu, T.; 

Demirci, B.; Baser, K. H. C.; Canbas, A. 

1737 Aroma Validation of a SPME method for headspace analysis 50/30µm DVB/CAR GC-MS 

components of wine aroma components headspace 

in wine Am J of Enology & Viticulture, 56, #1, 37-45 

Howard, Karen L.; Mike, James H.; Riesen, Roland 

1738 Volatiles from Interaction of soluble peptides and proteins from skeletal headspace GC 

meat curing muscle with volatile compounds in model systems as 

agents affected by curing agents 

J Agr Food Chem, 53, #5, 1670-1677 

Gianelli, M. Pia; Flores, Monica; Toldra, Fidel 

1739 Volatiles from Effect of Debaryomyces spp. on aroma formation and headspace GC-MS 

sausages sensory quality of dry-fermented sausages 

Meat Science, 68, #3, 439-446 

Flores, Monica; Dura, M-Asuncion; Marco, Aurora; Toldra, Fidel 

1740 Volatiles from Analysis of volatile components of fermented sausage headspace GC-MS 

sausages before and after ripeness by SPME-GC-MS 

Fenxi Ceshi Xuebao, 23, #6, 40-43 

Zhang, C. H. 

1741 Volatiles from Volatile compounds in Iberian dry-cured loin headspace GC-MS 

pig loin Meat Science, 68, #3, 391-400 

Muriel, E.; Antequera, T.; Petron, M.; Andres, A.; Ruiz, J. 

1742 Flavors in Characterization of Maltese goat milk cheese flavour headspace GC-MS 

goat milk using SPME-GC/MS 

cheese South African J of Animal Sci, 34, Suppl. 1, 176-180 

Chiofalo, B.; Zumbo, A.; Costa, R.; Liotta, L.; Mondello, L.; 

Dugo, P.; Chiofalo, V. 

1743 Volatiles Comparison of efficiency and stability of two headspace GC-MS 

from cheese preconcentration techniques (SPME and INDEx) coupled 

to an MS-based "Electronic Nose" 

Mitteilungen aus Lebensmitteluntersuchung und Hygiene 

Hygiene, 95, #1, 85-90 

Pillonel, L; Altieri, D; Tabacchi, R; Bosset, J 

1744 2-heptanone Significance of 2-heptanone in evaluating the effect of headspace GC-MS 

in goats milk microfiltration/pasteurisation applied to goats' milk 

International Dairy Journal, 14, #10, 915-921 

Avalli, Andrea; Povolo, Milena; Carminati, D; Contarini, G 

1745 Volatiles Qualitative and quantitative composition of the flavour headspace GC-MS 

from fruit components of Taiwan calamondin and Philippine Calamansi 

fruit 

European J of Horticultural Science, 69, #3, 117-124 

Yo, S.-P.; Lin, C.-H. 

1746 Off flavors Properties of soy protein isolate prepared from aqueous headspace GC-MS 

from soy alcohol washed soy flakes 

protein Food Res. Int., 38,#3, 273-279 

Hua, Yufei; Huang, Youru; Liu, Xiaoya; Qiu, Aiyong 





1747 Volatiles SPME analysis of volatile compounds from unfermented 65µm PDMS-DVB GC-MS 

from olives olives sujected to thermal treatment. headspace 

Anal & Bioanal Chem, 379, #5, 812-817 

Navarro, T.; de Lorenzo, C.; Perez, R. A.* 

1748 Volatiles A multivariate study of the relationship between fatty acids GC-MS 

from olive & and volatile flavor components in olive and walnut oils 

walnut oils J AO C Society, 82, #2, 105-110 

Torres, M.; Martinez, M.; Maestri, D. 

1749 Volatiles Simultaneous determination of volatile and semi-volatile headspace GC-MS 

from olive oil aromatic hydrocarbons in virgin olive oil by 

headspace SPME coupled to GC-MS 

J. Chromatogr. A, 1090. #1-2, 146-154 

Buxaderas, S.; Conte, L.; LopezTamames, E.; 

Pizzale, L.; Vichi, S. 

1750 Cannabinoids Determination of cannabinoids in hemp food MSTFA derivative GC-MS 

in food products by use of headspace SPME-GC-MS headspace 


Kroener, L.; Lachenmeier, ; Madea, B.; Musshoff, 

1751 Flavors from Use of SPME analysis for adsorption of the volatile 65µm PDMS-DVB GC-MS 

pineapple compounds in juices clarified by microfiltration. headspace 

juice Alimentaria, 41, #355, 35-39 

Carvalho, L.; Godoy, R..; Silva, C.; Miranda, R.; 

Figueira, J. 

1752 Volatiles in Analysis of volatile compounds in some typical 100µm PDMS GC-MS 

Brazilian fruits Brazilian fruits and juices by SPME-GC method 20min @ 50°C 

and juices Food Additives and Contaminants, 22, #6, 508-513 headspace 

Cardeal, Z.; Guimaraes, E.; Parreira, F. 

1753 Flavors from Storage and ultraviolet-induced tissue stress headspace GC 

pineapple effects on fresh-cut pineapple. 

J Sci Food and Agri, 84, #14, 1812-1816 

Lamikanra, O.; Richard, O. A. 

1754 Flavors from High pressure processing of Australian navel orange headspace GC-MS 

navel oranges juices: Sensory analysis and volatile flavor profiling 4°C and 10°C 

Innovative Food Sci. Emerg. Tech., 6, #4, 372-387 

Baxter, I.; Easton, K; Schneebeli, K; Whitfield, F 

1755 Thiabendazole Determination of thiabendazole in orange juice and rind headspace GC-MS-SIM 

in orange by LC w/fluorescence detection and confirmation by 

juice & rind GC-MS after extraction by matrix solid-phase dispersion 

J AOAC Int, 87, #3, 664-670 

Albero, B; Sanchez-Brunete, C; Tadeo, Jose L. 

1756 Sweetners Effects of carbohydrate and noncarbohydrate headspace GC 

in orange sweeteners on the orange spirit volatile compounds 

spirits Food Sci. Technol., 39, #2, 159-165 

Cordaro, F.; Da Porto, C.; Marcassa, N. 

1757 Volatiles Comparison of two headspace SPME fibres for the 100µm PDMS GC 

in orange detection of volatile chemical concentration changes 85µm polyacrylate 

juice due to industrial processing of orange juice headspace 

J Sci of Food & Agi, 85, #6, 1065-1071 

Jordan, M.; Goodner, K.; Castillo, M; Laencina, J. 

1758 Volatiles in Studies on the aroma of cupuassu liquor by 75µm Carboxen GC-MS, GC-AED 

liquor headspace SPME and gas chromatography. headspace 

J Chromatogr A, 1025, #1, 115-124 

de Oliveira, A; Pereira, N; Marsaioli, A; Augusto, F 





1759 Volatils from Seasonal, populational and ontogenic variation in the headspace GC 

oregano plants volatile oil content and composition of individuals of 

Origanum vulgare subsp. Hirtum , assessed by GC 

headspace analysis and by SPME sampling of 

individual oil glands. 

Phytochemical Analysis, 15,#5, 286-292 

Johnson, C; Kazantzis, A.; Skoula, M.; 

Mitteregger, U.; Novak, J. 

Polymers & Coatings 

791 Organics in The simplest sample treatment techniques to assess the Review article 

packaging materials quality and safety of food packaging materials. 

Reviews in AnalChem (2000) 19(6), 435-465 

Nerin, C.; Rubio, C.; Salafranca, J.; Batlle, R. 

254 Degradation products SPME as an Effective Means to Isolate Degradation 

in polymers Products in Polymers 

J. Environ. Polym. Degrad. 5 (2): 67-73 (1997) 

Hakkarainen, M., Karlsson, S., Albetsson, A. 

361 Volatile solvents in Direct VOC Analysis of Water-Based Coating by GC and SPME 65µm Carbowax/PDMS GC-FID 

water-based coatings J. Coating Technology, June 1997 5 min 

Censullo, A., Jones, D., Wills, M. headspace 

salt added 

626 Volatile solvents in Analysis of exempt paint solvents by GC using SPME 65µm Carbowax/PDMS GC-FID 

water-based coatings J. Coat Technol. (2000), 72(900), 69-74 5 min 

Bodrian, R., Censullo, A., Jones, D., Rashkin, M., Wills, M. headspace 

salt added 

466 Volatiles from Analysis of volatile varnishes of coated wires by SPME GC-MS 

varnished wire Fresenius' J. Anal. Chem. 1999, 364(7), 641-642 

Hinz, D., Kwarteng-Acheampong, W., Wenclawiak, B. headspace 

426 Acetaldehyde in Determination of Residual Acetaldehyde in Polyethylene 

polyethylene bottles Terephthalate Bottles on SPME 

Czech J. Food Sci. (1998), 36(8), 401-405 

Cizkova, H., Voldrich, M., Dobias, J. 

761 Terephthalic acid, Determination of plastic monomers in water by SPME 85µm polyacrylate LC-UV 

vinyl acetate in coupled with liquid chromatography 65µm DVB/PDMS 

water J.AOAC Intl. Vol 84, No. 2, 2001, 432-436 20min. Immersed 

Batlle, R., Sanchez, C., Nerin, C. 5% salt, pH 5.7 

853 Vinyl chloride in Vinyl chloride analysis with (SPME)-GC-MS 75µm Carboxen/PDMS GC-MS 

plastic and water applied to analysis in materials and aqueous samples. 

Analusis (2000) 28(10) 980-987 

Charvet, R.; Cun, C.; Leroy, P 

headspace 

467 Bisphenol A Abbreviated analysis of bisphenol A with SPME 

in plastic in tableware and food containers 

Shigen Kankyo Taisaku, 1999, 35(5), 447-451 

Takao, Y., Arizono, K. 

876 Poly(L-lactide) Characterization by SPME-GC-MS of matrix changes of GC-MS 

poly(L-lactide) exposed to outdoorsoil environment 

Polym. Degrad Stab, 71(2000) 147-151 

Gallet, G., Lempianinen, R., Karlsson, S 

943 Off odors Identification of a pharmaceutical packaging off-odor using 100µm PDMS GC-MS 

pharmceutical solid phase microextraction GC/MS 

packaging J Pharm Biomedical Analysis (2001), 25(3-4), 379-386 

Burinsky, D.; Polowy, K.; Sides, S.; Thornquest, A. 

heaspace 





902 Residual solvents Residual solvents determination in pharmaceutical products 

pharmaceutical by GC-HS and Gc-MS-SPME 

samples J Pharm & Biomedical Analysis 1998, 18(4-5), 623-638 

Camarasu, C., Mezei, M., Varga, G. 

468 Residual solvents Headspace SPME method optimization for 65µm DVB/PDMS 

pharmaceutical residual solvent analysis 30 min headspace 

samples Acta pharm. Hung., 1999, 69(2), 77-84 

Camarasu, C., Mezei, M., Szabo, A 

2gm NaCl, 

823 Residual solvents Improving GC determination of residual solvents in 100µm PDMS GC-MS 

pharmaceutical pharmaceuticals by the combined use of headspace SPME 16min. @ 20°C 

samples and isotopic delution 

J. Chromatogr A, 915 (2001) 209-216 

Coran, S,, Giannellini, S., Massimo, B., Pinzauti, S. 

heaspace 

845 Degradation product The use of SPME-GC-MS for the determination of GC-MS 

of diphenhydramine- degradation products of volatile and semivolatile compounds 

HCl J Microcolumn Separations (2001) 13(1), 1-7 

Snow, Nicholas H.; Karaisz, Kenneth 

1035 

1084 

1109 

VOCs in multi-layer 

packaging. 

1176 Polyamide 

thermooxidation 

1321 

1345 

1366 

New PVC materials for medical applications - The release profile of 

PVC/polycaprolactone-polycarbonate aged in aqueous environments GC-MS 

Polym Degradation Stab (2003) 80 (3), 451-458. 

Hakkarainen, Minna 

Solid-phase microextraction (SPME) in polymer characterization - Long-term 

properties and quality control of polymeric materials GC-MS 

Journal of Applied Polymer Science (2003) 89 (3), 867-873. 

Albertsson, Ann-Christine; Groning, Mikael; Hakkarainen, Minna 

Multiple headspace solid-phase microextraction for the quantitative 

determination of volatile organic compounds in multilayer packagings Carboxen/PDMS, DVB/carboxen/PDMS 


Ezquerro, Oscar; Pons, Begona; Tena, Maria Teresa 

Headspace solid-phase microextraction with gas chromatography/mass 

spectrometry reveals a correlation between the degradation product pattern 

and changes in the mechanical properties during the thermooxidation of inplant 

recycled polyamide 6,6 

J. Appl. Polym. Sci (2002) 86(13), 3396-3407 GC-MS 

Groning, Mikael; Hakkarainen, Minna 

Qualitative and quantitative solid-phase microextraction gas 

chromatographic-mass spectrometric determination of the low-molecularmass 

compounds released from poly(vinyl chloride)/polycaprolactonepolycarbonate 

during ageing. GC-MS 


Hakkarainen, M. 

Effect of polymer concentration on partitioning and molecular recognition in 

plasticized poly(vinyl chloride). 


Zhang, X.; Zhao, H.; Chen, Z.; Nims, R.; Weber, S. G.* 

Headspace solid-phase microextraction long dash a tool for new insights 

into the long-term thermo-oxidation mechanism of polyamide 6.6. GC-MS 


Groening, M.; Hakkarainen, M. * 





1437 Polymer/additives 

1518 

1302 

Residual styrene 

monomer 

1209 Diethyl sulfide 

1268 

1434 

Monocyclic aromatic 

compounds in heavy 

fuel oil. 

Methylcyclopentadienylmanganese 

tricarbonyl 

Direct solid sampling methods for gas chromatographic analysis of 

polymer/additive formulations GC-FTIR-MS 

Polymer Testing (2001) 20(7), 729-740. 

Bart, J.C.J. 

Analysis of residual styrene monomer and other volatile organic compounds 

in expanded polystyrene by headspace solid-phase microextraction followed 

by gas chromatography and gas chromatography/mass spectrometry. 

Journal of Separation Science (2002) 25(8), 539-542 

Kusch, Peter; Knupp, Gerd 

Headspace solid-phase micro-extraction - gas chromatography - mass 

spectrometry applied to quality control in multilayer-packaging manufacture. 


Ezquerro, O.; Pons, B.; Tena, M. T.* 

TiO/sub2/ reactivation in photocatalytic destruction of gaseous diethyl 

sulfide in a coil reactor 

Applied Catalysis B: Environmental (2003) 44 (1), 25-40. 

Lion, Claude; Savinov, Evgueni N.; Smirniotis, Panagiotis G.; Vorontsov, 

Alexandre V. 

A GC-MS method for analysis of volatile monocyclic aromatic compounds in 

heavy fuel oil using headspace-solid phase microextraction. 


Mangani, G.; Berloni, A.; Maione, M. * 

Determination of methylcyclopentadienyl-manganese tricarbonyl by solid 

phase microextraction-direct thermal desorption-quartz furnace atomic 

absorption spectrometry 

Spectrochim Acta Part B At Spectrosc (2001) 56(2), 215-221. 

Alava-Moreno, Fausto; Bendicho, Carlos; Fragueiro, Maria Sandra; Lavilla, 

Isela 

75um Carboxen PDMS, 

headspace 

1760 Organo- Thermal stability analysis of organo-silicates, using headspace TGA, GC-MS 

silicates from solid phase microextraction techniques 

polyurethane Thermochim Acta, 429, #1, 13-18 

Edwards, G.; Halley, P.; Kerven, G.; Martin, D. 

1761 Volatiles Use of SPME to monitor gases resulting form headspace GC 

from polymer thermal plasma pyrolysis. 

pyrolysis Chromatographia, 60, #1-2, 85-88 

Cubas, A.; Carasek, E; Debacher, N. ; de Souza, I. 

GC-MS 

GC-MS 

1762 Volatiles Probing the microwave degradation mechanism of phenol- heaspace from 20° to GC-MS 

from phenolic containing polymeric compounds by sample pretreatment 80°C 

polymers and GC-MS analysis 


Chang, Yu-Cheng; Chu, Tieh-Chi; Ko, Chu-Jung; Ko, Fu 

1763 Thermal SPME to concentrate volatile products from thermal 100µm PDMS, GC-MS 

byproducts of degradation of polymers 75µm Carboxen 

polypropylene Polym Degradation Stab, 89, #1, 33-37 

Bortoluzzi, J.; Carasek, E; Pinheiro, E.; Soldi, V 

1764 Odours from Emission of possible odourous low molecular weight heaspace GC-MS 

polypropylene compounds in recycled biofibre/polypropylene composites 

composites monitored by head-space SPME-GC-MS 

Polym Degradation Stab, 90. #3, 555-562 

De Las Heras, Luis A.; Espert, Ana; Karlsson, Sigbritt 

1765 Odor Development and analytic of odor absorber headspace GC 

removal by Tenside Surfactants Deterg, 41, #6, 282-286 

Zn ricinoleate Bohmer, Thomas; Muller, Felix; Peggau, Jorg 





1766 Volatiles from Headspace-SPME-GC-MS identification of volatile organic 75µm Carboxen GC-MS 

polystyrene compounrds released from expanded polystyrene headspace 

J. Polym. Environ., 12, #2, 83-87 

Knupp, Gerd; Kusch, Peter 

1767 2-cyclopentyl- Correlation between emitted and total amount of headspace GC-MS 

cyclo- 2-cyclopentyl- cyclopentanone in polamide 6.6 GC-RI 

pentanone in allows rapid assessment by Head Space and HS-SPME . 

polamide 6.6 under non-equilibrium conditions 

J. Chromatogr. A, 1052, #1-2, 151-159 

Groning, Mikael; Hakkarainen, Minna 

1768 2-cyclopentyl- Multiple headspace SPMEof 2-cyclopentyl- cyclopentanone headspace GC-MS 

cyclo- in polyamide 6.6: Possibilities and limitations in the 

headspace analysis of solid hydrogen-bonding matrices 

pentanone in J. Chromatogr. A, 1052, #1-2, 61-68 

polamide 6.6 Groning, Mikael; Hakkarainen, Minna 

1769 Hydrocarbons Determination of aromatic hydrocarbons in asphalt release headspace GC-MS 

from asphalt agents using headspace SPME-GC-MS 

J Chromatogra, A, 1069, #2, 235-244 

Isacsson, Ulf; Tang, Bing 

Natural Products 

401 Volatiles Analysis of Tobacco Volatiles with SPME 100µm PDMS GC-MS 

in tobacco Dr. W.D. Koller, Federal Research Centre for Nutrition, 10 min 

Institute of Process Engineering, Engesserstr. 20, 

76131 Karlsruhe/Deutschland 

headspace 

402 Pesticides in A Simple Screening for Pesticide Residues in Tobacco 100µm PDMS GC-MS 

water/MeOH extract Dr. W.D. Koller, Federal Research Centre for Nutrition, 10 min 

Institute of Process Engineering, Engesserstr. 20, 

76131 Karlsruhe/Deutschland 

immersion 

102 Flavor additives Qualitative and Quantitative Analysis of Flavor Additives 65µm Carbowax/DVB GC-FID 

in tobacco on Tobacco Products Using SPME-GC-MS 95°C, 15 min 



KCl added 

430 Alkaloids Determination of Tobacco Alkaloids Using SPME and GC-NPD 100µm PDMS GC-NPD 

in tobacco Chromatographia (1998), 47(7/8), 443-448 12 min, immersed 

Yang, S., Smetena, I. 1% NH3OH solution 

627 Acetates Quantitative analysis of acetates in cigarette tobacco GC-MS 

in cigarette tobacco using SPME-GC-MS 

J. Chromatogr. Sci (2000), 38(4), 137-144 

Watson, C., Ashley, D. 

headspace 

137 Phenols in Quantitative Determination of Phenols in Mainstream Smoke 85µm polyacrylate GC-FID 

cigarette smoke with SPME-GC-Selected Ion Monitoring Mass Spectrometry 60 min 



stirring 

628 Azo dyes Study on determination of prohibited azo dyes by SPME GC-MS 

in leather & textiles Fenxi Deshi Xuebao (2000), 19(1), 76-78 reduced to aromatic 

Xu, H., Tong, H. amines w/Na2SO4 

Azo dyes Development of a SPME method for detection of the use of 

in leather & textiles banned Azo dyes in coloured tectiles and leather 

Rapid Commun.Mass Spectrom. 13, pp1833-1837 

Cioni, G., Bartolucci, G., Pieraccini, G., Meloni, S., Moneti, G. 





916 Hexachlorobenzene Rapid Quantification of hexachlorbenzene in the color 100µm PDMS GC-MS 

in color additives additives D&C Red Nos. 27 & 28 (phloxine B) using SPME GC-MS 25min @ 26°C 

J Chromatogr A (1999) 863(1) 37-46 immersed 

Andrezejewski, D., Weisz, A. stirred 

210 Solvents in Derivatization Solid-Phase Microextraction Gas 65µm Carbowax/DVB GC-FID 

water-based coatings Chromatographic Mass Spectrometric Determination of 5 min 

Organic Acids in Tobacco headspace 

J. Chromatogr. Sci. 35 (5): 209-212 (1997) stirring 

Clark, T., Bunch, J. salt added 

836 Biproducts from Screening of biotransformation products of carvone GC-MS 

carvone enantiomers enantiomers by headspace-SPME/GC-MS 

Z. Naturforsch., C: J. Biosci(2001) 56(1/2) 58-64 

Demirci, F; Kirimer, N; Demirci, B; Noma, Y; Baser, K 

72 Monoterpenes Analysis of Monoterpenes from Conifer Needles Using SPME 100µm PDMS GC-FID 

in conifer needles J. High Res. Chromatogr. 18: 587-592 (1995) 40°C, 5 min 

Schafer, B., Hennig, P., Engewald, W. headspace 

399 Monoterpenes Changes in the Flavor of Monoterpenes During Their 65µm Carbowax/DVB GC-MS 

in conifer needles Autoxidation Under Storage Conditions 40°C, 10 min 

Dept. of Food Chemistry, Prague Institute of Chemical 

Technology, Technicka 5, CZ-16628 Prague 6, Czechia 

Pokorny, J., Pudil, F., Volfova, J., Valentova, H. 

headspace 

806 Monoterpenes SPME for the determination of volatile organics in the 

Microchemical Journal (2000) 65(3), 269-276 

Vereen, D. A.; McCall, J. P.; Butcher, D. J 

159 Terpenoids Head-Space SPME for the GC-MS Analysis of Terpenoid GC-MS 

in herbs in Herb-Base Formulations 

Fresenius’ J. Anal. Chem. 356: 80 (1996) 

Czerwinski, J., Zygmunt, B., Namiensnik, J. 

629 Terpenoids SPME of Volatile Components from Natural Grassland Plants 100µm PDMS GC-MSD 

in plant materials J. Agric.Food Chem. 2001, 49, 203-209 15 min @ 44°C 

Cornu, A., Carnat, A., Martin, B., Coulon, J., headspace, 

Lamaison, J, Berdague,J 1 gm in 40mL vial 

848 Monoterpens Monoterpene biosynthesis in Agathosma crenulata (Buchu) GC-MS 

in essential oils Flavour and Fragrance Journal (2001) 16(2), 123-135 

Mosandl, Armin; Fuchs, Sabine; Sewenig, Sabine 

320 Terpenoids Head Space SPME for the GC-MS Analysis of Terpenoids in GC-MS 

in herbs Herb-Based Formulations 

J. Anal. Chem. 356 (1): 80-83 (1996) 

Czerwinski, J., Zygmunt, B., Namiesnik, J. 

630 Monoterpens Examination of the enatomeric distribution of certain GC-MS 

in essential oils monoterpene hydrocarbons in selected essential oils by 

automated SPME-chiral GC -Mass spectrometry. 

J. Chromatogr. Sci., Mar.2000, 38(3), 95-99 

Coleman, W., Lawrence, B. 

6 se. headspace 

631 Monoterpens & Monoterpene composition essential oil from peppermint 100um PDMS GC-MS 

essential oils (Mentah x piperita L.) w/regard to Leaf position using 1 min @ 25°C 

in peppermint SPME and GC-MS Analysis 

J.Agric. Food Chem 1999, 3782-3786 

headspace 





632 Monoterpens & Biogenesis study of essential oils by SPME enatio- GC-MS 

essential oils multidimensional GC-MS (MDGC/MS) 

in mint plant GIT Lbor-Gachz (2000), 44(4), 358-362 

Fuchs, S., Beck, T., Mosandl, A. 

859 Review article Sample preparation for chromatographic analysis 

of plant material 

J Planar Chromatog- Modern TLC (2000) 13(6) 404-413 

Namiesnik, Jacek; Gorecki, Tadeusz 

863 Volatiles Emission of volatile compounds by seeds under GC-MS 

from seeds different environmental conditions 

American Midland Naturalist (2001) 145(2) 419-422 

Jorgensen, Eric 

633 Essential oils Chemical composition of the essential oil and headspace GC-MS 

in quava fruit SPME of the quava fruit 

J. Essent. Oil Res (2000), 12(2), 153-158 

Paniandy, J., Chane-Ming, J., Pieribattesti, J. 

headspace 

469 Essential oils Rapid GC with resistance heated capillary columns. 

from aromatic plants Analysis of essential oils from aromatic plants 

Git Spez. Sep. (1999), 19(1), 40-43 

Theuerl, T., Kleibohmer,W., Blanke, R. 

389 Cuticular Solid Phase Microextraction and Cuticular Hydrocarbon GC-MS 

hydrocarbons Differences Related to Reproductive Activity in the 

in Dinoponera Queenless Ant 

quadriceps ants J. Chemical Ecology, 24: 473-490, 1998 

Monnin, T., Malosse, C., Peeters, C. 

89 Pheromones Solid Phase Microextraction, an Alternative Method 100µm PDMS GC-FID 

in insects for the Study of Airborne Insect Pheromones 5 min 

(Metamasius hemipterus, Coleoptera, Curculionidae) 

J. High Res. Chromatogr. 18: 669-670 (1995) 

Malosse, C., Ramirez-Luca, P., Rochat, D., Morin, J. 

headspace 

818 Pheromones Use of SPME in the investigation of chemical 7µm PDMS GC-MSD 

in insects communication in social wasps 

J Chromatogr A, 873, (2000), 73-77 

Sldege, M., Moneti, G., Pieraccini, G., Turillazzi, S. 

10min @ 170C 

434 Pheromones SPME, A New Tool in Pheromone Identification in Lipidoptera 7µm PDMS GC-FID or 

in insects J High Resolut. Chromtogr. (1997), 20(6), 340-342 5 min GC-FTD 

Frerot, B., Malosse, C., Cain, A. rubbed on fiber 

850 Pheromones (Z)-dodec-3-en-1-ol, a novel termite trail pheromone identified GC-MS 

in termite trail after SPME from Macrotermes annandalei. 

J Insect Physiology (2001) 47(4-5) 445-453 

Bordereau, C; Bonnard, O; Ginies, C; Lettere, M; Peppuy, A; 

Robert, A; Semon, E 

634 Pheromones Role of SPME in the identification of highly volatile Carboxen/PDMS GC-MS 

of Rhinoceros Pheromones of two Rhinoceros beetles Scapanes australis 30 min 

beetles and Strategus aloeus (Coleoptera, Scarabaeidae, Dynastinae) immersion 

J Chromatogr. A, 885 (2000) 433-444, Rochat, D, 

Ramirez-Lucas,P., Malosse,C., Aldana,R. Kakul,T. Morin,J 

NaCl, borax buffer (pH9.2) 





945 Insecticides Measurement of Insecticide Uptake and Effective 

Fraction in a Beneficial Insect Using SPME 

Anal. Chem (2001) 73(13), 3107-3111 

Alix, A.; Collot, D.; Nenon, J.; Anger, J. 

635 Volatiles The measurement of volatile compounds in Foray 48B, an 

in insecticide insecticide prepared from Bacillus thuringiensis var. kurstaki 

Sci. Total Env., (2000) Vol. 263, No. 1-3, 155-160 

van Netten, C., Bartlett, K., Chow, Y., Leung, V., Teschke, K. 

120 NH3, putrescine, Solid Phase Microextraction Analysis of Static-Air Emissions 100µm PDMS FID 

methylamine in of Ammonia, Methylamine, and Putrescine from a Lure 10 min 

lure cultures for the Mexican Fruit Fly 


Robacker, D., Bartelt, R. 

headspace 

825 Fly Pheromones SPME-GC-direct depostioon infrared spectrometry as 100µm PDMS GC-MS 

in insects a convenient method for the determination of volatile 

compounds from living organisms 

J. Chromatogr. A 819 (1998) 45-50 

Auger, J., Rousset, S., Thibourt, E., Jaillais, B. 

1min. 

937 Chemical attractants The use of (SPME) devices in analysis for potential GC-MS 

from mosquito oviposition attractant chemicals from 

cyanobacterial mats. cyanobacterial mats. 

Aquatic Ecology (2000), 34(4), 413-420 

Rejmankova, E.; Lege, M.; Andre, R.; Higashi, .; Roberts, D. 

398 Chemical attractants Chemicals Attractive to Mexican Fruit Fly from 100µm PDMS GC-MS 

in soy broth culture Klebsiella pneumonia and Citrobacter freundii Cultures 27°C, 30 min 

Sampled by SPME headspace 

J. Chemical Ecology, Vol. 23, No., 12, 1997, 2897-2915 

Robacker, D., Bartelt, R. 

470 Pheromones Pheromone analysis using capillary GC techniques 

J. Chromatogr., A 1999, 843(1+2), 199-236 

Jones, G., Oldham, N. 

review of use of SPME GC 

124 Pheromones Solid Phase Microextraction Technique Used for Collecting 100µm PDMS GC-MS 

in insects Semiochemicals, Identification of Volatiles Released by 1-3 hr 

Individual Signaling Phylionorycter sylvella Moths 

Z. Nturforsch. C: Giosci. 51: 599 (1996) 

Karlson-Borg, A., Mozuaitis, R. 

headspace 

410 Pheromones in Purification, Identification, Concentration and Bioactivity GC-MS 

elephant urine of (Z)-7-dodecen-1-yl acetate: Sex Pheromone of the 

Female Asian Elephant, Elephas maximus 

Chem. Senses 22: 417-437 

Rasmussen, L.E.L., Lee, T.D., Zhang, A., Roelofs, W.L., 

and Daves Jr., G.D. 

773 Fungal volatiles Application of SPME for the determination of fungal 

volatile metabolites 

Prog. Biotechnol (2000) 17, 369-377 

Jelen, H.; Wasowicz, E 

394 Free fatty acids Sampling Techniques for GC-MS Analysis of Long-Chain 100µm PDMS, GC-MS 

in exocrine secretions Free Fatty Acids from Insect Exocrine Glands 65µm Carbowax/DVB 

J. Chromatogr. A 816 (1998) 169-175 140°C, 30 min 

Maile, R., Dani, F., Jones, G., Morgan, D., Orthius, D. headspace 





382 Volatile attractants Attractants from Stryphylococcus aureus Cultures from 100µm PDMS GC-MS 

in cultures Mexican Fruit Fly, Anastrepha ludens 5 min - 24 hr 

J. Chemical Ecology, Vol. 21, No. 11, 1861-1874 (1995) 

Robacker, D., Flath, R. 

headspace 

471 Volatile attractants Volatiles of bracket fungi Fomtopsis pinicola GC-MS 

in bracket fungi and Fomes fomentarius and their functions as 

insect attractants 

J. Chem. Ecol. (1999), 25(3), 567-590 

Faldt, J., Jonsell, M., Norlander, G., Borg-Karlson, A. 

584 Alcholols, aldehydes Volatiles from Fusarium verticillioides (Sacc.) Nirenb. 100µm PDMS GC-FID/MS 

in air and their attractiveness to Nitidulid beetles. 30 min 

J-Agric-Food-Chem. Jun 1999; 47(6): 2447-2454 

Bartelt,-RJ; Wicklow,-DT 

472 Volatile attractants Identification of a new blend of apple volatiles GC-FID 

from apples attractive to the apple maggot, 

Rhagoletis pomonella 

J. Chem. Ecol., 1999, 25(6), 1221-1232 

Zhang, A., Linn, C., Wright, S., Prokopy, R. 

Reissig, W., Roelogs, W. 

889 Volatile attractants Volatiles from apple (Malus domestica) eliciting antennal GC-Electrofrom 

apples antennal responses in female codling moth Cydia pomonella antennography 

(L.) (Lepidoptera: Tortricidae): Effect of plant injury and s 

sampling technique 

Zeitschrift fuer Naturforschung Sec C (2001) 56(3-4) 262-268 

Backman, A; Bengtsson, M; Karlsson, A; Liblikas, I; Witzgall, P 

636 Pyrazine Headspace SPME method for determining 3-akyl-2 methoxy- 100µm PDMS/DVB GC-NPD 

in Must pyrazine in musts by PDMS fibers 4 hr.@30°C 

J Chromatogr. Sci (2000), 880(1+2), 93-99 headspace 

Sala, C., Mestres, M, Marit, M., Busto, O., Guasch, J. NaCl added 

892 Pesticides Development of a SPME-GC-ECD methodology for GC-ECD 

in must & wine selected pesticides in must and wine samples 

Fresenius' J Anal Chem) 369(7-8) 647-651 

Alves, A; Correia, M; Delerue-Matos, C 

211 Musk compounds Headspace SPME and Gas Chromatography with 100µm PDMS GC-AED 

in cosmetic products Atomic-Emission Detection 80°C, 30 min 


Struppe, C., Schaefer, B., Engewald, W. 

headspace 

835 Volaitles from SPME-GC-MS analyses of hazelnut creams GC-MS 

hazelnut creams Lab. 2000 (2000) 14(7), 86-88 

Saba, A.; Cuzzola, A.; Raffaelli, A.; Salvadori, P. 

821 Fragrances A novel technology to study the emission of 100µm PDMS GC-MS 

on skin fragrance from the skin 30-60min 

Perfumer& Flavorist, vol. 23 (1998) 1-11 

Mookherjee, B., Patel, S., Trenkle, R., Wilson, R. 

headspace 

637 Volatiles Analysis of headspace constituents of Gardenia flower by 100µm PDMS GC-MS 

in Gardenia flower GC-MS with SPME and dynamic headspace sampling 60 min @ 28°C 

Sepu, (2000-09) 18(5) 425-455 

Liu, B., Gao, Y. 

headspace 

882 Fragrance On-site field sampling and analysis of fragrance from living 100µm PDMS GC-MS 

in Lavender flowers Lavender (Lavandula angustifolia L.) flowers by SPME 10 min @ 28°C 

coupled to GC and io-trap mass spectrometry 

J. chromatogr. A 917(2001) 245-250 

An, M., Haig, T., Hatfield, P. 

headspace 





125 Fragrance IFF Announces New Method for Living Flower Analysis 75µm Carboxen/PDMS GC-MS 

in flowers Spray Technology & Marketing Oct. 1996, pp 26-30 

Anon 

headspace 

126 Fragrance Flavors of Heliotrope Flowers, Analyzed by SPME Method GC-MS 

in flowers Gakkaishi 2: 6 (1995) 

Nippon, Shokuhin Kagaku 

874 Aroma compounds Analysis of the aroma compunds of the pulp of Borassus GC-MS 

in pulp aethiopum L (Palmaceae) from Cameroon using GC-MS, 

SPME-GC-MS and olfactormetry 

Ernaehung (Vienna) 24(2000) 159-161 

Jirovetz, L., Buchbauer, G., Ngassoum, M. 

746 Volatiles Influence of fiber coating in headspace SPME-GC analysis Carboxen/DVB/PDMS GC-FID 

from plants of aromatic and medicinal plants 1hr, headspace 

J.Chromatogr. A (2000) 892, 469-485 

Bicchi, C., Drigo, S., Rubiolo, P. 

792 Pesticides in SPME associated with microwave assisted extraction PDMS GC-ECD 

medicinal plants of organochlorine pesticides in medicinal plants 

Anal. Chim. Acta (2001) 428(1), 111-120 

Ho, W.-H.; Hsieh, S.-J 

90min, 

465 C2-C10 Acid, phenols, Evaluating Peats for their capacities to remove 85µm Polyacrylate GC-MS 

aldehydes odorous compounds from liquid swine manure 20 min @ 72°C 

in swine manure using headspace SPME 

J. Environ. Sci.Health, B34(4), 709-748 (1999) 

Rizzuti, A., Cohen, A., Hunt, P., Vanotti, M. 

headspace, pH 2 

127 Cinnamon Classification of the Botanical Origin of Cinnamon by SPME-GC 

Chromatographia 42: 2187 (1996) 

Miller, K,. Poole, C., Pawlowski, T. 

321 Epicuticular SPME of Insect Epicuticular Hydrocarbons for GC-MS Analysis GC-MS 

hydrocarbons Rapid Commun. Mass Spectrom. 11 (8): 857-862 (1997) 

in insect culture Moneti, G., Dani, F., Pieraccini, G., Turillazzi, S. 

811 Volatile hydrocarbon Development of a method for the application of SPME GC-FID 

from bacterial to monitor biodegradation of volatile hydrocarbons 45min @ 30°C 

growth during bacterial growth on crude oil 

J Indus Microb & Biotech (2000) 25(3), 155-162 

Van Hamme, J. D.; Ward, O 

headspace 

1054 


from Eucalyptus. 

Solid-phase microextraction of volatile compounds from the chopped leaves 

of three species of Eucalyptus. 


Pawliszyn, Janusz; Caramao, Elina B.; Christensen, Eva; Zanin, Kelen D.; 

Zini, Claudia A. 

1082 Aromas and fragrances Sampling and sample preparation for analysis of aromas and fragrances. 

Trends in Analytical Chemistry (2003) 22 (3), 160-169. 

Augusto, Fabio; Leite e Lopes, Alexandre; Zini, Claudia Alcaraz 

1092 

Selenium and sulfur 

from plants. 

Simultaneous monitoring of volatile selenium and sulfur species from Se 

accumulating plants (wild type and genetically modified) by gas 

chromatography-mass spectrometry and gas chromatography-inductively 

coupled plasma mass spectrometry using solid-phase microextraction for 

sample introduction. GC-ICP MS 


Meija, J.; Montes-Bayon, M.; Le Duc, D. L.; Terry, N.; Caruso, J. A.* 





1120 Volatiles from flowers 

1121 Methyl jasmonate 

1139 Sulcatol from beetles 

1165 Mercury and tin 

1170 Ethanol from wood pulp 

Use of solid-phase micro-extraction as a sampling technique in the 

determination of volatiles emitted by flowers, isolated flower parts and pollen 


Cioni, Pier Luigi; Flamini, Guido; Morelli, Ivano 

Identification and quantification of methyl jasmonate in leaf volatiles of 

Arabidopsis thaliana using solid-phase microextraction in combination with 

gas chromatography and mass spectrometry. GC-MS 

Phytochemical Analysis (2003) 14 (3), 155-159. 

Dubery, Ian A.; Meyer, Riaan; Rautenbach, George F. 

Identification of sulcatol, a potential pheromone of the ambrosia beetle 

Gnathotrichus materiarius (Col., Scolytidae). 

Journal of Applied Entomology (2003) 127 (4), 189-194. 

Flechtmann, C. A. H.; Berisford, C. W. 

Elevated lead levels: A possible factor behind the forest die back of 

Montane forests in Sri Lanka? 

Journal De Physique. IV : JP (2003) 107 (II), 1439. 

Dissanayake, C.B.; Ranasinghe, P.N. 

PDMS GC-MIP/AES 

Determination of methanol released from wood and mechanical pulp by 

headspace solid-phase microextraction 

J Pulp Pap Sci (2002) 28(6), 199-203 

Eckerman, C.; Holmbom, B.; Pranovich, A.V. 

1171 Volatiles in wood On-line wood species sensor 

Process Control News Pulp Paper Industry (2002) 22(1), 10-11 

Fuhr, B.; Henry, D.; Sedgwick, G.; Smith, G.; Woolley, J. 

GC 

1173 

1181 

1183 

VOCs in herbal drug 

preparations 

Reevaluation of the chemical secretion of the sternal glands of Polistes 

social wasps (Hymenoptera Vespidae). 

Ethology Ecology & Evolution (2003) 15 (1), 73-82. 

Dani, F. R.; Jones, G. R.; Morgan, E. D.; Turillazzi, S. 

Characterization of Citrus unshiu ( C. unshiu Marcov. forma Miyagawa-wase 

) blossom aroma by solid-phase microextraction in conjunction with an 

electronic nose. GC-MS 


Choi, H. S. 

Chemical composition of some traditional herbal drug preparations: 

Essential oil and aromatic water of costmary (Balsamita suaveolens Pers.). 


Gallori, Sandra; Bilia, Anna Rita; Flamini, Guido; Landini, Andrea; Morelli, 

Ivano; Vincieri, Franco Francesco 

1195 Floral scent SPME - A valuable tool for investigation of flower scent 


Bartak, Petr; Bednar, Petr; Cap, Lubomir; Ondrakova, Lenka; Stransky, 

Zdenek 

Carboxen/PDMS GC-MS 

1204 Catnip aroma. Sensory and instrumental evaluation of catnip (Nepeta cataria L.) aroma. 

1239 Alpha pinene, ocimene. 


Venskutonis, Rimantas P.; Baranauskiene, Renata; Demyttenaere, Jan C. 

R. 

GC-MS 

Analysis of volatile components of Chrysanthemum coronarium L. by gas 

chromatography-mass spectrometry with solid-phase microextraction. GC-MS 


Weng, X. X.; Deng, C. H.; Song, G. X.; Hu, Y. M.; Zheng, X. H. 


1276 

1318 

1324 





Brazilian aromatic 

plants. 


from Scots pine seeds. 

VOC's in coniferous 

needle litter. 

1327 Volatiles in tobacco 

1352 

Volatiles in Michelia 

alba 

1379 Biogenic VOC's 

Application of headspace solid-phase microextraction and gas 

chromatography to the screening of volatile compounds from some Brazilian 

aromatic plants. 


Sartoratto, A.; Augusto, F. * 

100 um PDMS GC-MS 

Volatile compound analysis of ageing Pinus sylvestris L. (Scots pine) 

seeds. GC-MS 


Tammela, P.; Hiltunen, R.; Hopia, A.; Laakso, I.; Nygren, M.; Vuorela, H. 

HS-SPME analysis of volatile organic compounds of coniferous needle litter 

Atmospheric Environment (2003) 37 (33), 4645-4650. 

Isidorov, V.A.; Rafalowski, K.; Vinogorova, V.T. 

Optimization of headspace sampling using solid-phase microextraction for 

volatile components in tobacco. 


Yang, S. S.; Huang, C. B.; Smetena, I. 

Rapid determination of volatile constituents of Michelia alba flowers by gas 

chromatography-mass spectrometry with solid-phase microextraction 


Hu, Yaoming; Deng, Chunhui; Hu, Keji; Shang, Chunqing 

100um PDMS, 25 degrees C, 4 

hours, headspace 

Monitoring biogenic volatile compounds (BVOC) emitted by Eucalyptus 

citriodora using SPME 

Analytical Chemistry (2001) 73(19), 4729-4735. 

Alcaraz Zini, C.; Augusto, F.; Christensen, E.; Smith, B. P.; Caramao, E. B.; 

Pawliszyn, J. * 

PDMS/DVB GC 

1398 Volatiles from potential hosts of Rhopalicus tutela a bark beetle parasitoid. Carbowax/DVB 

Journal of Chemical Ecology (2001) 27(11), 2219-2231. 

Pettersson, Eva M 

GC-MS 

1404 Pheromones in termites 

1455 Terpenoids in olibanum 

1458 

1466 

Terpenes in black 

currant 


roses 

1467 Volatiles in flowers 

GC-MS 

GC-MS 

Species specificity of trail pheromones of fungus-growing termites from 

northern Vietnam. GC-MS 

Insectes Sociaux (2001) 48(3), 245-250. 

Bordereau, C.; Bonnard, O.; Peppuy, A.; Robert, A.; Semon, E.; Son, Ngo 

Truong 

Optimization of headspace solid phase microextraction for gas 

chromatography/mass spectrometry analysis of widely different volatility and 

polarity terpenoids in olibanum. 

Journal of Chromatograpy A (2003) 1018(1), 73-78 

Hamm, S.; Lesellier, E.; Bleton, J.; Tchapla, A. 

Influence of stage of ripeness on the enantiomeric distribution of chiral 

terpenes in blackcurrant fruits (Ribes nigrum L.). 


Ruiz del Castillo, M. L.; Dobson, G. 

Analysis of rhythmic emission of volatile compounds of rose flowers. 

Molecular Methods of Plant Analysis (2002) 21, 199-221 

Verstappen, F. W. A.; Helsper, J. P. F. G.; Davies, J. A. 

Detection of physiologically active flower volatiles using gas 

chromatography coupled with electroantennography. 

Molecular Methods of Plant Analysis (2002) 21, 173-198 

Schiestl, F. P.; Marion-Poll, F. 



GC-FID

1469 




Fragrance compounds 

from Lavandula 

1477 Selenium in plants 

1508 

Volatiles from medicinal 

plants 

1510 Capsaicin 

1512 

1513 

Fragrances from Laurus 

nobilis 

Aroma volatiles from 

Eruca stavia 

1544 Volatiles in Eucalyptus 

1545 Volatiles in mint oils 

1549 Volatiles from flowers 

1553 Volatiles in sachalinmint 

1138 

Comparison of different extraction methods for the analysis of fragrances 

from Lavandula species by gas chromatography-mass spectrometry. 


Lee, Dong-Sun; Kim, Nam-Sun 

Selenium in plants by mass spectrometric techniques: Developments in bioanalytical 

methods. Plenary Lecture. 

Journal of Analytical Atomic Spectrometry (2002) 17(9), 1015-1023 

Caruso, Joseph A.; Grant, Tyre D.; Meija, Juris; Montes-Bayon, Maria 

A review of modern sample-preparation techniques for the extraction and 

analysis of medicinal plants. 

Analytical and Bioanalytical Chemistry (2002) 373(1-2), 23-30 

Huie, Carmen W. 

Extraction methods for Capsaicin encountered in aerosol defense sprays; a 

comparative analysis. 

Abstracts of Papers American Chemical Society (2002) 223(1-2), ANYL 76 

Spicer, Oliver; Almirall, Jose R. 

Differences in the fragrances of pollen and different floral parts of male and 

female flowers of Laurus nobilis. 


Flamini, Guido; Cioni, Pier Luigi; Morelli, Ivano 

Aroma compound analysis of Eruca sativa (Brassicaceae) SPME 

headspace leaf samples using GC, GC-MS, and olfactometry. 


Jirovetz, Leopold; Buchbauer, Gerhard; Smith, David 

Automation of solid-phase microextraction-gas chromatography-mass 

spectrometry extraction of eucalyptus volatiles. 

Journal of Chromatographic Science (2002) 40(3),140-146 

Zini, Claudia A.; Pawliszyn, Janusz; Lord, Heather; de Assis, Teotonio F.; 

Caramao, Elina B.; Christensen, Eva 

Semiquantitative determination of off-notes in mint oils by solid-phase 



Coleman, W. M., III; Cole, S. K.; Lawrence, B. M. 

Analysis of the essential oil of the aerial parts of Viola etrusca from Monte 

Labbro (South Tuscany, Italy) and in vivo analysis of flower volatiles using 

SPME 

Flavour and Fragrance Journal (2002) 17(2), 147-149 

Flamini, Guido; Cioni, P. L.; Morelli, I. 

Essential oil composition of sachalinmint from Norway detected by solidphase 

microextraction and gas chromatography-mass spectrometry 

analysis. 


Rohloff, Jens 

100um PDMS GC-MS 

GC-ICP-MS 


GC-ITMS 

GC-MS 

Production of volatile compounds by hairy root cultures of Cichorium intybus 

L under the influence of fungal elicitors and their analysis using solid-phase 

micro extraction gas chromatography-mass spectrometry. GC-MS 

Journal of the Science of Food and Agriculture (2003) 83 (8), 769-774. 

Bais, Harsh Pal; Dattatreya, B. S.; Ravishankar, G. A. 





1317 Volatile constituents of benzoin gums: Siam and Sumatra. Part 1. 


Lizzani-Cuvelier, Louisette; Delbecque, Claire; Fernandez, Xavier; Loiseau, 

Andre-Michel; Perichet, Christine 

Carboxen/PDMS, carbowax/DVBGC-MS 

1397 Terpenoids 

1022 Lindane and heptachlor 

1094 

1333 

1039 Pyrene 

1198 

1343 

Quantitative analysis of terpenoids in the gas phase using headspace solidphase 

microextraction (HS-SPME). PDMS 


Zabaras, D.; Wyllie, S. G. 

The use of pine bark as a natural adsorbent for persistent organic 

pollutants: Study of lindane and heptachlor adsorption. GC-ECD 

Journal of Chemical Technology and Biotechnology (2003) 78 (2-3), 347- 

351. 

Alves, Arminda; Botelho, Cidalia; Ratola, Nuno 

Bioconcentration of organic chemicals: is a solid-phase microextraction fibre 

a good surrogate for biota? 

Environmental Science and Technology (2002) 36 (24), 5399-5404. 

Leslie, H. A.; Ter Laak, T. L.; Busser, F. J. M.; Kraak, M. H. S.; Hermans, J. 

L. M. 

15 um PDMS GC-ECD 

Classification of Duvernay sourced oils from central and southern Alberta 

using Compound Specific Isotope Correlation (CSIC) CF-IRMS 

Bulletin of Canadian Petroleum Geology (2003) 51 (5), 357-368. 

Fowler, Martin G.; Harris, Scott A.; Whiticar, Michael J. 

Sorption of pyrene to dissolved humic substances and related model 

polymers. 2. Solid-phase microextraction ( SPME ) and fluorescence 

quenching technique (FQT) as analytical methods. 


MacKenzie, K.; Georgi, A.; Kumke, M.; Kopinke, F. -D.* 

PDMS GC-FID 

Analysis of the volatile constituents of Apium graveolens L. and Oenanthe L. 

by gas chromatography-mass spectrometry, using headspace solid-phase 

microextraction. 


Deng, C. H.; Song, G. X.; Zheng, X. H.; Hu, Y. M.*; Zhang, X. M. 

PDMS/DVB GC-MS 

Analysis of the volatile constituents of Schisandra chinensis (Turz.) Bail by 

gas chromatography-mass spectrometry, using headspace solid-phase 

microextraction. PDMS, carbowax/DVB GC-MS 


Deng, C. H.; Song, G. X.; Hu, Y. M.*; Zhang, X. M. 

1770 Cuticular Diet-mediated inter-colonial aggression in Formosan headspace GC-MS 

hydrocarbons subterranean termite Coptotermes formosanus 

from wood J Chemical Ecology, 30, #12, 2559-2574 

Florane, C.; Bland, J.; Husseneder, C; Raina, A. 

1771 Phermones Evaluation of the major female Eurytoma amygdali headspace GC 

from wasp sex pheromone components, (Z,Z)6,9-tricosadiene and 

(Z,Z)-6,9-pentacosadiene for male attraction in field tests 

J Chemical Ecology, 30, #6, 1245-1255 

Mazomenos, B.; Athanassiou, C; Kavallieratos, N; Milonas, P 

1772 Volatiles from Avian exocrine secretions. I. Chemical characterization dimethyl disulfide GC-MS 

secretion of the volatile fraction of the uropygial secretion of derivatization 

the green woodhoopoe, Phoeniculus purpureus 


Burger, B.; Reiter, B.; Borzyk, O.; Du Plessis, M. 

1773 Essential oil Volatile constituents of different organs of Headspace GC, GC-MS 

P. bituminosa Psoralea bituminosa L 

from leaves Flavour Fragrance J., 19,#2, 166-171 

Bertoli, A; Menichini, F; Morelli, I; Noccioli, C; Pistelli, L 





1774 Volatiles from Volatile constituents of different parts (roots, stems Headspace GC, GC-MS 

plants and leaves) of Smyrnium olusatrum L 

Flavour Fragrance J., 19,#6, 522-525 

Bertoli, A.; Fraternale, D.; Giamperi, L..; Morelli, I.; 

Pistelli, L.; Ricci, D. 

1775 Formaldehyde Quantitative determination of formaldehyde in 65µm PDMS-DVB GC-MS 

in cosmetics cosmetics using a combined SPME- pentafluorophenyl 

isotope dilution mass spectrometry method. hydrazine derivative 

J. Chromatogr. A, 1029, #1-2, 217-222 headspace 

Rivero, R. T.; Topiwala, V. 

1776 Solvent Vapor-phase analysis of isobutyl acetate, isopropyl headspace GC-MS 

esters acetate, n-propyl acetate and their respective 

alcohols using SPME-GC w/ mass selective detector 

J Chromatography, A, 1066, #1-2, 225-230 

Cobb, G.; Cox, S.; Polydore, C.; Radtke, C. 

1777 Solvents in Disposable ionic liquid coating for headspace SPME headspace GC-FID 

paint of benzene, toluene, ethylbenzene, and 

xylenes in paints followed by GC-FID 

J. Chromatogr. A, 1066, #1-2, 27-32 

Liu, Jing-Fu; Li, Ning; Jiang, Gui-bin; Liu, Jie-min; 

Jonsson, Jan Ake; Wen, Mei-juan 

1778 Terpenes in Comparison of terpene composition in Engelmann spruce headspace GC 

spruce trees (Picea engelmannii) using hydrodistillation, SPME and PLE 

Zeitschrift fuer Naturforschung, 59, #9-10, 641-648 

Mardarowicz, M; Wianowska, D., A.; Sawicki, R. 

1779 Fugal volatiles Use of headspace SPMEand headspace sorptive headspace GC-MS 

on Agar extraction for the detection of the volatile 

metabolites produced by toxigenic Fusarium species. 

J Chromatogr A, 1027, #1-2, 147-154 

Demyttenaere, J; Morina, R; De Kimpe,N; Sandra, P 

1780 Terpenes Natural variability of the enantiomeric composition headspace GC-MS 

in plant of bioactive chiral terpenes in Mentha piperita 

emissions J Chromatogr A, 1054,#1-2, 87-93 

Blanch, G.P.; Herraiz, M.; Ruiz Del Castillo, M.L. 

1781 Terpenes Analysis of enantiomeric and non-enantiomeric 65µm PDMS-DVB GC-MS 

in plant monoterpenes in plant emissions using portable dynamic direct air sampling 

emissions air sampling/SPME and chiral GC-MS 

Atmos. Environ., 39, #27, 4875-4884 

Williams, Jonathan; Yassaa, Noureddine 

1782 Terpenes The release of terpenes during storage of biomass headspace GC-MS 

in biomass Biomass Bioenergy, 28, #1, 29-34 

Rupar, Katarina; Sanati, Mehri 

1783 Volatiles Analysis of Platycladus orientalis volatiles and their headspace in situ GC-MS 

from trees electroantennogram responses with Semanotus 

bifasciatus 

Forest Research, 18, #3, 260-266 

Kong X; Zhang Z; Wang H; Yang Jie; Hu Y 

1784 Volatiles of Determination of volatile components of Amomum headspace GC-MS 

dried fruit villosum Lour. by GC-MS with head-space SPME 

Amomum Fudan Xuebao Zirankexueban, 43, #4,676-679 

villosium Song Guo-xin; Deng Chun-hui; Wu Dan; Hu Y 

1785 Volatiles A direct quantitative analysis method for monitoring 50/30µm DVB/CAR GC-MS 

from leaves biogenic volatile organic compounds released 20 min extract 

from leaves of Pelargonium hortorum in situ. headspace 

Anal and Bioanal Chemistry, 380, #7-8, 950-957 

Deng, X.; Peng, J.; Luo, B.; Wei, M.; Hu, W.; Du, J. 





1786 Ocytl-, nonyl- Determination of nonylphenol and octylphenol in paper Headspace GC-MS 

phenol in by microwave-assisted extraction coupled to headspace 

paper SPME and GC-MS 

J Chromatogra, A, 1065, #2, 251-256 

Barcelo, D.; Lacorte, S.; Latorre, A.; Montury, M. 

1787 Nicotine in SPME-based approach to determine free-base nicotine in headspace GC-MS 

cigarette trapped mainstream cigarette smoke total particulate matter. 

smoke J Agr Food Chem, 52, #24, 7240-7245 

Watson, C. H.; Trommel, J. S.; Ashley, D. L. 

1788 Flavour aroma Analysis of aroma constituents in tobacco flavour by 100µm PDMS GC-MS 

in tobacco GC-MS with solid-phase microextraction. 85µm polyacrylate 

Fenxi Shiyanshi, 23, #10, 22-25 headspace 

Dong, L.; Zhu, S. K.; Su, X. L.; Wu, C. Y.; 

Xiong, G. X.; Chen, Z. G.; Li, D. 

1789 Diterpenes The moss Physcomitrella patens releases a Headspace GC 

from moss tetracyclic diterpene 

Plant Cell Reports, 22, #10, 780-786 

von Schwartzenberg, K.; Schultze, W.; Kassner, H. 

1790 Volatiles from Identification and synthesis of volatiles released by headspace GC 

crocatus the myxobacterium Chondromyces crocatus 

Tetrahedron, 60, #17, 3863-3872 

Schulz, Stefan; Fuhlendorff, Jens; Reichenbach, H. 

1791 Volatiles in Determination of volatile compounds in Magnolia headspace GC-MS 

magnolia bark by microwave-assisted extraction coupled 

bark to headspace SPME and GC-MS 

Analytical Sciences, 20, #5, 857-859 

Sha, Y. F.; Huang, T. M.; Shen, S.; Duan, G. L.* 

1792 Volatils of Chemical components of Vetiveria zizanioides volatiles. headspace GC-MS 

zizanioides Yingyong Shengtai Xuebao, 15, #1, 170-172 

Huang Jinghua; Li Huashou; Yang Jun; Chen Yufen; 

Liu Yinghu; Li Ning; Nie Chengrong 

1793 Terpens in Headspace solid-phase microextraction (HS-SPME): A headspace GC/MS 

coniferos microscale sampling technique for determination of mononeedles 

terpene hydrocarbons in coniferous needles by GC-MS 


Chvilickova, I.; Kuban, V. 

1794 Volatile odors Determination of odour-causing volatile organic compounds 50/30µm DVB/CAR GC-MS 

from cork in cork stoppers by multiple headspace SPME 45min @ 100°C 

J. Chromatogr. A, 1068, #2, 201-208 headspace 

Ezquerro, Oscar; Tena, Maria Teresa 

1795 Essential oils Rapid determination of essential oil in Acorus tatarinowii 10min @ 60°C GC-MS 

from chinese Schott. by pressurized hot water extraction followed headspace 

medicine followed by SPME-GC-MS 

J. Chromatogr. A, 1059, #1-2, 149-155 

Deng, Chunhui; Li, Ning; Zhang, Xiangmin 

1796 Volatiles from Identification of volatile organic compounds emitted by headspace GC-MS 

aged book a naturally aged book using SPME-GC-MS. contact sampling 

J. Chromatogr. A, 1026, #1-2, 9-18 

Lattuati-Derieux, A.; Bonnassies-Termes, S.; Lavedrine, B. 

1797 Volatiles from Identification by GC-MS of the volatile organic compounds headspace GC-MS 

wood fungi emitted from the wood-rotting fungi Serpula lacrymans and 

Coniophora puteana, and from Pinus sylvestris timber 

Mycological Research, 108, #7, 806-814 

Ewen, Richard J.; Jones, Peter R. H.; Ratcliffe, N.; 

Spencer-Phillips, Peter 

1798 t-2-hexenal Chemical released from host Acacia by feeding headspace GC 

from herbivores is detected by symbiotic Acacia-ants. 

acacia leaves. Caribbean J of Science, 40, #3, 396-399 

Wood, William F.; Wood, Brenda 





1799 volatile flavor Aroma evaluation of an aquatic herb, changpo (Acorus headspace GC-MS 

changpo calamus var. angustatus Bess), by AEDA and SPME 

J Agr Food Chem, 52, #26, 8099-8104 

Choi, H. S. 

1800 Volatiles from Aroma-active compounds of Pinus densiflora 100µm PDMS GC-MS 

pine needles (red pine) needles 75µm Carboxen 

Flavour Fragrance J., 19, #6, 532-537 headspace 

Kim, Kyoung Heon; Kim, Tae Hwan; Lee, Hyong Joo; Yu, E 

1801 Hydrocarbons Evaluation of hydrocarbon emissions from heart-And headspace @ 50°, 70°, GC-MS 

emissions sapwood of Scots pine using a laboratory-scale wood drier and 90°C 

from pine Holzforschung, 58, #6, 660-665 

Bengtsson, Peter; Sanati, Mehri 

1802 Odors from Representativeness of extracts of offset paper 100µm PDMS GC-MS 

packaging packaging and analysis of the main 3 min @ 40°C 

odor-active compounds headspace 

J Agr Food Chem, 52, #8, 2326-2334 

Landy, P.; Nicklaus, S.; Semon, E.; Mielle, P.; Guichard, E. 

1803 E coli volatiles SPME, GC, and MS coupled w/discriminant factor headspace @ 37°C GC-MS 

coli from analysis and multilayer perceptron neural network for 

brooth detection of Escherichia coli 

J of Food Protection, 67, #8, 1597-1603 

Siripatrawan, Ubonratana; Linz, John E.; Harte, Bruce R. 

1804 Floral Catnip, Nepeta cataria (Lamiales: Lamiaceae) headspace GC-MS 

volatiles A closer look: Seasonal occurrence of epetalactone 

from catnip isomers and comparative repellency of three 

terpenoids to insects 

Environmental Entomology, 33, #6, 1562-1569 

Schultz, G; Simbro, E; Belden, J; Zhu, J; Coats, Joel 

1805 Volatiles Comparison of different extraction methods for the headspace GC-MS 

from plants analysis of volatlle secondary metabolites of 

Lippia alba )Mill) N.E. Brown, grown in Colombia, and 

evaluation of its in vitro antioxidant activity. 

J Chromatogr A, 1025, #1, 93-103 

Stashenko, E.; Jaramillo, B.; Martinez, J 

1806 Rose/nerol Biotransformation of (R)-(+)-and (S)-(-)-citronellol headspace GC-MS 

oxides by Aspergillus sp. and Penicillium sp, and the use steam distillation @ 

of SPME for screening. 3.5 pH 

J Chromatogr A, 1027,#1-2, 137-146 

Demyttenaere, J; Vanoverschelde, J; De Kimpe, N 

1807 Fragrances Headspace-SPME & hydrodistillation of two fragrant Artemisia headspace GC, GC-MS 

from Artemicia Flavour Fragrance J., 20. #4, 395-398 

plants Baser, K. Husnu Can; Demirci, Betul; Demirci, Fatih 

1808 Volatiles from Volatiles associated with preferred and non- direct sampled GC-EAD 

slash/ loblolly preferred hosts of the Nantucket pine tip moth, 

pine Rhyacionia frustrana 


Asaro, C.; Sullivan, B.; Dalusky, M.; Berisford, C. 

1809 Pheromone Neocembrene A, a major component of the trail-following headspace GC-MS 

of canalifrons pheromone in the genus Prorhinotermes (Insecta, 

Isoptera, Rhinotermitidae) 

Chemoecology, 15, #1, 1-6 

Sillam-Dusses, D.; Semon, E.; Moreau, C.; 

Valterova, I.; Sobotnik, J.; Robert, A.;Bordereau, C 

1810 Pheromone Partial elucidation of Trichogramma putative sex headspace for GC-MS 

from wasp pheromone at trace levels by SPME-GC-MS studies 20-50hr 

J. Chromatogr. A, 1067, #1-2, 311-321 

Melo, R; Posthumus, M.; Silva, I.; Van Beek, T 





1811 Sesiidae sex New type of sesiidae sex pheromone identified headspace GC-MS 

pheromone from the hornet moth Sesia apiformis 2-alkenals derivative 

from hornet J Chemical Ecology, 30, #4, 805-817 

moth Francke, W.; Karalius, V.; Plass, E.; Lehmann, L.; 

dos Santos, A.; Buda, V.; Mozuraitis, R. 

Borg-Karlson, A.; 

1812 Pheromone Flight activity and further evidence for a female- headspace GC-EAD 

emission produced sex pheromone of the apple leaf 

from leaf midge, Dasineura mali, in Nova Scotia 

midge Northeastern Naturalist, 12, #1, 93-102 

Heath, J.; Zhang, Aijun; R., Wendell L.; Smith, R. 

1813 Pheromone Effect of aging on pheromone emission from a headspace GC-MS 

emission commercial beet armyworm (Lepidoptera : 

from traps Noctuidae) lure and trap efficiency 

J Economic Entomology, 98, #2, 373-377 

Showler, A..; Salgado, E.; Fraser, I.; Robacker, D. 

1814 Pheromone A cost of alarm pheromone production in cotton headspace GC-MS 

from apids apids, Aphis gossypii 

Naturwissenschaften, 92, #2, 69-72 

Byers, John A. 

1815 Pheromone SPME for the investigation of sex pheromone of headspace GC-MS 

from fruit Eucosam notanthes Meyrick 5min @ 20°C 

borer Talanta, 65, #3, 743-749 

Chu, T. Y.; Hung, C. C.; Hsu, C. Y. 

1816 Fragrance Rapid determination of volatile compounds emitted headspace GC-MS 

from flowers from Chimonanthus praecox flowers by headspace 

SPME-GC-MS 

Zeitschrift fuer Naturforschung, 59, #9-10, 636-640 

Deng, Chunhui; Song, Guoxin; Hu, Yaoming 

1817 Fragrance Single step determination of fragrances in Cucurbita 65µm PDMS-DVB GC-MS-MS 

from flowers flowers by coupling headspace SPME low-pressure 5min @ 60°C 

GC-tandem mass spectrometry headspace 

J. Chromatogr. A, 1045, #1-2, 173-179 

Egea Gonzalez, F.; Garrido Frenich, A.; Guerra Sanz, J.; 

Martinez Vidal, J.L.; Mena Granero, A. 

1818 Fragrance Sex and developmental stage of carob flowers headspace GC-MS 

from Carob affects composition of volatiles 

flower J Horticultural Sci & Biotechnology, 79, #5, 689-692 

Custodio, L.; Nogueira, J. M. F.; Romano, A. 

1819 Essential oils SPME-GC and olfactory analysis of the scent and headspace GC-FID and GC-MS 

from Chinese fixative properties of the essential oil of Rosa 

rose oil damascena L. from China 

Flavour and Fragrance J, 20, #1, 7-12 

Jirovetz, Leopold; Buchbauer, Gerhard; S, A; 

Balinova, A.; Guangjiun, Z.; Xihan, Ma 

1820 Volatiles from Comparison of odorous volatile compounds from fourteen headspace GC 

compost different commercial composts using SPME. 

Trans. Am. Soc. Agric. Eng., 48, #1, 315-320 

Kim, H.; McConnell, L.L.; Millner, P. 

1821 Nectar odors Why are some floral nectars scented? headspace GC-MS 

from flowers Ecology (Washington D C), 85, #6, 1486-1494 

Raguso, Robert A. 

1822 Volatiles Quality assessment of Flos Chrysanthemi Indici from 65µm PDMS-DVB GC-M 

from China different growing aras in China by SPME-GC-MS 30min @ 60°C 

medicine J. Chromatogr. A, 1047, #2, 281-287 headspace 

Chen, J; Deng, C; Fu, D; Sha, Y; Shen, S Zhang, X 





1823 Volatiles SPME-GC-MS analysis of volatile compounds in compounded 100µm PDMS GC-MS 

from China Chinese medicinal prescription, Xiao-Cheng-Qi-Tang 20min @ 90°C 

medicine Journal of Pharma Biomed Analysis, 36, #2, 381-385 stirring, headspace 

Sha, Yunfei; Shen, Shun; Duan, Gengli 

1824 Volatiles from Application of HS-SPME and GC-MS to characterization of 65µm CW/DVB GC-MS 

osmanthus volatile compounds emitted from osmanthus flowers 10 min @ 22°C 

flowers Annali di Chimica, 94, #12, 921-927 headspace 

Deng, Chunhui; Song, Guoxin; Hu, Yaoming 

1825 Odors from An evaluation of SPME for analysis of odorant 75µm Carboxen GC-MS 

biosolids emissions from stored biosolids cake headspace 

Water Res., 38, #17, 3800-3808 

Parker, W.J.; Visan, M. 

1826 Volatiles from Effects of petroleum spray oils on oviposition behaviour and headspace GC 

maize plants larval survival of Helicoverpa armigera Hubner (Lepidoptera : 

Pharmaceutical 

Noctuidae) and Ostrinia nubilalis Hubner (Lepidoptera:Pyralidae) 

Intl J of Pest Mgmt, 51, #2, 111-119 

Mensah, Robert; Frerot, Brigitte; Al Dabel, Faiza 

147 Volatiles in Application of Head-Space SPME for the Analysis of GC-MS 

biological fluids Volatile Metabolites 

J. Microbiol. Methods 25: 245 (1996) 

Milsson, T., Larsen, T., Montanarella, L., Madsen, J. 

338 Solvents in Determination of Residual Solvents in Pharmaceuticals 100µm PDMS GC-FID 

pharmaceutical with Automated SPME 15 min 

products Chem. N. Z. 61 (4): 10-12 (1997) 

Penton, Z. 

headspace 

149 Components Analysis of Components in Crude Drugs by Headspace 

in drugs SPME Method 

Zasshi 16: 251 (1996) 

Yakugaku 

473 Residual solvents Headspace SPME method optimization for 65µm DVB/PDMS GC 

pharmaceutical residual solvent analysis 30 min headspace 

samples Acta pharm. Hung., 1999, 69(2), 77-84 

Camarasu, C., Mezei, M., Szabo, A 

2gm NaCl, 

919 Residual solvents Headspace SPME method development for the analysis of 

pharmaceutical volatile polar residual solvents by GC-MS 

samples J. Pharm. & Biomediecal Aanlysis 2000, 23(1) 197-210 

Camarasu, C. 

Verapamil drug metabolism studies by automated in-tube solid phase 

1002 Verapamil 

microextraction. LC-MS 

Jnl of Pharmaceutical and Biomedical Analysis (2002) 30 (2), 307-319. 

Walles, M.; Mullett, W. M.; Levsen, K.; Borlak, J.; Wuensch, G.; Pawliszyn, 

J. 

1006 Trends New trends in sample preparation for clinical and pharmaceutical analysis 

TrAC-Trends in Analytical Chemistry (2003) 22 (4), 232-244. 

Kataoka, Hiroyuki 

1024 clenbuterol 

Solid-phase micro extraction (SPME) and headspace derivatization of 

clenbuterol followed by GC-FID and GC-SIMMS quantification. 85 um polyacrylate GC-FID, GC-SIMMS 


Wenclawiak, B. W.; Engelmann, M. D.; Hinz, D. 





1032 Review 

1101 MPHP in urine 

1107 Residual solvents 

1133 

1142 

Residual solvents in 

drug products 

Volatile residual solvents 

in Chinese medicines. 

1169 Clenbuterol in urine 

1279 

Endocrine disruptor 

contaminants. 

1308 Drug analysis 

1312 

1336 

Pharma process 

impurities 

Residual solvent testing: A review of gas-chromatographic and alternative 

techniques. 

Pharmaceutical Research (Dordrecht) (2003) 20 (3), 337-344. 

B'Hymer, Clayton 

New designer drug 4'-methyl-alpha-pyrrolidinohexanophenone: Studies on 

its metabolism and toxicological detection in urine using gas 

chromatography-mass spectrometry. GC-MS 

Journal of Chromatography B (2003) 789 (1), 79-91. 

Maurer, Hans H.; Fritschi, Giselher; Peters, Frank T.; Springer, Dietmar 

Use of solid-phase microextraction coupled with gas chromatography for the 

determination of residual solvents in pharmaceutical products Various 


Dugay, Jose; Legrand, Stephanie; Vial, Jerome 

Unknown residual solvents identification in drug products by headspace 

solid phase microextraction gas chromatography-mass spectrometry. 

Chromatographia (2002) 56(supplement), S131-S135 

Camarasu, C. C. 


Determination of volatile residual solvents in traditional Chinese medicines 

by headspace solid-phase microextraction and cryogenic gas 

chromatography with flame ionization detection PDMS/DVB GC-FID 


Jiang, Guibin; Liu, Jiemin; Liu, Jingfu; Liu, Jiyan; Wen, Meijuan; Zhou, 

Qunfang 

Quick analysis of small beta -agonists in urine by solid-phase 

microextraction with headspace derivatization and gas chromatographymass 

spectrometry. 

Fenxi Huaxue (2003) 37 (3), 326-328. 

Polyacrylate GC-MS 

Liang, Y. L.; Yin, B. Z.; Hu, X. Z.*; Yu, J. X.; Liu, H. W.; Lin, Y. F.; Wu, T. 

Simple and rapid analysis of endocrine disruptors in liquid medicines and 

intravenous injection solutions by automated in-tube solid-phase 

microextraction/high performance liquid chromatography. HPLC 

Journal of Pharmaceutical and Biomedical Analysis (2003) 32 (3), 469-478. 

Mitani, K.; Narimatsu, S.; Izushi, F.; Kataoka, H. * 

Solid-phase microextraction and liquid chromatography/mass spectrometry 

in drug analysis LC-MS 

Analytica Chimica Acta (2003) 492 (1-2), 49-67. 

Kumazawa, Takeshi; Lee, Xiao-Pen; Sato, Keizo; Suzuki, Osamu 

Determination of pharmaceutical process impurities by solid phase 

microextraction gas chromatography Carboxen/PDMS/DVB GC 


Frost, Richard P.; Hussain, Mumtaz S.; Raghani, Anil R. 

Development and evaluation of a solid-phase microextraction probe for in 

vivo pharmacokinetic studies polypyrrole 


Fahie, Brian; Grant, Russell P.; Incledon, Bev; Lord, Heather L.; Pawliszyn, 

Janusz B.; Walles, Markus 

1361 Drugs in biological fluids 

Automated sample preparation using in-tube solid-phase microextraction 

and its applications long dash a review. 

Analytical and Bioanalytical Chemistry (2002) 373(1-2), 31-45. 

Kataoka, H. 

LC-MS 





1392 Drugs in plasma 

1470 Amphetamine-like drugs 

1497 


pharmaceuticals 

1514 Delorazepam in urine 

1201 

1280 

Application of solid-phase micro-extraction technology to drug screening 

and identification. 

Annals of Clinical Biochemistry (2001) 38(5), 541-547. 

Mosaddegh, M. H.; Richardson, T.; Stoddart, R. W.; McClure, J. 

Polyacrylate, carbowax/DVB GC-MS 

Simultaneous detection of amphetamine-like drugs with headspace solidphase 

microextraction and gas chromatography-mass spectrometry. 

Journal of Chromatography B (2002) 780(1), 183-192 

Macchia, Teodora; Chiarotti, Marcello; Gentili, Stefano; Marsili, Remo; 

Torresi, Alessio 

High-speed gas chromatographic analysis of solvents in pharmaceuticals 

using solid phase microextraction 

Journal of Pharmaceutical and Biomedical Analysis (2002) 29(3), 507-518 

Raghani, A. R. 

Determination of delorazepam in urine by solid-phase microextraction 

coupled to high performance liquid chromatography. 

Journal of Pharmaceutical and Biomedical Analysis (2002) 28(5), 965-972 

Zambonin, Carlo Giorgio; Aresta, Antonella; Monaci, Linda 

Rapid screening of 2-"fluorine-18"-fluoro-2-deoxy-D-glucose infusions for 

volatile organic compound contaminants by solid phase microextraction with 

gas chromatography-selective ion monitoring mass spectrometry (SPME- 

GC-SIMMS). 

Applied Radiation and Isotopes (2003) 58 (2), 193-200. 

Kanu, A. B.; Dixon, M.; Zu, Y. Y.; Bailey, J.; Gillies, J. M.; Zweit, J.; Thomas, 

C. L. P.* 


65um PDMS DVB 

50um Carbowax TPR, 60um 

PDMS DVB 

Determination of trace retinoic acid by capillary electrophoresis-solid-phase 

microextraction with direct UV detection. CE 

Journal of Chromatographic Science (2003), 41 (6), 301-304). 

Fang, M.; Xu, G. W. 

1827 Pharmaceuticals Study of multiple SPME combined off-line w/HPLC 100µm PDMS & HPLC 

in urine Application in analysis of pharmaceuticals in urine 85µm polyacrylate 

Anal. Chim. Acta, 516, #1-2, 197-204 immersed 

Aikaterini Lontou, M.; Gondova, T.; Michopoulos, F.; salt added 

Sucha, M.; Theodoridis, G. 

Biological 

638 Anesthetics Evaluation of SPME for the study of protein binding in human 60µm Carbowax/DVB NPD 

in plasma plasma samples 32°to 40°C 

J. Chromatogr. Sci. (2000), 38(10), 458-464 pH 6.4-9.4 

Abdel-Rehim, M., Calsson, G., Bielenstein, M., Arvidsson, T., 

Blomberg, L. 

99 Aniline, nitrobenzene, Measurement of the Free Concentration Using SPME: 85µm polyacrylate GC-MS 

4-n-pentylphenol, Binding to Protein 24°C, 9-14 min 

4-chloro-3-methylphenol J. Anal. Chem. 68: 4463-4467 (1996) stirring 

in bovine serum albumin Vaes, W., Ramos, E., Verhaar, H., Seinen, W., Hermens, J. K2PO4 buffered 

GC-MS 

GC 

HPLC-UV 

140 Protein in Solid Phase Microextraction of Biopolymers, Exemplified 85µm polyacrylate HPLC-UV 

bovine serum albumin with Adsorption of Basic Proteins onto a Fiber Coated 5-240 sec 

with Polyacrylic Acid 

J. Microcolumn Sep. 8: 1 (1996) 

Liao, J., Zeng, C., Hjerten, S., Pawliszyn, J. 

immersion 





411 Proteins Optimization of SPME-Capillary Zone Electrophoresis-MS for capillary zone 

High Sensitivity Protein Identification electrophoresis- 

Electrophoresis (1998), 19(13), 2338-2347 

Figeys, D., Ahang, Y., Aebersold, R. 

Bio-compatible in-tube SPME capillary for the direct extraction and HPLC 

MS 

988 Drugs in human serum determination of drugs in human serum. 

J.Chromatogr. A (2002) 963(1-2), 325-334 

Mullett, W.M.; Levsen, K.; Lubda, D.; Pawliszyn, J. 

HPLC 

1020 Rapid diagnosis of GI infection from flatus. 

Gut (2003) 52 (Supplement 1), A93. 

Probert, C. S.; Jones, P.; Ratcliffe, N. 

1036 Semi-volatiles in saliva 

1037 Amphetamines in hair. 

1038 Volatiles in breath 

1056 

Pheromones from male 

bugs. 

1057 Review article 

1076 Organophosphorus 

pesticides in blood 

1060 

Phthalic monoesters in 

urine. 

1104 PAHs in urine. 

Solid-phase micro-extraction-gas chromatography-mass spectrometry and 

headspace-gas chromatography of tetrahydrocannabinol, amphetamine, 

methamphetamine, cocaine and ethanol in saliva samples PDMS GC-MS 

Journal of Chromatography B: Analytical Technologies in the Biomedical 

and Life Sciences (2003) 789 (1), 73-78. 

Alves Silva, Ovandir; De Moraes Moreau, Regina Lucia; Tawil, Nadia; 

Yonamine, Mauricio 

Determination of amphetamines in human urine by headspace solid-phase 

microextraction and gas chromatography 100 um PDMS GC-FID 



Christopoulou, Klio; Psaroulis, Dimitrios; Raikos, Nikolaos; Theodoridis, 

Georgios; Tsoukali, Heleni 

Application of low-temperature glassy carbon-coated macrofibers for solidphase 

microextraction analysis of simulated breath volatiles PDMS-DVB 


Giardina, Matthew; Olesik, Susan V. 

Male bugs modulate pheromone emission in response to vibratory signals 

from conspecifics. 

Journal of Chemical Ecology (2003) 29 (3), 561-574. 

Renou, Michel; Lasnier, Therese; Miklas, Nadege 

New developments and applications of solvent-free sampling and sample 

preparation technologies for the investigation of living systems LC-MS 

Australian Journal of Chemistry (2003) 56 (2-3), 155-158. 

Pawliszyn, Janusz 

Simple determination of 22 organophosphorus pesticides in human blood 

using headspace solid-phase microextraction and gas chromatography with 

mass spectrometric detection. 


Musshoff, F.; Junker, H.; Madea, B. 

GC-MS 

Determination of phthalic monoesters in aqueous and urine samples by 

solid-phase microextraction-diazomethane on-fibre derivatization-gas 

chromatography-mass spectrometry. PDMS-DVB GC-MS 


Alzaga, R.; Pena, A.; Bayona, J. M.* 

25 C, 20 minutes, headspace 

Determination of polycyclic aromatic hydrocarbons in urine of coke oven 

workers by headspace solid phase microextraction and gas chromatographymass 


Chemico-Biological Interactions (2003) 145 (2), 165-174. 

Rappaport, Stephen M.; Waidyanatha, Suramya; Zheng, Yuxin 





1158 1,8-cineole in blood 

1162 Fatty acid esters in hair. 

1163 

1205 Busulphan in plasma 

1207 

Midazolam in human 

plasma 

1261 Elephant urine 

1262 Pheromones in urine. 

Application of solid-phase microextraction to the quantitative analysis of 1,8cineole 

in blood and expired air in a Eucalyptus herbivore, the brushtail 

possum ( Trichosurus vulpecula ). GC 

Journal of Chromatography, B: Analytical Technologies in the Biomedical 


Boyle, R. R.; McLean, S.; Brandon, S.; Pass, G. J.; Davies, N. W. 

Fatty acid ethyl esters in neonatal hair: A possible biomarker for in utero 

ethanol exposure. 

Alcoholism Clinical and Experimental Research (2003) 27 (5 supp), 39A. 

Koren, G.; Klein, J.; Caprara, D. 

Headspace solid-phase microextraction (SPME) and gas chromatographymass 

spectrometry (GC-MS) for the determination of 5alpha-androst-2-en- 

17-one and -17beta-ol in the female Asian elephant: Application for 

reproductive monitoring and prediction of parturition. GC-MS 

Journal of Steroid Biochemistry and Molecular Biology (2003) 84 (2-3), 383- 

391. 

Dehnhard, M.; Eulenberger, K.; Hatt, J.-M.; Ochs, A.; Strauss, G. 

On-line derivatization utilizing solid-phase microextraction (SPME) for 

determination of busulphan in plasma using gas chromatography-mass 

spectrometry (GC-MS). 

Therapeutic Drug Monitoring (2003) 25 (3), 400-406. 

Abdel-Rehim, Mohamed; Blomberg, Lars; Hassan, Moustapha; Hassan, 

Zuzana 

Carbowax/DVB GC 

Determination of midazolam in human plasma by solid-phase 

microextraction and gas chromatography/mass spectrometry. 


Davide Ferrara, Santo; Frison, Giampietro; Maietti, Sergio; Tedeschi, 

Luciano 

Use of SPME and GC-MS for chemical analysis of urine from African 

elephants in musth. 

Abstracts of Papers American Chemical Society (2003) 225 (1-2), CHED 

614. 

Hicks, Adam R.; Goodwin, Thomas E.; Dill, Whitney M.; Davis, Ben L.; 

Alberts, Susan C.; Hollister-Smith, Julie 

Chemical analysis of preovulatory female African elephant urine: A search 

for putative pheromones. 


409. 

Hicks, Adam R.; Goodwin, Thomas E.; Dill, Whitney M.; Davis, Ben L.; Loizi, 

Helen; Rasmussen, L. E. L.; Schulte, Bruce A. 

85um Polyacrylate GC-MS 

1301 

Analysis of odours in human armpit by GC-MS with headspace solid-phase 

Odours in human armpit. microextraction. 


Wu, D. H.; Xu, H. K.; Wang, Z. P.; Zhang, L.; Wang, X. L.* 

70 um DVB/carbowax GC-MS 

1310 

Amitraz in canine 

plasma. 

Determination of amitraz in canine plasma by solid-phase microextractiongas 

chromatography with thermionic specific detection PDMS GC-TSD 



Carvalho, D.; Farias, A.; Lancas, F.M.; Queiroz, M.E.C.; Valadao, C.A.A. 

1344 VOC's in exhaled breath 

Application of solid-phase microextraction and gas chromatography-mass 

spectrometry to the determination of volatile organic compounds in endexhaled 

breath samples. 


Prado, C.; Marin, P.; Periago, J. F. 

GC-MS 





1346 Pheromones in ants. 

1359 Volatile aldehydes 

1360 VOCs in body fluids 

1365 Hydrocarbons in cuticles 

1375 

1380 

p,p'-DDE in biological 

samples 

Perfluorocarbons in 

blood. 

1396 Ropivacaine in plasma 

1413 

1225 

Naltrexone, 6,betanaltrexol 

1159 Phthalates from toys 

1210 

Volatile fatty acids in 

rumen. 

Investigation by solid-phase microextraction and gas chromatography/mass 

spectrometry of trail pheromones in ants. GC-MS 

Rapid Communications in Mass Spectrometry (2003) 17 (18), 2071-2074. 

di Tullio, A.; de Angelis, F. *; Reale, S.; Grasso, D. A.; Visicchio, R.; 

Castracani, C.; , A.; le Moli, F. 

SPME determination of volatile aldehydes for evaluation of in-vitro 

antioxidant activity. GC-MS 


Stashenko, E. E.; Puertas, M. A.; Martinez, J. R. 

Cryogenic oven-trapping gas chromatography for analysis of volatile organic 

compounds in body fluids. GC-MS 


Watanabe-Suzuki, K.; Ishii, A.; Suzuki, O. 

Solid-phase microextraction for the detection of termite cuticular 

hydrocarbons. GC-MS 


Bland, J. M.; Osbrink, W. L. A.; Cornelius, M. L.; Lax, A. R.; Vigo, C. B. 

Solid-phase microextraction and GC-MS analysis of p, p' -DDE in biological 

samples. PDMS GC-MS 

Journal of Chromatography, B: Biomedical Applications (2001) 761(1), 93- 

98. 

Kusakabe, T.; Saito, T. *; Takeichi, S. 

Detection of perfluorocarbons in blood by headspace solid-phase 

microextraction combined with gas chromatography-mass spectrometry. GC-MS 

Biomedical Chromatography (2001) 15(7), 443-451. 

Mathurin, J. -C.; de Ceaurriz, J.; Audran, M.; Krafft, M. -P. 

Determination of ropivacaine and its metabolites in human plasma using 

solid phase microextraction and GC-NPD/GC-MS. Various Gc-MS 


Abdel-Rehim, M.; Andersson, M.; Portelius, E.; Norsten-Hoog, C.; 

Blomberg, L. G. 

Quantification of naltrexone and 6,beta-naltrexol in plasma and milk using 

gas chromatography-mass spectrometry. Application to studies in the 

lactating sheep. GC-MS 

Journal of Chromatography B (2001) 761(1), 85-92. 

Ilett, Kenneth F.; Bencini, Roberta; Chan, Chooi Fen; Chiswell, Gregory M.; 

Dusci, Leon J.; Hackett, L. Peter 

Monitoring and fast detection of mycotoxin-producing fungi based on 

headspace solid-phase microextraction and headspace sorptive extraction 

of the volatile metabolites. GC-MS 


Demyttenaere, J. C. R.; Morina, R. M.; Sandra, P. 

Determination of bis(2-ethylhexyl) phthalate of plastic toys leached in 

stimulant saliva by gas chromatography with solid-phase microextraction 


PDMS-fullerene GC 

Yang, Z. J.; Zhang, W. Y.; Pan, K. Y.; Yu, J. X.; Wu, C. Y.; Wang, C. Y. 

Characterizing volatile fatty acids and other gases in a rumen closed in vitro 

fermentation system using solid phase microextraction 

Transactions of the American Society of Agricultural Engineers (2003) 46 

(2), 585-588. 

Chirase, Norbert K.; Koziel, Jacek A.; Spinhirne, Jarett P. 

DVB/Carboxen/PDMS GC-MS 





1412 Volatile hydrocarbons 

1311 

1443 Organochlorine 

pesticides in fish 

1456 

1468 

1485 

1487 

1503 

1506 

Pheremones in mouse 

urine 

Sufentanil in human 

plasma 

Volatiles in live 

biological samples 

Pheremones from 

Lepidoptera 

Organic compounds in 

elephant urine 

C9-C20 hydrocarbons in 

shellfish 

Volatile hydrocarbon biodegradation by a mixed-bacterial culture during 

growth on crude oil. 

Journal of Industrial Microbiology & Biotechnology (2001) 26(6), 356-362. 

Van Hamme, J. D.; Ward, O. P 

Production of flavoured volatile organic compounds (VOCs) by Candida 

oleophila GK10: Optimisation using factorial design and response surface 

analysis GC-MS 

Enzyme and Microbial Technology (2003) 33 (5), 668-675. 

Buzzini, Pietro; Davoli, Paolo; Martini, Alessandro; Pagnoni, Ugo Maria 

Solid-phase microextraction as a clean-up and preconcentration procedure 

for organochlorine pesticides determination in fish tissue by gas 

chromatography with electron capture detection 


Blanco-Gonzalez, Elisa; Centineo, Giuseppe; Fidalgo-Used, Natalia; Sanz- 

Medel, Alfredo 

Identification of pheromones in mouse urine by head-space solid phase 

microextraction followed by gas chromatography-mass spectrometry. 


Kayali-Sayadi, M. N.; Bautista, Jose M.; Polo-Diez, L. M.; Salazar, Ignacio 

Solid-phase microextraction of human plasma samples for determination of 

sufentanil by gas chromatography-mass spectrometry. 

Therapeutic Drug Monitoring (2002) 24(6), 768-774 

Boulieu, Roselyne; Bolon, Magali; Dufresne, Christelle; Paradis, Chantal 

Applications of solid-phase microextraction to chemical analysis of live 

biological samples. 

Trends in Analytical Chemistry (2002) 21(6-7), 428-438 

Augusto, Fabio; Valente, Antonio Luiz Pires 

Lepidoptera (Sesamia nonagrioides (Lefebvre) (Lepidoptera Noctuidae)) by 

solid-phase microextraction 

Redia (2001) 84, 7-18 

Rotundo, Giuseppe; Germinara, Giacinto Salvatore; De Cristofaro, Antonio 

Implementation of SPME and GC-MS to identify organic compounds in 

African elephant urine. 

Abstracts of Papers American Chemical Society (2002) 223(1-2), CHED 

234 

dwin, Thomas E.; Dowdy, Nichole C.; Rasmussen, L. E. L. 

Determination of petroleum contamination in shellfish using solid phase 

micro-extraction with gas chromatography-mass spectrometry. 

Analytical and Bioanalytical Chemistry (2002) 373(3), 147-152 

Stack, Mary A.; James, Kevin J.; O'Connell, Sharon 

GC-ECD 

85um Carboxen PDMS GC-MS 

65um PDMS DVB, 10mins, 

immersion 

100um PDMS, 20mins, 120 

degrees C, headspace 

GC-MS 

GC-MS 


1519 Thymol in humans Systemic availability and pharmacokinetics of thymol in humans. LC-MS-MS 

Journal of Clinical Pharmacology (2002) 42(7) 731-737 

1529 Ethanol in blood 

Veit, Markus; Abel, Gudrun; Brinkhaus, Benno; Derendorf, Hartmut; Graefe, 

Eva-Ulrike; Kohlert, Claudia; Maerz, Reinhard W.; Schindler, Gernot 

Optimization of solid-phase microextraction conditions for gas 

chromatographic determination of ethanol and other volatile compounds in 

blood. 


Zuba, Dariusz; Parczewski, Andrzej; Reichenbacher, Manfred 


65um Carbowax DVB, 60 

degrees C, 10mins, stirring, 

NaCl addtion, headspace 

GC-FID

1532 

1533 

1540 




2-chlorovinylarsonous 

acid in human urine 

Fluoroacetic acid in 

biological samples 

Quantitation of 2-chlorovinylarsonous acid in human urine by automated 

solid-phase microextraction-gas chromatography-mass spectrometry. 


Calafat, Antonia M.; Ashley, David L.; Wooten, Joe V. 

Headspace solid-phase microextraction with 1-pyrenyldiazomethane onfibre 

derivatization for analysis of fluoroacetic acid in biological samples. 


Pragst, Fritz; Huebner, Sandra; Mills, Graham; Sporkert, Frank 

carbamazepine, 

carbamazepine epoxide, 

Determination of lamotrigine simultaneously with carbamazepine, 

phenytoin, 

carbamazepine epoxide, phenytoin, phenobarbital, and primidone in human 

phenobarbital, and 

plasma by SPME-GC-TSD. 

primidone in human 

plasma 

1427 Microcystins 


Lancas, F. M.; Carvalho, D.; Queiroz, M. E. C.; Silva, S. M. 

85um Carboxen PDMS 

Stableflex, on-fiber 

derivatization with 

1-pyrenyldiazomethane 

GC-MS 

Determination of microcystins in cyanobacterial blooms by solid-phase 

microextraction : High-performance liquid chromatography. HPLC 

Environmental Toxicology and Chemistry (2001) 20(8), 1648-1655. 

Lam, Michael Hon-wah; Lam, Paul K. S.; Poon, Ka-Fai; Wong, Bryan S. F. 

1828 Drugs in Rapid screening procedure based on headspace Headspace, GC-MS 

hair SPME-GC-MS for the detection of many 5min @ 90°C 

recreational drugs in hair. 

J. Chromatogr. B, 801, #2, 289-296 

Gentili, S.; Cornetta, M.; Macchia, T. * 

1829 Parabens in Determination of parabens in pharmaceutical formulations by GC-IMS 

pharmaceutics SPME ion-mobility spectrometry 

Anal. Chem., 77, #18, 5938-5946 

Lokhnauth, John; Snow, Nicholas 

1830 Amphetamine Simultaneous derivatization and extraction of amphetamine-like 100µm PDMS GC-MS 

drugs in drugs in urine with headspace SPME followed by GC-MS 30min @ 90°C 

urine Anal. Chim. Acta, 539, #1-2, 49-54 HFBA derivative 

Chia, Kan-Jung; Huang, Shang-Da headspace 

1831 Amphetamine Poly(methacrylic acid-ethylene glycol dimethacrylate) polycrylate coated HPLC-UV 

drugs in monolith in-tube SPME coupled to HPLC and analysis of capillary tube 

urine amphetamines in urine samples 

J. Chromatogr. A, 1074, #1-2, 9-16 

Da, Shi-Lu; Fan, Yi; Feng, Yu-Qi; Zhang, J; Zhang, M 

1832 Amphetamine Application of SPME combined with derivatization to 50µm CW-TPR HPLC-UV 

drugs in the determination of amphetamines by liquid chromatog FMOC derivative 

urine Analytical Biochemistry, 333, #2, 328-335 

Chafer-Pericas, C.; Campins-Falco, P.; Herraez-Hernandez, R. 

1833 Amphetamine Enantiomeric determination of amphetamines: Exploring 100µm PDMS GC-SIM-MS 

drugs in A novel one-step SPME-based approach 10min @ 70°C 

urine J. Chromatogr. B, 825, #1, 79-87 prolyl chloride 

Wang, Sheng-Meng derivative 

1834 Amphetamine SPME with LC-electrospray ionization-tandem MS LC-ESI-MS/MS 

in serum for analysis of amphetamine and methamphetamine in serum 

Anal. Chim. Acta, 538, #1-2, 49-56 

Chou, Chi-Chi; Lee, Maw-Rong 

1835 BTX solvents Quantitative analysis of benzene, toluene, headspace GC-MS 

in urine and xylenes in urine by headspace SPME 

J Chromatogr A, 1027, #1-2, 37-40 

Alkalde, T; Peralba, M; Zini, C; Caramao, E. 





1836 PCB metabolite SPME w/ on-fiber derivatization for the determination of 65µm PDMS-DVB GC/MS 

in urine hydroxy-polychlorinated biphenyl compounds in urine 60min @ 90°C 

Anal. Chim. Acta, 539, #1-2 55-60 BSTFA derivative 

Hong, Jee Eun; Lee, Won; Park, Song-Ja; Pyo, Heesoo headspace 

1837 Iodine in Single drop microextraction or SPME-GC-MS iodate derivatives GC 

various for the determination of iodine in pharmaceuticals, 

matrices iodized salt, mil powder and vegetables 

involving conversion into 4-iodo-N,N-dimethylaniline. 

J Chromatogr A, 1023, #1, 33-39 

Das, P; Gupta, M; Jain, A; Verma, K. 

1838 Diazipenes in Monitoring of drugs and metabolites in whole blood restricted access LC-MS 

biological fluid by restricted-access SPME coupled to LC-MS coated fibers 


Walles, M.; Mullett, W. M.; Pawliszyn, J. 

1839 Methyl An accurate and sensitive method for determination 100µm PDMS ICP-MS 

mercury from methylmercury in biological specimens methyl, ethyl, phenyl 

biological using GC-ICP-MS with solid phase microextraction derivatives 

specimens J Anal At Spectrom, 19, #12, 1546-1551 microwave extraction 

Christopher, S.J.; Davis, W. Clay; Day, Rusty D.; 

Long, S.E.; Schantz, Michele M.; Vander Pol, Stacy S. 

1840 Volatiles in Sampling and analysis of volatile organic compounds 50/30µm DVB/CAR GC-MS 

bovine breath in bovine breath by SPME-GC-MS 15min @ 22°C 


Spinhirne, J.; Koziel, J.; Chirase, N. 

1841 Phlated esters High-throughput analysis of phthalate esters in 85µm polyacrylate GC-MS 

in serum human serum by direct immersion SPME followed direct immersion 

by isotope dilution-fast GC/MS 

Anal. Bioanal. Chem., 380,#2, 275-283 

Colon, Ivelisse; Dimandja, Jean-Marie D. 

1842 Ligustilides Development of pressurized hot water extraction headspace GC-MS 

in Chinese followed by headspace SPME-GC-MS determination 

medicines ligustilides in Ligusticum chuanxiong and Angelica sinensis 

J. Sep. Sci., 28, #11, 1237-1243 

Deng, Chunhui; Ji, Jie; Wang, Xiaochuan; Zhang, X 

1843 Benzene Urinary benzene determination by SPME/GC-MS: 1 min @ 15°C GC-MS 

from urine A study of variables by fractional factorial headspace 

design and response surface methodology 

J. Chromatogr. B, 804, #2, 255-261 

Garrido, J.; Periago, J.F.; Prado, C. 

1844 Faty Acids in Rapid measurement of C13-enrichment of acetic, propionic 75µm Carboxen GC-MS 

plasma and butyric acids in plasma with SPME coupled to GC-MS 5min extract 

Anal. Chim. Acta, 512, #2, 305-310 headspace 

Champ, M.; Delepee, R.; Dumon, H.; LeBizec, B.; 

Martin, L.; Maume, D.; Moreau, N.; Nguyen,P 

1845 Monoterpenes cDNA isolation and functional expression of myrcene GC 

from Perilla synthase from Perilla frutescens 

frutescens Biological & Pharmaceutical Bulletin, 27, #12, 1979-1985 

Hosoi, Madoka; Ito, Michiho; Yagura, Toru; 

Adams, Robert Phillip; Honda, Gisho 

1846 Acetone in Rapid determination of acetone in human plasma 65µm PDMS-DVB GC-MS 

plasma by GC-MS and SPME with on-fiber derivatization PFBHA derivative 

J. Chromatogr. B, 805, #2, 235-240 

Deng, Chunhui; Zhang, Jie; Zhang, Wei; Zhang, Xiangmin 

1847 Amino acids Rapid determination of amino acids in neonatal blood headspace GC-MS 

in blood samples based on derivatization with isobutyl chloroformate 

chloroformated followed by SPME-GC-MS derivative 

Rapid Communications in Mass Spec, 18, #21, 2558-2564 

Deng, C. H.; Li, N.; Zhang, X. M.* 





1848 Trimethylamine Quantifying trimethylamine and trimethylamine- N -oxide GC 

in plasma in human plasma: interference from endogenous quaternary 

endogenous quaternary ammonium compounds. 

Analytical Biochemistry, 334, #2, 403-405 

Bain, M. A.; Faull, R.; Fornasini, G.; Milne, R. W.; 

Schumann, R.; Evans, A. M. 

1849 Anigotensin Fast assay of angiotensin 1 from whole blood by alkyl diol silica coating HPLC 

from blood cation-exchange restricted-access SPME immersed sampling LC-MS 

Anal. Chim. Acta, 537, #1-2, 231-237 

Musteata, F.; Pawliszyn, Janusz; Walles, M. 

1850 Fatty acid Concentration of fatty acid ethyl esters in hair of Headspace GC-MS 

ethyl esters alcoholics: Comparison to other biological Ethyl ester derivatives 

in hair state markers and self reported-ethanol intake. 

Alcohol and Alcoholism, 39, #1, 33-38 

Wurst, F.; Alexson, S.; Wolfersdorf, M.; Bechtel, G; 

Forster, S.' Alling.C.; Aradottir, S.; Jachau, K.; Huber, P.; 

Allen, J.; Auwaerter, V.; Pragst, F. 

1851 Fatty acid Comparison of ethyl glucuronide and fatty acid ethyl ester Headspace GC-MS/NCI 

ethyl esters concentrations in hair of alcoholics, social drinkers, Ethyl ester derivatives 

in hair and teetotallers 

Forensic Science Intl,145, #2-3, 167-173 

Yegles, M.; Labarthe, A.; Auwarter, V.; Hartwig, S.; Vater, H.; 

Wennig, R.; Pragst, F. 

1852 Anti- SPME with on-fiber derivatization for the analysis 85µm polyacrylate GC-MS 

inflamatory of anti-inflammatory drugs in water samples. MTBSTFA derivative 

drugs in J Chromatogr A, 1024, #1-2, 1-8 Headspace 

water Rodriguez, I.; Carpinteiro, J.; Quintana, J. B.; . 

Carro, A. M.; Lorenzo, R. A.; Cela, R 

1853 Fluoroacet- Application of SPME-GC-MS in analysis of poison LC-MS 

amide in body Zhipu Xuebao, 25, Suppl, 151-152 

fluids Cai, X. L.; Wu, G. P. 

1854 Fluoroacet- Fast detection of fluoroacetamide in body fluid 100µm PDMS GC-MS 

amide in body using GC-MS after SPME. 25min @ 70°C 

fluids J Chromatogr, B:802, #2, 239-245 immersed 

Cai, X.; Zhang, D.; Ju, H. X.; Wu, G.; Liu, X. 

1855 Trichloro- Sensitive methods for trace level analysis of headspace @ 55°C GC-MS 

ethylene in trichloroethylene (TCE) in rat blood and tissues. 

blood/tissues Proc. 50th ASMS Conf. Mass Spectrom. Allied Top. 

2002, p629-630 

Bartlett, Michael G.; Brown, Stacy D.; Bruckner, James V.; 

Dixon, Amy M.; Muralidhara, S. 

1856 Benzodiaze- Analysis of benzodiazepines from whole blood 50µm CW-TPR LC-MS-MS 

pines in by SPME coupled to LC-MS-MS 

whole blood Proc. 50th ASMS Conf. Mass Spectrom. Allied Top. 

2002, p513-514 

Grant, R; Incledon, B; Lord, H; Pawliszyn, Janusz 

1857 Benzene in Application of the standard addition approach for the headsapce GC-MS 

urine quantification of urinary benzene 

J. Chromatogr. B, 818, #2, 293-299 

Acampora, A.; Basilicata, P.; Miraglia, N; 

Pieri, M.; Sannolo, N.; Soleo, L. 

1858 Cresols in Determination of urinary ortho- and meta-cresol in 100µm PDMS GC-MS 

urine humans by headspace SPME-GC-MS headsapce 

J. Chromatogr. B, 817, #2, 309-317 

Campo, L.; Foa, V.; Fustinoni, S.; Mercadante, R.; 

Scibetta, L.; Valla, C. 

1859 Ibuprofen SPME and chiral HPLC analysis of ibuprofen in urine 65µm PDMS- DVB HPLC-UV 

in urine J. Chromatogr.B, 818, #2, 285-291 immersion sampling 

Bonato, P.; Cesarino, E.; De Oliveira, A. 





1860 Ibuprofen Stereoselective determination of the major ibuprofen 50µm CW-TPR HPLC 

metabolites metabolites in human usrine by off-linecoupling SPME-HPLC immersion sampling 

in urine Anal. Chim. Acta, 538, #1, 25-34 

De Oliveira, A;, DeSantana, Fo; Bonato, P 

1861 Barbiturates Simultaneous determination of barbiturates in human immersion sampling GC-MS 

in blood/urine biological fluids by direct immersion SPME and GC-MS salt added 

J. Chromatogr. B, 806, #1, 65-73 

Arinobu, T.; Hattori, H.; Ishii, A.; Iwai, M.; Suzuki, O.; 

Kumazawa, T., Noguchi, H., Noguchi, H.; Seno, H. 

1862 Acrolein in Monitoring of urinary acrolein concentration in headsapce GC-MS 

urine patients receiving cyclophosphamide and ifosphamide 

J. Chromatogr. B, 806, #1, 59-63 

Namera, A.; Sakura, N.; Takamoto, S.; Yashiki, M. 

1863 Rivastigmine Headspace SPME and capillary GC-MS determination 65µm PDMS/DVB GC-MS 

in plasma of rivastigmine in canine plasma samples 30min @ 100°C 

J. Chromatogr. B, 806, #2, 271-276 headspace 

Deng, Chunhui; Duan, Gengli; Huang, Taomin; Liu, Zhen; NaOH/NaCO 3 buffer 

Sha, Yunfei; Yang, Bei 

1864 Mycophnolic Determination of the immunosuppressant mycophenolic 50µm CW-TPR HPLC-UV 

acid in serum acid in human seum by SPME coupled to LC headspace 

J. Chromatogr. B, 806, #2, 89-93 

Aresta, A; Palmisano, F; Zambonin, C 

1865 JP-8 fuel on Dose related absorption of JP-8 jet fuel GC-FID 

porcine skin hydrocarbons through porcine skin w/ quantitative 

structure permeability relationship analysis 

Toxic Mechanisms & Methods 14, #3, 159-166 

Muhammad, F.; Baynes, R.; Monteiro-Riviere, N.; 

Xia, X.; Riviere, J. 

1866 Volatiles in GC-MS analysis of volatile compounds from 100µm PDMS GC-MS 

Houttuynia Houttuynia cor-data Thunb after extraction by SPME, headspace 

cordata thunb flash evaporation and steam distillation 

Analytica Chimica Acta, 531, #1,07-104 

Liang, M; Qi, M; Zhang, C; Zhou, S; Fu, R; Huang, J 

1867 Serotonin Rapid screening of selective serotonin re-uptake 65µm PDMS-DVB GC-MS 

in urine inhibitors in urine samples using SPME-GC-MS in-situ derivatization 

Anal. Bioanal. Chem., 382, #6, 1351-1359 30min analysis 

Cela, R.; Garcia-Jares, Carmen; Lamas, J.; 

Llompart, M.; Salgado-Petinal, C. 

1868 Chlorinated Determination of dichloromethane, trichloroethylene and 75µm Carboxen GC-MS 

hydrocarbons perchloroethylene in urine samples by HD-SPME-GC-MS 22°C, saturated salt 

in urine J. Chromatogr. B, 820, #1, 95-102 headspace 

Andreoli, R; Franchini, I; Manini, P; Mutti, A; Poli, D agitated 

1869 Organo- SPME-GC analysis of organophosphorus pesticides headspace GC-NPD 

phosphorus in biological samples 

pesticides in J. Chromatogr. B,822, #1-2, 194-200 

blood, urine Grigoratou, I; Raikos, N; Theodoridis, G; Tsoukali, H 

1870 Tramadol Rapid determination of tramadol in human plasma by 65µm PDMS-DVB GC/MS 

in plasma headspace SPME and capillary GC-MS 30min @ 100°C 

J Pharma and Biomed Analysis, 37, #1, 143-147 0.1 M NaOH 

Sha, Y. F.; Shen, S.; Duan, G. L. headspace 

1871 Cancer Investigation of volatile biomarkers in lung cancer headspace GC/MS 

Biomakers blood using SPME and capillary GC-MS 

in blood J. Chromatogr. B, 808, #2, 269-277 

Deng, Chunhui; Li, Ning; Zhang, Xiangmin 





1872 Cancer A study of an electronic nose for detection of lung headspace GC/MS 

Biomakers cancer based on a virtual SAW gas sensorsarray 

in blood and imaging recognition method 

Meas. Sci. Technol., 16, #8, 1535-1546 

Cao, M.; Chen, X.; Hu, W.; Li, Yi.; 

Pan, H.; Wang, P.; Ying, K. 

1873 Trichloro- Optimization of SPME for analysis of trichloroethylene in rat headspace GC/MS 

ethylene in blood and tissues by SPME-GC/MS 5 min 

rat blood Instrum Sci Technol, 33, #2, 175-186 

Bartlett, M.; Brown, S.; Bruckner, J.; Dixon, A.; 

Muralidhara, S. 

1874 Fatty Rapid measurement of 13 C-enrichment of acetic, 75µm Carboxen GC-MS 

acids in propionic, and butyric acids in plasma w/ SPME 5 min extract 

plasma coupled to GC-MS 


Moreau, N. M.; Delepee, R.; Maume, D.; le Bizec, B.; 

Nguyen, P..; Champ, M..; Martin, L..;Dumon, H. 

1875 Animal testing Toward more useful in vitro toxicity data with measured in-vitro sampling GC 

free concentrations 

Environ. Sci. Technol., 38. #23, 6263-6270 

Busser, F; Heringa, M.; Hermens, J.; Schreurs, R.; 

Van Der Burg, Bart; Van Der Saag, Paul T. 

1876 Volatiles in SPME followed by GC-MS analysis of the volatile headspace GC-MS 

chinese components of Flos Chrysanthemi indici in 

medicines different growing areas. 


Wu, Q.; Deng, C. H.; Shen, S.; Song, G. X.; Hu, Y. 

M.; Fu, D. X.; Chen, J. K.; Zhang, X. M.* 

1877 Diethyl Application of SPME to in vitro skin permeation experiments GC 

phthalate example using diethyl phthalate 

on skin Toxicology In Vitro, 19, #2, 253-259 

Frasch, H. Fred; Barbero, Ana M. 

1878 Volatiles from Identification of biogenic organotellurides in Escherichia 75µm Carboxen GC-MS 

cell culture coli K 12 headspace gases using SPME-GC headspace 

Analytical Biochemistry, 331. #1, 106-114 

Swearingen, J.; Araya, M.; Plishker, M.; Saavedra, C.; 

Vasquez, C.Chasteen, T. 

1879 Faecal Odor The effect of oligofructose on urea metabolism and headspace GC 

from cats faecal odour components in cats 

J Animal Physiology and Animal Nutr, 89, #3-6, 208-214 

Hesta, M.; Hoornaert, E.; Verlinden, A.; Janssens, G. P. J. 

1880 Strychnine Application of SPME to determination of strychnine in blood 65µm CW-DVB GC/EI-MS 

in blood J Chromatogra B, 816, #1-2, 29-34 20min extraction 

Barroso, M.; Gallardo, E.; Margalho, C; Avila, S; immersion sampling 

Marques, E; Vieira, D. N.; Lopez-Rivadulla, M. 

1881 Hexanal, Development of headspace SPME w/ on-fiber derivatization 65µm PDMS-DVB GC-MS 

heptanal for determination of hexanal and heptanal in human blood 8min @ 60°C 

in blood J Chromatogr, B: 813, #1-2, 47-52 PFBHA derivatives 

Deng, C. H.; Li, N.; Zhang, X. M.* headspace 

1882 Methyl tert- Identification and elimination of polysiloxane curing agent headspace GC-MS 

butyl ether interference encountered in the quantification of lowin 

blood picogram per milliliter methyl tert-butyl ether in blood by 

SPME headspace analysis 

Anal. Chem, 77,#9, 2912-29-19. 

Blount, Benjamin C.; Chambers, David M.; Hughes, T.; 

Mauldin, J.; McElprang, David 

1883 Ephedrine SPME coupled w/ ion mobility spectrometry for the immersion sampling IMS 

in urine analysis of ephedrine in urine 

J. Sep. Sci.28. #7,612-618 

Lokhnauth, John K.; Snow, Nicholas H. 





1884 Ehtanol in Determination of ethanol in human blood and urine by headspace GC 

biological automated headspace SPME and capillary GC 

fluids Anal. Chim. Acta, 522, #2, 163-168 

De Martinis, B.; Martins R., Maria A.; Santos M., Carmen C. 

1885 Aldehydes in A simple, rapid and sensitive method for determination PFBHA derivative GC-MS 

blood aldehydes in human blood by GC-MS and SPME headspace 

with on-fibre derivatization. 

Rapid Communications in Mass Spect, 18, #15, 1715-1720 

Deng, C. H.; Zhang, X. M.* 

1886 Acetone in Determination of acetone in human breath by GC-MS 65µm PDMS-DVB GC-MS 

human breath and SPME with on-fiber derivatization PFBHA derivative 

& plasms J. Chromatogr. B , 810, #2, 269-275 4 min extract 

Deng, Ci; Yu, X; Zhang, J; Zhang, W Zhang, X agitated 

1887 Breath marker Impact of inspired substance concentrations on the results headspace GC-MS 

in blood & of breath analysis in mechanically ventilated patients 

breath Biomarkers, 10, #2-3, 138-152 

Schubert, J.; Miekisch, W.; Birken, T.; Geiger, K.; 

Noelge-Schomburg, G 

1888 Flavins Capillary LC determination of cellular flavins in-tube silica-ODS LC-MS 

J. Chromatogr. A, 1053, #1-2, 71-78 

Jia, Li; Tanaka, Nobuo; Terabe, Shigeru 

1889 Protein Study of ligand-receptor binding using SPME: Investigation restricted access LC-MS 

binders of receptor, free, and total ligand concentrations molecularly imprinted 

J of Proteome Res, 4, #3, 789-800 immobilized antibodies 

Musteata, Florin Marcel; Pawliszyn, Janusz 

1890 Sterols in Determination of sterols in biological samples by SPME BSTFA derivative GC-FID 

serum with on-fiber derivatization and GC/FID headspace 

samples Anal. Bioanal. Chem., 381, #8, 1576-1583 

Domeno, Celia; Nerin, Cristina; Ruiz, Barbara 

1891 Basic drugs Poly (methacrylic acid-ethylene glycol dimethacrylate) polymethacrylate HPLC-UV 

in serum monlithic capillary for intube SPME coupled to HPLC and its coated tube 

application to determination of basic drugs in human serum 

Anal. Chim. Acta, 523, #2. 251-258 

Da, Shi-Lu; Fan, Yi; Feng, Yu-Qi; Shi, Zhi-Guo 

1892 Volatiles from Analysis of Rhioxma Curcumae Aeruginosae volatiles by headspace GC-MS 

Chinese SPME w/GC-MS 

medicine Zeitschrift fuer Naturforschung Section C J of Biosciences 

59, #7-8, 533-537 

Sha, Yuri F.; Shen, Shun; Duan, Geng L. 

1893 BTEX in Analytical method for evaluation of exposure to benzene, headspace GC 

blood toluene, xylene in blood by GC preceded by SPME 

J Chromatogr B, 809, #1, 183-187 

Alegretti, Ana Paula; Thiesen, Flavia V.; Maciel, Gisele 

1894 1,2,3,4- Chronic toxicity and body residues of the nonpolar narcotic headspace GC 

tetrachloro- 1,2,3,4-tetrachlorobenzene in Chironomus riparius 

bezene in Env Toxicology and Chem, 23, #8, 2022-2028 

body residue Leslie, Heather A.; Kraak, Michiel; Hermens, Joop L. 

1895 Chlorobenzene Baseline toxicity of a chlorobenzene mixture and total body headspace GC 

in body residues measured and estimated with SPME 

residue Env Toxicology and Chemistry, 23, #8, 2017-2021 

Leslie, Heather A.; Hermens, Joop L. M.; Kraak, Michiel H. S. 

1896 Chlorinated Use of SPME followed by on-column silylation for determining 85µm polyacrylate GC-MS-SIM 

bisphenol A chlorinated bisphenol A in human plasma by GC-MS BSTFA derivative 

in plasma J Chromatogra, B, 817, #2, 167-172 

Del Olmo, M.; Gonzalez-Casado, A.; Suarez, B.; Taoufiki, J. 

Vilchez, J.L.; Zafra, A. 


Toxicology 




639 Drugs Microextraction of drugs 

J. Chromatogr.,A, 922(2000) 17-63 

Lord, H., Pawliszyn, J. 

review article 

912 Drugs High-temperature SPME procedure for the detection of 85µm polyacrylate GC-MS 

drugs by GC-MS 10min @200°C 

J. Chromatogr. B (2000) 745(2), 399-411 headspace 

Staerk, U., Külpmann, W. acetic anhydride-pyridine 

640 Drugs Solid phase microextraction in biomedical analysis review article 

in body fluids J. Chromatogr.,A, 902(2000) 167-194 

S. Ulrich 

641 Volatile, Headspace SPME procedures for gas chromatographic review article GC 

semivolatiles analysis of biological fluids and materials. 

in biological fluids J. Chromatogr.,A, 902(2000) 267-287 

Mills, G., Walker, V. 

847 Volatile, Headspace SPME profiles of volatile compounds in urine: 75µm Carboxen/PDMS GC-MS 

in urine Application to metabolic investigations 

J. Chromatogr.,B 753(2001) 259-268 headspace 

Mills, G., Walker, V. pH 9 

642 Hydrocarbon mixture Accessing the aquatic toxicity of complex hydrocarbons 

in water mixtures using SPME 

Toxicol. Lett. 2000, 112-1113, 273-282 

Parkerton, T, Sone, M., Letiski, D. 

643 Methadone SPME in the determination of methadone in human 100µm PDMS 

in saliva saliva by GC-MS 

J. Anal Toxicol (2000), 24(2), 93-96 

Dos Santos Lucas, A., Bermejo, A., 

Fernandez, P., Tabernero, M 

30 min 

29 Methadone Gas Chromatographic Analysis of Methadone in Urine Samples 100µm PDMS GC-MS 

in urine after Solid Phase Microextraction 15 min 

J. Microcolumn Sep. 6: 577-581 (1994) immersion 

Chiarotti, M., Marsili, R. pH 7.7 

644 Methadone, EDDP Use of SPME for the determination of methadone and 100µm PDMS GC-MS 

in human hair EDDP in human hair by GC-MS 

Forensic Sci. Int (2000) 107(1-3), 225-232 

Luca, A., Bermejo, A., Tabernero, M., Fernadez, P., 

Strano-Rossi, S. 

30 min, immersed 

563 Methadone, EDDP Use of SPME for the determination of Methadone and 100µm PDMS GC-MS 

in plasma its main metabolite, EDDP, in plasma by GC-MS 30 min immersion 

J. Anal. Toxicol. 24, 66-69 (2000) 

Bermejo, A., Seara, R., dos Santos Lucas, A., 

Tabernero, M., Fernandez, P., Marsili, R. 

1:4 delution @ pH 9 

474 Anorectics SPME and GC analysis of anorectic compounds in GC-MS 

in urine human urine 

J.Microcolumn Sep. 1997, ((4), 249-252 

Chiarotti, M. Strano-Rossi, S., Marsili, R. 

645 Tetramine Rapid detection of tetramethylenedisulfotertramine 100µm PDMS GC-FPD 

in blood in human blood by SPME-GC 

Anal. Chim. Acta (2000), 404(2), 329-334 

Luan, T., Li, G., Zhao, M., Zhang, Z. 





930 Anesthetics SPME-GC-MS method for the determination of 50:30µm DVB/Carboxen/ GC-MS 

in urine inhalation anesthetics in urine PDMS 

J. Chromatogr. B (1999), 732(1) 115-125 20min headspace 

Poli, D., Bergamaschi, E., Maini, P., Andreoli, R., Mutti, A. 10% NaCl 

65 Anesthetics Detection of Ten Local Anesthetics in Human Blood Using 100µm PDMS GC-FID 

in human blood Solid Phase Microextraction and Gas Chromatography 100°C, 40 min 

Jpn. J. Forensic Toxicol. 13 (2): 182-188 (1995) headspace 

Kumazawa, T., Lee, X., Sato, K., Seno, H., Ishii, A., Suzuki, D. perchloric acid added 

144 Anesthetics Extraction of Local Anesthetics from Human Blood 100µm PDMS GC-FID 

in blood by Direct Immersion-SPME 40 min 

Chromatographia 43: 59-62 (1996) immersion 

Kumazawa, T., Sato, K., Seno, H., Ishii, A., Suzuki, O. stirring 

salt added 

342 Anesthetics Simple Analysis of Local Anesthetics in Human Blood Using 100µm PDMS GC-MS 

in human blood Headspace SPME and GC-MS-Electron Impact Ionization 120°C, 45 min 

Selected Ion Monitoring headspace 

J. Chromatog. B, 709 (1998), 225-232 

Watanabe, T., Namera, A., Yaskiki, M., Iwasaki, Y., Kojima, T. 

NaOH added 

475 Nereistoxin in Simple and Sensitive Analysis of Nereistoxin and its 65µm DVB/PDMS GC-MS 

human serum Metabolites in Human Serum using Headspace 30 min @ 70°C 

SPME-GC-MS NaCl added, 

J. Chromatographic Science 37(3):77-82(1999) 

Namera,A., Watabe,T., Yashiki,Y., Kojima,T., Urabe,T. 

headspace 

419 Lidocaine Direct SPME Combined with Gas and Liquid Chromatography GC, HPLC 

in urine for the Determination of Lidocaine in Human Urine 

Chromatographia (1998), 47(11/12), 678-684 

Koster, E., Hofman, N., DeJong, G . 

646 Lidocaine Determination of lidocaine in plasma by direct SPME 65µm PDMS/DVB GC 

in plasma combined with GC 10 min 

J. Chromatogr., B. Biomed Sci. Appl (2000), 739(1), 175-182 immersed 

Koster, E., Wemes, C., Morsink, J., deJong, G. salt added 

647 Lidocaine Evaluation of SPME in combination with GC as a tool Carbowax-DVB GC-NPD 

in plasma for quantitative bioanalysis 

J. Microcolumn Sep. 2000, 12(5), 308-315 

Abdel-Rehim, M., Bielenstein, M, Arvidsson, T. 

pH 9 

420 Organochlorine Determination of Persistent Organochlorine Compounds in GC-ECD 

compounds Blood by SPME Extraction and GC-ECD 

in blood Fresenius' J. Anal. Chem. (1998), 361(2), 192-196 

Roehrig, L., Puettmann, M., Meisch, H. 

141 Chloroethers Determination of Chloroethenes in Environmental Biological 

in biological samples Samples Using GC Coupled with SPME 

Chromatographia 42(5/6): 313-17 (1996) 

Xu, N., Vandegrift, S., Sewe, G. 

67 Solvent thinners Simple Analysis of 5 Thinner Components in Human-Body 100µm PDMS GC-FID 

in urine, blood Fluids by Headspace SPME 

J. Legal Medicine 107: 310-313 (1995) 

80°C, 5 min 

Lee, X., Kumazawa, T., Sato, K. headspace 

877 Solvent thinners Improved extraction of thinner components from human 65µm Carboxen/PDMS 

in urine, blood body fluids by headspace SPME with a Carboxen/PDMS 

coated fiber 

Leg. Med. 1(1999) 231-237 

Lee, X., Kumazawa, T., Kondo, K., Furuta, S., Sato, K. 





648 Volatile organics Determination of volatile organic compounds in blood 100µm PDMS GC-FID 

in blood by headspace SPME-GC 

Weosjemg Uamkoi 2000, 29(1), 37-39 

Hao, S., Kang, J., Zhou, S, Cui, J., Qi, Q., Han, K. 

10 min 

649 Volatile organics The use of SPME in conjunction with benchtop quadropole MS 100µm PDMS GC-MS 

in blood for the analysis of volatile organic compounds in human 

blood at low ppt. Levels 


Cardinali, F., Ashley, D., Wooten, J., McCraw, J., Lemire, S. 

10 min, headspace 

795 Benzene Urinary benzene as a biomarker of exposure among GC-MS 

in urine occupationally exposed and unexposed subjects. 

Carcinogenesis (Oxford) (2001) 22(2), 279-286 

Rappaport, S; Bechtold, W; Dosemeci, M; Fustinoni, S 

Guilan, Li; Hayes, R 

914 PAHs Determination of PAHs in human blood seum by proteolytic 

in blood serum digestion-direct immersion SPME 

Analytica Chimica Acta (1999) 396(2-3) 303-308 

Poon, K., Lam, P., Lam, M. 

887 PAHs Quantification of the PAH (Polycyclic Aromatic hydrocarbons) 

metabolites as a biomarker for PAH exposure. 

Abstracts of Papers ACS (2001) 221(1-2) ANYL117 

Walcott, C; Smith, C; Patterson, D; Maggio, V; 

Huang, W; Grainger, J 

146 HydrocarbonsC9-C20 Analysis of Inflammable Substances in Blood Using 100µm PDMS GC-MS 

blood Head Space-SPME and Chemical Ionization and 10min.@90C 

in blood Chemical Ionization Selected Ion Monitoring 

Jpn. J. Forensic Toxicol. 13 (2): 189-194 (1995) NaOH added 

Iwasaki, Y., Yahiki, M., Nagsawa, N., Kojima, T., Miyazaki, T. headspace 

476 Flammables Analysis Method of Flammables in Blood by 100µm PDMS GC-MS 

blood, urine using headspace- SPME and Chemical 10 min @ 90°C 

ionized MS Detection 

Jpn. J. Legal. Med (49 Append): 80(1995) 

Iwasaki,Y., Yashiki,M., Nagasawa,N., 

Miyazaki,T., Kojima,T 

headspace 

195 Cresol, phenols Detection of Cresol Isomers and Phenol in Human Whole Blood 85µm polyacrylate GC-FID 

in human blood by Headspace SPME and Capillary GC 30 min @ 100°C 

Jpn. J. Forensic Toxicol. 15 (1): 21-28 (1996) NaCl added 

Lee, X., Kumazawa, T., Furuta, S., Kurosawa, T., Akiya, K., 

Skiya, I., Sato, K. 

headspace 

420 Chlorophenols Application of SPME and GC-MS for the Determination 85um polyacrylate GC-MS 

in urine of Chlorophenols in Urine 50 min, immersed 

J. Chromatogr. B: Biomed. Sci. Appl. (1998), 707(1+2), 91-97 

Lee, M., Yeh, Y., Hsiang, W., Chen, C. 

pH 1 

583 4-Chlorophenol Total 4-chlorophenol determination in urine samples of 85µm polyacrylate GC-MS 

in urine subjects exposed to chlorobenzene, using SPME and GC-MS. 30 min 

J-High-Resolut-Chromatogr. Jul 1999; 22(7): 427-428 

Guidotti,-M; Ravaioli,-G; Vitali,-M 

salt added 

477 PCBs in Determination of PCBs in human blood serum by SPME GC-ECD 

human serum Cheosphere, 1999, 39(6), 905-912 

Poon, K., Lam, P., Lam, M. 





68 Valproic acid Solid Phase Microextraction for the Determination of the 100µm PDMS GC-FID 

in human plasma Free Concentration of Valproic Acid in Human Plasma 3 min 

by Capillary GC immersion 

J. Chromatogr. B 673: 299-305 (1995) 

Krogh, M., Johansen, K., Gonnesen, F., Rasmussen, K. 

pH 2 

69 Nicotine, cotinine Rapid Analysis of Nicotine and Cotinine in Urine 100µm PDMS GC-MS 

in urine Using Head Space Solid Phase Microextraction 80°C, 5 min 

and Selected Ion Monitoring 

Jpn. J. Forensic Toxicol. 13 (1): 17-24 (1995) 

Yashiki, N., Magasawa, T., Kojima, T., Miyazaki, T., Iwasaki, Y. 

headspace 

478 Cartap Simple Analysis of Cartap and Its Metabolites Using Solid 65µm DVB/PDMS GC-MS 

in human serum Phase Microextraction and GC/MS 30 min @ 70°C 

Jpn. J. Forensic Toxicol. 16(2):142-143(1998) 

Namera,A., Watanabe,T., Yashiki,M., Iwasaki,Y., Kojima,T. 

immersed, NaOH added 

479 Nicotine, cotinine Analysis of Nicotine and Cotinine in biological fluid 100µm PDMS GC-MS 

in urine sample by SPME 80°C, 5 min 

Jpn. J. Legal. Med (49 Append): 80(1995) 

Iwasaki,Y., Yashiki,M., Nagasawa,N., Miyazaki,T., Kojima,T. 

headspace 

480 Stimulants Analysis of Stimulants and Narcotics 100µm PDMS GC-NPD 

in blood & urine Bunseki 10:816-822(1995) 20 min @100°C 

Yashiki,M., Kojima,T. 3pH, (NH4)2SO4,NaCl 

headspace 

918 Stimulants Determination of stimulants in human urine and hair samples polypyrrole capillary LC-MS 

urine, hair samples by polypyrrole coated capillary in-tube SPME coupled w/ LC-MS 

Talanta 2001, 54(4) 655-672 

Wu, J., Lord, H., Pawliszyn, J. 

650 Fenfluramine, Simple and simultaneous analysis of fenfluramine, GC-MS 

amphetamine, amphetamine, and methamphetamine in whole 15 min, headspace 

methamphetamine blood by GC-MS after headspace SPME and derivatization 

in blood Forensic Sci. Int. 2000, 109(3), 215-223 

Namera, A., Yahiki, M., Liu, M., Okajima, K., Hara, K., 

Imamura, T., Kojima, T. 

808 Amphetamine, Highly sensitive analysis of methamphetamine and GC-MS 

methamphetamine amphetamine in human whole blood using headspace GC-MS 30 min @ 90°C EI-SIM 

in blood Forensic Sci. Int. 2000, 116(1), 15-22 

Namera, A., Kojima, T, Okajima, K., Tskue, I., Yashiki, M. 

headspace 

842 4-(4-methoxybenzyl) Synthesis of 4-methyl-5-arylpyrimidines and GC-MS 

pyrimidine 4-arylpyrimidines: route specific markers for the Leuckardt 

in tablets preparation of amphetamine, 4-methoxyamphetamine and 

4-methylthioamphetamine. 

Forensic Sci Intl (2001) 115(1-2) 53-67 

Kirkbride, K.; Ward, A; Jenkins, N..; Klass, G.; Coumbaros, J. 

headspace 

866 Impurities Application of solid-phase microextraction to the profiling of 

from drug an illicit drug: Manufacturing impurities in illicit 

4-methoxyamphetamine 

J.Forensic Sciences (1999 )44(6), 1237-1242 

Kirkbride, K. Paul; Coumbaros, John C.; Klass, Gunter 

481 Amphetamines, SPME/Capillary GC for the profiling of confiscated 65µm DVB/PDMS GC-NPD 

ecstasy in ecstasy and amphetamine headspace/immersed 

powder & tablets Chromatographia, (1999) 50 (3/4), 247-252 0.1M acetate buffer 

Kongshaug, K., Pedersen-Bjergard, S., Krogh,M., 

Rasmussen, K 

pH 5 





482 Ecstasy and Automated determination of ecstasy and amphetamines 100µm PDMS GC-NPD 

amphetamines in urine by SPME and capillary GC after 16 min, immersed or MS 

in urine polylchloroformate derivatization. 

J. Pharm. Bomed. Anal. (1999), 19(3+4), 463-475 

Ugland, H., Kogh, M., Rasmussen, K. 

pH10 

927 Amphetamine, Determination of amphetamine, methamphetamine and 100µm PDMS GC-MS 

methamphetamine dimethamphetamine in human urine by SPME-GC-MS 30 min, immersed 

dimethamphetamine J. chromatogr. B (1998), 716(1-2) 359-365 pH 12.4 KOH, NaCl added 

in urine Myung, S., Min, H., Kim, S., Kim, M., Cho, J., Kim, T. stirred 

562 Amphetamines Rapid analysis of amphetamine, methamphetamine, 100µm PDMS GC-MS 

in urine MDA, and MDMA in urine using SPME, direct On-Fiber 10 min @ 100°C 

derivatization, and analysis by GC-MS headspace, 2N NaOH 

J. Anal. Toxicol. 24, 11-16 (2000) 20 min @ 60°C on fiber 

Jurado, C., Gimenez, M., Soriano, T., 

Menedez, M., Repetto, M. 

trifluoroacetic anhydride 

483 Amphetamines Rapid Analysis Amphetamines in Blood Using SPME 100µm PDMS GC-MS 

in urine & blood 20th Japan Biomedical Mass Spectrometry:127-130(1995) 5 min @ 80°C 

Yashiki,M., Kojima,T. immersed, NaOH added 

484 Amphetamines Detection of Amphetamines and Inflammable Compounds in 100µm PDMS GC-MS 

in urine & blood Biological Materials Using GC/MS and SPME 5 min @ 80°C 

Jpn. J. Forensic Toxicol. 12(2):120-121(1994) 

Yashiki, M., Kojima,T., Miyazaki,T. 


188 Amphetamines Quantitative and Qualitative Analysis of MDMA, MDEA, MA, 100µm PDMS GC-MS 

in urine and Amphetamine in Urine by Headspace/SPME and GC/MS 5 min @ 90°C 

Forensic Sci. Intl. 83 (3): 161-166 (1996) 

Centini, F., Masti, A., Comparini, I. 

headspace 

70 Amphetamines Detection of Amphetamines in Urine Using Head Space 100µm PDMS GC-FID 

in urine SPME and Chemical Ionization Selected Ion Monitoring 5 min 

Forensic Sci Intl., 76(2), 169-177 (1995) 80°C 

Yashiki, M., Kojima, T., Miyazaki, T., 

Nagasawa, N., Iwasaki, Y., Hara, K. 

stirring 

173 Amphetamines Rapid Analysis of Amphetamines in Blood Using Headspace 100µm PDMS GC-SIM-MS 

in blood SPME and Selected-Ion Monitoring 5 min @ 80°C 

Forensic Sci. Intl. 78 (2): 95-102 (1996) heptafluorobutyr- amide 

Nagasawa, N., Yashiki, M., Iwasaki, Y., Hara, K., Kojima, T. derivative 

327 Amphetamines Method Optimization for the Analysis of Amphetamines in 100µm PDMS GC-FID 

in urine Urine by SPME 15-60 min 

Anal. Chem. 69 (19): 3899-3906 (1997) headspace 

Lord, H., Pawliszyn, J. stirring 

192 Amphetamines Simple Clean-up of Methamphetamine and Amphetamine in 100µm PDMS GC-NPD 

in urine Human Urine by Direct-Immersion SPME 30 min @ 65°C 

Jpn. J. Forensic Toxicol. 14 (3): 228-232 (1996) Na2CO3 added 

Ishii, A., Seno, H., Kumazawa, T., Suzuki, O., 

Nishikawa, M., Watanabe, K., Hattori, H. 

immersed 

145 Amphetamines Application of SPME Technique for the Detection of Urinar GC 

in urine Methamphetamine and Amphetamine by GC 

J. Can. Soc. Forensic Sci. 29(2): 43-48, (1996) 

Ameno, K., Fuke, C., Ameno, S., Kinoshita, H., Ijirei, I. 

421 Amphetamines, Determination of Amphetamine and Methamphetamine in Human Hair 100µm PDMS GC-NPD 

methamphetamine by Headspace SPME and GC-NPD 15 min @45°C 

in hair J. Chromatogr. B: Biomed. Sci. Appl. (1998), 707(1+2) 99-104 

Koide, I., Noguchi, O., Okada, K., Yokoyama, A., Oda, H., 

Yamamoto, S., Kataoka, H. 






194 Methamphetamine, Rapid Analysis of Methamphetamine and Cocaine in the 100µm PDMS GC-FTD 

cocaine Urine of Drug Abusers with SPME 15 min 

in urine Chromatography 18 (3): 185-188 (1996) immersion 

Makino, Y., Takgi, T., Ohta, S., Hirobe, M. pH 10.5 

198 Amphetamines Screening Procedure for 21 Amphetamine-Related 100µm PDMS GC-MS 

in urine Compounds in Urine Using SPME and 80°C, 10 min 

Gas Chromatography-Mass Spectrometry headspace 


Battu, C., Marquet, P., Fauconnet, A., Lacassie, E., 

Lachatre, G. 

salt added 

566 Amphetamines in Automated drug analysis by in-tube SPME-LC-MS 60cm x 0.25mm ID tube LC-MS 

urine Chromatography. Jun 1999; 20(2): 142-145 

Kataoka,-H; Lord,-HL; Pawliszyn,-J 

Omegawax 250 electrospray 

651 Amphetamines Simple and rapid determination of amphetamine, In-tube Omegawax 250 LC-MS 

in urine methamphetamine and their methylenedioxyl derivatives in 

urine by automated in-tube SPME coupled with LC-electrospray 

ionization mass spectrometry 

J. Anal. Toxicol (2000), 24(4), 257-265 


60cmx0.25mmi.d.x0.25µm electrospray 

652 Amphetamines Determination of amphetamine and methamphetamine PDMS GC-MS 

methamphetamine in serum via headspace derivatization SPME-GC-MS 40 min, headspace 

in serum J. Chromatogr. A, 896, (2000) 265-273 pH 9.5 

Lee, M., Song, Y., Hwang, B., Chou, C. heptafluorobutyric 

anhydride ethyl acetate 

831 Amphetamines On-fiber derivatization for direct immersion SPME part I: 

acylation of amphetamine with pentafluorobenzoyl chloride 

J. Sep. Sci. (2001) 24(2), 116-122 

Koster, E; Bruins, C.; Wemes, C; De Jong, G. 

765 Beta blockers Determination of automated In-tube SPME-LC-MS In-tube Omegawax 250 LC-MS 

in urine, serum for drug analysis 

J.MIcroSeparation,(2000-9), 12(9), 493-500 


electrospray 

794 Beta blockers Determination of beta-blockers by HPLC w/SPME 85µm polyacrylate HPLC 

in urine, serum from urine and plasma samples 

Analytical Letters (2001) 34(1), 91-101 

Tanabe, S; Shimokawa, K; Matsuda, Y.,Katayama, M; 

Daimon, H,Hara. I; Kaneko, S; Sato, T. 

71 Amphetamines, alcohols Comparison of New Solid Phase Extraction Methods for 100µm PDMS, GC-FID 

in urine, serum Chromatographic Identification of Drugs in Clinical 85µm polyacrylate 

Toxicology Analysis 60°C, 15 min 

Degel, F., Weidemann, G. headspace 

485 Amphetamines in Some Problems of Detecting Amphetamines in Biological 100µm PDMS GC-MS 

biological fluids Materials by using Triage 5 min @ 80°C 

Pract. Forens. Med. 40:99-102 (1997) CaCO3 added 

Watanabe,T., Namera,A., Yashiki,M., Iwasaki,Y., Kojima,T. headspace 

234 Drug Summary Analysis of Drugs and Poisons in Legal Medicine Various fibers & 

J. Mass Spectrom. Soc. Jpn. 44: 321-333 (1996) 

Suzuki, O., Seno, H., Ishii, A. 

conditions 





79 Drugs of abuse Determination of Drugs of Abuse Using SPME (German) 100µm PDMS, GC-MS 

in urine Labor-Med. 18 (2): 112-118 (1995) 85µm polyacrylate 

Singer, K., Wenz, B., Seefeld, V., Speer, U. 40°C, 20 min 

immersion, stirring 

81 Cocaine Detection of Cocaine in Human Urine by SPME and Capillary 100µm PDMS GC-FPD 

in urine GC with Nitrogen-Phosphorus Detection 30 min 

Jpn. J. Forensic Toxicol. 13 (3): 207-210 (1995) immersion, stirring 

Kumazawa, T., Watanabe, K., Sato, K., Seno, H., 

Ishii, A., Suzuki, O. 

NaF added 

653 Volatiles SPME/GC-MS characterization of volatiles associated 30/50Carboxen/DVB/PDMS GC-MSD 

from cocaine, heroin with cocaine and heroin 85µm polyacrylate 

Am. Lab, Sept. 2000, 32-34 90 min 

Vu, D., Nicholas, P. Erikson, C. headspace 

486 Methyl Benzoate Field and Laboratory comparison of the sensitivity and GC-MS-MS 

on currency reliability of cocaine detection on currency using 

chemical sensors, humans, K-Os and SPME/GC/MS 

Proceeding SPIE-Int. Soc. Opt. Eng, 3576:41-46 (1999) 

Furton, K., Hsu, Y., Luo, T., Norelus, A., Rose, S. 

907 Daidzein, isoflavon Detection of the isoflavone aglycones genistein and daidzein LC-MS 

aglycones genistein in urine using SPME-HPLC-electrospray MS 

in urine J. Chromatogr. B (2001), 759(1) 33-41 

Satterfield, M., Black, D., Brodbelt, J. 

164 Barbiturates Determination of Barbiturates by SPME and Ion Trap GC-MS 65µm Carbowax/DVB GC-MS 

in water J. Chromatogr. A 777: 275-282 (1997) 20 min 

Hall, B., Brodbelt, J. immersion, stirring 

572 Benzoylecgonine Aqueous phase hexyl chloroformate derivatization and SPME 100µm PDMS GC-EMIS 

in urine determination of benzoylecgonine in urine by GC- 10 mi. @ 55°C 

Quadrapole ion trap mass spectrometry hexyl chloroformate 

J-Forensic-Sci. May 1999; 44(3): 527-534 

Hall,-BJ; Parikh,-AR; Brodbelt,-JS 

derivative 

224 Barbiturates Determination of Barbiturates by SPME and Capillary polyvinyl coated electrophoresis 

in urine and serum Electrophoresis metal rod 230nm 

Anal. Chem. 69: 1217-1222 (1997) 

Li, S., Weber, S. 

5, 10, 30 min 

80 Meperidine Detection of Meperidine (Pethidine) in Human Blood and Urine 100µm PDMS GC-FID 

596 Barbiturates Artificial receptor-facilitated SPME of barbiturates. PVC/steel rod CE 

in urine/serum Anal-Chem. 1 Jun 1999; 71(11): 2146-2151 5 min 

Li,-S; Sun,-LF; Chung,-Y; Weber,-SG immersed 

654 Meperidine Detection of Meperidine (Pheonthiazin) in human blood and 100°C, 30 min GC 

in urine and blood urine by Headspace SPME and Gas Chromatography headspace 


Seno, H., Kumazawa, T., Ishii, A., Nishikawa, M., 

Hattori, H., Suzuki, O. 

salt & NaOH added 

196 Phencyclidine in Simple Extraction of Phencyclidine from Human Body Fluids 100µm PDMS GC-surface 

blood and urine by Headspace SPME 90°C, 30 min ionization 

Chromatographia 43 (5-6): 331-333 (1996) 

Ishii, A., Kumazawa, T., Watanabe, K., Hattori, H., Suzuki, O. 

headspace detector 

487 Diphenylmethane Simple Analysis of Diphenylmethane Antihistaminics 100µm PDMS GC-FID 

blood and urine and their Analogous in bodily Fluids by headspace 10 min @ 98°C 

SPME capillary gas chromatography 

J. Chromatogr. Sci. 35:275-279(1997) 

Nishikawa,M., Seno,H., Ishii,A. Suzuki,O., 

Kumazawa,T., Watanabe,K., Hattori,H. 

10N NaOH 





179 Ethanol Blood Alcohol Determination with Automated SPME: 65µm Carbowax/DVB GC-FID 

in blood A Comparison with Static Headspace Sampling 3 min 

J. Can. Soc. Forens. Sci. 30(1): 7-12 (1997) headspace 

Penton, Z. salt & NaF added 

191 Ethanol in Detection of Ethanol in Human Body Fluids by Headspace 65µm Carbowax/DVB GC-MS 

blood, urine SPME/Capillary GC 70°C, 10 min 

Chromatographia 43 (7-8): 393-397 (1996) 

Kumazawa, T., Seno, H., Lee, X., Ishii, A., 

Suzuki, O., Sato, K. 

headspace, (NH4)2SO4 

418 Ethanol in Improved Extraction of Ethanol from Human Body Fluids Carboxen/PDMS 

blood, urine by Headspace SPME with a Carboxen/PDMS Fiber 

Chromatographia (1998), 47(9/10), 593-595 

Lee, Z., Kumazawa, T., Sato, K., Seno, H., Ishii, A., 

Suzuki, O. 

206 Antihistamine drugs Simple Analysis of Diphenylmethane Antihistamines 100µm PDMS GC-FID 

in blood, urine and Their Analogue in Bodily Fluids by Headspace 90°C, 10 min 

SPME-Capillary Gas Chromatography 

J. Chromatogr. Sci. 35 (6): 275-279 

Nishikawa, M., Seno, H., Ishii, A., Suzuki, O., 

Kumazawa, T., Watanabe, K., Hattori, H. 

headspace 

64 Tricyclic Simple Extraction of Tricyclic Antidepressants in Human Urine 100µm PDMS GC-FID 

antidepressants by Headspace SPME 100°C, 15 min 

in urine Jpn. J. Forensic Toxicol. 13 (1): 25-30 (1995) headspace 

Kumazawa, T., Lee, X., Tsai, M., Seno, H., Ishii, A., Sato, K. stirring 

95 Tricyclic Detection of Tricyclic Antidepressants in Whole Blood by 100µm PDMS GC-FID 

antidepressants Headspace SPME-Capillary GC 100°C, 60 min 

in blood J. Chrom. Sci. 35: 302-308 (1997) headspace 

Lee, X., Kumazawa, T., Sato, K. NaOH added 

488 Tricyclic Analysis of Tricyclic Antidepressant and that application 100µm PDMS GC-MS 

antidepressants for fatal intoxication by Headspace SPME 45 min @ 120°C 

in urine, blood Jpn. J. Legal. Med. 52:69(1998) 

Watanabe,T., Namera,A., Yashiki,M., Iwasaki,Y., Kojima,T. 

headspace, NaOH 

352 Tetracyclic Simple Analysis of Tetracyclic Antidepressants in Blood 100µm PDMS GC-MS 

antidepressants Using Headspace SPME and GC-MS 120°C, 45 min 

in blood J. Anal. Toxicology, Vol. 22 (5), 1998, 396-400 headspace 

Namera, A., Watanabe, T., Yahiki, M., Iwasaki, Y., Kojima, T. NaOH added 

655 Antidepressant Direct coupling of microcolumn liquid chromatography In-tube HPLC 

in urine with in-tube SPME for the analysis of antidepressant drugs 

Analyst (Cambridge UK) 2000, 125(5), 807-809 

Saito, Y., Kawazoe, M, Jinno, K., Nayhashida, M. 

227 Diazepam Solvent-Modified Solid-Phase Microextraction for the 85µm polyacrylate GC-FID or FPD 

in serum Determination of Diazepam in Human Plasma Samples 4 min 

by Capillary Gas Chromatography immersion 

J. Chromatogr. B 689: 357-364 (1997) pH 5.5 

Krough, M., Grefslie, H., Rasmussen, K. 1-octanol added 

656 Amitriptyline SPME coupled with microcolumn LC for the analysis of HPLC 

in human urine amitriptyline in human urine 

Chromatographia, (2000 Sept.) 52(5-6) 309-313 

Jinno, K., Kawazoe, M., Hayashida, M. 





371 Benzophenone-3 Determination Benzophenone-3 and Metabolites in Water and 65µm Carbowax/DVB GC-MS 

in water and urine Human Urine by SPME and Quadrupole Ion Trap GC-MS 45 min 

Anal. Chimica Acta 371 (1998) 195-203 

Felix, T., Hall, B., Brodbelt, J. 

immersion 

871 Benzoylecgonine Aqueous phase hexylchloroformate derivatization and SPME 100µm PDMS GC-MS 

in urine Determination of benzoylecgonine in urine by GC 

quadrupole ion trap mass spectrometry. 

J Forensic Sci (1999) 44(3) 527-534 hexyl chloroformate 

Brodbelt, Jennifer S.; Hall, Brad J.; Parikh, Aashish R. derivative 

168 Antidepressants Solid Phase Microextraction with Capillary GLC and NDPD for 100µm PDMS GC-NDPD 

in blood the Assay of Antidepressant Drugs in Human Plasma 60 min 

J. Chromatogr. B 696: 217-234 (1997) 

Ulrich, S., Martens, J. 

immersion 

657 Phenothiazines Determination of Phenothiazines in human body fluids by 85µm Polyacrylate LC-MS 

urine, blood SPME and LC-tandem mass spectrometry 60 min @ 40°C 

J.Mass Spec. (2000-9) 35(9) 1091-1099 pH 8 

Seno, H., Kumazawa, T., Ishii, A., Hattori, H., 

Nishikawa, M., Watanabe, K., Suzuki, O. 

stirring 

142 Phenothiazines Detection of Some Phenothiazines by Headspace SPME 100µm PDMS GC-FID 

urine, blood and GC 40 min @ 140°C 

Jpn. J. Forensic Toxicol. 14: 30 (1996) headspace 

Kumazawa, T., Seno, H.,, Ishii, A., Hattori, H., Sato, K., 

Watanabe, K., Suzuki, O. 

NaCl added 

947 Propranolol In-Tube Molecularly Imprinted Polymer SPME for the selective 

Determination of Propranolol 

Anal. Chem (2001) 73(11) 2383-2389 

Mullett, Wayne M.; Martin, Paul; Pawliszyn, Janusz 

946 Carbofuran Application of (SPME) technique for the detection of 

in seum carbofuran in serum 

J. Can. Soc. Forensic Sci(2001) 34(1), 23-26 

Ameno, K.; Lee, S-K.; Ameno, S.; Kinoshita, H.; Kubota, T.; 

Zhang, X.; Ijiri, 

908 Dinitroaniline Headspace SPME and GC determination of dinitroaniline 100µm PDMS GC-ECD 

in blood, urine herbiciede s in human blood, urine and environmental water 30 min @ 70°C 

and water J. Chromatogr. B. (1998), 714(2), 205-213 headspace 

Guan, F., Watanabe, K., Ishii, A., Seno, H., Kumazawa, T., 

Hattori, H., Suzuki, O. 

NaSO4 

183 Herbicides SPME and GC-ECD Determination of Dinitroaniline Herbicides in 100µm PDMS GC-ECD 

in water and Surface Water and Biological Fluids 30 min @ 70°C water 

biological fluids Jpn. J. Forensic Toxicol. 15 (2): 151-153 (1997) @ 90°C blood 

Prosen, F., Watanabe, K., Ishii, A., Seno, H., Suzuki, O. Na2SO4, headspace 

860 Organochlorine & Gas chromatographic determination of organochlorine and GC/ECD/FPD 

organophosphorus organophosphorus pesticides in human fluids using SPME 

pesticides in Analytica Chimica Acta (2001) 433(2) 217-226 

biological fluids Hernandez, F.; Beltran, J.; Egea, S.; Lopez, F. J.; Pitarch, E. 

66 Organophosphate Detection of Organophosphate Pesticides in Human Body 100µm PDMS GC-NPD 

pesticides Fluids by Headspace SPME and Capillary GC with 100°C, 20 min 

in urine, blood Nitrogen-Phosphorus Detection 

Chromatogrphia 42(3/4): 135-140 (1996) 

Lee, X., Kumazawa, T., Taguchi, T., Sato, K., Suzuki, O. 

pH 3 with HCl 





875 Organophosphorus Optimisation of SPME conditions for headspace analysis 

pesticides in of organophophorus pesticides in whole blood 

whole blood Z Zagadnien Nauk Sadowych, 42(2000) 47-59 

Asri, K., Anderson, R. 

103 Malathion Rapid Analysis of Malathion in Blood Using Head Space 100µm PDMS GC-MS 

in blood Solid Phase Microextraction and Selected Ion Monitoring 90°C, 5 min 

Forensic Sci. Int. 88: 125-131 (1997) 

Namer, A., Yashiki, M., Nagasawa, N., Iwasaki, Y., 

Kojima, T. 

headspace 

489 Parathion Rapid analysis of parathion in biological samples using GC-MS 

in blood headspace SPME and GC-MS 

Clin. Chem. Lab. Med. 1999, 37(6), 639-642 

Musshoff, F., Junker, H., Madea, B 

headspace 

136 Carbamate in Determination of Some Carbamate Pesticides in Human Body 100µm PDMS GC-NPD 

urine, serum Fluids by Headspace SPME/GC 70°C, salt 


Seno, H., Kumazawa, T., Ishii, A., Nishif, M. 

headspace 

797 Amino pesticides Separation methods for amino group-possessing pesticides 100µm PDMS GC-FID, NPD 

in biological samples in biological samples. 30min @ 95°C, salt 

J Chromatogr B (2000) 747(1&2), 241-254 

Kumazawa, T; Suzuki, O. 

headspace 

490 Arylamide Herbicides Simple Analysis of Arylamide Herbicides in Serum using 100µm PDMS GC-MS 

in Serum Headspace SPME and GC-MS 45 min @ 90°C 

6th Indo Pacific Congress on Legal Medicine and 

Forensic Science. 770-773(1998) 

Namera,A., Watanabe,T., Yashiki,M., Iwasaki,Y., Kojima,T. 

headspace, NaCl 

107 Diazepams in Solid-Phase Microextraction/Liquid Chromatography (SPME/LC) 85µm polyacrylate HPLC-UV, 

biological fluids for Drug Analysis in Biological Fluids 

Chromatography (1997), 18(4), 244-245, 

Jinno, K 

30°C, 3 hr 200nm 

658 Drugs SPME of drugs from biological matrices review article 

in biological fluids J. Chromatogr. A 885(2000) 445-455 

Snow, N. 

234 Drugs in Analysis of Drugs and Poisons in Legal Medicine 100µm PDMS & GC-MS 

biological fluids J. Mass Spectrom. Soc. Jpn. 44: 321-333 (1996) 85µm polyacrylate 

Suzuki, O., Seno, H., Ishii, A. headspace 

NaCl, Na2SO4, 

108 Volatiles Confirmation of Volatiles by SPME and GC-MS in the 85µm polyacrylate GC-MS 

in urine Investigation of Two Traffic Fatalities 60°C, 10 min 

J. Anal. Toxicol. 1997, 21(4), 286-290 

Brewer, W., Galipo, R., Morgan, S., Habben, K. 

headspace 

564 Tetarchoroethylene Tetrachloroethylene and trichloroethylene fatality: 100µm PDMS GC-ECD 

trichloroethylene in case report and simple headspace SPME-capillary 1 min headspace 

tissue, urine, serum GC determination in Tissues 

J. Anal.Toxicol, 24 (1), 22-26, (2000) 

Dehon, B., Humbert, L., Devisme, L., Stievenart, M., Mathieu, D. 

Houdret, N., Lhermitte, M. 

60°C 

113 Estrogen, steroids in Analysis of Steroids from Human Serum by SPME with 85µm polyacrylate GC-MS 

water/biological fluids Headspace Derivatization & GC 30 min 

J. High Res. Chromatogr. 20: 171-173 (1997) immersion, stirring 

Okeyo, P., Rentz, S., Snow, N. BSTFA derivative 





373 Estrogen, steroids in Analysis of Estrogens and Anabolic Steroids by SPME with 85µm polyacrylate GC-MS 

water/biological fluids On-Fiber Derivatization and GC-MS 30 min 

J. Microcolumn Separations, 10(7) 551-556 (1998) immersion, stirring 

Okeyo, P., Snow, N. BSTFA derivative 

404 Estrogen, steroids in On-Fiber Derivatization for Analysis of Steroids by SPME-GC-MS 60µm Carbowax/DVB GC-MS 

water/biological fluids Book chapter 60°C, 30 min 

Snow, N. immersion 

stirring 

BSTFA derivative 

200 Ethanol, acetone, Solid Phase Microextraction for the Analysis of Human Breath 100µm PDMS GC-MS 

isoprene in Anal. Chem. 69 (4): 587-596 (1997) 10-60 sec 

human breath Grote, C., Pawliszyn, J. headspace 

659 Isoprene Determination of isoprene in human expired breath using Carboxen/PDMS GC-MS 

in human breath SPME with GC-MS 10 min @ 40°C from 

J. Chromatogr, B. Biomed Appl. 739(1), 183-190 

Hyspler, R, Crhova, S. Gasparic, J., Cizkova, M., 

Balasova, V., Zadak, Z. 

tedlar bag sample 

322 Chloroethenes Determination of Chloroethenes in Environmental Biological 

in biological fluids Samples Using GC Coupled with SPME 

Chromatographia 42 (5/6): 313-317 (1996) 

Xu, N., Vadegrifts, S., Sewell 

660 Halothane Rapid analysis of halothane in biological samples GC-MS 

in biological samples using headspace SPME and GC-MS - 

a case of double homicide 

J. Anal. Toxicol. (2000), 24(5), 372-376 

Musshoff, G., Junker, H., Madea, B. 

867 4-Heptanone Urine 4-heptanone: A beta-oxidation product of GC-MS 

in urine 2-ethylhexanoic acid from plasticisers 

Clinica Chimica Acta (2001) 306(1-2) 51-61 

Walker, Valerie; Mills, Graham A 

491 Clozapine in SPME for the assay of clozapine in human plasma 100µm PDMS 

human plasma Fresenius' J. Anal. Chem, 1999, 364(7), 654-655 30 min 

Kruggel, S., Ulrich, S. pH adj. NaOH 

843 Levomepromazine SPME for the assay of levomepromazine in human plasma 100µm PDMS GC-NPD 

in human plasma Therapeutic Drug Monitoring (2000) 22(6), 723-728 30 min @30°c 

Kruggel, S., Ulrich, S. chloramitriptyline added 

0. 1 M -NaOH 

575 Homocysteine in Determination of homocysteine and its related compounds 85µm polyacrylate GC-MS 

plasma/water by SPME-gas chromatography-mass spectrometry. 30 min immersed 

J-Chromatogr,-B:-Biomed-Appl. 30 Apr 1999; 727(1-2): 1-8 

Myung,-S-W; Kim,-M-S; Min,-H-K; Yoo,-E-A; Kim,-K-R 

pH 3 

906 Ranitidine Automated in-tube SPME-LC-electrospray ionization mass 

spectrometry for the determination of ranitidine. 

J. Chromatogr.B (1999), 731(2), 353-359 

Kataoka, H., Lord, H., Pawliszyn, J. 

LC-MS 

949 g-Hydroxybutyrate Determination of gamma-hydroxybutyrate in water and GC-MS 

in human urine human urine by SPME-GC/quadrupole iontrap MS 

and water J. Forensic Sci (2001), 46(3), 688-693 

Blair, S.; Song, M.; Hall, B.; Brodbelt, J. 





869 g-Hydroxybutyrate Simple extraction of gamma-hydroxybutyrate in human whole 

in human whole blood by headspace solid-phase microextraction 

blood Jpn. J. Forensic Toxicol (2001) 19(1) 38-45 

Kurihara, R; Ishii, A; Watanabe-Suzuki, K; Kumazawa, T; 

Seno, H; Suzuki, O; Katsumata, Y 

405 g-Hydroxybutyric Determination of gamma-Hydroxybutyric Acid (GHB) in 50µm Carbowax/TPR100 GC-PICI-MS 

acid in Plasma and Urine by Headspace SPME and GC-Positive 70°C, 15 min 

plasma, urine Ion Chemical Ionization MS headspace 

Rapid Commun. Mass Spec(2000) 14(24), 2401-2407 pH 6-7 

Frison, G; Tedeschi, L; Maietti, S; Ferrara, Santo D 

323 1-Phenylethylamine Simple Extraction of 1-Phenylethylamine in Human Urine 65µm PDMS/DVB GC-NPD 

in urine by Headspace SPME 30 min @ 90°C 

Jpn. J. Forensic Toxicol. 15(3): 189-193 (1997) 10M NaOH, K2CO3 

Ishii, A., Seno, H., Prosen, F., Watanabee, K., 

Kumanzawa, T., Hattori, H., Suzuki, O. 

headspace 

324 Benzodiazepines Detection of Benzodiazepines in Human Urine by 65µm PDMS/DVB GC-FID 

in urine Direct Immersion SPME-GC 


30 min 

Seno, H., Kumazawa, T., Ishii, A., 

Watanbe, K., Hattori, H., Suzuki, O. 

immersion 

325 Benzodiazepines Determination of Five Benzodiazepines in Aqueous 65µm Carbowax/DVB GC-FID, 

in water & urine Solution and Biological Fluids, Using SPME with 45°C, 60 min GC-MS 

Carbowax/DVB Fiber Coating stirring 

J. Microcolumn Sep. 10 (2): 193-201 (1998) 

Luo, Y., Pan, L., Pawliszyn, J. 

pH 7, salt added 

351 Benzophenones SPME and GC-ECD of Benzophenones for Detection of 100µm PDMS GC-ECD 

in urine Benzodiazepines in Urine 30 min 

J. Anal. Toxicology, Vol. 23, Jan/Feb 1999 , 54-61 immersion, stirring 

Prosen, F., Seno, H., Ishii, A., Watanabe, K., pH 9.4 

Kumazawa, T., Hattori, H., Suzuki, O. KOH added 

357 Benzodiazepines SPME-Microcolumn LC for the Analysis of Benzodiazepines Carbowax/TPR100 HPLC-UV 

in urine in Human Urine 60 min 220nm 

Analusis (1998), 26(5), M27-M30 

Jinno, K., Taniguchi, M., Hayashida, M. 

immersion 

779 Benzodiazepines Automated in-tube solid-phase microextraction coupled Supelco-Q capillary LC-ESI-MS 

in urine & serum with LC-electrospray ionization MS for the 

determination of selected benzodiazepines 

J. Anal. Toxicology, (2000) Vol. 24(8),718-725 

Yuan, H. ; Mester, Z.; Lord, H.; Pawliszyn, J. 

60cmx0.25mm I.d. 

326 SPME for Sample Preparation During Drug Metabolism Studies 

Pharmazie 53 (3): 172-177 (1998) 

Kroll, C., Borchert, H. 

328 Cyanide Analysis of Cyanide in Blood by Headspace SPME and Carbowax/DVB GC-NPD 

in blood Capillary GC 50°C, 45 min 

Chromatographia 47 (3/4): 209-214 (1998) headspace 

Takekawa, K., Oya, M., Kido, A., Suzuki, O. Na2SO4 added 

492 Lead in Determination of Lead in Blood and Urine by SPME-GC 

whole blood & Urine Anal. Chem. 1999, 71(15), 2998-3002 headspace 

Yu, X., Yuan, H., Gorecki, T., Pawliszyn, J. sodium tetraethyl 

borate derivative 





747 Lead in Speciation of Alkyllead and Inorganic lead by derivatization 100µm PDMS GC-MS 

whole blood & Urine with deuterium-labeled sodium tetraethylborate and 10 min, headspace 

SPME GC-MS sodium tetraethyl 

Anal. Chem. 2000, 72,1788-1792 

Yu, X, Pawliszyn, J. 

borate derivative 

416 Methylmercury Determination of Methylmercury in Biological Samples and 5cm fused silica fiber GC-AA 

in biological fluids Sediments by Capillary GC Coupled with Atomic Adsorption 90 min 

or sediment after hydride derivatization and SPME headspace 

J. Anal. At. Spectrom. (1998), 13(10), 1141-1144 

He, B., Jiang, G., Ni, Z. 

KBH4 derivative 

493 Alkalated Hg, Pb, Sn Simultaneous determination of Hg(III) and alkylated Hg, Pb, 100µm PDMS GC-MS-MS 

in urine and Sn species in human body fluids using SPME-GC-MS-MS 10 min 

Fresenius' J.. Anal. Chem. (1999), 363(5-6), 466-468 NaBEt4 derivatives 

Dunemann, L., Hajimiragha, H., Begerow, J. pH 5.3 

661 Organometallic Coupling of SPME and GC-AED for the determination of 

organometallic compounds 

Mikrochim Acta, (2000) 135 (No.1&2) 91-95 

Mothes, S, Wennrich, R. 

GC-AED 

329 Methanol Simple Extraction of Methanol in Human Whole Blood by Carboxen/PDMS GC-FID 

in blood Headspace SPME 60°C, 10 min 

Jpn. J. Forensic Toxicol. 16 (1): 64-68 (1998) headspace 

Lee, X., Kumazawa, T., Jurosawa, T., 

Akiya, K., Akiya, Y., Fruta, S., Sato, K. 

stirring 

330 Aromatic amines in Solid Phase Microextraction of Monocyclic Aromatic Amines 65µm PDMS/DVB GC-FID 

urine, blood, milk from Biological Fluid 45°C, 15 min 

Anal. Chem. 70 (9): 1986-1992 (1998) headspace, salt added 

DeBruin, L., Josephy, P., Pawliszyn, J. KOH added, pH >13 

494 Trimethylamineuria Quantitative determination of trimethylamine in urine by 

65µm Carboxen/PDMS, 100µm 

PDMS GC-MS 

in urine SPME-GC-MS 15 min @ 59°C 

J. Chromatogr. B: Biomed Sci. Appl., 1999, 723(1+2), 281-285 headspace 

Mills, G., Walke, V., Mughal, H. stirred 

950 Acrolein Determination of acrolein by headspace SPME-GC-MS 

in bioligical fluids J. Chromatogr., B: Biomed (2001), 758(1), 123-128 

Takamoto, S.; Sakura, N.; Yashiki, M.; Kojima, T. 

331 PAHs Fast Screening Method for the Profile Analysis of Polycyclic 85µm polyacrylate GC-MS 

in urine Aromatic Hydrocarbon Metabolites in Urine, Using 35°C, 45 min 

Derivatization-SPME stirring 

J. Chromatogr. G: Biomed. Sci. Appl. 705 (1): 132-138 (1998) 

Gmeiner, G., Krassnig, C., Schmid, E., Tausch, H. 

BSTFA derivative 

495 BTEX in SPME and GC-MS for determination of monoaromatic 75µm Carboxen/PDMS GC-MS 

in urine & blood hydrocarbons in blood and urine. Application to people 

exposed to air pollutants 

Chromatographia, 1999, 50(3/4), 167-172 

Andreoli, R., Manini, P. Bergamaschi, E., Brustolin, A., Mutti. A. 

headspace 

591 BTEX in Headspace solid-phase micro-extraction for the 100µm PDMS GC-EMIS 

urine determination of BTEX in urine. 15 min @ 30°C 

J-Chromatogr,-B:-Biomed-Appl. 19 Feb 1999; 723(1-2): 105-115 

Fustinoni,-S; Giampiccolo,-R; Pulvirenti,-S; Buratti,-M; Colombi,-A 

headspace 





662 Toluene The comparison of toluene determination between 100µm PDMS 

in blood headspace SPME and Headspace methods in glue 

sniffer's blood and urine samples 

J. Forensic Sci. (2000), 45(3), 702-707 

Kim, N., Park, S. 

496 Toluene, xylene Method for analyzing urinary toluene and xylene by SPME 100µm PDMS GC-FID 

in urine and its application to workers using organic solvents 5 min, 

Bull. Environ, Contam. Toxicol. (1999), 62(2), 109-116 

Asakawa, F., Jitsunari, F., Choi, J., Suna, S., Takeda, N., 

Kitamado, T. 

NaCl, stirring 

497 Toluene, benzene Biomonitoring of benzene and toluene in human blood by 65µm Carboxen/PDMS GC-MS 

in human blood headspace SPME 30 min @ 20°C 

Fresenius' J. Anal. Chem. (1999), 363(1)m 88-91 

Schimmiing, E., Levsen, K., Koehme, C., Schuermann, W. 

headspace 

332 Erythromycin A Study of Erythromycin A Decomposition Products in 65µm PDMS/DVB LC-MS 

in water Aqueous Solution by SPME-LC-MS 15 min 

Rapid Commun. Mass Spectrom. 10 (2): 225-234 (1998) immersed 

Volmer, D., Hui, J. 50% MeOH extr. 

333 Corticosteroids Rapid Determination of Corticosteroids in Urine by Combined LC-MS 

in urine SPME-LC-MS 

Rapid Commun. Mass Spectrom. 11 (17): 1926-1934 (1997) 

Volmer, D., Hui, J. 

663 Beta blockers Polypyrrole coated capillary in-tube SPME coupled Polypyrrole capillary LC-ESI-MS 

in urine, serum with HPLC electrospray ionization MS for the 

determination of beta blockers in urine and serum samples 

J. Microcolumn Sep. (2000) 12(4), 255-266 

Wu, J., Lord, H., Pawliszyn, J., Kataoka, H. 

334 Flavor compounds Evaluation of SPME for Analysis of Volatile Metabolites 100µm PDMS, GC-FID 

in staphylococci Produced by Staphylococci 85µm polyacrylate 

J. Agric. Food Chem. 46 (1): 228-234 (1998) headspace 

Vergnaise, L., Masson, F., Montel, M., Berdague, J., Talon, R. stirring, salt added 

pH 3 for esters 

498 Aldehydes, esters Application of SPME to measure volatile metabolites 

100µm PDMS, 85µm 

polyacrylate GC-FID 

from bacteria produced by Staphylococcus carnosus and 15 min, stirring 

Staphylococcus xylosus esters @ 80°C, 

Book- Applied SPME, 1999, 364-371 Royal Society of aldehydes @ 25°C 

Chemistry, Cambridge, UK Coden: 67TUA8 

Talon, R, Montel, M. 

headspace 

392 Volatile metabolites Application of Head-Space SPME for the Analysis of Volatile 100µm PDMS, GC-MS 

in penicillium fungi Metabolites Emitted by Penicillium Species 85µm polyacrylate 

J. Microbiological Methods, 25 (1996) 245-255 25°C, 30 min (PDMS), 

Nilsson, T., Larsen, T., Montanarrella, L., Madsen, J. 50 min (PA) 

895 Volatile metabolites Biotransformation of (R)-(+)- and (S)-(-)-limonene by 

from limonen fungi and the use of SPME for screening. 

Phytochemistry (Oxford) (2001) 57(2) 199-208 

Demyttenaere, J.; De Kimpe, N; Van Belleghem, K 

802 Volatile metabolites Biotransformation of geraniol, nerol and citral by sporulated 

in penicillium fungi surface cultures of Aspergillus niger and Penicillium sp. 

Phytochemistry (2000) 55(4), 363-373 

Demyttenaere, J.,del Carmen Herrera, M.; De Kimpe, N 





393 Volatiles in Use of Digital Aroma Technology and SPME GC-MS to Compare 100µm PDMS GC-MS 

bacteria on poultry Volatile Compounds produced by Bacteria Isolated from 37°C, 30 min 

Processed Poultry 

J. Sci Food Agric. 1998, 78, 343-348 

Arnold, J., Senter, S. 

headspace 

664 Volatiles in Evaluation of SPME for the Isotopic Analysis of volatile 70µm Carboxen/PDMS GC-C-IRMS 

lactic acid bacteria compounds produced during fermentation by lactic 10 min 

acid bacteria headspace 

J. Agric Food Chem. 2000, 48, 2222-2227 

Goupry, S., Rochut, N., Robins, R., Gentil, E. 

salt added 

570 Fatty acid esters Headspace SPME with l-pyrenyldiazomethane in-fiber 85µm polyacrylate GC-EMIS 

in faeses derivatization for analysis of fecal short-chain fatty acids 15 min 

J-Chromatogr,-B:-Biomed-Appl. 25 Jun 1999; 730(1): 113-122 1-pyrenyldiazomethane 

Mills,-GA; Walker,-V; Mughal,-H derivative 

335 Cannabinoids Determination of Cannabinoids in Water and Human Saliva by 30µm PDMS GC-MS 

in water/saliva SPME and Quadrupole Ion Trap GC-MS 10 min 

Anal. Chem. 70 (9): 1788-1796 (1998) 

Hall, B., Satterfield-Doeerr, M., Parikh, A., Brodbelt, J. 

immersion 

665 Dibenzylamine Direct comparison of SPE and SPME for the GC 85µm polyacrylate GC-MS 

in saliva determination of dibenzylamine in artificial saliva 

leachates from baby bottle teats 

Anal Chim Acta 2000, 414(1-2), 133-140 

Niessner, G., Klampfl, C. 

pH 10 

340 Cannabinoids Solid-Phase Microextraction for Cannabinoids Analysis in Hair 30µm PDMS GC-MS 

in hair and Its Possible Application to Other Drugs 15 min, immersion 

J. Anal. Toxicology, Vol. 23, Jan./Feb. 1999 hair digested with 

Strano-Rossi, S., Chiarotti, M. 1N NaOH 

666 Lipophilic drugs Use of headspace SPME in hair analysis for 

in hair organic compounds headspace 

Forensic Sci. Int. (2000), 107(1-3), 129-148 hair digested with 

Sporkiert, F., Pragst, F. 4% NaOH 

941 Lipophilic drugs Analysis of hair by headspace SPME and GC-MS. headspace 

in hair Chromatogr Separation Tech (2001), 17(2), 4-8 hair digested with 

Pragst, F 4% NaOH 

336 Review of use SPME in Forensic Toxicology various fibers 


Namera, A., Yashiki, M., Kojima, T., Fukunaga, N. 


337 Acylcarnitines Determination of Urinary Acylcarnitines by ESI-MS Coupled ESI-MS 

in urine with SPME 

J. Mass Spectrom. 32 (11): 1195-1204 (1997) 

Mioder, M., Loster, H., Hraschuh, R., Popp, R. 

499 Methylxanthines Extraction of methylxanthines from human body fluids 65µm Carbowax/DVB GC-NPD 

in blood/urine by SPME 1 hr @ 40°C 

Anal. Chim. Acta., 1999, 387(1), 53-60 

Kumazawa, T., Seno, H., Lee, X., Ishii, A. 

1ml of 1M HCl04 

414 Organic acid esters Urinary Organic Acid Screening by SPME of the Methyl Esters 85µm polyacrylate GC-FID, -MS 

in urine J. Chromatogr. B: Biomed Sci. Appl. (1998), 713(2), 427-432 20 min 

Liebich, H., Gesele, E., Woll, J. immersion w/stirring 

trimethyloxonium 

tetrafluoroborate 





667 Semivolatile Validation of negligible depletion SPME as a tool to 

in tissue/blood determine tissue/blood partition coefficient for semivolatiles 

and nonvolatile organic chemicals 

Toxicol. Appl. Pharmacol. (2000), 166(2), 138-144 

Garicano, E., Vaes, W., Hermens, J. 

415 New Mass Spectrometric Methods for the Fast Analysis 

of Biomedical-Relevant Substances 

CLB Chem. Labor Biotech. (1998), 49(11), 414-420 

Volmer, D. 

GC-MS 

417 Verpamil & SPME-HPLC Determination of Verpamil and Norverpamil HPLC 

norverapamil Enantiomers in Urine 

in urine J. Mass Spectrom. (1997), 32(11), 1195-1204 

Asafu-Adjaye, E., Shiu, G. 

971 Pesticides in water Pesticide toxicity assessment using an electrochemical biosensor. 

Analytical and Bioananalytical Chemistry (2002) 373(8), 696-703 

Farre, M.; Goncalves, C.; Lacorte, S.; Barcelo, D.; Alpendurada, M.F. 

GC-MS 

1034 Jet fuel in porcine skin. 

1050 PAH 

1294 

1349 

1381 

1391 

1417 

Fatty acid ethyl esters in 

hair 

Tricyclic antidepressants 

in urine. 

Fatty acid ethyl esters in 

hair. 

Absorption through porcine skin exposed to various doses of jet fuel marker 

components determined with GC-FID using head space SPME fiber. 

Toxicological Sciences (2003) 72 (S-1), 383. 

Xia, X. R.; Riviere, J. E.; Muhammad, F.; Monteiro-Riviere, N. A.; Baynes, R. 

E. 

Determination of selected monohydroxy metabolites of 2-, 3- and 4-ring 

polycyclic aromatic hydrocarbons in urine by solid-phase microextraction 

and isotope dilution gas chromatography-mass spectrometry. GC-MS 

Journal of Chromatography, B: Analytical Technologies in the Biomedical 

and Life Sciences (2002) 778 (1-2), 157-164. 

Smith, C. J.; Walcott, C. J.; Huang, W. L.; Maggio, V.; Grainger, J.; 

Patterson, D. G., Jr. 

Biomimetic solid-phase microextraction to predict body residues and toxicity 

of chemicals that act by narcosis. 

Environmental Toxicology and Chemistry (2002) 21(2), 229-234 

Leslie, Heather A.; Busser, Frans J. M.; Hermens, Joop L. M.; Kraak, 

Michiel H. S.; Oosthoek, Annelies J. P. 

GC-MS 

Fatty acid ethyl esters in hair as markers of alcohol consumption. 

Segmental hair analysis of alcoholics, social drinkers, and teetotalers. GC-MS 

Clinical Chemistry (2001) 47(12), 2114-2123. 

Auwaerter, V.; Sporkert, F.; Hartwig, S.; Pragst, F. *; Vater, H.; 

Diefenbacher, A. 

Sample preparation with fibre-in-tube solid-phase microextraction for 

capillary electrophoretic separation of tricyclic antidepressant drugs in 

human urine. 

Electrophoresis (2001) 22(17), 3785-3790. 

Jinno, K.; Kawazoe, M.; Saito, Y.; Takeichi, T.; Hayashida, M. 

Analysis of fatty acid ethyl esters in hair as possible markers of chronically 

elevated alcohol consumption by headspace solid-phase microextraction 

(HS SPME ) and gas chromatography-mass spectrometry (GC-MS). 65 um PDMS/DVB GC-MS 

Forensic Science International (2001) 121(1-2), 76-88. 

Pragst, F.; Auwaerter, V.; Sporkert, F.; Spiegel, K. 

Pollution prevention screening of simulated Hanford waste for 

polychlorinated biphenyls by solid phase microextraction/GC-ECD. 

Abstracts of Papers American Chemical Society (2001) 222(1-2), ANYL118. 

Okemgbo, Asopuru A.; Metcalf, Steven G. 


1438 

1489 

1501 




Methylene chloride in 

urine 

Fentanyl and midazolam 

in plasma 

Amphetamines and 

designer drugs in hair 

1511 Drugs of abuse 

1021 

1530 

Monitoring of occupational exposure to methylene chloride: Sampling 

protocol and stability of urine samples. 

Journal of Toxicology Clinical Toxicology (2003) 41(5), 735-735 

Tabak, A.; Scherb, I.; Hoffer, E.; Bentur, Y.; Weiner, A. 

Simultaneous determination of fentanyl and midazolam in plasma using 

direct solid-phase microextraction before gas chromatography-mass 

spectrometry analysis. 


Dufresne, C.; Bureau, J.; Favetta, P.; Gonin, R.; Guitton, J. 

Fully automated determination of amphetamines and synthetic designer 

drugs in hair samples using headspace solid-phase microextraction and gas 

chromatography-mass spectrometry. 


Musshoff, Frank; Junker, Heike P.; Kroener, Lars; Lachenmeier, Dirk W.; 

Madea, Burkhard 

Detection and identification of illicit drugs including GHB, Rohypnol, 

Ketamine, and Psilocybin by refocused Solid Phase Microextraction High 

Performance Liquid Chromatography Mass Spectrometry, 

(SPME/HPLC/MS). 


Sabucedo, Alberto; Furton, Kenneth G.; Benson, Andrew; Almirall, Jose 

65um PDMS/DVB 

GC-MS 

HPLC-MS 

allyl alcohol (2-propen-1- 

A fatal human intoxication with the herbicide allyl alcohol (2-propen-1-ol). 

ol) 

Journal of Analytical Toxicology (2002) 26(1), 55-57 

Toennes, S. W.; Schmidt, K.; Fandino, A. S.; Kauert, G. F. 

GC-MS 


cocaine 

Gas chromatographic-mass spectrometric analysis of residual solvent 

trapped into illicit cocaine exhibits using head-space solid-phase 



Chiarotti, Marcello; Marsili, Remo; Moreda-Pineiro, Antonio 

Forensics 

748 Review The use of SPME-GC in forensic analysis 


Furton, K., Wang, J., Hsu, Y. Walton, J, Almirall, J. 


500 Gasoline The detection and analysis of ignitable liquid residues 100µm PDMS GC-FID 

on skin extracted from human skin using SPME-GC 15 min 

Almirall, J., Wang, J., Lothridge, K, Furton, K. headspace 

85 Accelerants A Simple, Inexpensive, Rapid, Sensitive and Solventless 100µm PDMS GC-FID 

in fire debris Technique for the Analysis of Accelerants in Fire 40°C, 20 min 

Debris Based on SPME 


Furton, K., Bruna, J., Almirall, J. 

headspace 

105 Gasoline, kerosene Forensic Application of the SPME Method to the Analysis 100µm PDMS GC-NPD 

in fire debris of Gasoline and Kerosene 22°C for 1 hr, or 

Kaneko, T., Nakada, M. 80°C for 5 min 

headspace 

114 Accelerants Novel Method for Analysis of Gasoline from Fire Debris Using 100µm PDMS GC-FID 

in fire debris Headspace Solid Phase Microextraction 

J. Forensic Sci. 41: 12-22 (1996) 

Furton, K., Almirall, J., Bruna, J. 

40°C, 20 min 





115 Accelerants The Recovery of Accelerants in Aqueous Samples from Fire 100µm PDMS GC-FID 

in liquid residue Debris Using SPME 20 min @ 40°C 

Science & Justice 36 (4): 283-287 (1996) 

Almirall, J., Furton, K., Bruna, J. 

143 Accelerants Determination of Liquid Accelerants in Arson Suspected Fire 100µm PDMS GC-FID 

in fire debris Debris Using Headspace SPME 15 min @ 70°C 

Anal. Commun. 33: 129 (1996) 

Steffen, A., Pawliszyn, J. headspace 

594 Accelerants A comprehensive sample preparation scheme for a GC, GC-MS 

in fire debris accelerants in suspect arson cases. 

J-Forensic-Sci. May 1999; 44(3): 504-515 

Ren,-QL; Bertsch,-W 

668 TNT, 2,4-DNT, RDX Development of field screening methods for TNT, 2,4-DNT, 

in soil and RDX in soil. 

Talanta, 39: 419-28 (1992) 

T Jenkens, et al 

812 RDX, HMX Detection of the cyclic nitramine explosives hexahydro 65µm PDMS/DVB GC-MS 

in soil 1,3,5-trinitro-1,3,5-triazine (RDX) and octahydro-1,3,5,7- 20MIN @55°c LC-MS 

tetranitro-1,3,5,7-tetrazine (HMX) and their degradation 

products in soil environments 

J Chromatog A (2001) 909(1), 53-60 

Hawari, J; Beaudet, S; Groom, C.; Halasz, A; Paquet, L 

PFBHA derivative 

344 explosives Trace Analysis of explosives in Seawater Using SPME and 65µm Carbowax/DVB GC-MS 

in salt water GC-Ion Trap Mass Spectrometry 60 min 

Anal. Chem., Vol. 70, No. 14, July 15, 1998, pg. 3015-3020 immersion 

Barshick, S., Griest, W. stirring 

669 Explosives Application of SPME to the recovery of explosives and 65µm Carbowax/DVB GC-ECD 

from solids, water ignitable liquid residues from forensic specimens 25 min, 25% NaCl HPLC 

J. Chromatogr A, 885(2000) 419-432 immersion 

Furton, K., Almirall, J., Bi, M., Wang, J., Wu, L. stirring 

592 explosives An improved interface for coupling SPME to HPLC 50µm Carbowax/TPR HPLC-UV 

in water applied to the analysis of explosives 

J-High-Resolut-Chromatogr. May 1999; 22(5): 279-282 

Wu,-L; Almirall,-JR; Furton,-KG 

254nm 

886 Explosives Optimization of SPME for the recovery of explosives from 65µm Carbowax/DVB GC-ECD 

from solids, water aqueous and post-explosion debris followed by gas and 50µm Carbowax/TPR HPLC 

liquid chromatographic analysis 30 min, 25% NaCl 

J. Forensic Sci. 45: 845-852 (2000) immersion 

Furton, K., Wu, L., Almirall, J. stirring 

985 

Acetic and formic acid in 

museum environment 

Acetic acid and formic acid concentrations in the museum environment 

measured by SPME-GC/MS Polyacrylate GC-MS 

Atmospheric Environment (2002) 36 (24), 3909-3916 

Ryhl-Svendsen, M.; Glastrup, J. 

986 Explosives in soil Detection of explosives and their degradation products in soil environments. 

J.Chromatogr. A (2002) 963(1-2), 411-418 

Halasz, A.; Groom, C.; Zhou, E.; Paquet, L.; Beaulieu, C.; Deschamps, S.; 

Thiboutot, S.; Ampleman, G.; Dubois, C.; Hawari, J. 

GC-MS 

989 

Methylmercury in human 

hair 

Determination of methylmercury in human hair by ethylation followed by 

headspace SPME/GC GC-CVAFS 

J.Chromatogr. A (2002) 963(1-2), 345-351 

Diez, S.; Bayona, J.M. 


990 

991 




Methylmercury in 

biologicals 

Ethanol in post-mortem 

samples. 

Methylmercury determination in biological samples by derivatization, SPME 

and GC. 

J.Chromatogr. A (2002) 963(1-2), 313-323 

Rodil, R.; Carro, A.M.; Lorenzo, R. A.; Abuin, M.; Cela, R. 

PDMS GC-MS 

Automated headspace SPME and capillary GC analysis of ethanol in postmortem 

species. 

Forensic Science International (2002) 128(3), 115-119. 

de Martinis, B.S.; Santos Martin, C.C. 

Polyacrylate GC 

1003 L-methadone Fatal mixed intoxication caused by L-methadone and chloral hydrate. 

Archiv fuer Kriminologie (2003) 211 (3-4), 90-97. 

Weinmann, Wolfgang; Goerke, Rolf; Perdekamp, Markus Grosse; Thurau, 

Kirsten; Vogt, Susanne 

GC-MS 

1013 TNT in sediment 

1025 

Drugs of abuse in hair 

samples. 

1031 Fatty acid esters in hair. 

1033 

Nondestructive, minimal-disturbance, direct-burial solid-phase 

microextraction fiber technique for measuring TNT in sediment Polyacrylate 


Conder, Jason M.; La Point, Thomas W.; Lotufo, Guilherme R.; Steevens, 

Jeffery A. 

Aplication of tandem mass spectrometry combined with gas 

chromatography and headspace solid-phase dynamic extraction for the 

determination of drugs of abuse in hair samples. PDMS GC-MS-MS 


Lachenmeier, Dirk W.; Kroener, Lars; Madea, Burkhard; Musshoff, Frank 

Fatty acid ethyl esters in scalp, pubic, axillary, beard and body hair as 

markers for alcohol misuse. 

Alcohol and Alcoholism (2003) 38 (2), 163-168. 

Pragst, Fritz; Auwaerter, Volker; Hartwig, Sven 

Investigation by solid-phase microextraction and gas chromatography/mass 

spectrometry of secondary metabolites in lichens deposited on stone 

monuments. GC-MS 


Di Tullio, Alessandra; De Angelis, Francesco; Ceci, Roberta; Quaresima, 

Raimondo; Reale, Samantha 

1079 Review article ASTM standards for fire debris analysis: A review. 

Forensic Science International (2003) 132 (1), 63-67. 

Stauffer, Eric; Lentini, John J. 

1135 Cannabinoids in hair. 

1242 Drugs of abuse in hair. 

1273 

Gamma-hydroxybutyric 

acid 

Fully automated determination of cannabinoids in hair samples using 

headspace solid-phase microextraction and gas chromatography-mass 


Journal of Analytical Toxicology (2002) 26 (8), 554-560. 

Musshoff, F.; Junker, H. P.; Lachenmeier, D. W.; Kroener, L.; Madea, B. 

Application of tandem mass spectrometry combined with gas 

chromatography and headspace solid-phase dynamic extraction for the 

determination of drugs of abuse in hair samples. GC-TMS 


Lachenmeier, D. W.; Kroener, L.; Musshoff, F.; Madea, B. 

Development of a GC/MS method for detection of gamma-hydroxybutyric 

acid (GHB) and its precursors. GC-MS 


209. 

Helwig, Katie; Dema, Anne C.; Wetmore, Lori A. 


1286 




Thiopental and 

pentobarbital in hair. 

1287 Cannabinoids in hair. 

1293 Drugs of abuse in saliva 

1509 Gamma-hydroxybutyric 

acid (GHB) 

1548 Methamphetamine 

1550 Gamma-hydroxybutyrate 

(GHB) in human urine 

1235 

1328 

1556 

1557 

Detection of thiopental and pentobarbital in head and pubic hair in a case of 

drug-facilitated sexual assault. GC-MS-MS 

Forensic Science International (2003) 133 (1-2), 171-174. 

Ferrara, Santo Davide; Favretto, Donata; Frison, Giampietro; Tedeschi, 

Luciano 

Automated headspace solid-phase dynamic extraction for the determination 

of cannabinoids in hair samples. GC-MS 

Forensic Science International (2003) 133 (1-2), 32-38. 

Musshoff, Frank; Kroener, Lars; Lachenmeier, Dirk W.; Madea, Burkhard 

Simultaneous detection of some drugs of abuse in saliva samples by SPME 

technique. GC/MS 

Forensic Science International (2003) 134 (1), 40-45. 

Fucci, Nadia; Chiarotti, Marcello; De Giovanni, Nadia 

SPME on-fiber derivatization of gamma-hydroxybutyric acid (GHB) in 

forensic analysis. 


Meyers, Jodi E.; Almirall, Jose R.; Galiana, Gigi 

SPME/GC-MS characterization of volatiles associated with 

methamphetamine: Toward the development of a pseudomethamphetamine 

training material. 

Journal of Forensic Sciences (2002) 46(5), 1014-1024 

Vu, Doan-Trang T. 

Determination of gamma-hydroxybutyrate in water and human urine by solid 

phase microextraction-gas chromatography/quadrupole ion trap 

spectrometry. 

Journal of Forensic Sciences (2002) 46(3), 688-693 

Brodbelt, Jennifer; Blair, Sheryl; Hall, Brad; Song, Meansup 

Identification of canis familiaris active odor signature chemicals in controlled 

substances and high explosives. 

Abstracts of Papers American Chemical Society (2003) 225 (1-2), PRES 25. 

Lopez, Claudia; Furton, Kenneth G.; Harper, Ross; Hsu, Ya-Li; Walton, John 

GC-MS 

65 um PDMS/DVB GC-MS 

Laboratory and field experiments used to identify Canis lupus var. familiaris 

active odour signature chemicals from drugs, explosives, and humans. 


Lorenzo, N.; Wan, T. L.; Harper, R. J.; Hsu, Y. L.; Chow, M.; Rose, S.; 

Furton, K. G.* 

CW/DVB and PDMS GC-ECD & GC-M 

TNT isomers from land 

mines Chemical signatures of TNT-filled land mines. 

Talanta 54(3), 2001, 501-514. 

Jenkins, T; Leggett, D; Miyares, P.; Walsh, M.; Ranney, T.; Cragin, J.H.; 

George, V. 

Headspace 

Odor chemicals from 

explosives. 

The scientific foundation and efficacy of the use of canines as chemical 

detectors for explosives. 

Talanta 54(3), 2001, 487-500. 

Furton, K.G.; Myers, L.J. 

1897 Terpenes in Headspace SPME for screening for the presence of headspace GC 

resins resins in Egyptian archaeological samples. 

J Separation Sci, 27, #3, 235-243 

Hamm, Sandrine; Bleton, Jean; Tchapla, Alain 





1898 Methyl Improvements in the methylmercury extraction from headspace GC-cold vapour 

mercury from human hair by headspace SPME followed by GC- ethyl derivative atomic spectromet 

human hair cold-vapour atomic flourescence spectrometry 

J Chromatogr A, 1025, #1, 71-75 

Montuori, P; Jover, E; Alzaga, R; Diez, S; Bayona, J. 

1899 TNT in sand Transport of explosives TNT in soil and its Headspace for 20min TEEM-GC/MS 

equilibrium vapor immersion in GC/ECD 

Proc SPIE Int Soc Opt Eng, 5415, #2, 1389-1399 water extract 

Baez, B; Briano, J; Castro, M.; Correa, S; De Jes, M.; 

Hernandez-Rivera, Samuel P.; Mina, Nairmen 

1900 Oxidation Oxidation of TNT by photo-Fenton process GC-MS 

byproducts of Chemosphere, 57, #9, 1107-1114 

TNT Chen, Jong-Nan; Liou, Ming-Jer; Lu, Ming-Chun 

1901 Ammonium New developments in SPME. Part 2: analysis of Alkylchloroformate GC-MS 

nitrate ammonium nitrate-based explosives. derivative 

explosive J Forensic Sci, 49, #2, 215-221 

Brown, H.; Kirkbride, K.*; Pigou, P. .; Walker, G. 

1902 Signature odor Laboratory and field experiments used to identify Canis 50µm CW/DVB GC/MS 

explosives lupus var. familiaris active odor signature chemicals PDMS coatings GC/ECD 

drugs, and from drugs, explosives, and humans 

humans Anal. Bioanal. Chem., 376, #8, 1212-1224 

Chow, M.; Furton, K.; Harper, R.; Hsu, Ya-Li.; 

Lorenzo, N.; Rose, S.; Wan,T. 

1903 TATP in Improved method for the detection of TATP after explosion 65µm PDMS-DVB GC/MS 

post J Forensic Sci, 49, #5, 935-938 headspace 

explosives Muller, D.; Levy, A.; Shelef, R.; Abramovich-Bar, S.; 

Sonenfeld, D.; Tamiri, T. 

1904 GHB in water Analysis of gamma-hydroxybutyric acid (GHB) in spiked derivative on-fiber GC-MS 

water and beverage samples using SPME on fiber 

derivatization/gas chromatography-mass spectrometry 

J Forensic Sci, 50, #1, 31-36 

Meyers, Jodi E.; Almirall, Jose R. 

1905 Explosives Solid phase microextraction with GC/MS for the GC-MS 

in soil, water, trace analysis of explosives GC-ECD 

and swab Proc. 50th ASMS Conf. Mass Spectrom. Allied Top. 

samples 2002, p669-670 

Maslanka, D; McDonald, J.; Miller, M. 

1906 FAEE from Wipe-test and patch-test for alcohol misuse based headspace GC-MS 

skin samples on the concentration ratio of fatty acid ethyl esters LC-PDA 

and squalene C FAEE / C SQ in skin surface lipids. 

Forensic Sci Intl, 143, #2-3, 77-86 

Pragst, F.; Auwaerter, V.; Kiessling, B.; Dyes, C. 

1907 Methyl Headspace SPME for the GC analysis of methyl- 85µm polyacrylate GC-NPD 

parathion parathion in postmortem human samples: application headspace 

in biological in a suicide case by intravenous injection. salt added 

samples Forensic Sci Intl, 143, #2-3, 127-132 

Tsoukali, H.; Raikos, N.; Theodoridis, G.; Psaroulis, D. 

1908 Cocaine in Detection of cocaine and cocaethylene in sweat immersed in 0.2M GC-MS 

sweat by SPME-GC-MS sodium acetate buffer 

J. Chromatogr. B, 811, #1, 37-40 pH 5 

Follador, M; Moreau, R; Silva, O.; Yonamine, M. 

1909 PAHs in identification of gasoline soot in suspect arson 100µm PDMS GC-MS 

gasoline soot cases by using headspace SPME-GC-MS 75µm Carboxen 

Analytical Letters, 236, #7, 1373-1384 heaspace 

Wu, Chia-Hao; Chen, Chin-Lien; Huang, Ching-Te; 

Lee, Maw-Rong; Huang, Chih-Ming 





1910 Propane in Quantification of propane in biological materials headspace GC-MS 

biological by headspace GC 

materials Forensic Science International, 151, #2-3, 165-170 

Park, J; Min, Ji-Sook; Heo, S.; Lim, Mi-Ae; Park, S 

1911 Volatile The study of fingerprint characteristics of the emanations headspace GC-MS 

organics from human arm skin using the original sampling 30min sampling 

from human system by SPME-GC-MS 

skin J. Chromatogr. B, 822, #1-2, 244-252 

Cai, Ji-Jin; Li, Gong-Ke; Ruan, Gui-Hua; Zhang, Zhuo-Min 

1912 Capsaicin Extraction of capsaicin in aerosol defense sprays from fabrics headspace GC 

from fabrics Talanta, 67, #2, 377-382 

Almirall, Jose R.; Spicer Jr., Oliver 

1913 Odor Identification of dominant odor chemicals emanating from headspace GC-MS 

chemicals in explosives for use in developing optimal training aid GC-ECD 

explosive combinations and mimics for canine detection 

Talanta, 67, #2, 313-327 

Almirall, Jose R.; Furton, Kenneth G.; Harper, Ross J. 

Environmental 

1914 Auto exhaust Formation and reaction of hydroxycarbonyls from the pentafluorobenzyl API-MS 

reaction of OH radicals with 1,3-butadiene and isoprene hydroxyl amine GC/FID 

Environ. Sci. Technol., 39. #11, 4091-4099 derivatives 

Arey, Janet; Atkinson, Roger; Baker, Jillian 

1915 Carboxylic Photochemical sources of organic acids. 1. Reaction headspace GC-MS 

acids of ozone with isoprene, propene, and 2-butenes 

in air under dry and humid conditions using SPME 

J Phys Chem A, 109, #24, 5358-5365 

Orzechowska, Grazyna; Paulson, Suzanne 

1916 Byproducts Rate coefficients for the gas-phase reaction of headspace GC/FID 

of reactions isoprene with N0 3 and NO 2 

Int J Chem Kinet, 37, #2, 57-65 

Johnson, M.; Langer, S.; Stabel, J. 

1917 Hydroxyl- 1,4-Hydroxycarbonyl products of the OH radical initiated on-fiber hydroxylamine GC-MS 

carbonyls reactions of C5-C8 n-alkanes in the prescence of NO derivatives GC/FID 

in Air Environ. Sci. Technol., 39. #12, 4447-4453 

Arey, Janet; Aschmann, Sara M.; Atkinson, Roger; Reisen, F 

1918 Volatile sulfur Occurrence and abatement of volatile sulfur headspace GC-MS 

from biogas compounds during biogas production 

production J. Air Waste Manage. Assoc, 54, #7, 855-861. 

Andersson, F.; Ejlertsson, J.; Karlsson, A.; Svensson, B. 

1920 Sulfur compd Headspace SPME followed by GC/PFPD for the analysis of 65µm PDMS-DVB GC/PFPD 

industrial malodorous sulfur compounds liquid industrial effluents 75µm Carboxen 

effluents Anal and Bioanal Chemistry, 378, #1, 190-196 5 or 60 min 

Desauziers, V.; Fanlo, Jean-Louis; Lestremau, F. headspace 

1921 PAHs in Air/polymer distribution coefficients for PDMS coated fibers GC-MS 

air PAHs by SPME sampling. 

J Chromatography, A, 1029, #1-2, 263-266 

Kolar, K.; Ciganek, M.; Malecha, J. 

1922 Organo- Selective extraction of trace levels of polychlorinated and GC/MS/MS 

halogenated polybrominated contaminants by supercritical fluid-SPME and 

in fish feed determination by GC-MS. Application to aquaculture fish 

feed and cultured marine species 

Anal. Chem., 77, #7, 2259-2265 

Carro, A.M.; Lorenzo, R.A.; Rodil, R.; Torrijos, R. Cela 

1923 Ethylene oxide Laboratory and field validations of a SPME 75µm Carboxen GC 

in air device for the determination of ethylene oxide. HBr on-fiber derivative 

J Chromatogr A, 1026, #1-2, 25-30 25°C 

Tsai, S; Tsai, S; Wang, V; Lai, J 





1924 Methyl Blank correction considerations for isotope dilution and GC-ICP-MS 

mercury from reverse isotope dilution calibration: Determination of 

fish tissue methylmercury in fish tissue 

J of Anall Atomic Spectrometry, 20, #8, 724-729 

Yang, Lu; Sturgeon, Ralph E. 

1925 PCBs in Selective determination of PCBs in waste oils using 65µm PDMS-DVB GC-AED 

waste oil liquid-liquid partition followed by headspace SPME headspace 

and GC with atomic emission detection 

J. Chromatogr. A,1056, #1-2, 263-266 

Cela Torrijos, R.; Ramil Criado, M.; 

Rodriguez Pereiro, I. 

1926 Degradation Confirmation of the formation of dichlorodibenzo-p- 100µm PDMS GC-EI/MS 

byproducts dioxin in the photodegradation of triclosan by photo-SPME headspace 

of triclosan Anal. Bioanal. Chem., 381,#6, 1294-1298 

Cela, R.; GarciaJares, C.; Llompart, M.; 

Lores, M.; SanchezPrado, L. 

1927 Acids from Degradation and corrosive activities of fungi in a diesel-mild headspace @ 30°C GC 

diesel fuel steel-aqueous system 

World J Microbiology & Biotechnology, 21, #2, 135-142 

Bento, F.; Beech, I.; Gaylarde, C.; Englert, G.; Muller,I. 

1928 PCBs in Determination of PCBs in ash using dimethylsulfoxide 65µm PDMS-DVB GC-ECD and GC-M 

ash microwave assisted extraction followed by SPME headspace 

Talanta, 63, #3, 533-540 stirring 

Criado, M.; Pereiro, I. ; Torrijos, R. 

1929 Chemical Detection of gas-phase chemical warfare agents direct air sampling GC-MS 

warfare agemt using field-portable GC-MS systems: instrument 

in air and sampling strategy considerations. 

Trends in Anal Chem, 23, #4, 296-306 

Smith, P.; Lepage, C.; Koch, D.; Wyatt, H., Hook, G.; 

Betsinger, G.; Erickson, R., Eckenrode, B. 

1930 Chemical Towards smaller and faster GC-MS systems




1936 Roxarsone Sensitive method for the determination of roxarsone using 65µm PDMS-DVB GC-MS 

in water w/ SPME multi-detector gas chromatography 15min @ 70°C GC-PFPD 

J Chromatogr A, 1057, #1-2, 177-183 1,3-propanedithiol 

Aldstadt III, Joseph H.; Roerdink, Aaron R. derivatives 

1937 Selenium Speciation of volatile selenium species in plants using headspace GC-ICP-MS 

from plants GC-ICP-MS 

Sepu, 22, #1, 16-19 

Meija, J.; Montes-Bayon, M.; Caruso, J.; Leduc, D.; Terry, N. 

1938 Sulfur & N2 Analysis of sulfur & nitrogen odorants using SPME and GC-MS headspace GC-MS 

odorants in Water Sci. Technol., 50, #4, 115-120 

biomass Chiu, P.C.; Dentel, S.K.; Hepner, S.; Turkmen, M. 

1939 Odors from Characterization of odors from limed biosolids treated headspace GC-MS 

biosolids with nitrate and anthraquinone 

J. Environ. Sci. Health, 40, #1, 139-149 

Abu-Orf, M; Choi, H.; Kim, H.; McConnell, L.; 

Peot, C.; Ramirez, M. 

1940 Organics Sampling and analysis of volatile organic pollutants emitted 85µm polyacrylate GC-MS 

in stack by an industrial stack headspace 

emmisions Anal. Chim. Acta, 524, #1-2, 51-62 

Campo, L.; Domeno, C.; Martinez-Garcia, Fca.; Nerin, C. 

1941 Volatile Quantitative determination of volatile organic compounds in headspace GC-UV 

organics in indoor dust using gas chromatography-UV spectrometry 

dust Environ. Int., 31, #8, 1141-1148 

Bornehag, C; Lagesson, V; Nilsson, A; Sundell, J; Tagesson, C 

1942 Volatiles Analysis of volatile components in concrete by 50/30µm DVB/CAR GC-MS 

in concrete SPME-GC-Mass Spetrometry 65°C, headspace 

Zhipu Xuebao, 25, #4, 225-228 

Liao, K. 

1943 Volatiles Identification of volatile components in yunyan and yanmo headspace GC-MS 

in concrete concrete by SPME -GC-MS 

Zhipu Xuebao, 25, #1, 32-37 

Zhu, S. M.; Li, J.; Lin, P. 

1944 Chlorophenols Chlorophenols in leachates originating from different landfills headspace GC-FID 

from landfills and aerobic composting plants 

J. Hazard. Mater., 124. #1-3, 107-112 

Ozkaya, Bestamin 

1945 Organics Qualitative analysis of organics in atmospheric 100µm PDMS GC-MS 

from particulates by headspace SPME-GC/MS 10min headspace 

particulate Atmos. Environ., 38, #40, 6917-6925 

Khanal, O.; Shooter, D. 

1946 Pesticides Determination of pesticides and their degradation products Review GC-MS 

from soil IN soil: Critical review and comparison of methods headspace SPME LC-MS 

TrAC Trends Anal. Chem., 23, #10-11, 772-789 

Andreu, Vicente; Pico, Yolanda 

1947 Organics SPME to predict bioavailability and accumulation of organic 30µm PDMS GC-MS 

from soil micropollutants in terrestrial organisms after exposure headspace 

to a field-contaminated soil 10 days exposure 

Environ. Sci. Technol., 38, #18, 4842-4848 

Barendregt, A; Fleuren, R; Hermens, J.; Jager, T; Sinnige, T.; 

Van Der Wal, Leon; Van Gestel, Cornelis A. M. 

1948 PAHs in SPME coupled to GC-MS for determining PAH-micelle 85µm polyacrylate GC-MS 

micelles micelle partition coefficients 100µm PDMS 

Anal. Chem., 76, #15, 4572-4578 

Alfonso, Ana M.; Ayala, Juan H.; Gonzalez, V; Pino, V. 





1949 Odors from Implementation of new methods to characterise headspace GC-MS 

pig sheds atmospheres in piggeries 

Int. J. Environ. Anal. Chem., 84, #9, 647-659 

Begnaud, F.; Berdague, Jean-Louis; Lebost, J.; 

Murat, C.; Peres, C. 

1950 Organics in In-tube solid-phase microextraction and online 5 M X 0.53mm ID GC 

water coupling with high-resolution GC. 1.2µm PDMS 

LC-GC Europe, 17, #3, 144-151 

Wang, H. W.; Liu, W. M.; Guan, Y. F. 

1951 Odor from Characterization of volatile organic compounds on 75µm Carboxen GC 

swine airborne dust in a swine finishing barn 100µm PDMS 

facilities 

Water 

Trans. Am. Soc. Agric. Eng., 47, #4, 1231-1238 

Jeon, I.J.; Maghirang, R.G.; Razote, E.B.; Seitz, L.M 

headspace 

778 Volatile organics Solid Phase Microextraction of volatile organic compounds 100µm PDMS GC 

in environmental in environmental applications 85µm Polyacrylate 

samples Am Laboratory (2001)33(4), 18-20 

Van Longenhove, H; Dewulf, J. 

15 min. 

858 Organic pollutants SPME - a convenient tool for the determination of organic 

in environment pollutants in environmental matrices 

Crit. Rev. Anal. Chem (2001) 31(1) 1-18 

Zygmunt, Bogdan; Jastrzebska, Anna; Namiesnik, Jacek 

1 BTEX compounds, The Application of Chemically Modified Fused Silica uncoated fiber GC-FID 

PCBs, solvents Fibers in the Extraction of Organics from Water Matrix 1 min 

in water Samples and Their Rapid Transfer to Capillary Columns 

Water Pollution Research J. Canada 24: 179 (1989) 

Belardi, R., Pawliszyn, J. 

3 VOCs Solid Phase Microextraction for the Direct Analysis of 100µm PDMS GC-FID 

in water Water: Theory and Practice 2-5 min 

LC-GC 10: 656-661 (1992) 

Arthur, C., Potter, D., Buchholz., K, Motlagh, S., Pawliszyn, J. 

salt added 

4 VOCs, PCBs, Practical and Theoretical Aspects of Solid Phase 100µm PDMS GC-FID 

solvents in water Microextraction for the Direct Analysis of Groundwater 5-14 min 

Proceedings 15th Annual EPA Conference-Analysis 

of Pollutants in Environment, Norfolk, VA, May 1992 

Arthur, C., Buchholtz, K., Motlagh, S., Killam, L., Pawliszyn, J. 

salt added 

6 BTEX, gasoline Analysis of Substituted Benzene Compounds in 56µm PDMS GC-FID 

in water Groundwater Using SPME 2-6 min 

J. Env. Sci. Technol. 26: 979-983 (1992) 

Arthur, C., Potter, D., Lim, M., Motlagh, S., 

Killam, L., Pawliszyn, J. 

stirring 

7 BTEX compounds Dynamics of Organic Compounds Extraction from 56µm PDMS GC-FID 

in water Water Using Liquid-Coated Fused Silica Fibers 2-6 min 

Anal. Chem. 64: 1187-1199 (1992) 

Louch, D., Motlagh, S., Pawliszyn, J. 

stirring 

10 BTEX compounds Detection of Substituted Benzenes in Water at the pg/mL 100µm PDMS GC-FID 

in water Level Using Solid Phase Microextraction and 30 min 

GC-Ion Trap Mass Spectrometer 

J. Chromatogr. 625: 247-255 (1992) 

Potter, D., Pawliszyn, J. 

stirring 

11 Organics Environmental Analysis of Organic Compounds in 100µm PDMS GC-MS 

in water Water Using Solid Phase Microextraction 14 min 


Arthur, C., Pratt, K., Belardi, R., Motlagh, S., Pawliszyn, J. 

stirring 





14 Phenols Determination of Phenols by SPME and GC Analysis 85µm polyacrylate GC-FID, -MS 

in water J. Environ. Sci. Technol. 27 (13): 2844-2848 (1993) 60 min 

Buchholz, K., Pawliszyn, J. stirring 

salt added, pH 2 

230 Phenols Determination of Phenolic Compounds in Waste Water GC-MS 

in water by Solid-Phase Microextraction 

Fresenius’ J. Anal. Chem. 357: 326-332 (1997) 

Moeder, M., Schrader, S., Franck, U., Popp, P. 

670 Phenols Sorption of phenols to dissolved organic matter 

in water investigated by SPME 

Sci. Total Environ. (2000), 253(1-3), 63-74 

Ohlenbusch, G., Kumke, M., Frimmel, F. 

922 Phenolic compounds SPME coupled to liquid chromatography for the analysis 50µm CW/TPR HPLC 

in water of phenolic compounds in water 65µm DVB/PDMS 

J. Chromatogr. A (2001) 923(1-2), p45-52 30min immersed 

Toledo, E., Prat, M., Alpendurada, M. salt added, pH 2 

951 Chlorinated phenolics Application of SPME in pre-concentration of chlorinated 

in water phenolic compounds from cellulose bleaching effluents 

J. Sep. Sci (2001), 24(4), 309-312 

Dos Santos, L.; Vale, M.; De Araujo, M. 

Bertrand C.; Caramao, E.; Oliveira, E. 

15 VOCs, phenols, Recent Advances in Solid-Phase Microextraction 100µm PDMS GC-MS 

semivolatiles (SPME) of Environmental Samples 5 min (volatiles) 

in water Proceedings Water Quality Technology Conference 10 min (semivolatiles) 

Miami, FL, Nov. 1993 headspace 

Arthur, C., Pratt, K., Belardi, R., Motlagh, S., Pawliszyn, J. stirring, salt added 

671 4-Quinolones Influence of pH and other modifying factors on the CW/TPR HPLC 

in water distribution behaviors of 4-Quinolones to Solid phase and 10min. 260NM 

humic acids studied by "negligible-depletion" SPME-HPLC pH 3-5.5 

Environ Sci Technol. 20000, 34, 4989-4994 

Lutzhoft, H. Vaes, W., Freidig, A., Halling-Sorrensen, B. 

Hermens, J. 

stirred 

501 24 Semivolatiles Development of SPME-GC method for the determination of GC 

in waste water organic compounds in waste water 

Acta Hydrochim. Hydrobiol. 1999, 27(4), 1913-199 

Grote, C., Belau, E., Levsen, K., Wunsch, G. 

938 Organics An improved automatic analyzer for organic compounds in GC 

in water water based on headspace (SPME) coupled to GC 

Field Anal. Chem. Technol (2001) 5(1-2), 37-49 

Belau, E.; Grote, C.; Spiekermann, M.; Levsen, K. 

565 Semivolatiles Polyacrylate-Coated SPME fibers as a tool to simulate body 85µm polyacrylate GC-MS 

in fish, water residues and target concentrations of complex organic 

mixtures for estimation of baseline toxicity 

Environ. Sci. Technol. 2000, 34, 324-331 

Verbruggen, E., Vaes, W., Parkerton, T., Hermens, J. 

5-150 min 

785 Halogenated Impact of a lignite seam on contaminated groundwater in the 

hydrocarbons aquifer system of the Bitterfeld region 

in water Water Air Soil Pollut (2000) 125(1-4), 157-170 

Christoph, G; Dermietzel, J. 

19 Chlorohydrocarbons Determination of Volatile Chlorinated Hydrocarbons in 100µm PDMS GC-ECD 

in water Air and Water with Solid-Phase Microextraction 20 min (immersion) 

Analyst(Cambridge,UK) 118: 1501-5, Dec. 1993 

Chai, M., Arthur, C., Pratt, K., Pawliszyn, J., Belardi, R. 

10 min (headspace) 





436 Chlorohydrocarbons Analysis of Volatile Halogenated Hydrocarbons in Water by 100µm PDMS GC-MS 

in water SPME and GC-MS 20 min 

Chem. Listy (1998), 92(9), 633-642 

Janda, V., Viden, I. 

stirred 

20 PAHs, PCBs Rapid Determination of Polyaromatic Hydrocarbons 15µm PDMS GC-MS 

in water and Polychlorinated Biphenyls in Water Using 10 min 

Solid-Phase Microextraction and GC/MS stirring 

J. Environ. Sci. Technol. 28(2): 298-305 (1994) 

Potter, D., Pawliszyn, J. 

900 Aromatic compounds SPME of aromatic hydrocarbons from water samples 

in water Chemija (2000) 11(4) 206-210 

Seduikiene, I.; Vickackaite, V.; Kazlauskas, R 

672 PAHs Quantitative analysis of PAHs in water by SPME-HPLC HPLC 

in water Huanjing Huaxue (2000) 19(4), 382-384 

Li, Y., Zhang, X., Xu, R., Cai, W., Wang, G., Song, Y. 

22 VOCs, BTEX, PAHs Analysis of Organic Compounds in Environmental 100µm PDMS GC-MS 

in wastewater, Samples Using Headspace Solid Phase Microextraction stirring, varied time 

sludge J. High Res. Chromatogr. 16(12): 689-692 (1993) saturated salt 

Zhang, A., Pawliszyn, J. 

673 Jet fuels Source identification of underground fuel spills by GC 

in ground water SPME/High Resolution GC/genetic algorithms 

Anal. Chem. (2000), 72(2), 423-433 

Lavine, B., Ritter, J., Moores, A., Wilson, M., 

Faruque, A., Mayfield, H. 

674 Organic chemicals Quantification of synthetic organic chemicals in 85µm polyacrylate GC-FID 

in waste water biological treatment process effluent using SPME-GC 

Water Environ. Res, (2000), 72(1), 98-104 

Magbanua, B., Mitchell, D., Gehniger, S., Bowyer, R., 

Grady, C., Leslie, J. 

675 Musk fragrances Optimization of SPME for the GC-MS determination of 65µm PDMS/DVB GC-MS 

in water synthetic musk fragrances in water samples 45 min @ 30°C 

J. Chromatogr. A, (2000) 903(1-2), 203-210 headspace 

Winkler, M., Headley, J., Peru, K. agitation 

502 Polycyclic musk Occurrence and distribution of organic compounds in the GC-MS 

in surface water aquatic system in Berlin, Germany. Part 3, Determination of 

synthetic musks in Berlin surface water applying 

SPME and GC-MS 

Acta Hydrochim Hydrobiol (1999), 27(3), 150-156 

Heberer, T., Gramer, S., Stan, H. 

787 Polyolefins Ultrasonication and microwave assisted extraction of GC-MS 

in soil degradation products from degradable polyolefin blends 

aged in soil 

J. Appl. Polym. Sci (2001) 79(6), 1101-1112 

Contat-Rodrigo, L; Haider, N; Karlsson, S; Ribes-Greus, A 

940 Pyrene Sorption of pyrene to dissolved humic substances and related 

on humic material model polymers. 1. Structure-property correlation 

Environl Scie & Tech (2001), 35(12), 2536-2542 

Kopinke, F.; Georgi, A.; Mackenzie, K. 

676 PAHs SPME and headspace SPME for the determination of high 100µm PDMS GC-FID 

in water/soil molecular-weight PAHs in water and soil samples 85µm polyacrylate 

J. Chromatogr. Sci., (2000) 38(12) 528-534 

Doong, R., Chang, S., Yuh-Chang 

20-60 min @60°C 





677 PAHs Determination of Distribution Coefficients of priority 100µm PDMS 

in water/soil PAHs using SPME 85µm polyacrylate 

Anal. Chem. 2000, 72(15), 3647-3652 

Doong, R., Chang, S., 

20-60min. 

678 PAHs SPME FOR determining the Distribution of 16 USEPA 100µm PDMS GC-MS 

in water/soil PAHs in water 85µm polyacrylate 

J.. Chromatogr.. A 2000, 879(2), 177-188 

Doong, R., Chang, S., Sun,, Y. 

20-60 min 

585 PAHs in Interaction between natural organic matter (NOM) and (PAH) 7µm PDMS GC-MS 

water/humic material comparison of fluorescence quenching and SPME. 

Fresenius'-J-Anal-Chem. Jun 1999; 364(4): 313-319 

Doll,-TE; Frimmel,-FH; Kumke,-MU; Ohlenbusch,-G 

20 min 

25 PAHs, semivolatiles Solid Phase Microextraction -- A Solventless Sample 7µm PDMS (PAHs) GC-FID, -ECD 

in water Preparation Method for Organic Compounds in Water polyacrylate (semivol) 

American Environmental Lab April 1994, p 43-45 15 min, stirring 

Shirey, R., Mani, V., Savrock, J. saturated salt 

679 Volatiles Optimization of Extraction Conditions for Low-Molecular- six different fibers GC-MS 

in water Weight analytes using SPME 15 min headspace 

J. Chrom. Sci., Vol. 38, March 2000, 109-116 

Shirey, R. 

sat. salt, pH2,7,11 

680 Semivolatiles Optimization of Extraction Conditions and Fiber Selection for seven different fibers GC-MS 

in water Semivolatile Analytes using SPME 30 min, immersed 

J. Chrom. Sci., Vol. 38, July 2000, 279-288 sat. salt, pH2,7,11 

Shirey, R. 

440 PAHs in Solvent-Free Method for the Determination of PAHs in 100µm PDMS HPLC-PAD 

water Wastewater by SPME-HPLC with Photodiode-Array Detector 45°C, 30 min 

J. Chromatogr. A (1998), 823(1+2), 211-218 stirring 

Negrao, M., Alpenduradu, M. 

26 BTEX compounds Analysis of BTEX in Water by Commercially Available 100µm PDMS GC-FID 

in water SPME and CLOT Column Gas Chromatography 35 min 

J. Chromatogr. 677: 201-205 (1994) stirring 

Sama, L., Webster, G., Friesen-Fisher, M., Ranjai, R. 

30 Nitrobenzenes Determination of the Semi-Volatile Compounds 100µm PDMS GC-FID 

in water Nitrobenzene, Isophorone, 2,4-Dinitrotoluene and 15 min 

2,6-Dinitrotoluene in Water Using SPME with stirring 

Polydimethylsiloxane-Coated Fiber saturated salt 

J. Chromatogr. A Vol 678(2): 313 (1994) 

Horng, J., Huang, S. 

31 VOCs, chloropesticides Rapid Analysis of Environmental Samples Using SPME 100µm PDMS GC-MS 

in water and Narrow Bore Capillary Columns 15 min 

J High Res. Chromatogr. 18(8): 495-499 (1995) stirring 

Shirey, R. saturated salt 

47 BTEX compounds Determination of BTEX Compounds in Water by 100µm PDMS GC-FID 

in water Solid-Phase Microextraction and Raman Spectroscopy 

Anal. Chem. 67(3): 600-605 (1995) 

Wittkamp, B., Tilotta, D. 

681 Volatiles A new method for the rapid determination of volatile 

substances: the SPME-direct method Part 1: Apparatus 

and working conditions 

Sens, Acatuators, B. (2001) B72 (2) 184-187 

Bene, A., Fornage, A., Luisier, J., Pichler, P., Villettaz, J. 





830 Methyl, ethylmercury Direct hydride derivatization of methyl- and ethylmercury GC-MS 

chlorides chlorides in acqueous solution with KBH4 

in water J Environ Sci (China) (2000) 12(3) 275-278 

Jiang Gui-bin; He Bin 

48 Methylmercury Determination of Methymercury in Fish and River Water 100µm PDMS GC-MS 

derivatives Samples Using in situ Sodium Tetraethylborate 10 min 

in water and fish Derivatization Followed by SPME and GC-MS stirring 

J. Chromatogr. 696: 113-122 (1995) headspace 

Cai, Y., Bayona, J. sodium tetraborate 

407 Organomercury SPME and GC-MIP-AED for the Speciation Analysis of 100µm PDMS GC-MIP-AED 

in water and soil Organomercury Compounds 25°C 

J. High Resol. Chromatogr. 1999, 22 (3) 181-182 50 min (immersion) 

Mothes, S., Wennrich, R. 20 min (headspace) 

18 Bismuth III Solid Phase Microextraction of Metal Ions bare, or 100µm PDMS UV / VIS 

in water Microchim. Acta 112: 41-6 (1993) 60 min 460nm 

Otu, E., Pawliszyn, J. immersion 

682 Dimethylarsinic acid Speciation of dimethylarsinic acid and monomethyl- 100µm PDMS GC-MS 

arsonic acid arsonic acid by SPME-GC-ion trap MS 

J. Chromatogr.A 2000, 873(1), 129-135 

40min @20°C 

Mester, Z., Pawliszyn, J. thioglycol methylate derv. 

96 Organo Hg, Sn, Pb Sensitive, Simultaneous Determination of Organomercury 100µm PDMS ICP-MS 

in water Lead, and Tin Compounds with Headspace SPME 10 min 

Capillary GC Combined with Inductively Coupled Plasma MS headspace 

Anal. Chem. 69: 1604-1611 (1997) stirring 

Moens, L., DeSmaele, T., Dams, R., VanDen Broeck, P., pH 5.3 

Sandra, P. NaBEtr derivative 

873 Tin & lead SPME-GC-glow discharge-optical emission detection for GC-OES 

in water tin and lead speciation 

J Anal At Spectrom (2001) 16(4), 376-381 

Orellana-Velado, N.G.; Pereiro, R.; Sanz-Medel, A NaBEtr derivative 

796 Organo Sn Speciation of organotins in environmental samples by FPD, PFPD 

in water SPME-GC: comparison of four specific detectors: MIP-AES 

J. Anal. At. Spectrom (2001) 16(3), 263-269 

Aguerre, S; Lespes, G; Desauziers, V; Potin-Gautier, M 

ICP-MS 

153 Organo Sn, Pb Preconcentration and Determination of Sn- and Pb-Organic GC-AED 

in water Species in Environmental Samples by SPME and GC-AED 

Fresenius’ J. Anal. Chem. 354: 587-91 (1996) 

Tutschiku, S., Mothes, S., Wennrich, R. 

215 Organo Sn Determination of Organotin Compounds in Water Samples GC-MS 

in water by Solid-Phase Microextraction (SPME) and GC-MS 

Ann. Chim. (Rome) 87: 497-504 (1997) 

Guidotti, M., Vitali, M. 

152 Methyltin Rapid Determination of Methyltin Compounds in Aqueous 100µm PDMS GC-FPD 

in water Samples Using SPME and Capillary GC Followed by 29°C, 2-35 min 

in situ Derivatization with Sodium Tetraethylborate headspace 

J. High Res. Chromatogr. 18: 767 (1995) stirring 

Morcillo, Y., Cai, Y., Bayona, J. NaBEtr derivative 

161 Lead derivatives Determination of Tetraethyllead and Inorganic Lead in Water 100µm PDMS GC-MS 

in water by SPME-GC 10 min 

Anal. Chem. 68: 3008 (1996) headspace 

Gorecki, T., Pawliszyn, J. 





683 Lead derivatives Determination of Tetraethyllead by SPME-thermal desorption AA 

in water quartz furnace atomic absorption spectrometry 

J. Anal. At. Spectrom. 2000, 15(16), 705-709 

Sandra Fraguairo, M, AlavapMoreno, F., Isela, B. 

10 min, headspace 

23 Organotin compounds Rapid Determination of Butyl, Phenyl and Cyclohexyl Tin 100µm PDMS GC-FPD 

in water Compounds in Aqueous Samples Using SPME and 30 min 

Capillary Gas Chromatography Following in situ Derivatization immersion 

with Sodium Tetraethylborate stirring 

CID-CSIC Jordi Girona, 18-26, E-8034, Barcelona, Spain 

Morcillo, Y., Cai, Y., Porte, C., Bayona, J. 

NaBEt4 derivative 

503 Organo-tin, -lead, Determination of organometallic compounds in surface 100µm PDMS GC-ICPMS 

-mercury water and sediment samples with SPME-CGC-ICPMS 10 min 

in water Mikrochim. Acta (1999), 130(4), 241-251 

De Smaele, T., Moens, L., Sandra, P., Dams, R. 

headspace 

235 Rare earth elements Separation of Cerium from Other Rare-Earth Elements with 

Application to Samarium-Neodymium and Lanthanum- 

Cerium Chronometry 

Nucl. Instrum. Methods Phys.Res.Sect.B 117: 201-208 (1996) 

Rehkaemper, M., Gaertner, M., Galer, S., Goldstein, S. 

580 Selenite, selenate Selective determination of selenite and selenate using GC-MS 

in water SPME and GC-MS 35 min, agitation 

J-High-Resolut-Chromatogr. Jul 1999; 22(7): 414-416 piazselenol derivative 

Guidotti,-M; Ravaioli,-G; Vitali,-M immersed 

49 Nitroaromatics Enrichment of Nitroaromatic Compounds from Water 

in water Samples by SPME 

GIT Spex Chromatogr. 14: 85-87 (1995) 

Schaefer, B., Engewald, W. 

809 Nitroarenes Analysis of nitroarenes by SPME/GC-Ion trap MS 

Chromatography (2000) 21(2),123-124 

Kataoka, Hiroyuki; Lord, Heather L.; Pawliszyn, Janusz 

GC-MS 

160 Hetero aromatics Trace Analysis of Hetero Aromatic Compounds in 85µm polyacrylate GC-MS 

in water Water by SPME 60-200 min 

J. High Res. Chromatogr. 19(11): 627-632 (1996) stirring 

Johansen, S., Pawliszyn, J. pH 8, salt added 

218 BTEX Determination of Benzene Derivatives in Water by SPME 

in water Anal. Chim. Acta 343: 101-108 (1997) 

Huang, S., Cheng, C., Sung, Y. 

50 Nitrophenols Enrichment of Nitrophenols from Water by Means of SPME 100µm PDMS GC-NPD 

in water Fresenius’ J. Anal. Chem. 352(5): 535-6 (1995) 5 min 

Schafer, B., Engewald, W. stirring 

pH




684 VOCs Determination of volatile organic compounds (VOCs) in 100µm PDMS GC-MS 

in water drinking water using SPME 

Anal. Sci. Technol. (2000) 13(3), 277-281 

Park, G., Lee, S. 

832 VOCs Chemical and microbiological characterization of drinking 100µm PDMS GC-MS 

in water water after filtration with a domestic-size charcoal column 10min. 

and ultraviolet sterilization headspace 

Urban Water (2000) 2(1), 13-20 

Serpieri, N.; Moneti, G.; Pieraccini, G.; Donati, R.; 

Mariottini, E.; Dolara, P 

NaCl added 

82 VOCs An Evaluation of Solid Phase Microextraction for Analysis 100µm PDMS GC-MS 

in water of Volatile Organic Compounds in Drinking Water 20-80°C, 60 min 

J. High Res. Chromatogr. 18: 617-624 (1995) headspace 

Nilsson, T., Ogaard-Madison, J., Montanrilla, L., Larsen, B., 

Facchetti, S., Pelusioj, F. 

stirring 

685 MTBE Determination of MTBE in surface water by use of SPME Carboxen/DVB/PDMS GC-MS 

in surface water Environ, Sci.Technol. (2000), 34(7), 1359-1364 69 min 

Achten, C., Puettmann, W. 25% NaCl, stirred 

935 MTBE Sensitive methods for measuring methyl tert-butyl-ether Carboxen/DVB/PDMS GC-MS 

in surface water in water 69 min 

Umwelt-Technol. Aktuell (2000) 12(1), 22-25 

Achten, C., Puettmann, W. 

25% NaCl, stirred 

686 MTBE, Ethanol, other Trace Analysis of Ethanol, MTBE, and related Oxygenate Carboxen/DVB/PDMS GC-MS 

oxygenates in water Compounds in Water using SPME and GC-MS 25 min immersed 

Anal. Chem. 2000, 72, 4654-4658 stirred 

Cassada, D., Zhang, Y., Snow, D., Spalding, R. Sat. salt, 

910 MTBE, TBE, BTEX High levels of monoaromatic compounds limit the use of 75µm Carboxen/PDMS Ion trap 

in water SPME of MTBE and Tert butyl alcohol 65µm DVB/PDMS GC-MS 

Environ Sci Technol, 2001, 35 (15) 3190-3192 1-25min. 

Black, L., Fine, D. saturated salt 

354 MTBE, EBE, BTEX Analysis of Water Samples for Trace Levels of Oxygenated 75µm Carboxen/PDMS GC-FID 

in water and Aromatic Compounds Using Headspace SPME and 40°C, 10 min 

Comprehensive Two-Dimensional Gas Chromatography headspace 

J. Microcolumn Separations, 10 (7), 597-604 (1998) 

Gaines, R., Ledford, E., Stuart, J. 

saturated salt 

952 MTBE Measurement of Henry's law constant for MTBE using SPME 

in water Environ. Toxicol. Chem (2001), 20(8), 1625-1629 15°-40°C 

Bierwagen, B.G.; Keller, A.A. headspace 

581 Tetrachloroethene Role of humic acids in the titanium oxide-photocatalysed 100µm PDMS GC-MS 

in water degradation of tetrachloroethene in water. 

Water-Res. Jun 1999; 33(8): 1827-1836 

Selli,-E; Baglio,-D; Montanarella,-L; Bidoglio,-G 

175 Trihalomethanes Detection and Quantification of Trihalomethanes in 

in water Drinking Water from Alexandria, Egypt 

Contam. Toxicol. 56: 397-404 (1996) 

Hassan, A., Benfenati, E., Fanelli, R. 

687 Dichlorobenzene Analysis of dichlorobenzene in water by SPME 100um PDMS GC-ECD 

in water J. Chin. Chem. Soc (2000) 47(2) 415-420 30 min 

Liu, Y., Ho, W. 





813 Chloroform Analysis of chloroform in drinking water by 85µm Polyacrylate GC-FID 

in water headspace solid-phase microextraction and GC 45°C 

Fenxi Shiyanshi (2000), 19(5), 65-67 

Liu, Z. L.; Wang, C. H.; Wang, X 

headspace 

858 Chloroform Chloroform formation during kraft pulp bleaching with 

from Kraft pulp bleach chlorine and chlorinated compounds -determination of 

chloroform amounts by solid phase microextraction 

Kami Pa Gikyoshi (2000) 54(11) 1555-1563 

Oi, Hiroshi; Masuzawa, Kiyoshi (Japanese) 

83 Benzene, halobenzene Application of Solid Phase Microextraction (SPME) in GC-FID 

in water Combination with GC/FID: The Determination of Benzene and 

Halogenated Benzenes in Pure and Octanol-Saturated Water 

Chem-Anal (Warsaw) 40: 897-904 (1995) 

Popp, P., Paschke, A., Schroeter, U., Oppermann, G. 

688 Benzene derivatives Matrix effect for several derivatives of benzene in water 

in surface water by SPME 

Chromatographia 2000, 51(suppl.) S328-S330 

Javorszky, E., Molnar, E., Torkos, K. Borossay, J. 

86 Organics Comparison of On-line SPE-HPLC and SPME-GC for HPLC 

in water the Analysis of Microcontaminants in Water 


Rivasseau, C., Caude, M. 

217 Haloethers Determination of Haloethers in Water by SPME 100µm PDMS GC-FID 

in water J. Chromatogr. A 769: 239-246 (1997) 40 min, immersion 

Huang, S., Ting, C., Lin, C. saturated salt 

586 Trichlorofluoroether Anaerobic biotransformation of trichlorofluoroethene in 100µm PDMS GC-MS 

in water groundwater microcosms. headspace 

Environ-Sci-Technol. 15 Jun 1999; 33(12): 2040-2045 salt, agitation 

Vancheeswaran,-S; Hyman,-MR; Semprini,-L 

90 Aromatics Determination of Volatile Organic Compounds in Water parafilm, GC-FID 

in water by Solid Phase Micro-Extraction and Infrared Spectroscopy 30 min 

Environ. Sci. Technol. 30: 1212-1219 (1996) 

Heglund, D., Tilotta, D. 

926 Poly(dimethylsiloxane) films as sorbent for SPME couple PDMS IR 

infrared spectroscopy 

J. Chromatogr. A (1998), 829(1-2) 377-384 

Merschman, S., Lubbad, S., Tilotta, D. 

942 Volatile organics Development of headspace SPME/attenuated total reflection IR 

in water infrared chemical sensing method for the determination o 

of volatile organic compounds in aqueous solutions headspace 

Analytica Chimica Acta (2001), 436(1), 31-40 

Yang, Jyisy; Tsai, Shu-Sha 

505 Hydroxyaromatics Determination of hydroxyaromatic compounds in water by PDMS/DVB or CW-TPR HPLC 

in water SPME coupled to HPLC 

J. Chromatogr. A. (1999), 835(1+2), 127-135 

Wu, Y., Huang, S. 

280nm 

229 71 organics Calibration of a Commercial Solid-Phase Microextraction 100µm PDMS GC-FID 

in gaseous mixture Device for Measuring Headspace Concentrations of 25°C, 30 min 

Organic Volatiles 

Anal. Chem. 69: 364-372 (1997) 

Bartlet, R. 

headspace 





155 VOCs Sampling Volatile Organic Compounds Using a Modified 100µm PDMS GC-MS 

in water Solid Phase Microextraction Device 10 min 

J High Res. Chromatogr. 19(3): 155-60 (1996) headspace 

Zhang, Z., Pawliszyn, J. stirring, saturated salt 

205 Volatiles Solid Phase Microextraction of Volatile Compounds Using 75µm Carboxen/PDMS GC-FID, ECD 

in water Carboxen-Polydimethylsiloxane Fibers 30 min 

Chromatographia 46: 419-424 (1997) headspace 

Popp, P., Paschke, A. stirring 

240 Volatiles Application of Solid-Phase Microextraction to the Analysis 100µm PDMS, GC-FID 

in water of Volatile Organic Compounds in Water 85µm polyacrylate 

J. Chromatogr. A 742: 181-189 (1996) 12 min 

Santos, F., Galceran, M., Fraisse, D. stirring 

689 BTEX Static headspace, SOME and headspace SPME for BTEX 100µm PDMS GC-FID 

in water determination in aqueous samples by GC 

Anal. Chim. Acta. 2000, 415(1-2), 9-20 

Menendex, J., Sanchez, M., Uria, J., Martinez, E., Medel, A. 

506 BTEX in In-tube SPME-GC of volatile compounds in aqueous solution 1 meter capillary GC-FID 

water Analyst (Cambridge, UK), 1999, 124(5), 651-655 

Tan, B, Marriott, P., Morrison, P., Lee, H. 

117 Solvents, C2-C4 acids Carbon Isotope Analysis of Semivolatile Organic Compounds polyacrylate, Carbowax, GC-MS 

in water in Aqueous Media Using SPME and Isotope Ratio cyclodextrin 

Monitoring GC/MS 10-30 min 

Anal. Chem. 69: 944-950 (1997) 

Dias, R., Freeman, K. 

stirring 

225 Organochlorine Application of Solid-Phase Microextraction to the Headspace 100µm PDMS GC-ELCD 

semivolatiles in water GC Analysis of Semivolatile Organochlorine 87°C, 45 min 

Contaminants in Aqueous Matrices headspace & 

J. Chromatogr. A 757: 173-182 (1997) immersion 

Page, B., Lacroix, G. salt added 

507 Polar organics Analysis of organochlorine compounds in water by SPME/GC 100µm PDMS GC-ECD 

in water Fenxi Huaxue, 1999, 27(7), 768-772 70°C, headspace 

Zhang, D, Zhou, Z., Tang, Y., Wu, C., Zhen, W. Xu, Y. Chinese 

151 BTEX Protocol for the Analysis of High Concentrations of Benzene, 100µm PDMS GC-FID 

in water Toluene, Ethylbenzene, and Xylene Isomers in Water Using 5 min 

Automated SPME-GC-FID 

Environ. Sci. Technol. 30: 1521 (1996) 

Thomas, S., Ranjan, S., Webster, G., Sarna, L. 

immersion 

154 Organics Solid Phase Microextraction Coupled to GC: A New Method various fibers GC-MS, AED 

in water for the Analysis of Organics in Water 

J. Chromatogr. A 733: 143 (1996) 

Eisert, R., Levson, K. 


909 Endocrine Column siylation method for determining endocrine 

disruptors disruptors from environmental water samples by SPME 

in water Talanta 2001, 54(6) 1039-1047 

Helaleh, M., Fujii, S., Korenaga, T. 

767 Ibuprofen, NBBS Elimination of Ibuprofen and NBBS in municipal purification 

in water plant analyzed by SPME 

Schiftenr (1999), 95, 1-148 

Huppert, N. (in german) 





162 Surfactants SPME Coupled with HPLC for Determination of Alkylphenol Carbowax/TPR 100 HPLC 

in water Ethoxylate Surfactants in Water 50 min UV, 220nm 

Anal. Chem. 68: 1521-9 (1996) immersion 

Boyd-Boland, A., Pawliszyn, J. stirring 

897 Surfactant Identification of alkyl dimethylbenzylammonium surfactants LC/MS 

in water in water samples by SPME followed by ion trap 

LC/MS and LC/MS/MS 

Environ. Sci. Technol 92001) 35(12) 2583-2588 

Ferrer, Imma; Furlong, Edward 

690 Surfactant Identification and characterization of Fenton oxidation 

in water products of surfactants by EMS and SPME-GC-MS 

Fatty alcohol polyethoxy sulfates. 

Rapid Commun, Mass Spectrom 2000, 14(10), 834-839 

Cuzzola, A., Raffaelli, A., Saba, A., Salvadori, P. 

928 Surfactant Assessment of polycystalline graphites as sorbents for 

in water SPME of nonionic surfactants 

J. Chromatogr. A (2000) 888(1-2) 35-41 

Aranda, R., Kruus, P., Burk, R. 

508 Diethylphthalate Trace determination of diethylphthalate in aqueous media 60µm DVB/PDMS HPLC 

in water by SPME-HPLC 15 min immersed UV, 226nm 

J. Chromatogr. A 841(1999) 177-185 

Kelly, M., Larroque, M. 

NaCl 

804 Phthalic diesters Determination of phthalic diesters in water by solid-phase 100µm PDMS 

in water microextraction-capillary gas chromatography 

Sepu (2000) 18(6), 568-570 headspace 

Liu, Z. L.; Xiao, C. H.; Wu, C. Y.; Han, H. M. (in Chinese) 

588 Phthalates esters In-tube SPME-LC analysis of phthalate esters in 40m x 0.25mm capillary HPLC 

in water water samples 

Chromatography. Jun 1999; 20(2): 124-125 

Saito,-Y; Nakao,-Y; Jinno,-K 

782 Butylphthalates Fiber-in-tube solid-phase microextraction: a fibrous rigid-rod HPLC 

in water heterocyclic polymer as the extraction medium 

Fresenius' J AnalChem (2000) 368(7), 641-643 

Saito, Y.; Nakao, Y.; Imaizumi, M.; Takeichi, T.; Kiso, Y.; Jinno, K 

20min. 

691 Phthalates esters Determination of phthalate esters in water samples by 85µm polyacrylate GC-MS 

in water SPME and GC with mass spectrometric detection 90min @ 45°C 

J. Chromatogr. A (2000), 872 (1&2), 191-201 

Penalver, A., Pocurull, E, Borrull, F., Marce, R. 

NaCl added 

801 Phthalates esters Methods for routine analysis of phthalates in food GC-FID/MS 

in water and the environment 

Deutsche Lebensmittel-Rundschau (2000) 96(11), 411-417 

Baerwinkel, D.; Haufe, J.; Kroh, L. W 

178 4-Nonylphenol Determination of 4-Nonylphenol. Part 2: Orthogonal Array 100µm PDMS GC-FID 

in sea water Design as a Chemometric Method for the SPME of 30 min 

4-Nonylphenol in Water immersion 

J. Microcolumn Sep. 8 (2): 131-136 (1996) 

Chee, K., Wong, M., Lee, H. 

stirring 

219 BTEX Direct Solid Phase Microextraction for the Determination 100µm PDMS GC-FID 

in water of BTEX in Water and Waste Water 10 min 


Valor, I., Cortada, C., Molto, J. 

stirring 





208 BTEX compounds A New Porous-Layer Activated-Charcoal-Coated Fused 100µm charcoal coated GC-FID 

in water Silica Fibre: Application for Determination of BTEX fiber / PDMS 

Compounds in Water Samples Using Headspace SPME and 25°C, 15 min 

Capillary Gas Chromatography stirring 


Djozan, D., Assadi, Y. 

salt added 

169 Chlorinated Analysis of Chlorinated 1,3-Butadienes by SPME and GC-MS 100µm PDMS GC-MS 

1,3-butadienes J. Chromatogr. A 737: 85-91 (1996) 30 min 

in water Fattore, E., Benfenati, E., Fanelli, R. immersion 

692 Styrene SPME method for the quantitative analysis of styrene in water 85µm polyacrylate GC-FID 

in water J. Chromatogr.Sci. (2000), 38(7), 315-318 10mn @ 55°C 

Silva, F., DeCarvalho, C., Cardeal, Z. headspace 

776 Dioxin, Furans Determination of dioxins and furans in water sample by GC-MS 

in water HRGC/HRMS and pretreatment using SPME 

Organohalogen Compd (2000) 45, 68-71 

Eom, S; Ahn, So; Kim, M; Shin, J 

170 Semivolatiles Trends in Extraction of Semivolatile Compounds from Water 

in water for Environmental Analysis 

Anal. Commun. 33 (9): 15H-17H 

Poole, S., Poole, C. 

509 Semivolatiles Studies of the composition of distillates from leachate by GC-ms 

in water GC-MS coupled to SPME pH 4 or 10 

Rapid Commun. Mass Spectrom (1999), 13(10), 966-970 

Saba, A., Pucci, S., Raffaekki, A., Salvadori, P. 

headspace/immersed 

807 Petroleum Application of SPME chromatography with mass 

hydrocarbons spectrometry to the analysis of gasoline content in water 

in water Huaxue Fence (2000) 36(10) 465-466 

Chen, X. D.; Zhou, H (in chinese) 

216 Petroleum Water Analysis by Solid-Phase Microextraction Based on 100µm PDMS GC-FID 

hydrocarbons Physical Chemical Properties of the Coating 30 min 

in water Anal. Chem. 69(11): 1992-1998 (1997) headspace 

Saraullo, A., Martos, P., Pawliszyn, J. stirring 

272 BTEX Application Methods of SPME for the Classification of BTEX 

GIT Labor-Fachz. 41 (12): 1191-1195 (1997) 

Van der Heide, M., Petry, P. 

273 SPME as a Method for Preparing Environmental Samples 

Pol. J. Environ. Stud. 6 (5): 5-12 (1997) 

Ligor, M., Buszewski, B. 

274 SPME in Pretreatment of Environmental Samples 

Huaxue Jinzhan 10 (1): 74-84(1998) 

Jia, J., He, Y., Huang, J. 

275 Aqueous samples Direct SPME of Complex Aqueous Samples with Hollow 

Fiber Membrane Protection 

Anal. Commun. 33 (7): 219-221(1996) 

Zhang, Z., Poerschmann, J., Pawliszyn, J. 

693 Alkanes, PCBs,PAHs Sorption of very hydrophobic organic compounds onto 7um, 30um PDMS GC-MS 

in humic material PDMS and dissolve humic organic matter. 1. Adsorption or 20 min SIMS 

partitioning of VHOC on PDMS coated SPME fibers- stirring 

never-ending story 

Environ Sci Technol 2000, 34, 3824-3830 

Poerschmann, J., Gorecki, T., Kopinke, G. 





844 Hydrophobic organics Sorption of hydrophobic organic compounds on nonpolar PDMS, polyacrylate GC-MS 

in humic material SPME fibres and dissolved humic organic matter long dash 

Part III: Application of the solubility parameter concept to 

interpret sorption on SPME fibre coatings 

J Microcolumn Separations (2000) 12(12), 603-612 

Poerschmann, J. 

923 Use of SPME for measuring oil-water partition coefficients and 

correlation with HPLC methods for lipophilicity 

J. Chromatogr A (1999) 864(2) 183-189 

Pollein, P., Roberts, D. 

HPLC 

276 Phenols, PAHs SPME for Determining Distribution of Chemicals in 100µm PDMS GC-MS 

in wastewater Aqueous Matrixes 10 sec 

Anal. Chem. 69 (4): 597-600 (1997) 

Zhang, A., Kopinke, G., Pawliszyn, J. 

stirring 

277 Chlorinated organics Water Solubility and Octanol/Water-Partitioning of 

in water Hydrophobic Chlorinate Organic Substances Determined 

by Using SPME/GC 

Fresenius’ J. Anal. Chem. 360 (1): 52-57 (1998) 

Paschke, A., Popp, P. 

278 Phenols Determination of Phenols by Solid-Phase Microextraction 85µm polyacrylate GC-FID 

in water J. Chromatogr. A 767 (1+2): 171-175 (1997) 25°C, 60 min 

Bartak, P., Cap, L. headspace 

pH 1, salt added 

439 Chlorophenols Determination of Chlorophenols Using SPME and GC/MS 

in water Ann. Chim. (Rome) (1998), 88(9-10), 629-635 

Guidotti, M., Ravaioli, G. GC-MS 

777 Organics Solid phase extraction techniques for drinking water GC-MS 

in drinking water abstraction monitoring and investigation of pollution 

incidents 

J Water Supply Res and Tech (2000) 49(2), 103-109 

Gardner, M.; Comber, S. ; Rogers, H. 

944 Organics Determination of water contaminants at trace levels using 

in water large volume sampling techniques: Comparison of LVPTVI, 

LVOCI, and SPME. 

American Laboratory (2001) 33(11), 45-47 

Trisciani, A.; Munari, F.; Anelli, L.; Castanho, J. 

279 VOCs Pollution of Ground and Drinking Water with Volatile GC-MS 

in water Organic Compounds, SPME and GC/MS Analysis 

Toxicol. Environ. Chem. 55 (1-4): 73-81 (1996) 

Hassan, A., Benfenati, E., Facchini, G., Fanelli, R. 

280 Trihalomethanes Determination of Trihalomethanes in Drinking Water by GC-ECD 

in water SPME-GC with Electron-Capture Detection 

Toxicol. Environ. Chem. 60(1-14): 39-45 (1997) 

Chen, M., Mao, I., Hsu, C. 

281 Chloroacetic acid esters Determination of Chlorinated Acetic Acids in Drinking 30µm PDMS GC-ECD 

in water Water by in situ Derivatization and Solid Phase 1 min 

Microextraction headspace 

Int. J. Environ. Anal. Chem. 66 (3): 215-224(1997) stirring 

Aikawa, B., Burk, R. methanolic HCl added 





510 Sulfur compounds in Studies on the application of SPME for analysis of volatile FPD-GC 

water, N2 & propane organic sulfur compounds in gaseous and liquid samples 

Chem. Anal. (Warsaw), 1999, 44(3A), 485-493 

Wardencki, W., Namiesnik, J. 

339 Geosmin, 2-MIB Rapid Analysis of Geosmin and 2-Methylisoborneol in Water 100µm PDMS GC-MS 

in water Using SPME Procedures 40°C, 30 min 

Water Research Vol. 32, No. 7, 2140-2146 (1998 headspace, stirring 

Lloyd, S., Lea, J., Zimba, P., Grimm, C. salt added 

362 2-MIB, geosmin Analysis of 2-Methylisoboreneol and Geosmin in Catfish 100µm PDMS GC-MS 

in catfish by Microwave Distillation-SPME 40°C, 30 min 

J. Agri. Food Chem., 47, No. 1, pg. 164-169, 1999 headspace, stirring 

Lloyd, S., Grimm, C. salt added 

446 MIB & geosmin Determination of Geosmin and 2-Methylisoboreneol in Water 80µm Carboxen/DVB/PDMS GC-MS 

in water Using SPME and GC-Chemical Ionization/Electron Impact 60°C, 30 min 

Ionization Ion Trap MS headspace 

Analyst (Cambridge, U.K.) (1998), 123 (10), 2155-2160 stirring 

McCallum, R., Pendleton, P., Scumann, R., Trinh, M. salt added 

511 34 Odor compounds Headspace SPME for the determination of trace levels of 65µm DVB/PDMS GC-Ion trap 

in water taste and odor compounds in water samples 40 min @ 20°C MS 

Analyst (Cambridge, UK) 1999, 123(4), 459-466 NaCl, stirring 

Bao, M., Mascini, M., Griffini, O., Burrini, D., Santianni, D., 

Barbieri, K. 

immersion/headspace 

282 Chemical warfare On-Site Sample Work-Up Procedures to Isolate Chemical 

compounds Warfare-Related Compounds, Using SPE & SPME Technology 

Analytical Chemistry Associated with the Destruction of 

Chemical Weapons NATO ASI Ser., Ser. 1 13: 65-76 (1997) 

Alcaraz, A., Hulsey, S., Whipple, R., Andresen, B. 

116 Nerve agents Determination of Chemical Warfare Agents in Natural 65µm PDMS/DVB GC-FID 

in water Water Samples by SPME 30 min GC-MS 

Anal. Chem. 69: 1866-1872 (1997) headspace 

Lakso, H., Ng, W. saturated salt 

762 Lewisite oxide Determination of Lewisite oxide in soil using SPME 100µm PDMS GC-FPD/or 

in soil followed by GC w/FPD or Mass spectormetric detection 20min. GC-MS 

J. Chromatogr-A, 909 (2001) 13-28 agitated 

Tomkin, B., Sega, G., Ho, C. 1,3-propanedithiol derv. 

560 Chemical warfare In-situ derivatisation of degradation products of chemical 65µm Carboxen/PDMS GC-MS 

agents in water warfare agents in water by SPME and GC-MS analysis 20°C, 

J. Chromatogr-A, Feb 1999, 832(1+2), 173-182 N-methyl-N-(tert-butyl 

Sng, M., Ng., W. dimethylsilyl) trifluoroacetamide 

derivative 

283 Volatiles Rapid Determination of Volatile Organic Compounds in 

in wastewater Environmentally Hazardous Wastewaters, Using SPME 

Anal. Chem. 358 (7-8): 833-837 (1997) 

James, K., Stack, M. 

284 TNT, DNT salt Trace salt Signatures from World War II 65µm PDMS/DVB directly 

in seawater/ Unexploded Undersea Ordinance 15 min into MS 

sediment Environ. Sci. Technol. 32 (9): 1354-1358 (1998) pH 8 

Darrach, M., Chutjian, A., Plett, G. agitation 





285 Aromatic amines Determination of Aromatic Amines by SPME-GC-MS 65µm Carbowax/DVB GC-MS 

in water in Water Samples 30 min 

J. Chromatogr. A 791(1+2): 221-230 (1997) stirring 

Muller, L., Fattore, E., Benfenati, E. pH 7.6, salt added 

578 Aromatic amines SPME coupled with HPLC for the determination of 65µm PDMS/DVB, CW-TPR HPLC-UV 

in water aromatic amines. 

Anal-Chem. 15 Jan 1999; 71(2): 310-318 

Wu,-Y-C; Huang,-S-D 

280nm 

286 Volatiles Inter-Laboratory Studies for the Validation of SPME for 100µm PDMS GC-ECD 

in water the Quantitative Analysis of Volatile Organic Compounds 30 min 

Compounds in Aqueous Samples headspace & 

Anal. Chim. Acta 356 (2-3): 113-123 (1997) immersion 

Nilsson, T., Ferrari, R., Facchetti, S. stirring 

597 Volatiles (BTEX) Solid-phase micro-extraction of volatiles from water 100µm PDMS GC-FID 

in water using open cap vials 5 min. @ 25C 

Chromatographia. May 1999; 49(9-10): 513-519 

Matisova,-E; Sedlakova,-J; Simon,-P; Welsch,-T 

stirred 

287 VOCs, pesticides Capabilities for the Direct Determination of Triphenyl- Carboxen/PDMS, GC-MS 

in water and air and Triethylarsine in Water by SPME Followed by GC-A 100µm PDMS 

Amer. Environ. Lab, 9 (10): cover, 5-6 (1997) 

Mothes, S., Wennrich. R. 

various conditions 

374 Organoarsenicals Determination of Organoarsenicals in the Environment by 100µm PDMS GC-MS 

in water and soil SPME-GC-MS 10 min 

J. Chromatogr. A 807 (1998) 253-263 immersion 

Szostek, B., Aldstadt, J. methyl thioglycolate 

(derivative) 

879 Organoarsenicals SPME method for GC w/MS and pulsed Flame photometric 100µm PDMS GC-MS 

in water detection: studies of organoarsenical speciation 10 min GC- PFPD 

J. Chromatogr. A 918(2001) 169-175 immersion 

Killelea, D., Aldstadt, J. methyl thioglycolate 

(derivative) 

790 Organoarsenicals Speciation of organoarsenic compounds by poly(pyrrole)- Polypyrrol capillary LC-EI-MS 

in water coated capillary in-tube SPME coupled with HPLC-EI-MS 


Wu, J. C.; Mester, Z.; Pawliszyn, J. 

815 Metal hydrides Sampling and determination of metal hydrides by SPME Carboxen/PDMS, ICP-MS 

in water thermal desorption inductively coupled plasma MS 

J. Analytical Atomic Spectrometry (2000) 15(11) 1461-1465 

Mester, Z.; Sturgeon, R. E.; Lam, J. W 

Sodium Borohydride/HCl 

288 Iodinated volatiles SPME with Temperature-Programmed Desorption for the 85µm polyacrylate GC-ECD 

in water Analysis of Iodinated Disinfection Byproducts 15 min 

Anal. Chem. 70 (3): 638-644 (1998) immersion 

Frazey, P., Barkley, R., Siever, R. stirring 

289 Chloroethers Determination of Chloroethers in Aqueous Samples, GC-FID or MS 

in water Using SPME 

Acta Hydrochim. Hydrobio. 25 (6): 329-334 (1997) 

Wennrich, L., Engewald, W., Popp, P. 

513 Chloroethers GC trace analysis of haloethers in water: Comparison of GC-FID or MS 

in water different extraction techniques 

Int. J. Environ.Anal. Chem (1999), 73(1), 31-41 

Wennrich, L., Engewald, W., Popp, P. 





514 Aliphatic aldehydes Influence of extraction parameters and medium on efficiency 100µm PDMS GC-MSD 

in water/oil of SPME sampling in analysis of aliphatic aldehydes 30 min @ 40°C 

J. Chromatogr., A 1999, 845(1+2), 337-347 

Keszler, A., heberger, K. 

immersed/headspace 

515 Glycerol ethers Improved extraction of glycerol ethers from water by SPME 75µm Carboxen/PDMS GC-FID 

in water by Carboxen-PDMS coated fiber 25°C, sat. NaCl 

Chromatogrophia, 1999, 50 (3/4), 155-159 

Bensoam, J., Cicolella, A., Durjardin, R. 

immersed 

516 Amines/alcohols Evaluation of SPME for the anlaysis of hydophilic 75µm Carboxen/PDMS 

in water compounds 

J. Exposure Anal.Environ. Epidemiol. 1999, 9(3) 181-191 

Shoemaker, J. Munch, J., Behmer, T. 

517 Polar volatiles SPME of volatile polar compounds in water 85µm polyacrylate GC-MS 

in water J. High Resolut. Chromatogr. (1999), 22(2), 109-115 50°C 

Matisova, E, Sedlakova, J., Slezackova, M., Welsch, T. headspace 

290 VOCs, pesticides On-Site Sampling for Volatiles and Pesticides, Using SPME 100µm PDMS, GC-MS 

in water and air Amer. Environ. Lab. 10 (2): 21-22 (1998) 75µm Carboxen/PDMS 

Shirey, R., Mani, V, Mindrup, R. 2-3 min, headspace 

stirring, salt added 

291 Petroleum Solvent-Free and Rapid Determination of Petroleum 

hydrocarbons Hydrocarbons in Water by SPME 

in water UFZ-Ber. Optimierung Umweltvertiraeglicher 

Analysenverfahren fuer Mineraloelkohlenwasserstoff 

IM Boden 12: 14-17 (1997) 

Christall, B. 

367 C3-C16 hydrocarbons Partition Infrared Method for Total Gasoline Range Organics 130µm Teflon film IR 4000-2690 

in water in Water Based on SPME 30 min cm-1 

Environ. Sci. Technol, 1999, 33, 814-819 

Stahl, D., Tilotta, D. 

immersion 

518 MMT in Determination of methylcyclopentadienylmanganese 100µm PDMS GC-AED 

water tricarbonyl (MMT) in aqueous samples by SPME-GC-AED 15 min @ 20°C 

Analyst (Cambridge, UK), (1999), 124(1), 71-73 

Yang, F., Chau, Y. 

headspace 

849 MMT in Determination of methylcyclopentadienylmanganesel GC-AED 

water tricarbonyl by SPME-direct thermal desorption-quartz 

furnace atomic absorption spectrometry 

Spectrochim. Acta, Part B (2001) 56B(2) 215-222 

Fragueiro, M. S.; Alava-Moreno, F.; Lavilla, I.; Bendicho, C 

519 VOCs, BTEX, Efficiency of direct SPME from water: Comparison of variety of fibers 

pesticides, PCBs different fiber types including a new C8-coating 

from water Chromatographia, 1999, 49(11/12), 686-690 

Popp, P., Paschke, A. 

904 pesticides Analysis of fire ant pesticides in water by SPME and GC-MS GC-MS & 

in water and LC-MS 

Analytica Chimica Acta 2001, 436(1) 11-20 

Reyzer, M., Brodbelt, J. 

LC-MS 

770 Chlorine, nitrogen Multiresidual method for determination of chlorine, GC/ECD/NPD 

phosphorus nitrogen, and phosphorus containing pesticides in surface 

pesticides and drinking water by SPME and GC/ECD/NPD 

in water Boll. Chim. Ig., Parte Sci. (2000) 51(S3), 99-103 

de Luca, Giuseppe; Mura, Michele (in Italian) 





512 Iodinated THMs SPME for the determination of iodinated trihalomethanes in 65µm CW/DVB/PDMS GC-ECD 

in drinking water drinking water 10 min @ 20°C 

J. Chromatogr., A (1999), 841(2), 197-206 

Cancho, B., Ventura, G., Galceran, M. 

NaCl used 

292 Iodinated organics Solid Phase Microextraction and Analysis of Iodinated 85µm polyacrylate GC-ECD 

in water Organic Compounds 

Avail. UMI, Order No. DA9812871 from: 

Diss. Abstr. Int., B 58 (10): 5364 (1998) 

Frazey, P. 

288 Iodinated volatiles SPME with Temperature-Programmed Desorption for the 85µm polyacrylate GC-ECD 

in water Analysis of Iodinated Disinfection Byproducts 15 min 

Anal. Chem. 70 (3): 638-644 (1998) immersion 

Frazey, P., Barkley, R., Siever, R. stirring 

694 Cyanogen chloride Simultaneous determination of cyanogen chloride and Carboxen/DVB/PDMS GC-ECD 

in water cyanogen bromide in treated water at sub-ug/L levels by a 15 min, headspace 

new SPME-GC-ECD method 2-3pH, 25% salt added 

J. Chromatogr. A 897(2000) 307-315 

Cancho, B., Ventura, F., Galceran, M. 

695 Acetic acid Determination of acetic acid in aqueous samples, by 85µm Polyacrylate GC-FID 

in water water-phase derivatization, SPME, and GC headspace 

J. Chromatogr. A., (2000), 874(2), 225-234 benzenal bromide derv. 

Wittmann, G., Van Langenhove, H., Dewulf, J. 

411 Chloroacetic acids Determinationof Chlorinated Acetic Acids in Drinking 

in water Water by in-situ Derivatization-SPME 

Interri J. Environ. Anal. Chem. 66: 215-224 (1997) 

Aikawa, B., Burk, R. 

520 Haloacetic acids SPME coupled with GC-ion trap mass spectrometry for the GC-Iontrap 

in water analysis of haloacetic acids in water MS 

J. Chromatogr., A 1999, 859(2), 159-172 

Sarridon, M., Santos, F., Galceran, M. 

696 Haloacetic acids In situ derivatization/SPME for the determination of Carboxen/PDMS GC-ITMS 

in water haloacetic acids in water 

Anal. Chem. 2000 Oct. 15, 72(20), 4865-4873 headspace 

Sarrion, M. Santos, F., Galceran, M. dimethyl sulfate derv. 

353 Chlorobenzenes Using SPME to Determine Partition Coefficients to Humic Acids 7µm PDMS GC-FID 

in water and Bioavailable Concentrations of Hydrophobic Chemicals 20 min 

Environ.Sci Technol, 1998, 32, 3430-3435 immersion 

Ramos, E., Meijer, S., Vaes, W., Verhaar, H., Hermens, J. pH 7 

576 Chlorobenzenes SPME-capillary GC determination of chlorobenzene 100µm PDMS GC-ECD 

in water compounds in water 5 min, agitated 

Lihua-Jianyan,-Huaxue-Fence. Mar 1999; 35(3): 103-105 0.5gm NaOH 

Yang,-HB immersed 

697 Chlorinated Trace analysis of ten chlorinated benzenes in water 100µm PDMS GC-MS 

benzenes in by headspace SPME headspace 

water J. Chromatogr. A (2000) 874(1), 149-154 

He, Y., Wang, Y., Lee, H. 

salt, agitated 

698 Fungicides Determination of fungicides in natural waters using SPME and 100µm PDMS GC-MS 

in water GC coupled with ECD and MS detection 30 min, agitated 

J. Chromatorgr A., 893 (2000), 143-156 20% NaCl, pH 4 

Lambropoulou, D., Konstantinou, I., Albanis, T. immersed 

699 Chlorothalonil Determination of aqueous chlorothalonil with SPME-GC 100µm PDMS GC-ECD 

in water J. Chromatogr. A, 896 (2000) 105-110 

Chen, S., Su, Y., Jen, J. 

40 min, 





800 Alachlor Optimization of alachlor solid-phase micro-extraction from 60µm PDMS/DVB HPLC 

in water water samples using experimental design. 120min @ 25°C 

J. Chromatogr. A (2000) 896(1-2), 373-379 

Gonzalez-Barreiro, C.; Lores, M.; Casais, M. C.; Cela, R. 

stirred 

293 Acidic herbicides Gas-Phase Post-Derivatization Following SPME for 85µm polyacrylate GC-MS 

in water Determining Acidic Herbicides in Water 50 min 

Anal. Chem. 70 (9): 1963-1968 (1998) immersion, stirring 

Lee, M., Lee, R., Lin, Y., Chen, C., Hwang, B. pH 1, salt added 

diazomethane (deriv.) 

905 Acidic herbicides Derivatisation/SPME followed by GC-MS for the analysis GC-MS 

in water of phenoxy acid herbicieds in aqueous samples 

J. Chromatogr. A (1998),826(2), 211-216 

Nilsson, T., Baglio, D., Miguez, I., Madsen, J., Facchetti, S. 

898 Acidic herbicides Automated on-line in-tube SPME followed by LC/electrospray LC-MS 

in water ionization mass spectrometry for the determination of 

chlorinated phenoxy acid herbicides in environmental waters 

Analyst (Cambridge, U. K.) 2001 , 126(5) 602-608 

Takino, Masahiko; Daishima, Shigeki; Nakahara, Taketoshi 

763 Profoxydim Application of on-site SPME in aquatic dissipation studies 50µm Carbowax-TPR HPLC-UV 

in water of profoxydim in rice 30min. 

J. Chromatogr A, 909 (2001) 29-36 salt added 

Eisert, R, Jackson, S., Krotzky, A. immersed 

521 Fungicides SPME of the antifouling Irgarol 1051 and fungicides 85µm polyacrylate GC-MS 

in water dichlofluanid and 4-chloro-3-methylphenol in water samples 1 hr. @ 60°C 

J. Chromatogr. A, (1999), 839(1+2), 253-260 

Penalver, A., Pocurull, E., Borrull, F., Marce, R. 

immersion, salt added 

568 T2 mycotoxin Determination of trichothecene (T2 mycotoxin) in aqueous 85µm polyacrylate GC-FID 

in water sample with solid-phase microextraction technique 75 min, immersed 

followed by GC-FID satr. salt 

J-High-Resolut-Chromatogr. Jul 1999; 22(7): 424-426 

Lee,-PK; Kee,-SYK; Ng,-W; Gopalakrishnakone,-P 

stirred 

294 PAHs SPME of PAHs from Aqueous Samples, Using Fibers Coated 100µm silica/epoxy GC-FID, -MS 

in water with HPLC Chemically Bonded Silica Stationary Phases 60°C, 30 min 

Anal. Chem. 69 (24): 5001-5005 (1997) 

Liu, Y., Lee, M., Hageman, K., Yang, Y, Hawthorne, S. 

headspace 

295 PAHs Separation and Determination of Polycyclic Aromatic 

Hydrocarbons by SPME/Cyclodextrin-Modified Capillary 

Electrophoresis 

Anal. Chem. 69 (9): 1726-1731 (1997) 

Nguye, A., Luong, J. 

700 PAHs Monitoring of PAH in water using headspace SPME 

in water and capillary GC 

Microchem J. (1999), 63(2), 276-284 

Djozan, D., Assadi, Y. 

701 PAHs SPME for determining the distribution of sixteen USEPA 

in water polycyclic aromatic hydrocarbons in water samples 

J. Chromatogr. A. (2000) 879, 177 

Doong, R., Chang, S., Sun, Y. 





296 Aromatics Determination of Aromatic Compounds in Water by SPME PDMS chip UV spectroscopy 

in water and Ultraviolet Absorption Spectroscopy 30-50 min 220-300nm 

Anal. Chem. 69 (1): 1197-1203 (1997) 

Wittkamp, B., Hawthorne, S., Tilotta, D. 

immersion 

344 RDX, TNT metabolites Trace Analysis of salt in Seawater Using SPME and Carbowax/DVB GC-MS 

in salt water GC-Ion Trap Mass Spectrometry 10 min 

Anal. Chem., Vol. 70, No. 14, July 15, 1998, pg. 3015-3020 immersion 

Barshick, S., Griest, W. stirring 

297 Phthalates, surfactants Characterization of Water-Soluble Components of Slurries 65µm Carbowax/TPR LC-MS 

in water Using SPME Coupled to LC-MS 1-15 hr. 

J. Microcolumn Sep. 10 (2): 225-234 (1998) pH 2, satr. salt 

Moder, M., Popp, P., Pawliszyn, J. 

598 Organophosphorus Comparative studies of the leachate of an industrial landfill GC-MS 

compounds by GC-MS,LC-nuclear magnetic resonance and LC-MS 

in leachate J-Chromatogr,-A. 29 Jan 1999; 831(2): 243-256 

Benfenati,-E; Pierucci,-P; Fanelli,-R; Preiss,-A 

Godejohann,-M; Astratov,-M; Levsen,-K; Barcelo,-D 

702 Fatty acids Development of a headspace SPME procedure for the 85µm Carboxen/PDMS GC-FID, MS 

in waste water determination of free volatile fatty acids in waste water headspace 

J Chromatogr. A,(2000) 873(1), 107-115 stirring 

Abalos, M., Bayona, J., Pawliszyn, J. 

703 Fatty acids Application of GC coupled to chemical ionisation MS following 85µm Carboxen/PDMS GC-CI-MS 

in water headspace SPME for the determination of free volatile 20 min headspace 

fatty acids in aqueous samples. 

J. Chromatogr. A 891 (2000) 387-294 

Abalos, M., Bayona, J. 

3.75 g NaCl, pH 1.5 

593 Fatty acids Analysis of volatile fatty acids in waste water 65µm Carbowax/DVB GC-MS 

in waste water collected from a pig farm by a SPME method. 20 min 

Chemosphere. Feb 1999; 38(4): 823-834 immersion 

Yo,-S-P stirred 

913 Aromatic acids/bases SPME with pH adjustment for the determination of aromatic 

in water acids and bases in water 

J. Chromatogr. A (1998) 829(1-2) 223-233 

van Doorn, H., Grabanski, C., Miller, D., Hawthorne, S. 

704 Volatile, Solid Phase microextraction: a promising technique for review article 

semivolatiles sample preparation in environmental analysis 

in water & soil J. Chromatogr. A 889 (2000) 3-14 

Alpendurada, M. 

972 Alkyl sulfides in water Determination of volatile alkyl sulfides in wastewater. 

J.Chromatogr. A (2002) 963(1-2), 249-257 

Abalos, M.; Prieto, X.; Bayona, J.M. 

PDMS/carboxen GC-MS 

975 MTBE in water Determination of MTBE in water by GC-FID 

J.Chromatogr. A (2002) 963(1-2), 259-264 

Dron, J.; Garcia, R.; Millan, E. 

65 um PDMS/DVB GC-FID 

976 Butyltin in water 

Rapid determination of butyltin species in water samples by multicapillary 

GC GC-AED 

J.Chromatogr. A (2002) 963(1-2), 195-203. 

Carpinterio Botana, J.; Rodriguez Pereiro, I.; Cela Torrijos, R. 

978 BHT in bottled water Determination of butylated hydroxytoluene in bottled drinking water. 

J.Chromatogr. A (2002) 963(1-2), 179-183 

Tombesi, N.B.; Freije, H. 

GC-MS 





979 Nonylphenols in water 

980 

Determination of short ethoxy chain nonylphenols and their brominated 

analogs in raw and treated water. 

J.Chromatogr. A (2002) 963(1-2), 159-167 

Diaz, A.; Ventura, F.; Galceran, M.T. 


Phenolic pollutants in 

water Method for the analysis of thirty phenolic pollutants in water samples. 

J.Chromatogr. A (2002) 963(1-2), 137-148 

Llompart, M.; Lourido, M; Landin, P.; Garcia-Jares, C.; Cela, R. 

75 um carboxen/PDMS GC-MS 

981 Carbofuran in water Comparison of SPE and SPME for carbofuran in water. HPLC 

J.Chromatogr. A (2002) 963(1-2), 117-123 

Lopez-Blanco, M.C.; Cancho-Grande, B.; Simal-Gandara, J. 

983 

993 

Sulfur in gaseous 

matrices 

Quantification of volatile sulfur compounds in complex gaseous matrices by 

SPME 75 um carboxen/PDMS GC-MS 

J.Chromatogr. A (2002) 963(1-2), 57-64 

Nielsen, S.T.; Jonnson, S. 

Musk compounds in 

water. Optimization of SPME method for synthetic musk compounds in water. Various GC 

J.Chromatogr. A (2002) 963(1-2), 277-285 

1001 VOC's in water/soil 

1005 Nonylphenols in water 

1015 MTBE in water 

1023 Nonylphenol in water 

1026 

1029 

MTBE, TAME and TBA 

in water. 

Antifouling agents in 

water 

1041 Hydrocarbons in water 

1042 

Aromatic amines and 

PAH in water. 

Garcia-Jares, C.; Llompart, M.; Polo, M.; Salgado, C.; Macias, S.; Cela, R. 

Determination of volatile organic compounds (VOC) in water and soil using 

solid phase microextraction. PDMS GC-MS 

Chemia Analityczna (2002) 47 (4), 507-530. 

Wypych, J.; Manko, T 

Determination of estrogenic short ethoxy chain nonylphenols and 

metabolites in river and treated water by SPE (solid phase extraction) and 

SPME (solid phase microextraction) 

Water Sc. Technol. Water Supply (2003) 3 (1-2), 329-334. 

Diaz, A.; Galceran, M.T.; Ventura, F. 

Determination of MTBE in a recreational harbor using solid-phase 

microextraction GC-MS 

Chemosphere (2003) 51 (8), 805-810. 

Ganske, Jane A.; Green, David B.; Zuccarello, Joseph L. 

Trace analysis of technical nonylphenol, bisphenol A and 17alphaethinylestradiol 

in wastewater using solid-phase microextraction and gas 

chromatography-mass spectrometry. Various GC-MS 

J.Chromatogr. A (2003) 988(1), 41-51. 

Braun, P.; Engewald, W.; Kuschk, P.; Moeder, M.; Popp, P.; St. Schrader 

Improved analysis of MTBE, TAME, and TBA in petroleum fuelcontaminated 

groundwater by SPME using deuterated internal standards 

with GC-MS PDMS-carboxen GC-MS 

Environmental Science & Technology (2003) 37 (7), 1392-1397. 

Dewsbury, Paul; Lerner, David N.; Thornton, Steven F. 

Headspace solid phase microextraction for the analysis of the new 

antifouling agents Irgarol 1051 and Sea Nine 211 in natural waters. 

Analytica Chimica Acta (2002) 468 (1), 171-180. 

Lambropoulou, D. A.; Sakkas, V. A.; Albanis, T. A.* 

65 um PDMS-DVB GC-MS 

Characterization and source identification of hydrocarbons in water 

samples using multiple analytical techniques. GC-MS 


Wang, Z. D.; Li, K.; Fingas, M.; Sigouin, L.; Menard, L. 

Characteristics of poly(methylphenylvinylsiloxane) fibre probe for solidphase 

microextraction poly(methylphenylvinylsiloxane) GC 

Fenxi Shiyanshi (2002) 21 (5), 75-78. 

Zeng, Z. R.; Wang, Y. L.; Yang, M.; Tian, S. Z. 


1043 




Methamidophos in 

water. Determination of methamidophos residues in water by SPME-CGC-MS. 

Fenxi Shiyanshi (2002) 21 (5), 28-30 

Li, Q.; Liu, H. L.; Wang, J. L.; Chen, H. 


1049 MTBE in water Identification of MTBE in water by SPME and GC-MS. 

American Laboratory (2002) 34 (21), 34. 

Guidotti, M.; Blasi, G.; Lucarelli, E.; Onorati, B.; Ravaioli, G.; Stella, D. 

75 um Carboxen/PDMS GC-MS 

1058 Chlorophenols in water. 

1059 Phenols in water 

1069 

PAHs from drinking 

water. 

1093 Cedrol in sea water 

1095 

1100 

Aromatic compounds in 

aqueous solutions. 

n-alkanes from aqueous 

samples 

1103 Organic acids in water 

1110 

Determination of chlorophenols in waste water using direct solid-phase 

microextraction-GC 85 um polyacrylate GC-ECD 

Fenxi Kexue Xuebao (2002) 18 (5), 421-423. 

Zhang, H. Y.; Zhang, J.; Huang, X. H. 

260 C, 5 minutes 

Determination of phenols in water by solid-phase microextraction-gas 


Fenxi Huaxue (2002) 30 (10), 1240-1242. 

Zhao, R. S.; Liu, R. M.*; Cui, Q. X 

Coating of solid-phase microextraction fibers with chemically bonded silica 

particles: selective extraction of polycyclic aromatic hydrocarbons from 

drinking water samples. Various 

Journal of Chromatographic Science (2002) 40 (9), 489-494. 

Rodrigues, R.; Lacerda, C. A.; Lancas, F. M.* 

Determination of cedrol in sea water by SPME-GC-MS and its content 

variations in redtide sea water. 


Zhao, M. Q.; Li, G. K.; Chen, H.; Zhang, Z. X. 

Various GC-MS 

Infra-red reflection-absorption method for the detection of aromatic 

compounds in aqueous solutions with limited sample volumes. 

Analytical Sciences (2002) 18 (11), 1247-1252. 

Yang, J.; Chen, P. Y.* 

Analysis of n-alkanes at sub microgram per liter level after direct solid 

phase microextraction from aqueous samples. GC-FID 

Analytical Sciences (2002) 18 (11), 1221-1226. 

Farajzadeh, M.; Hatami, M. 

Gas-phase analysis of trimethylamine, propionic and butyric acid, and sulfur 

compounds using solid-phase microextraction 

Analytical Chemistry (2002) 74(5), 1054-1060 

Kim, H.; Nochetto, C.; McConnell, L. L. 

Phthalate esters from 

water. Hollow-fibre liquid-phase microextraction of phthalate esters from water 


Kalogerakis, Nicolas; Psillakis, Elefteria 

1111 Haloanisoles in water. 

1116 Alkylbenzenesulfonates 

Simultaneous determination of "earthy-musty" odorous haloanisoles and 

their corresponding halophenols in water samples using solid-phase 

microextraction coupled to gas chromatography with electron-capture 

detection GC-ECD 


Bruchet, Auguste; Dugay, Jose; Hennion, Marie-Claire; Malleret, Laure 

Determination of linear alkylbenzensulfonates in aqueous matrices by ionpair 

solid-phase microextraction-in-port derivatization-gas chromatographymass 

spectrometry GC 


Alzaga, Roberto; Bayona, Josep Maria; Ortiz, Laura; Pena, Araceli 





1122 Chlorophenols in water 

1151 

PAH, PCB and 

phthalates in water. 

1153 Endosulfan in water. 

1154 PAH's in water 

1155 Phthalate esters 

Improved determination of chlorophenols in water by solid-phase 

microextraction followed by benzoylation and gas chromatography with 

electron capture detection. 


Bianchi, F.; Careri, M.; Mucchino, C.; Musci, M. 

65um DVB PDMS, 

pentafluorobenzoyl chloride 

derivatization 

GC-ECD 

MultiSimplex optimization of the solid-phase microextraction-gas 

chromatography-mass spectrometric determination of polycyclic aromatic 

hydrocarbons, polychlorinated biphenyls and phthalates from water 

samples. 


Cortazar, E.; Zuloaga, O. *; Sanz, J.; Raposo, J. C.; Etxebarria, N.; 

Fernandez, L. A. 

PDMS GC-MS 

Optimization of solid-phase extraction and solid-phase microextraction for 

the determination of small alpha - and small beta -endosulfan in water by 

gas chromatography-electron-capture detection. GC-ECD 


Lopez-Blanco, M. C.; Reboreda-Rodriguez, B.; Cancho-Grande, B.; Simal- 

Gandara, J. * 

Application of the novel benzo-15-crown-5 sol-gel coating for solid-phase 

microextraction in rapid determination of trace PAHs in water at nonequilibrium 

situations. GC 


Wang, D. H.; Xing, J.; Wu, C. Y.* 

Application of time-resolved luminescence methodology to the 

determination of phthalate esters. 

Analytical Letters (2003) 36 (5), 1017-1027. 

Casas-Hernandez, A. M.; Aguilar-Caballos, M. P.; Gomez-Hens, A. * 

1164 Butyltin SPME-GCMS for speciation of butyltin compounds in marine environment 

Journal De Physique. IV : JP (2003) 107 (II), 1313-1316. 

Mahapatra, S.; Puranik, V.D.; Sadasivan, S.; Tripathi, R.M. 

PDMS GC-MS 

1071 

VOC, SVOC in aqueous 

solutions. 

Fibre introduction mass spectrometry: fully direct coupling of solid-phase 

microextraction with mass spectrometry. 


Meurer, E. C.; Tomazela, D. M.; Silva, R. C.; Augusto, F.; Eberlin, M. N.* 

PDMS FIMS 

1072 Extractions with superheated water. 


Smith, R. M. 

1112 Organotin 

1228 BTEX 

1167 Glycol ethers 

Rapid determination of organotin compounds by headspace solid-phase 

microextraction GC 


Le Gac, Marjorie; Lespes, Gaetane; Potin-Gautier, Martine 

Determination of siloxane-water partition coefficients by capillary extractionhigh-resolution 

gas chromatography. Study of aromatic solvents. 


Nardi, L. 

Optimization of the headspace solid-phase microextraction for 

determination of glycol ethers by orthogonal array designs. 

Journal of Chromatography, A (2002) 977(1), 11-15 

Huang, C. T.; Su, Y. Y.; Hsieh, Y. Z. 


75um Carboxen PDMS GC-FID

1168 




Oestrogenic short 

ethoxy chain 

nonylphenols in water 

1182 Biocides in water 

Simultaneous determination of oestrogenic short ethoxy chain nonylphenols 

and their acidic metabolites in water by an in-sample derivatization/solidphase 

microextraction method. 


Diaz, A.; Ventura, F.; Galceran, M. T. 

Comparison of the performance of analytical methods based on solid-phase 

extraction and on solid-phase microextraction for the determination of 

antifouling booster biocides in natural waters. GC-MS 


Konstantinou, I. K.; Hela, D. G.; Lambropoulou, D. A.; Sakkas, V. A.; 

Albanis, T. A.* 

1184 Phthalates in water Solid-phase microextraction of phthalates from water. 


Luks-Betlej, K.; Janoszka, B.; Paschke, H.; Popp, P. 

70um Carbowax DVB 

1188 Mercury in sea water. 

1189 

Endosulfan in aqueous 

samples. 

Speciation of mercury compounds by gas chromatography with atomic 

emission detection. Simultaneous optimization of a headspace solid-phase 

microextraction and derivatization procedure by use of chemometric 

techniques. 


Carro, A. M.; Neira, I.; Rodil, R.; Lorenzo, R. A. 

PDMS GC-MIP AES 

Optimization and application of SPME for the gas chromatographic 

determination of endosulfan and its major metabolites in the ng L-1 range in 



Frimmel, F. H.; Deger, A. B.; Gremm, T. J.; Mendez, L. 

PDMS GC-ECD 

1206 MTBE in water Methyl tert-butyl ether (MTBE) in urban and rural precipitation in Germany. 75um Carboxen PDMS GC-MS 

1213 VOC's in groundwater. 

Atmospheric Environment (2001) 35(36), 6337-6345 

Achten, Christine; Kolb, Axel; Puettmann, Wilhelm 

Monitoring and evolution of the pollution by volatile organic compounds 

(VOCs) in the groundwaters of the Najerilla River Basin (Spain) 75 um Carboxen/PDMS GC-FID 

International Journal of Environmental Analytical Chemistry (2003) 83 (6), 

495-506. 

Fernandez-Torroba, Miguel A.; Ortiz, Gustavo; Pons, Begona; Tena, Maria 

Teresa 

1221 BTEX In-tube solid-phase microextraction sampler for long-term storage. 


Nardi, L. 

1222 PAHs 

1223 Phthalates in water 


Determination of polycyclic aromatic hydrocarbons in water by capillary solidphase 

microextraction coupled with high-performance liquidchromatography. 

HPLC 

Fenxi Huaxue (2003) 31 (2), 171-174. 

Chen, S.; Hahn, J. H.; Quan, X.; Lim, K. S.; Yang, F. L. 

Solid-phase microextraction coupled with high performance liquid 

chromatography-UV detection for the determination of di- n -propylphthalate, 

di- iso -butyl-phthalate, and di-cyclohexyl-phthalate in 

environmental water samples. HPLC 

Analytical Letters (2003) 36 (2), 389-404. 

Cai, Y. Q.; Jiang, G. B.*; Liu, J. F. 

Validation, using a chemometric approach, of gas chromatographyinductively 

coupled plasma-atomic emission spectrometry (GC-ICP-AES) for 

organotin determination. GC-ICP-AES 

Analytical and Bioanalytical Chemistry (2003) 376 (1-2), 226-235. 

Lespes, Gaetane; Aguerre, Sandrine; Pecheyran, Christophe 


1241 




Chlorinated paraffins in 

water. 

1256 Dioxin in water 

1258 Beta-endosulfan 

1260 PCBs in water. 

Solid-phase microextraction for the analysis of short-chain chlorinated 

paraffins in water samples. 


Castells, P.; Santos, F. J.; Galceran, M. T.* 

Various. GC-ECD 

Rapid determination of 2,3,7,8-tetrachlorodibenzo- p -dioxin in water 

samples by using solid-phase microextraction followed by gas 

chromatography with tandem mass spectrometry. 


Various GC-TMS 

Landin, P.; Llompart, M.; Lourido, M.; Garcia-Jares, C.; Carro, N.; Cela, R. 

Application of single-drop microextraction and comparison with solid-phase 

microextraction and solid-phase extraction for the determination of small 

alpha - and small beta -endosulfan in water samples by gas 

chromatography-electron-capture detection. GC-ECD 


Lopez-Blanco, M. C.; Blanco-Cid, S.; Cancho-Grande, B.; Simal-Gandara, J. 

* 

Analysis of polychlorinated biphenyls in aqueous samples by microwaveassisted 

headspace solid-phase microextraction 


Huang, Yaping; Shu, Youn Yuen; Tardif, Mylaine; Wang, Shu Shing 

Headspace GC-FID 

1263 PCBs in water Determination of PCBs in the Housatonic River, MA by SPME and GC-ECD. 


317. 

Wells, James; Schaumloffel, John C. 

1264 n-alkanes in water 

1265 PAHs from water 

A new selective SPME fiber for some n-alkanes and its use for headspace 

sampling of aqueous samples Cellulose acetate, PVC 


Farajzadeh, Mir Ali; Hatami, Mehdi 

Extraction of polycyclic aromatic hydrocarbons and organochloride 

compounds from water: A comparison between solid-phase microextraction 

and stir bar sorptive extraction GC-MS 


Bauer, Coretta; Hauser, Barbara; Keil, Petra; Popp, Peter; Wennrich, Luise 

1267 

Experimental design applied to the determination of several contaminants 

Solvents from varnishes. in Duero River by solid-phase microextraction. 


Salafranca, J.; Domeno, C.; Fernandez, C.; Nerin, C. * 

Various GC-MS 

1278 VOCs in groundwater. 

1298 

Trace organic 

compounds in waste 

water. 

1300 Triazines in water. 

Development and validation of a solid-phase microextraction method for the 

analysis of volatile organic compounds in groundwater samples. 

Chromatographia (2003) 41 (6), 301-304. 

Alonso, A.; Fernandez-Torroba, M. A.; Tena, M. T.; Pons, B. * 

Various GC 

Development of an SPME-GC-MS method for trace organic compounds in 

waste water from a petrochemical refinery. GC-MS 

Sepu (2003) 21 (1), 76-80. 

Xiao, K.; Wang, Y.; Lu, X.; Kong, H. W.; Yao, Q. H.; Xu, G. W.* 

Optimization of a solid-phase microextraction procedure for the 

determination of triazines in water with gas chromatography-mass 

spectrometry detection. 


Frias, S.; Rodriguez, M. A.*; Conde, J. E.; Perez-Trujillo, J. P. 

Various GC-MS 





1322 Aldehydes in water 

1335 Phenol species in water. 

1340 PAH's in water. 

1351 Phenols from water. 

1357 Phthalates in water. 

1358 

Analysis of aldehydes in water by solid-phase microextraction with on-fiber 

derivatization 


Chang, Chun-Ming; Tsai, Shih-Wei 

PDMS/DVB GC-MS 

Determination of iodinated phenol species at parts-per-trillion concentration 

levels in different water samples by solid-phase microextraction/offline GC- 

ICP-MS Various GC-ICP-MS 


Caruso, Joseph A.; De Wuilloud, Jorgelina C.A.; Vonderheide, Anne P.; 

Wuilloud, Rodolfo G. 

Solid-phase microextraction to monitor the sonochemical degradation of 

polycyclic aromatic hydrocarbons in water. GC-MS 

Journal of Environmental Monitoring (2003) 5 (1), 135-140. 

Psillakis, E.; Ntelekos, A.; Mantzavinos, D.; Nikolopoulos, E.; Kalogerakis, 

N. 

Investigations on the sorption of phenols to dissolved organic matter by a 

QSAR study. 

Chemosphere (2001) 45(3), 323-327. 

Ohlenbusch, G.; Frimmel, F. H. 


Miniaturized solid-phase extraction as a sample preparation technique for 

the determination of phthalates in water. HPLC 


Saito, Y.; Nakao, Y.; Imaizumi, M.; Morishima, Y.; Kiso, Y.; Jinno, K. * 

PAH, PCB, pesticides 

and VOC Sorptive sample preparation long dash a review. 


Baltussen, E.; Cramers, C. A.; Sandra, P. J. F. 

PDMS 

1374 Tin and lead. 

1376 

1383 

1405 


water. 

Phenylurea herbicides in 

water. 

Organophosphorous 

pesticides in water. 

1407 Butyltin in water 

Determination of tin- and lead-organic compounds by SPME-GC-atomicemission 

detection (SPME-GC-AED) after in situ propylation with sodium 

tetrapropylborate. GC-AED 

Journal of Analytical Atomic Spectrometry (2001) 16(10), 1160-1166. 

Crnoja, M.; Haberhauer-Troyer, C.; Rosenberg, E. *; Grasserbauer, M. 

Simultaneous determination of traces of hydrophilic and volatile compounds 

in water by solid-phase microextraction and GC/MS. GC-MS 

Bunseki Kagaku (2001) 50(10), 685-693. 

Miyazaki, T.; Kadokami, K.; Tukamoto, H. 

Determination of phenylurea herbicides in natural waters at concentrations 

below one nanogram-per-litre using solid-phase extraction, derivatization, 

and solid-phase microextraction-gas chromatography-mass spectrometry. Polyacrylate GC-MS 


Gerecke, A. C.; Tixier, C.; Bartels, T.; Schwarzenbach, R. P.; Mueller, S. 

R.* 

Comparison between solid-phase extraction methods for the 

chromatographic determination of organophosphorus pesticides in water. 

Journal of Environmental Science and Health Part B Pesticides Food 

Contaminants and Agricultural Wastes (2001) B36(5), 517-527. 

Lancas, Fernado M.; Carvalho, Dermeval; Queiroz, Maria E. C.; Silva, 

Silvana M 

Occurrence of butyltin compounds in the waters of selected lakes, rivers 

and coastal environments from China. GC-FID 

Environmental Pollution (2001) 115(1), 81-87. 

Jiang Gui-bin; Liu Ji-yan; Wu Di-jing; Zhou Qun-fang 


1408 

1416 

1419 




Alkylphenols and 

bisphenol-A 

Nitroaromatic 

compounds in water. 

Phthalate esters from 

water. 


1431 Organotin compounds 

1432 Tributyltin 

1436 Chloroanilines in water 

1444 Amines in water 

1449 Amines in water 


Alkylphenols and bisphenol-A in the coastal environment of Singapore and 

their rapid extraction from seawater and biological materials. 

Abstracts of Papers American Chemical Society (2001) 222(1-2), ENVR155. 

Lee, Hian Kee; Chanbasha, Basheer 

Screening method for nitroaromatic compounds in water based on solidphase 

microextraction and infrared spectroscopy. IR 

Environmental Science & Technology (2001) 35(17), 3507-3512. 

Tilotta, David C.; Stahl, Danese C. 

Comparison of different fibers for the solid-phase microextraction of 

phthalate esters from water. 


Pocurull, E.; Borrull, F.; Marce, R. M.; Penalver, A. 

65 um PDMS/DVB GC-MS 

A rapid and sensitive method for methyl tert-butyl ether analysis in water 

samples by use of solid phase microextraction and gas chromatographymass 

spectrometry. 

Chemosphere (2001) 44(4), 539-544. 

Roda, Aldo; Barbieri, Anna; Piazza, Francesco; Violante, Francesco 

Saverio 


Optimisation of the hyphenation between solid-phase microextraction , 

capillary gas chromatography and inductively coupled plasma atomic 

emission spectrometry for the routine speciation of organotin compounds in 

the environment GC-ICP-AES 

J Anal At Spectrom (2001) 16(12), 1429-1433. 

Aguerre, S.; Donard, O.F.X.; Krupp, E.; Lespes, G.; Pecheyran, C.; Potin- 

Gautier, M. 

Speciation without chromatography: Part I. Determination of tributyltin in 

aqueous samples by chloride generation, headspace solid-phase 

microextraction and inductively coupled plasma time of flight mass 

spectrometry PDMS/DVB ICP-TOFMS 


Lam, J.W.; Maxwell, P.S.; Mester, Z.; Peter, L.; Sturgeon, R.E. 

Comparison of SPME/Transmission IR and SPME/ATR-IR spectroscopic 

methods in detection of chloroanilines in aqueous solutions 

Applied Spectroscopy (2001) 55(7), 919-926. 

Tsai, F.-P.; Yang, J. 

Analysis of carcinogenic aromatic amines in water samples by solid-phase 

microextraction coupled with high-performance liquid chromatography 

Anal. Chim. Acta (2003) 495(1-2) 109-122 

Chang, Wei-Yan; Huang, Shang-Da; Sung, Yu-Hsiang 

Determination of aliphatic amines using N-succinimidyl benzoate as a new 

derivatization reagent in gas chromatography combined with solid-phase 


Journal of Chromatography A (2003) 1021 (1), 175-181 

Cai, Ling-Shuang; Jing, Zhi-Zhong; Wang, Hong; Yu, Jian-Xin; Zhang, Hua- 

Shan; Zhao, Yuan-Yuan 

Reevaluation of headspace solid-phase microextraction and gas 

chromatography-mass spectrometry for the determination of methyl tertbutyl 

ether in water samples 


Bucciferro, Anthony; Chu, Shaogang; Fang, Fu; Hong, Chia-Swee; Kou, 

Wenpeng 


Various fibers compared HPLC 

Headspace after derivatization 

with N-succinimidyl benzoate 

GC-FID, GC-MS 

GC-MS




1460 PCBs in water 


1480 MIB in drinking water 

1484 

1488 

1493 

2-hydroxy-4methoxybenzophenone 

and octyldimethyl-paminobenzoic 

acid 

sunscreen agents in 

water 

Organochlorines in 

water 

Estrogenic compounds 

in water 

1504 Mehylmercury in water 

1536 

1538 

Phthalic acid esters in 

water 

Phenolic compounds in 

water 

1552 Chlorophenols in water 

1354 

Aldehydes in drinking 

water 

Strategically designed sample composition for fastest screening of 

polychlorinated biphenyl congeners in water samples. 

Journal of Environmental Monitoring (2002) 4(4), 490-497 

Martinez, E.; Llompart, M. P.; Landin, P.; Cela, R.; Carro, A. M. 

Sensitive method for determination of methyl tert-butyl ether (MTBE) in 

water by use of headspace-SPME/GC-MS. 

Fresenius' Journal of Analytical Chemistry (2001) 371(4), 519-525 

Achten, Christine; Kolb, Axel; Puettmann, Wilhelm 

Correlation of musty odor and 2-MIB in two drinking water treatment plants 

in South Taiwan. 

Science of the Total Environment (2002) 289(1-3), 225-235 

Lin, Tsair-Fuh; Kao, Hsiao-Pin; Wong, Jiun-Yue 

Gas chromatographic determination of 2-hydroxy-4-methoxybenzophenone 

and octyldimethyl-p-aminobenzoic acid sunscreen agents in swimming pool 

and bathing waters by solid-phase microextraction 


Albanis, T. A.; Giokas, D. L.; Karayannis, M. I.; Lambropoulou, D. A.; 

Sakkas, V. A. 

Determination of organochlorides in water using solid-phase microextraction 

coupled to gas chromatography. 

American Laboratory (2002) 34(17), 12-14 

Ou Qing-Yu; Liang Bing; Li Ju-bai; Huang Min-jia 

Method based on solid-phase microextraction-high-performance liquid 

chromatography with UV and electrochemical detection to determine 

estrogenic compounds in water samples. 


Pocurull, E.; Borrull, F.; Marce, R. M.; Penalver, A. 

Application of SPME for the quantitative determination of methylmercury in 


Abstracts of Papers American Chemical Society (2002) 223(1-2) CHED 

125 

Moore, J. Taylor; McDowell, Derek R.; Ambler, Rich B. 

Development of a solid-phase microextraction method for the determination 

of phthalic acid esters in water. 


Holadova, Katerina; Hajslova, Jana; Poustka, Jan; Prokupkova, Gabriela 

Solid-phase microextraction coupled to high-performance liquid 

chromatography to determine phenolic compounds in water samples. 


Marce, R. M.; Borrull, F.; Penalver, A.; Pocurull, E. 

Determination of chlorophenols by solid-phase microextraction and liquid 

chromatography with electrochemical detection. 


Galceran, M. T.; Santos, F. J.; Sarrion, M. N. 

Determination of aldehydes in drinking water using 

pentafluorobenzylhydroxylamine derivatization and solid-phase 



Ventura, Francesc; Cancho, Beatriz; Galceran, Ma. Teresa 


75um Carboxen/PDMS, 

headspace 

100um PDMS, 85um 

Polyacrylate 

85um Polyacrylate 

GC-MS 

GC-MS 

GC 

HPLC-UV, HPLC- 

ED 

Various fibers compared GC-ECD 

85um Polyacrylate HPLC-UV 

Various fibers compared HPLC-ELCD 

65um DVB PDMS, on-fiber 

derivatization with PFBHA 

GC-ECD




1156 Chlorophenols 

1166 

Mercury and tin in 

environmental samples. 

1074 Tributyltin 

Solid-phase microextraction liquid chromatography/tandem mass 

spectrometry for the analysis of chlorophenols in environmental samples. 


Sarrion, M. N.; Santos, F. J.; Moyano, E.; Galceran, M. T.* 

Carbowax/TPR LC-TMS 

Simultaneous mercury and tin speciation in environmental samples by GC- 

MIP/AES after preconcentration by solid phase microextraction PDMS GC-MIP/AES 

Journal De Physique. IV : JP (2003) 107 (II), 1423. 

Carrera, R.; De Diego, A.; Delgado, A.; Madariaga, J.M.; Sanz, J.; Zuloaga, 

O. 

Improvement of measurement precision of SPME-GC/MS determination of 

tributyltin using isotope dilution calibration. GC-MS 


Bancon-Montigny, C.; Maxwell, P.; Yang, L.; Mester, Z.; Sturgeon, R. E. 

1952 Methyl Determination of methylphosphonic acid in water by SPME-GC GC 

phosphoric Fenxi Ceshi Xuebao, 23, #1, 106-108 

acid in wate Yuan, L.; Xu, D. N. 

1953 Nickle-cadmium Electrochemically controlled (EC) SPME based sulfortated polypyrrole ETAAS 

from water on over oxidized sulfonate polypyrrole coated fiber 

Talanta, 67, #1,, 245-251 immersed 

Ertas, N; Pekmez, K; Sahin, Y; Tamer, U Udum, Y.; 

Yildiz, A. 

1954 Industrial Risk assessment of domestic and industrial effluents GC-MS 

effluent in unloaded into a freshwater environment 

freshwater Ecotoxicology & Environmental Safety, 61, #3, 380-391 

Di Marzio, W.; Saenz, M.; Alberdi, J.; 

Tortorelli, M.; Silvana, G. 

1955 Alkanethiols Low part per trillion determination of reactive N-ethylmaleimide GC-MS 

in wastewater alkanethiols in wastewater by in situ derivatization- derivatives 

SPME followed by GC/MS immersion sampling 

Anal. Chem., 77, #18, 6012-6018 

Alzaga, R.; Bayona, J.M.; Garcia-Jares, C.; 

Llompart, M.; Salgado-Petinal, C. 

1956 Chromium in Determination of total chromium in seawater by PDMS fiber ICPMS 

seawater isotope dilution sector field ICPMS using GC s TFA derivatives 

sample introduction headspace 

Anal. Chem., 76, #13, 3510-3516 

Abranko, L; Mester, ; Sturgeon, .; Yang, L 

1957 Chromium in Determination of chromium(III) in water by SPME polyimide fiber GC-FPD 

Water w/ polyimide-coated fiber and GC-FPD TFA derivatives 

J. Chromatogr. A, 1062, #1, 49-55 

Ding, Tzuoo-Huei; Lin, Huang-Huei; Whang, Chen-Wen 

1958 Organics SPME: A powerful sample preparation tool prior to review article GC-MS, LC-MS 

in water mass spectrometric analysis 

J. Mass Spectrom.(2004) 39(3), 233-254 

Vas, Gyorgy; Vekey, Karoly 

1959 Butyltin in Comparison between headspace and aqueous phase SPME headspace & GC 

sea water method for speciation analysis of butyltin compounds immersion sampling 

in sea water 

J Food and Drug Analysis, 12, #3, 205-211 

Hsia, Meng-Pei; Hsu, Tau-Being; Liu, Shiu-Mei 

1960 Hg,Pb,Tn Multielemental speciation analysis of organometallic Various fibers GC-MS 

in water & compounds of mercury, lead, and tin in natural water NaEt 4B derivatives 

seawater samples by headspace-SPME followed by GC-MS headspace 

J. Chromatogr. A, 1034,#1-2, 191-197 

Centineo, G; Gonzalez, E; Sanz-Medel, A 





1961 MTBE in Reevaluation of headspace SPME-GC-MS for the headspace GC-MS 

water determination of methyl tert-butyl either in water samples 

J. Chromatogr. A, 1021, #1-2, 157-164 

Fang, Fu; Hong, Chia-Swee; Chu, S; Kou, W; Bucciferro, A 

1962 Diacetyl Odor Identification of 2,3-butanedione (diacetyl) as the 75µm Carboxen GC-MS 

in water compound causing odor events at trace levels in the 30min @ 60°C 

Llobregat River and Barcelona's treated water (Spain) NaEt 4B derivative 

J. Chromatogr. A, 1034, #1-2, 175-182 Headspace 

Diaz, A.; Galceran, Ma. Teresa; Ventura, F. 

1963 Odors/volatiles Simultaneous determination of 22 volatile organic compounds, 100µm PDMS GC-MS 

in water methyl-tert-butyl ether,1,4-dioxane, 2-methylisoborneol and headspace 

geosmgeosmin in water by headspace SPME-GC-MS 

Anal. Chim. Acta, 548, #1-2, 79-85 

Daishima, Shigeki; Nakamura, Sadao 

1964 Alkyl lead Study of alkyl lead speciation by Head Space (HS)- Headspace GC-MS 

in water SPME coupled with GC-MS 

Fenxi Shiyansh, 23, #2, 14-17 

Shuai, Q.; Zheng, C; Shuai, Q.; Yang, W.; Zheng, Y. 

1965 C2-C7 Fatty Volatile fatty acids as malodorous compounds in headspace GC-CI-MS 

acids in wool scouring water and lanolin. Origin and 

water/lanolin characterization. 

Env Technology, 24, #12, 1465-1470 

Jover, E.; Abalos, M.; Ortiz, L.; Bayona, J. 

1966 Volatile SPME of volatile oxidation compounds in oil-in-water headspace GC-FID. 

oxidative emulsions 50°C for 20 min. 

products in Food Chemistry, 92, #3, 401-406 

oil-water Beltran, G; Aguilera, M; Gordon, Michael H. 

1967 Organometallic Full automation of derivatization:SPME-GC-MS phenyl derivative GC-MS 

derivatives with dual-arm system for the determination of headspace 

in water organometallic compounds in aqueous samples. 

J Chromatogr A, 1025, #1, 77-84 

Parkinson, D; Bruheim, I; Christ, I; Pawliszyn, J 

1968 Methyl Determination of methylmercury and mercury(II) in a marine headspace GC-MS 

mercury from ecosystem using SPME--GC-MS Na(C 6H 5) 4B 

seawater Anal. Chim. Acta, 551, #1-2, 192-198 derivative 

Bhalke, S.; Mishra, S.; Puranik, V.D.; Shukla, V.K.; Tripathi, R.M. 

1969 Mercury Speciation analysis of mercury by SPME and multicapillary 75µm Carboxen ICP-TOF-MS 

from wate/ GC hyphenated to ICP-TOF spectrometry. NaEt 4B derivatives 

sediment J Chromatogr A, 1055, #1-2, 197-207 headspace 

Jitaru, P.; Adams, F. C.* 

1970 BTEX in Diffusion-based calibration for SPMEof benzene, headspace GC 

water toluene, ethylbenzene, p-xylene and chlorobenzenes 

from aqueous samples 

J Chromatogr A, 1025, #1, 11-16 

Paschke, A.; Popp, P. 

1971 Chlorinated Indirect determination of low vapour pressures using SPME - minutes to hour GC 

benzenes Application to tetrachlorobenzenes & trachlorbenyltoluenes headspace 

J Chromatogr A, 1072, #1, 93-97 

Paschke, Albrecht; Schroter, Uwe; Schuurmann, Gerrit 

1972 Organo- Determination of organophosphorus pesticides in immersed sampling GC-MS 

phosphorus spiked river water samples using SPME-GC With GC-ICP-MS 

pesticides EI-MS and ICP-MS detection 

in water J Anal At Spectrom, 20, #9, 876-882 

Blanco-Gonzalez, E; Fidalgo-Used, N; Montes-Bayon, M; 

Sanz-Medel, A 





1973 Pyrethroids Determination of enantiomers of synthetic GC 

in water pyrethroids in water by SPME 

enantioselective gas chromatography. 

J Agrl Food Chem, 52, #4, 736-741 

Liu, W. P.; Gan, J. J.* 

1974 Polybrominate Development of a SPME-GC-MS method for poly- headspace GC-MS 

diphenyls/ brominated diphenyl ethers and polybrominated 

biphenyls biphenyls in water sample 

in water Analytical Chemistry, 76, #4, 1054-1062 

Polo, M.; Gomez-Noya, G.; Quintana, J. B.; Llompart, M.; 

Garcia-Jares, C.; Cela, R. 

1975 Polybrominate Photochemical studies of a polybrominated diphenyl GC 

diphenyl ether ethers (PBDES) technical mixture by SPME 

from water Chemosphere, 60, #7, 922-928 

Cela, R.; Garcia-Jares, C.; Gonzalez-Barreiro, C.; 

Llompart, M.; Lores, M.; Sanchez-Prado, L. 

1976 PCBs in Determination of PDMS-seawater distribution 100µm PDMS GC-MS 

water coefficients for PCBs and chlorinated biphenyls 12 day extraction 

and chlorinated pesticides by SPME-GC-MS immersion 

J. Chromatogr. A,1066, #1-2, 165-175 

Zeng, E; Tsukada, D; Noblet, J.; Peng, J 

1977 Phthalate Multivariate optimization of a SPME method for the Various fibers GC-MS 

esters in analysis of phthalate esters in environmental waters direct immersion & 

water J. Chromatogr. A,1072, #1, 63-72 headspace 

Cela, R; Garcia-Jares, C; Llompart, M Polo, M 

1978 Tin compounds New approach of SPME improving the extraction Ethylate derivatives GC 

in water yield of butyl and phenyltin compounds by combining headspace 

the effects of pressure and type of agitation agitated 

J. Chromatogr. A,1072, #1, 19-27 

Bueno, M; Darrouzes, J; Holeman, M; Pecheyran, C; 

Potin-Gautier, M 

1979 Aliphatic Determination of aliphatic amines using N-succinimidyl 60min @ 80°C GC-MS 

amines benzoate as a new derivatization reagent in headspace GC-FID 

in water GC combined with SPME succinimidyl benzoate 

J. Chromatogr. A,1021, #1-2, 175-181 derivatives 

Zhao, Y.; Cai, L.; Jing, Z.; Wang, H.; Yu, J.; Zhang, H. 

1980 Aromatic In situ derivatization/SPME determination of polar 65µm PDMS-DVB GC-MS 

amines in aromatic amines. diazotation/ iodination 

water Analytical Chemistry, 76, #4, 1028-1038 

Zimmermann, T.; Ensinger, W. J.; Schmidt, T. C.* 

1981 Aromatic Determination of aromatic amines in waste water by GC 

amines in SPME-GC 

water Fenxi Ceshi Xuebao, 23, #3, 18-21 

Peng, J. G.; Wang, D. H.; Wu, C. Y. 

1982 Phenols in Comparative study of the use of flow-through 80µm polyacrylate GC 

water systems with and without air segmentatio 100µm PDMS 

determination of phenols by SPME-GC immersed 


Nome, R. C.; Carasek, E. * 

1983 Aldehydes Determination of low-molecular mass aldehydes by automated headspace GC-FID 

in water headspace spme with in-fibre derivatisation PFBHA derivatives 

J. Chromatogr. A, 1071, #1-2, 147-154 

O'Reilly, John; Pawliszyn, Janusz; Wang, Qing 

1984 Aldehydes in Determination of low-molecular mass aldehydes by automated PFBHA derivatives GC-FID 

water headspace SPME with in-fibre derivatization headspace 

J. Chromatogr. A, 1071, #1-2,147-154 

Wang, Qing; O'Reilly, John; Pawliszyn, Janusz 





1985 Organochlorine Analysis of organochlorine pesticides in water by GC-MS 

pesticides novel activated carbon fiber SPME coupled w/GC-MS 

in water J. Environ. Sci. Health Part B, 39, #2, 235-248 

Fang, N; Jia, J; Sun, T; Wang, Y; Yu, J 

1986 Organochlorine Optimization of a methodology for the determination 85µm polyacrylate GC-MS 

pesticides of organochlorine pesticides in surface water by 40min @ >20°C 

in water SPME-GC-MS agitation 

J. Environ. Sci. Health Part B, 40, #4, 513-523 immersed sampling 

Brondi, Silvia Helena G.; Lancas, Fernando M. 

1987 Pesticides in GC-MS methodology using SPME for the multiresideu 65µm PDMS-DVB GC-SIM-MS 

surface water determination of pesticides in surface waters. 

Intl J Env Analytical Chem, 84, #14-15, 1079-1092 

Albanis, T; Hela, D.; Lambropoulou, D.; Sakkas, V. 

1988 Endosulfan, Pesticides in Esteros del Ibera (AR): Evaluation of immersed sampling GC-MS 

carbofuran impacts and proposal of guidelines for water 

in water quality protection 

Ecol. Model., 86, #1, 85-97 

Boia, C; Borrego, C; Silva, C; Valente, J 

1989 Endosulfan, Optimization and application of SPME for the GC 100µm PDMS GC-ECD 

in water determination of endosulfan and its major metabolites 30% NaCl GC-MS 

in the ng L/sup-1 / range in aqueous solutions 


Deger, A.B.; Frimmel, F.H.; Gremm, T.J.; Mendez, L. 

1990 Phthalates Application of membrane techniques to water 65µm CW/DVB GC-FID 

in water purification. Removal of phthalates 

Desalination, 162, #1-3, 121-128 

Bodzek, M; Dudziak, M; Luks-Betlej, K 

1991 PAHs Degradation of PAHs in aqueous solutions by 20°C & 40°C GC-MS 

in water ultrasonic irradiation immersed sampling 

J. Hazard. Mater., 108, #1-2, 95-102 sonicated 

Goula,G; Kalogerakis,N; Mantzavinos,D; Psillakis, E 

1992 Vinyl chloride Oxidative microbial transformation of vinyl chloride headspace GC-MS 

in water under anaerobic conditions in ground water 

Proc. of the Third Int. Conf. on Rem. of Chlorinated 

and Recalcitrant 2002, pp1571-1578 

Banwart, S; Holliger, C; Morgan, Pl; Shah, N.; Szynalski, K. 

1993 Adipate in Determination of adipate in water with Headspace GC-MS 

water headspace SPME and single ion monitoring GC-MS 


Zhang, W. Y.; Wang, C. Y.; Yang, Z. J. 

1994 Bisphenol in SPME coupled with HPLC w/ fluorimetric detection 50µm CW-TPR HPLC-Fluorimetric 

water for the determination of bisphenol A, 4-n-nonylphenol and 

4-t-octylphenol in environmental water samples. 

Analytical Letters, 37, #4, 739-753 

Cai, Y. Q.; Jiang, G. B.*; Liu, J. F.; Liang, X.; Yao, Z. W.; 

Liu, J. M.; Liu, J. Y.; Zhou, Q. X. 

1995 Volatiles from Electronic nose technology for the detection of microbial headspace @ 25°C GC 

Bacteria and chemical contamination of potable water 

in water Sens Actuators, B Chem, 106, #1, 3-6 

Canhoto, O.; Magan, N. 

1996 Herbicides On-fibre silylation following SPME for the determination of 85µm polyacrylate GC-MS 

in water acidic herbicides in water samples by GC MTBSTFA derivative 

Anal. Chim. Acta, 537, #1-2, 259-266 stirred 

Cela, R.; Gonzalez, R.; Quintana, J.; Rodriguez, I.; Rubi, E. 

1997 Herbicides Analysis of the chloroacetanilide herbicides in water using 75µm Carboxen GC-ECD 

in water SPME with CAR/PDMS and GC/ECD immersed sampling 

J of AOAC Intl, 88, #4, 1236-1241 

Hwanc, Ying-Ming; Wong, Yih-Gang; Ho, Wu-Hsiung 





1998 Triclosan in Optimization of SPMEconditions for the determination of 85µm polyacrylate GC-MS 

water triclosan and possible related compounds in water samples MTBSTFA derivative 

J Chromatogr A, 1072, #1, 107-115 30min extraction 

Canosa, P.; Rodriguez, I.; Rubi, E.; Cela, R. immersed sampling 

1999 Anti- Application of strategic sample composition to the screening 85µm polyacrylate GC-MS 

inflamatory of anti-inflammatory drugs in water samples using SPME silylated esterfication 

drugs in Anal. Chim. Acta, 524, #1-2, 63-71 headspace 

water Carpinteiro, J.; Carro, A.; Cela, R.; Lorenzo, R.; 

Martinez, E.; Quintana, J.; Rodriguez, I. 

2000 Estrogens in Applicability of SPME followed by on-fiber silylation for the 85µm polyacrylate GC-MS-MS 

sewage determination of estrogens in water samples by GC-MS-MS MSTFA derivatives 

water J Chromatogr A, 1056, #1-2, 179-185 immersed sampling 

Carpinteiro, J.; Carro, A.; Cela, R.; Lorenzo, R.A.; 

Quintana, J.; Rodriguez, I. 

2001 Chloro-brom- Determination of odorous mixed chloro-bromoanisoles in headspace GC-MS 

anisole in water by SPME-GC-MS 100µm PDMS 

water J Chromatogr A, 1064, #1-2, 97-106 

Diaz, A.; Ventura, F.; Galceran, M. 

2002 Nonylphenol Estimation of measurement uncertainty for the GC-MS 

in water determination of nonylphenol in water 

using SPME and SPME procedures. 


Diaz, A.; Vazquez, L.; Ventura, F.; Galceran, M. 

2003 Organotin Validation, using a chemometric approach, of GC- GC-ICP-AES 

in water and inductively coupled plasma-atomic emission 

sediment spectrometry (GC-ICP-AES) for organotin determination 


Aguerre, S.; Lespes, G.; Pecheyran, C. 

2004 Bethrodine Development of a novel SPME element for 30µm PDMS GC-MS 

herbicide in thermal desorption GC analysis 

water J. Chromatogr. A, 1035, #2, 277-279 

Hosaka, A.; Ohtani, H.; Tsuge, S.; Wang, L.; Watanabe, C. 

2005 Fumigants Application of SPME for the determination of soil fumigants soil headspace or GC/ECD/NPD 

in soil/water in water and soil samples immersed in water 

Journal of Separation Science, 28, #1, 98-103 

Fuster, S.; Beltran, J.; Lopez, F. J.; Hernandez, F. 

2006 Surfactants Impurity analysis of 1,4-dioxane in nonionic surfactants and headspace GC, GC-MS 

in water cosmetics using headspace SPME coupled w/GC & GC-MS 

J. Chromatogr. A, 1071, #1-2, 141-145 

Fuh, C. Bor; Lai, M.; Tsai, H. Y.; Chang, C. M. 

2007 Surfactants Rapid screening for trace nonyl-phenyl 14 hour SALDI-MS 

in water polyethylene glycol ether in water by SPME polycrystaline 

combining with laser desorption ionization MS graphite coated fiber 

Proc. 50th ASMS Conf. Mass Spectrom. Allied Top. 

2002, p597-599 

Chen, Yu-Chie; Sun, Mei-Chuan 

2008 Methylamine Analysis of methylamine by SPME and HPLC after 9-fluorenylmethyl HPLC 

in water on-fiber derivatization with 9-fluorenylmethyl chloroformate chloroformate 

Anal. Chim. Acta, 513, #2, 425-433 derivative 

Campins-Falco, P.; Chafer-Pericas, C.; Herraez-Hernandez, R. immersion sampling 

2009 Methylamine A new selective method for dimethylamine in water analysis 50µm CW-TPR HPLC 

in water by LC using SPME and two-stage derivatization with 9-fluorenylmethyl 

o-phthalaldialdehyde and 9-fluorenylmethyl chloroformate chloroformate 

Talanta, 66, #5, 1139-1145 derivative 

Chafer-Pericas, C; Herraez-Hernandez, R.; Campins-Falco, P immersion sampling 





2010 Bisphenol A Determining leaching of bisphenol A from plastic 85µm polyacrylate GC-MS 

from water containers by SPME-GC-MS 50min @ 65°C 

Anal. Chim. Acta, 539, #1-2, 41-47 BSTFA derivative 

Chang, Chia-Min; Chou, Chi-Chi; Lee, Maw-Rong headspace 

2011 Bisphenol A Determination of trace bisphenol-A in leachate by HPLC-UV 

from water SPME coupled with HPLC 

Fenxi Kexue Xuebao, 20, #5, 461-464 

Deng, L.; Zhang, W. H.; Feng, X. H.; Deng, N. S.* 

2012 THM & TBE Measurement of trihalomethanes and methyl headspace GC-MS 

in tap water tertiary-butyl ether in tap water using SPME-GC-MS. 

J Chrom Sci, 42, #4, 200-206 

Cardinali, F.; Ashley, D.; Morrow, J.; Moll, D.; Blount, B. 

2013 Ethanol in Methods for sampling and analysis of tropospheric headspace from GC-FID 

air & water ethanol in gaseous and aqueous phases. cryocooled sample 

Chemosphere, 52, #8, 1307-1319 

Monod, A.; Bonnefoy, N.; Kaluzny, P.; Denis, I.; 

Foster, P.; Carlier, P. 

2014 Aniline Determination of aniline in water by microwave- 65µm PDMS-DVB GC-FID 

in water assisted headspace SPME-gas chromatography. headspace 

Chromatographia, 59, #7-8, 517-520 pH12, salt added 

Yan, C. T.; Jen, J. F.* 

2015 PAHs Coupling of a modified in-tube spme technique w/ PDMS capillary tube HPLC 

in water HPLC-fluorescence detection for the ultra-trace 

determination of PAHs in water samples. 


Bagheri, H.; Salemi, A. 

2016 Aromatic SPME for qualitative and quantitative determination of headspace GC 

compounds migrated degradation products of antioxidants in an 

in 10% alcohol organic aqueous solution 

water mixture J. Chromatogr. A, 1080, #-2, 107-116 

Albertsson, Ann-Christine; Burman, L.; Hoglund, A. 

2017 Anatoxin Analysis of anatoxin-a using polyaniline as a sorbent in SPME 32µm polypyrrole film GC-MS 

in water coupled to GC-MS 10% salt 

J. Chromatogr. A, 1078, #1--2, 120-127 30min w/agitation 

Davarani, H.; Fallahi, M.; Ghassempour, A.; 

Mehdinia, A.; Najafi, N.; Nakhshab, M. 

2018 agrochemicals SPME-HPLCdetermination of Nabam, Thiram, and PDMS fiber HPLC-UV 

in water Azamethiphos in water samples with UV detection: headspace 

preliminary data 

Talanta, 66, #1, 266-270 

Aulakh, Jatinder Singh; Malik, A. K.; Mahajan, R. K. 

2019 Orgaonotin Headspace single-drop microextration for the headspace GC 

in water detection of organotin compounds 

Talanta, 63, #3, 555-560 

Bancon-Montigny, C; Colombini, V; Maxwell, P; 

Mester, Z; Sturgeon, R: Yang, Lu 

2020 Orgaonotin Determination of organotin compounds in water by headspace NaEt 4B derivatives GC-MS 

in water SPMEwith GC-MS 30min @ 45°C, pH 5 

J. Chromatogr. A, 1064 #1, 1-8 headspace 

Chou, Chi-Chi; Lee, Maw-Rong 

2021 Organotin Automated headspace-SPME-retention time locked- NaEt 4B derivatives GC-MS 

in water/ isotope dilution GC-MS for the analysis of organotin headspace 

sediment compounds in water and sediment samples 

J. Chromatogr. A, 1079, #1-2, 408-414 

David, F; Devos, C; Moens, L; Sandra, P.; 

Vliegen, M; Willaert, B 





2022 Phthalate Monitoring the sonochemical degradation of immersion sampling GC 

esters in phthalate esters in water using SPME 21°C & 50°C 

water Chemosphere, 54, #7, 849-857 NaCl addition 

Psillakis, E.; Mantzavinos, D.; Kalogerakis, N. 

2023 Drugs from SPME-GC-MS for the analysis of selective serotonin 65µm PDMS-DVB GC-MS 

water reuptake inhibitors in environmental water 100°C, direct extract 

J. Chromatogr. A, 1045, #1-2, 241-247 in situ acetylation 

Cela, R; Garcia-Jares, C; Gomez, Mo; Llompart, M; 

Pablo Lamas, J.;Salgado-Petinal, Carmen 

2024 Musty odors Analysis of earthy and musty odors in water samples headspace GC-ITMS 

in water bySPME coupled with GC-ion trap MS 

Talanta, 65, #2, 518-524 

Huang, Shang-Da; Li, Tzu-Ying; Sung, Yu-Hsiang 

2025 Triazine Optimization of a SPME procedure for the 65µm PDMS-DVB SPME-MEKC 

herbicides in detemination of herbicides by micellar electrokinetic 120 min 

ground water chromatography. 10% NaCl, stirring 

J Separation Sci, 27, #9, 660-666 

Frias-Garcia, S.; Sanchez, M..; Rodriguez-Delgado, M 

2026 Triazine Analysis of triazine in water samples by SPME-HPLC 50µm CW-TPR HPLC 

herbicides in Talanta, 64, #4, 887-893 100µm PDMS 

water Huang, Hsin-I; Huang, Shang-Da; Sung, Yu-Hsiang 

2027 Volatiles in A laboratory batch reactor test for assessing nonspeciated headspace GC 

wastewater volatile organic compound biodegradation in activated sludge 

Water Environ. Res., 75, #4, 342-354 

Allen, C.; Cano, M.; Huot, M.; Rhodes, I.; Saterbak, A; 

Van Compernolle,Remi; Williams, M. 

2028 Organics Determination of organic contaminants in LC-MS 

in seawater coastal water 

Trends in Anal Chemistry, 23, #4, 341-350 

Gimeno, R. A.; Marce, R. M.*; Borrull, F. 

2029 Musk Study of the photoinduced degradation of polycyclic PDMS fiber GC-MS 

compounds musk compounds by SPME and GC-MS headspace 

in water Rapid Comm in Mass Spec, 18, #111, 1186-1192 

Sanchez-Prado, L; Llompart,M; Lores,M; 

Garcia-Jares,C; Cela, R 

2030 PBDEs in Investigation of photodegradation products generated PDMS fiber GC-MS 

water after UV-irradiation of five polybrominated diphenyl 

ethers using photo SPME 

Journal of Chromatography A, 1071, #1-2, 85-92 

Sanchez-Prado, L.; Llompart,M.; Lores,M.; 

Garcia-Jares,C.; Cela, R. 

2031 Organics in Determination of organic contaminants in coastal water GC 

water TrAC Trends Anal. Chem., 23, #4, 341-350 

Borrull, F.; Gimeno, R.A.; Marce, R.M. 

2032 Acaricide Determination of the acaricide fenbutatin oxide in water headspace GC-MS 

fenbutatin samples by automated headspace-SPME-GC/MS NaEt 4B derivatives 

oxide in water J. Sep. Sci., 26, #7, 665-668 30min @ 80°C 

Devos, Christophe; Moens, Luc; Sandra, Pat 

2033 Alkylbezene- Linear alkylbenzensulphonic acids (LAS) oxidation by headspace GC-MS 

sulphonic acid H2O2 and O2: An investigation by GC & LC coupled w/MS 

in water Appl. Catal. B Environ.59, #1-2, 113-120 

Cuzzola, Angela; Raffaelli, Andrea; Salvadori, Piero 

2034 Dioxin, hexa- SPME for the evaluation of partition coefficients of a immersed GC-ECD 

chlorobenzene chlorinated dioxin and hexachlorobenzene into 

in water humic substances 

Analytical Sciences, 20, #5, 787-791 

Yabuta, H.; Fukushima, M. *; Tanaka, F.; 

Ichikawa, H.; Tatsumi, K. 





2035 Dioxin, hexa- Influence of chemical characteristics of humic substances on headspace GC-ECD 

chlorobenzene the partition coefficient of a chlorinated dioxin 

in water Chemosphere, 58,#10, 1319-1326 

Fukushima, Masami; Ichikawa, Hiroyasu; Kikuchi, Atsunori 

Tanaka, Fumiko; Tatsumi, Kenji; Yabuta, Hikaru 

2036 Molinate A case study of molinate application in a Portuguese immersed sampling GC-FPD 

herbicides rice field: Herbicide dissipation and proposal of a 

in water clean-up methodology 

Chemosphere, 59, #7, 1059-1065 

Castro, M; Manaia, C.; Nunes, O.; Silva-Ferreira, A. 

2037 Organics in Determination of organic contaminants in coastal water LC-MS 

seawater Trends in Analytical Chemistry, 23, #4, 341-350 

Gimeno, R. A.; Marce, R. M.; Borrull, F. 

2038 Organometals Simultaneous multi-elemental speciation analysis 65µm PDMS-DVB ICP-TOF-MS 

in water of organometallic compounds by SPME and multi- 75µm Carboxen 

capillary GC hyphenated to ICP-time-of-flight-MS headspace 

J Anal At Spectrom, 19, #7, 867-875 NaEt 4B derivatives 

Adams, Freddy C.; Infante, Heidi G; Jitaru, Petru 

2039 Mercury Speciation analysis of mercury by SPME and multi- 75µm Carboxen GC-ICP-MS 

in water capillary GC- inductively coupled plasma-TOF-MS headspace 

J. Chromatogr. A,1055, #1-2, 197-207 NaEt 4B derivatives 

Adams, Freddy C.; Jitaru, Petru 

2040 Iodophenols Fast speciation analysis of iodophenol compounds immersion sampling ICP-MS 

in river water in river waters by capillary electrophoresis- 

ICP-MS with off-line SPME 

Electrophoresis, 25, #12, 1843-1851 

Kannamikumarath, Sasi S.; Wuilloud, Rodolfo G.; 

Jayasinghe, Sarath; Caruso, Joseph A. 

2041 Organic Optimization of SPME for the GC-MS analysis of varios fibers GC/MS 

pollutants persistent organic pollutants 

from water J AOAC Int, 87, #4, 1021-1027 

Alpendurada, M.; Gago-MARTINEZ, A; Nogueiras, M, 

Prado, Juan; Rellan, Satvdra;Vetter, Walter 

2042 Amines, fatty Use of headspace SPME to characterize odour headspace GC/MS or GC/NPD 

acids, alky- compounds in subsurface flow constructed wetland 

sulfides in for wastewater treatment 

wastewater Water Sci. Technol., 49, #9, 89-98 

Aguirre, P.; Bayona, J.M.; Garcia, J.; Huang, Y.; 

Mujeriego, R.; Ortiz, L. 

2043 Odourous Development of a simple and sensitive method for the 75µm Carboxen GC/MS or GC/FID/O 

compounds characterization of odorous waste gasemissions by headspace 

from waste means of SPME-GC-MS/olfactometry 

gas Waste Manage., 25, #9, 872-879 

Jans, M.; Kleeberg, K.K.; Liu, Y.; Schlegelmilch, M.; 

Stegmann, R.; Streese, J. 

2044 PAHs in Comparison of strategies for extraction of high immersion sampling HPLC-FLD 

drinking water molecular weight PAHs from drinking waters 

J Agr Food Chem, 52, #23, 6897-6903 

Garcia-Falcon, M. S.; Perez-Lamela, M.; 

Simal-Gandara, J. 

2045 PAHs in Determination of PAHs in water by SPME-HPLC 35min immersed extract HPLC-FLD 

water Analytical Sciences, 20, #10, 1383-1388 added 1.5M sodium 

Chen, H. W. monochloroacetate 

2046 organochlorides Determination of organochlorides in water using 65µm PDMS-DVB GC 

in water solid-phase microextraction coupled to GC 45sec @ 50°C 

Am Lab, 34. #17, 12-14 

Huang, Min-Jia; Li, Ju-Bai; Liang, Bing; Ou, Qing-Yu 





2047 PAHs in SPME measurement of parent and alkyl PAHs in immersion sampling GC/ MS 

water milliliter sediment pore water samples and 

determination of K' values 

Environ. Sci. Technol,.39, #8,2795-2803 

Grabanski, C.; Hawthorne, S.; Kreitinger, J..; Miller, D. 

2048 Organics in Coupling of SPME with MCC/UV-IMS as a tool for rapid on-site headspace UV-IMS 

groundwater detection of groundwater and surface water contamination 


Baumbach, J.I.; Klockow, D.; Walendzik, G. 

2049 2,4,6-Trichloro- Detection of 2,4,6-trichloroanisole in chlorinated water at 100µm PDMS GC-ECD 

anisole in nanogram per litre levels by SPME-GC-ECD headspace 

chlorinated Anal. Bioanal. Chem., 382, #2, 341-346 

water Da Silva, Joaquim C. G. Esteves; Pinheiro, Paula B. M. 

2050 Clenbuterol SPME and headspace derivatization of clenbuterol followed 85µm polyacrylate GC-FID, GC-MS 

in water by GC-FID and GC-SIMMS quantification HMDS derivative 

Anal. Bioanal. Chem., 375, #3, 460-464 headspace 

Engelmann, M.D.; Hinz, D.; Wenclawiak, B.W. 

2051 Explosives Use of SPME-GC-ECD for the determination of energetic 65µm CW/DVB GC-ECD 

in water chemicals, in marine samples 30% salt added 

J Chromatogr A, 1066, #1-2, 177-187 

Monteil-Rivera, Fanny; Beaulieu, Chantale; Hawari, J. 

2051 Explosives SPME ion mobility spectrometer interface for explosive headspace Ion mobility 

in water and taggant detection spectrometry 

J Sep Science, 28, #2, 177-183 

Perr, Jeannette M.; Furton, Kenneth G.; Almirall, J. 

2052 Explosives Determination of explosives in environmental water samples 50µm CW-TPR HPLC-UV 

in water by SPME-liquid chromatography immersed 

J. Chromatogr. A, 1048, #2, 213-221 

Beaulieu,C.; Deschamps,S.; Hawari,J.; 

Monteil-Rivera,F.; Paquet,L. 

2053 Anthracen In-tube capillary solid-phase microextraction coupled In-tube capillary HPLC 

in water on-line to micro-HPL 


Shu, X.; Yang, B. C.; Tan, F.; Guan, Y. F. 

2054 Volatiles Further SPME-GC-MS applications: "On-fibre" and immersion sampling GC-MS 

from musks and aqueous photodegradation of nitro musks 

J. Chromatogr. A, 1048. #1, 73-80 

Cela, R.; Garcia-Jares, C.; Llompart, M.; Lores, M.; 

Lourido, M.; Sanchez-Prado, L. 

2055 2,4,6-trinitro- SPME for predicting the bioavailability of 85µm polyacrylate GC-MS 

toluene in 2,4,6-trinitrotoluene and its primary transformation 

water & products in sediment and water 

sediment Environ. Toxicol. Chem., 24, #5, 1059-1066 

Conder, Jason M.; La Point, Thomas W. 

2056 Aromatics Rapid analysis of aromatic contaminants in water samples GC-MS 

in water by means of laser ionization mass spectrometry 

Anal. Bioanal. Chem, 377, #7-8, 1124-1132 

Globig, Daniel; Weickhardt, Christian 

2057 phycoerythrin Coupling of SPME and capillary isoelectric focusing 10 min sampling CIEF-WCID 

in water w/ laser-induced fluorescence whole column imaging 

detection for protein analysis. 

Analytical Chemistry, 77, #1, 165-171 

Liu, Z.; Pawliszyn, J. * 

2058 Nitroaromatics Spme fibers for estimating the toxicity of nitroaromatic 85µm polyacrylate GC 

in sediment, compounds immersion sampling 

water Aquatic Ecosystem Health & Mgmt, 7, #3, 387-397 

Conder, J. M.; Lotufo, G. R.; Bowen, A. T.; Turner, P. K.; 

La Point, T. W.; Steevens, J. A. 





2059 Perfluoro- Determination of perfluorocarboxylic acids in aqueous headspace CI-MS 

carboxylic matrices by ion-pair SPME in-port derivatization GC butyl ester derivative 

acod in negative ion chemical ionization mass spectrometry 

water J Chromatogr, A, 1042, #1-2, 155-162 

Alzaga, R.; Bayona, J. M.* 

2060 perfluoro- Development of a procedure for the determination of headspace CI-MS 

carboxylic perfluorocarboxylic acids in sediments by pressurised 

acod in fluid extraction, headspace SPME followed by GCMS 

water Journal of Chromatography, A, 1083, #1-2, 1-6 

Alzaga, R.; Bayona, J.M.; Jover, E.; Salgado-Petinal, C. 

2061 Dialkyl ethers Determination of fuel dialkyl ethers and BTEX in water 65µm PDMS-DVB GC-FID 

in water using headspace SPME and GC-FID headspace 

J Chromatogra A, 1033, #2, 193-203 10min @ 10°C 

Arambarri, I.; Lasa, M.; Garcia, Rosa; Millan, E. 

2062 MTBE Identification of MTBE in water by SPME and GC-MS headspace GC/MS 

in water Am Lab, 34, #21, 34 

Blasi, G.; Guidotti, M.; Lucarelli, E.; Onorati, B.; 

Ravaioli, G.; Stella, D. 

2063 Taste/odor Analysis of taste- and odor-causing compounds review technique GC 

in water in drinking water using solid-phase microextraction 

Am Lab, 35, #17, 42-46 

Voit, Jim 

2064 MTBE Interlaboratory comparison study for the determination various fibers GC/MS 

in water of methyl tert-butyl ether in water GC-FID 


Fuhrer, M.; Kandler, W.; Krska, R.; 

Schuhmacher, R.; Stadlmann, C. 

2065 MTBE, TBA Comparison of SPME headspace analysis to U.S. 75µm Carboxen GC-MS 

in water EPA Method 5030/8260B for MTBE monitoring headspace 

Ground Water Monit. Rem., 25, #2, 52-58 

Oh, Keun-Chan; Stringfellow, William T. 

2066 MTBE Observations on SPME for MTBE analysis headspace GC-MS 

in water Chemosphere, 57, #6, 523-527 

Bergendahl, J.; Erdem-Senatalar, Ayse; Thompson, Robert W. 

2067 MTBE Sources, distribution and behaviour of methyl tert-butyl 75µm Carboxen GC-MS 

in water ether (MTBE) in the Tamar Estuary, UK 75% salt added 

Chemosphere, 57, #6, 429-437 headspace 

Bayona, Josep M.; Guitart, Carlos; Readman, James W. 

2068 Chromium in Spme for the determination of chromium in sea-water. 100µm PDMS GC-ECD 

sea water J of Anal Atomic Spectrometry, 19, #9, 1098-1103 headspace derivatives ICP-MS, EI-MS 

Abranko, L.; Yang, L.; Sturgeon, R. L.; Fodor, P.; Mester, Z. (trifluoroacetylacetone) 

2069 Saccharides Micro-solid-phase extraction with helical-solid-sorbent in headspace GC-MS 

from water & the presence of organic solvent for GC-MS analysis of - per- O -methylation 

juices per-O-methylated mono and disaccharides. 


Ciucanu, I.; Swallow, K. C.; Caprita, R. 

2070 Volatiles in Analysis of compound-specific carbon isotopic compositions cryofocused injection GC 

water of trace-level volatile organic compounds in aqueous phases. headspace sampling 

Sepu, 22, #4, 439-441 

Liu, G. Q.; Zhang, G.; Huang, S. Q.; Peng, X. Z.; Chen, H. H. 

2071 Volatiles in On-line coupling of in-tube SPME to capillary GC GC 

water for trace analysis of aqueous samples. 

Sepu, 22, #4, 354-357 

Guan, Y. F.; Wang, H. W.; Liu, W. M. 





2071 Chlorinated SPE versus SPME for the determination of chlorinated immersed fiber GC-NCI-MS 

parafins in paraffins in water using GC-negative chemical ion MS 

water J Chromatography, A, 1025, #2, 157-162 

Castells, P.; Santos, F. J.; Galceran, M. T.* 

2073 Chlorinated Development of a SPME-based method for sampling 100µm PDMS GC 

hydrocarbons of persistent chlorinated hydrocarbons in an in situ sampling 

in water urbanized coastal environment 18 to 43 days 

Environ. Sci. Technol., 38, #21, 5737-5743 

Diehl, Dario W.; Tsukada, David; Zeng, Eddy Y. 

2074 Odors from An automated headspace SPME-GC-ITMS technique for 65µm PDMS-DVB GC-ITMS 

water taste and odor compound identification headspace 

Water Qual. Res. J. Can., 39, #3, 213-222 

Davies, John-Mark; Furtula, Vesna; Mazumder, Asit 

2075 PAHs in Determination of PAHs in water by SPME-GC-MS agitation applied GC-MS 

water Anal. Chim. Acta, 523, #2, 259-267 immersed 

King, A.J.; Readman, J.W.; Zhou, J.L. 

2076 Phenols Determination of phenolic compounds in wastewater 85µm polyacrylate GC-FID 

in waste samples using a novel fiber by SPME coupled to GC 

water Analytica Chimica Acta, 538, #1-2, 63-70 

Zhou, Furong; Li, Xiujuan; Zeng, Zhaorui 

2077 Selenite SPME - capillary GC combined w/ microwave-Inducted NaEt 4B derivatives GC-MIP-AED 

in water plasma atomic-emission spectrometry for selenite headspace 

determination 

Anal& Bioanalytical Chem, 379, #5, 842-848 

Dimitrakakis, E.; Haberhauer-Troyer, C. *; Abe, Y.; 

Ochsenkuhn-Petropoulou, M. T.; Rosenberg, E. 

Pesticides 

441 Pesticides Determination of Pesticides in Aqueous Environmental 

in water Samples via SPME (Solid-Phase Microextraction) 

GIT Frachz. Lab. 39: 25-26 (1995) 

Eisert, R., Levsen, K. 

522 Pesticides Quantitative analysis of pesticides in water by SPME 100µm PDMS, 65µm GC-MS 

in water coupled with Mass Spectrometry DVB/PDMS 

Spectra. Anal. 1999, 28(208), 23-29 30 min 

Massat, F. Laurent, A. agitated 

523 Organochlorine & A Systematic Approach to Optimize SPME determination 

organophosphorus of Pesticides in Ethanol/Water mixtures 

in water/ethanol used as Food Simulates 

Anal. Chem. (1999), 71(13), 2417-2422 

Batlle, R, Sanchez, C., Nerin, C. 

442 Solid-Phase Microextraction (SPME) 

GIT Frachz. Lab. 39: 325-331 (1995) 

Popp, P., Kauert, A., Kalbitz, K. 

781 Organophosphorus Determination of organophosphorus insecticides in natural 85µm polyacrylate GC-FTD and 

pesticides waters using SPE-disks and SPME followed by GC-MS 

in water GC-FTD and GC-MS 

Fresenius' J Anal Chem (2000) 368(6) 616-623 

Lambropoulou, D.; Sakellarides, T.; Albanis, T. 

915 Organophosphorus Optimization of headspace SPME conditions for the 

pesticides determination of organophorus insecticides in natural water 

in water J. Chromatogr. A (2001) 922(1-2) 243-255 

Lambropoulou, D.; Albanis, T. 





123 Organophosphorus Pesticide Analysis by SPME 100µm PDMS GC-FID 

pesticides Am. Env. Lab. April 1997, pp 20-22 60 min 

in water Eisert, R., Gorecki, T., Pawliszyn, J. immersion 

104 Insecticides, Influence of Ethanol on Pesticide Extraction in 100µm PDMS GC-MS 

fungicides Aqueous Solutions by SPME 30 min 

in water J. Agric. Food Chem. 44: 3871-3877 (1996) 

Urruty, L., Montury, M. 

headspace 

122 Pesticides Simultaneous Determination of 60 Pesticides in Water 100µm PDMS GC-MS 

in water Using SPME and GC/MS 50 min 

Analyst 121: 929-938, July 1996 immersion 

Boyd-Boland, A., Magdic, S., Pawliszyn, J. stirring, salt added 

241 Nitrogen- & phosphate- Solid-Phase Microextraction of Nitrogen- and Phosphorus- 100µm PDMS GC-NPD 

pesticides Containing Pesticides from Water and GC Analysis 60 min 

in water Environ. Sci. Technol. 30: 3259-3265 (1996) immersion 

Choudhury, T., Gerhardt, K., Mawhinney, T. stirring, salt added 

52 Pesticides Determination of Organophosphorus, Triazine, and 100µm PDMS, GC-NPD 

in water 2,6-Dinitroanailine Pesticides in Aqueous Samples via 85µm polyacrylate 

SPME and GC with NPD Detection 25 min 

Fresenius J. Anal. Chem. 351: 555-562 (1995) immersion 

Eisert, R., Levsen, K. stirring, salt added 

443 Organophosphate Simple Extraction of Organophosphate Pesticides Using GC-NPD, -MS 

pesticides (SPME) Before Capillary Gas Chromatography 

in water Hochudoku 13 (2): 122-123 (1995) 

Lee, X., Kumazawa, T., Taguchi, T., Sato, K., Suzuki, O. 

167 Organophosphorus Analysis of Organophosphorus Insecticides from 85µm polyacrylate GC-NPD 

insecticides Environmental Samples Using SPME 60°C, 60 min 

in water J. Chromatogr. A 736: 219-228 (1996) immersion 

Magdic, S., Boyd-Boland, A., Jinno, K., Pawliszyn, J. salt added 

861 Organophosphorus Solventless sample preparation procedure for HPLC 

pesticides organophosphorus pesticides analysis using SPME and 

in water on-line supercritical fluid extraction/HPLC technique. 

Analytica Chimica Acta (2001) 433(2) 207-215 

Jinno, K; Kiso, Yoshiaki; S, Yoshihiro; S, Shamsul H 

93 Organophosphorus Matrix Effects on SPME of Organophosphorus 85µm polyacrylate GC-NPD 

pesticides Pesticides from Water 60°C, 45 min 

in water J. Chromatogr. A 767: 195-203 (1997) immersion 

Valor, I., Molto, J., Apraiz, D., Font, G. stirring 

839 52 Pesticides, PCBs SPME of 52 pesticides and polychlorinated biphenyls: 

efficiencies of the SPME coatings PDMS, polyacrylate, 

PDMS/DVB, Carboxen/PDMS, and Carbowax/DVB 

J. Sep. Sci. 2001) 24(1), 39-48 

Valor, I; Perez, M; Cortada, C; Apraiz, D; Molto, J; Font, G 

65µm PDMS/DVB 

118 Organophosphorus Solid Phase Microextraction of Organophosphorus 65µm PDMS/DVB 

pesticides Pesticides from Water 30 min 

in water J. Chromatogr. A 759: 225-230 (1997) 

Sng, M., Lee, F., Lakso, H. 

immersion 

524 Organophosphorus Determination of organophosphorus pesticides in water 100µm PDMS GC-MS 

pesticides using GC-MS 

in water Qim. Nova (1999), 22(2), 197-200 

Silva, F., Cardeal, Z., De Carvalho, C. 

Portuguese 





350 Organophosphorus The Application of SPME in the Analysis of 100µm PDMS GC-FPD 

pesticides Organophosphorus Pesticides in a Food Plant 90 min 

in food plant Environ Sci. Technol. 1998, 32, 3816-820 

Chen, W., Poon, K., Lam, M. 

immersion (water) 

525 Pyrethrins in Heterogenic catalytic hydrolysis and analysis of natural 100µm PDMS GC-FID or 

insect spray, pyrethrins in subcritcal water coupled w/SPME-GC-MS 20 min @ pH 2 MSD 

shampoo, flowers Fresenius'J. Anal. Chem. 1999, 364(7), 625-630 

Krappe, M, Hawthorne, S., Weclawiak, B. 

immersed 

705 Pyrethroids SPME of pyrethroid pesticides from water at low and 100µm PDMS GC-ECD 

in water sub-ppt levels at different temperature 5 min 

J.High Resolut.Chromatogr. (2000), 23(7/8), 485-488 

Barrionuevo, W., Lancas, F. 

40-90°C 

837 Pyrethroids Solid-phase extraction (SPE) and solid-phase microextraction 

in water ( SPME ) of pyrethroids in water 

Quim. Nova (2001), 24(2), 172-175 

Barrionuevo, W., Lancas, F. 

299 Organophosphorus Online Determination of Organophosphorus Pesticides in 30µm PDMS GC-TCD 

pesticides Water by SPME and GC with Thermionic-Selective Detection 30 min 

in water J. High Resolut. Chromatogr. 20 (9): 487-492(1997 immersion 

Lopez-Avial, V., Young, R., Becker, W. stirring 

390 Organophosphorus SPME for quantitative analysis of organophosphorus 100µm PDMS, GC-NPD 

pesticides Pesticides in Environmental Water Samples 85µm polyacrylate 

in water J. Chromatogr. A 808 (1998) 257-263 30 min 

Beltran, J., Lopez, F., Hernandez, F. stirring, salt added 

706 Pesticides SPME for the determination of systemic and non-volatile 100µm PDMS GC-NPD 

in water pesticides in river water using GC with NPC and ECD 15min ECD 

J. Chromatogr. A 893(2000) 347-358 

Sampedro, M.; et al 

immersed 

868 Herbicides Determination of herbicides in natural waters using (SPME) GC-MS 

in water and GC coupled with flame thermionic and MS detection 

Int. J. Environ. Anal. Chem (2000) 78(3-4), 223-240 

Lambropoulou, D.; Konstantinou, I; Albanis, T. 

707 Nitrogen herbicides Use of SPME for the Quantitative determination of Carbowax DVB GC-MS 

in water Herbicides in soil and water samples 30 min SIM mode 

Anal. Chem. 2000, 72, 2313-2322 

Hernandez, F., Beltran, J., Lopez, F, Gaspar, J. 

salt added, stirred 

28 Nitrogen herbicides Solid Phase Microextraction of Nitrogen-Containing 85µm polyacrylate GC-NPD 

in water Herbicides 50 min 

J Chromatogr. 704: 163-172 (1995) immersion 

Boyd-Boland, A., Pawliszyn, J. pH 2, salt added 

53 Triazine herbicides Automated Determination of S-Triazine Herbicides 100µm PDMS GC-NPD 

in water Using Solid-Phase Microextraction 15 min (manual) 

J. Chromatogr. 705: 305-312 (1995) 3 min (automated) 

Barnabas, I., Dean, J., Fowlis, I., Owen, S. immersion 

177 Triazine herbicides Determination of Triazine Herbicides in Environmental Samples 100µm PDMS GC-NPD 

J. Chromatogr. 733: 295-335 (1996) (review) 10 min 

Dean, J., Wade, G., Barnabas, I. immersion (water) 





111 Triazine herbicides Validation of SPME for the Analysis of Triazine Herbicides Carbowax/DVB GC-NPD, 

in water at ppt Level in Aqueous Samples 30 min GC-MS 

J. Chromatogr. A. 795 (1998) 371-376 immersion, stirring 

Nilsson, T., Ferrari, R., Basta, R., Dellavedova, P. salt added 

708 Urea herbicides Indirect analysis of urea herbicides from environmental 85µm polyacrylate GC-NPD 

in water water using solid phase microextraction immersed 

J. Chromatogr. A. 890 (2000) 303-312 

Berrada, H., Font,G., Molto, J. 

sat. salt, pH 4 

231 Pesticides Minimization of Solvent Consumption in Pesticide overview 

Residue Analysis 

J. Chromatogr. A 754: 43-47 (1996) 

Wan, H., Wong, M. 

article 

838 Chlorinated Determination of chlorine-containing pesticides in aqueous 

pesticides media by solid-phase microextraction method 

in water Zh. Prikl. Khim (2000) 73(11), 1877-1882 

Stolyarov, B. V.; Boiko, V. V 

156 Organochlorine Online Determination of Organochlorine Pesticides in Water 100µm PDMS GC-ECD 

pesticides by SPME and GC-ECD 20 min 

in water J. High Res. Chromatogr. 19(5): 24756 (1996) immersion 

Young, R., Lopez-Avila, V., Beckert, W. stirring 

180 Chlorinated pesticides Optimization of a Technique of SPME and Capillary GC with GC-ECD 

in water ECD for the Determination of Nine Organochlorine Pesticides 

in Drinking Water 

Analusis 25 (3): 51-54 (1997) 

Almeida, M., Conceicao, P., Alpendurada, M. 

709 Chlorinated Application of SPME and GC with ECD for the 100µm PDMS GC-ECD 

pesticides analysis of chlorinated pesticides in water 20min. 

in water Spectra Anal (2000) 29(213) 

Boussahel, R., Bouland, S., Montiel, A., Moussaoui, K 

864 Organochlorine Comparison of three analytical procedures for determination GC-ECD 

pesticides of organochlorine pesticides and their by-products in water GC-MS 

in water suspension during photocatalytic oxidation 

Chemia Analityczna (Warsaw) (2000) 45(6) 901-910 

Wiergowski, M.; Zaleska, A.; Biziuk, M.; Hupka, J. 

710 Organochlorine Monitoring organochlorine pesticides from landfill leachates 100µm PDMS GC-ECD 

pesticides by GC-ECD detection after solid phase microextraction 30 min @ 55°C 

in water J. Chromatogr. A 891 (2000) 305-311 immersion 

Bras, I., Santos, L., Alves, A. stirring 

711 Organochlorine SPME for organochlorine pesticides residues analysis in 100µm PDMS GC-MS 

pesticides Chinese herbal formulations 

in herbs J. Chromatogr. A 898 (2000) 245-256 

Hwang, B. H.; Lee, M. R 

43 Organophosphorus Element-Selective Detection of Pesticides by Gas 100µm PDMS GC-AED 

pesticides Chromatography-Atomic Emission Detection and SPME 20 min 

in water J. Chromatogr. A 683: 175-183 (1994) 

Eisert, R., Levsen, K., Wunsch, G. 

immersion 

526 Organophosphorus Determination of organophosphorus pesticides in water 85µm polyacrylate GC-FPD 

in water by SPME 

Talanta (1999), 49(2), 393-402 

Su, P., Huang, S. 





712 Pesticide residue Solid Phase microextraction in pesticides residue analysis review article 

various matrices J. Chromatogr. A 885 (2000) 389-404 

Beltran, J., Lopez, F., Hernandez, F. 

713 Pesticides An approach to solventless sample preparation HPLC 

in water procedure for pesticide analysis using SPME/supercritical 

fluid extraction technique 

Analytica Chimical Acta 2000, 418(1), 69-77 

Salleh, S., Saito, Y., Jinno, K. 

917 Organophosphorus Solventless sample preparation procedure for organo- HPLC 

pesticides phosphorus pesticides analysis using SPME and on-line 

in water supercritical fluid extraction/HPLC technique 

Analytica Cheimica Acta 2001, 433(2), 207-215 

Salleh, S., Saito, Y., Kiso, Y., Jinno, K. 

87 Pesticides Determination of Pesticides in Aqueous Samples by SPME GC-MS 

in water In-Line Coupled to Gas Chromatography-Mass Spectrometry 

Am. Soc. Mass Spectrom. 6: 1119-1130 (1995) 


157 Contaminants Development of a Prototype System for Quasi-Continuous 85µm polyacrylate GC-FID 

in water Analysis of Organic Contaminants in Surface or Sewage 10 min 

Water Based on In-Line Coupling of SPME to GC 

J. Chromatogr. A 737: 59 (1996) 

Eisert, R., Levsen, K., Wuensch, G. 

immersion 

77 Metolachlor Solid Phase Microextraction of the Herbicide Metolachlor 100µm PDMS GC-ECD 

in water in Runoff and Tile Drainage Water Samples 15 min 

J. Chromatogr. A 725: 129 (1996) immersion 

Webster, G., Gaynor, J., Ng, H., Graham, J., Sama, L. stirring 

193 Metolachlor Comparative SPE, SPME, and Immunoassay Analysis 100µm PDMS GC-ECD 

in water of Metolachlor in Surface Runoff and Tile Drainage 15 min 

J. Agric. Food Chem. 44: 2736-2741 (1996) immersion 

Graham, K., Ng, H., Tan, C., Gaynor, J., Cancilla, D., 

Webster, G., Drury, C., Welacky, T., Sarna, L. 

stirring 

112 Polar herbicides Application of SPME Coupled with HPLC for Analysis 

of Polar Herbicides 

Request from Environmental Institute, European Commission 

Joint Research Centre, 21020 Ispra (Va) Italy 

Nilsson, T. 

HPLC 

190 Pesticides Analysis of Pesticides in Environmental Water Sample 85µm polyacrylate HPLC-UV 

in water by SPME-HPLC 60°C, 60 min 220nm 

J. Chromatogr. A754: 137-144 (1996) immersion 

Jinno, K., Muramats, T., Saito, Y., Kiso, Y., Magdic, S., 

Pawliszyn, J. 

salt added 

242 Pesticides Pesticides by Solid-Phase Microextraction: Results of 100µm PDMS GC-MS 

in water Round Robin Test 45 min 

Analyst (Cambridge) 121: 1381-1386 (1996) immersion 

Gorecki, T., Mindrup, R., Pawliszyn, J. stirring 

438 Pesticides in SPME and GC for Rapid Analysis of Pesticides Review GC-MS 

water Aanalusis (1998), 26(6), M137-M143 

Miege, C., Dugay, J. 





298 Chlorinated pesticides Analysis of Organochlorine Pesticides by SPME 100µm PDMS GC-MS, -NPD 

J. Chromatogr. A 723(1): 111-112 (1996) 90 min 

Magdic, S., Pawliszyn, J. immersion 

salt added 

527 Organochlorine Optimization of SPME conditions using a response surface 85µm polyacrylate GC-ECD 

pesticides methodology to determine organochlorine pesticides in 45 min @ 60°C 

in water water by GC-ECS immersed 

J. Chromatogr. A (1999), 844(1+2), 425-432 

Aguilar, C., Penalver, A, Pocurull, E., Ferre, J., Borrull, F., 

Marce, R. 

agitated 

300 Pesticides Effect of Various Parameters Governing SPME for the Trace 65µm PDMS/DVB GC-NPD 

in water Determination of Pesticides in Water 25°C, 30 min 

J. Chromatogr., A 795 (1): 27-42 (1998) immersion 

Dugay, J., Miege, C., Hennion, M. pH 7, salt added 

301 Pesticides SPME and GC-MS Detection for the Determination of 85µm polyacrylate GC-MS 

in water Pesticides in Aqueous Samples 55°C, 45 min 

J. Chromatogr. A. 795 (1): 105-115 (1998) immersion 

Aguilar, C., Penalver, S., Pocurull, E., Borrull, F., Marce, R. stirring, salt added 

528 Pesticides Analysis of some pesticides in water samples using SPME- GC-MS 

in water GC with different Mass Spectrometric techniques 

J. Chromatogr, A, 859(2): 193-202 (1999) 

Natangelo, M., Tavazzi, S., Fanelli, R., Befenatti, E. 

714 Fentin Headspace SPME capillary GC-ICP-MS for the 100µm PDMS GC-ICP-MS 

in environmental determination of the organotin pesticide fentin in 10-20 min 

samples environmental samples 75-85°C 

J.Anal. At. Spectrom. (2000), 15(6), 651-656 NaBEt4 

Vercauteren, J., DeMeester, A, DeSmaele, T. 

Vanhaecka, F., Moens, L., Dams, R., Sandra, P. 

pH 8 

445 Pesticides Analysis of Pesticides in Environmental Water Samples by 85µm polyacrylate HPLC-UV 

in water SPME-HPLC 60°C, 60 min 220nm 

J. Chromatogr. A 754 (1+2): 137-144 (1996) immersion 

Jinno, L., Muramatsu, T., Saito, Y., Kiso, Y., Magdic, S., 

Pawliszyn, J. 


587 Pesticides Study on solventless sample preparation of pesticides with 85µm polyacrylate HPLC-UV 

SPME-SFE technique. 

Chromatography. Jun 1999; 20(2): 126-127 

Selleh,-SH; Saito,-Y; Jinno,-K 

3 hr @ 60°C 

715 Biologically active SPME-GC-MS of biologically active substance in 85µm polyacrylate GC-MS 

substance in water water samples 65µm Carbowax/DVB 

J. Chromatogr. A., (2000) 873(1), 95-106 

Moeder, M., Schrader, S., Winkler, M., Popp, P. 

30 min 

223 PCBs in SPME and Headspace SPME for the Determination of PCBs 100µm PDMS GC-MSD 

water in Water Samples 100°C, 30 min 

Anal. Chem. 1998, 70, 2510-2515 headspace/immersion 

Llompart, M., Fingas, M., Li, K. stirring 

973 


pesticides in water Determination of organochlorine pesticides in ground water. 

J.Chromatogr. A (2002) 963(1-2), 95-105 

Perez-Trujillo, J.P.; Frias, S.; Conde, J.E.; Rodriguez-Delgado, M.A. 

Various 





977 Pesticides in water Comparison of different fibers for the analysis of pesticides in water. 

J.Chromatogr. A (2002) 963(1-2), 19-26 

Goncalves, C.; Alpendurada, M.F. 

Various 

982 Pesticides in water Monitoring of pesticides in the Kalamas River (Greece) 

J.Chromatogr. A (2002) 963(1-2), 107-116 

Lambropoulou, D. A.; Sakkas, V.A.; Hela, D.G.; Albanis, T.A. 


998 Pesticides in oranges 

1000 

Pesticides in drinking 

water 

1004 Pesticides in water 

1009 

Pesticides in 

groundwater 

1011 Acetochlor in water 

1019 

1046 

1047 

Fenoxycarb in 

environmental samples 

Organonitrogen 

pesticides in water. 


pesticides. 

1048 Fenthion and parathion 

Comparison of microextraction procedures to determine pesticides in 

oranges by liquid chromatography-mass spectrometry. LC-MS 

J.Chromatogr. A (2002) 970(1-2), 201-212 

Blasco, C.; Font, G.; Pico, Y. 

Multiresidue method for the simultaneous determination of four groups of 

pesticides in ground and drinking waters, using solid-phase microextractiongas 

chromatography with electron-capture and thermionic specific detection. PDMS/DVB GC 

J.Chromatogr. A (2002) 968(1-2), 177-190. 

Goncalves, C.; Alpendurada, M. F.* 

Monitoring of priority pesticides using SPME (solid phase microextraction) in 

river water from Greece 

Water Sc. Technol. Water Supply (2003) 3 (1-2), 335-342. 

Albanis, T.A.; Hela, D.; Lambropoulou, D.A.; Sakkas, V.A. 

PDMS GC-MS 

Determination of atrazine and four organophosphorus pesticides in ground 

water using solid phase microextraction ( SPME ) followed by gas 

chromatography with selected-ion monitoring. 

J.Chromatogr. A (2002) 972(2), 183-194. 

Tomkins, B. A.; Ilgner, R. H. 

65 um PDMS/DVB GC-SIM 

An enzyme-linked immunosorbent assay (ELISA) for the detection of 

acetochlor GC-MS 

International Journal of Environ. Anal. Chem. (2002) 82 (11-12), 879-891. 

Belai, Ivan; Eremin, Sergei; Hegedus, Gyongyver; Krikunova, Vitalia; 

Szekacs, Andras 

Evaluation of an enzyme immunoassay for the detection of the insect 

growth regulator fenoxycarb in environmental and biological samples. GC-MS 

Pest Management Science (2003) 59 (4), 410-416. 

Szekacs, Andras; Le, Hong T. M.; Szurdoki, Ferenc 

Application of solid-phase microextraction for the determination of 

organonitrogen pesticides in aqueous samples by gas chromatography with 

nitrogen-phosphorus detector. 


691-703. 

Le Calvez, N.; Bodineau, L.; Fischer, J. C. 

Various GC 

Analysis of organochlorine pesticides by solid-phase microextraction 

followed by gas chromatography-mass spectrometry. 


651-657. 

Zambonin, C. G.; Aresta, A.; Nilsson, T. 

Various GC-MS 

Application of solid-phase microextraction for monitoring the photocatalytic 

decomposition of fenthion and parathion in aqueous TiO 2 suspensions. GC-MS 

Analytica Chimica Acta (2002) 467 (1-2), 233-243. 

Sakkas, V. A.; Lambropoulou, D. A.; Sakellarides, T. M.; Albanis, T. A.* 


1096 

1113 





insecticides in water. 

Herbicides in 

environmental samples. 

1123 Herbicides 

1148 Dichlorvos 

1152 

1172 

1177 

1192 

1219 DDT 

1299 

1309 

Polar pesticides in water 

and wine. 

Oxidation residues of 

herbicides 

Pesticides in water 

samples. 

Atrazine and 

organophosphorus 

pesticides in soil 


insecticide residues. 

Phenylureas herbicides 

in aqueous samples. 

Validation of an SPME method, using PDMS, PA, PDMS-DVB, and CW- 

DVB SPME fiber coatings, for analysis of organophosphorus insecticides in 

natural waters. Various 



Solid-phase microextraction for herbicide determination in environmental 

samples GC 


Krutz, L.J.; Sciumbato, A.S.; Senseman, S.A. 

Determination of herbicides, including thermally labile phenylureas, by solidphase 



Carabias-Martinez, R.; Garcia-Hermida, C.; Hernandez-Mendez, J.; 

Rodriguez-Gonzalo, E.; Soriano-Bravo, F.E. 

Polyacrylate GC-MS 

Determination of dichlorvos by online microwave-assisted extraction 

coupled to headspace solid-phase microextraction and gas chromatographyelectron-capture 

detection. GC-ECD 


Chen, Y. I.; Su, Y. S.; Jen, J. F.* 

Analysis of polar pesticides in water and wine samples by automated intube 

solid-phase microextraction coupled with high-performance liquid 

chromatography-mass spectrometry. ESI-MS 


Wu, J. C.; Tragas, C.; Lord, H.; Pawliszyn, J. * 

Determination of oxadiazon residues by headspace solid-phase 



Araujo, Lilia; Navalon, Alberto; Prieto, Avismelsi; Vilchez, Jose Luis 

Solventless sample preparation for pesticides analysis in environmental 

water samples using solid-phase microextraction-high resolution gas 

chromatography/mass spectrometry (SPME-HRGC/MS) Various 

Journal of Environmental Science and Health - Part B Pesticides, Food 

Contaminants, and Agricultural Wastes (2003) 48 (4), 417-428. 

Lancas, Fernando M.; Souza, Dalva A. 

Solid-phase microextraction method for the determination of atrazine and 

four organophosphorus pesticides in soil samples by gas chromatography. 


Camara, C.; Bouaid, A.; Fernandez, P.; Gonzalez, M. J.; Ramos, L. 

GC-MS 

On-fiber photodegradation after solid-phase microextraction of p,p '-DDT 

and two of its major photoproducts, p,p '-DDE and p,p '-DDD. GC-MS 


Llompart, M.; Lores, M.; Lourido, M.; Sanchez-Prado, L.; Cela, R. 

Determination of organophosphorus insecticide residues by solid-phase 

microextraction coupled with gas chromatography-mass spectrometry. 

Sepu (2003), 21 (3), 273-276. 

Shuai, Q.; Yang, W.; Zheng, Y. J.; Zheng, C. G. 

PDMS or polyacrylate. GC-MS 

Solid-phase microextraction coupled with high-performance liquid 

chromatography for the determination of phenylurea herbicides in aqueous 

samples 


Huang, Shang-Da; Lin, Hsin-Hang; Sung, Yu-Hsiang 

PDMS-DVB, CW-TPR HPLC 





1316 Dichlorvos in pesticides. 

1355 Pesticides in honey. 

1364 

1369 


pesticides 

Pesticides in 

strawberries. 

1395 Pesticides 

1406 Pesticides 

1439 Herbicides in water 

1445 

1459 

1483 

Organochlorine pest. In 

water 

Methyl parathion in 

apples 

triazole in wine and 

strawberries 

1494 Organochlorine 

pesticides in water 

Pesticide vapours in confined atmospheres. Determination of dichlorvos by 

SPME-GC-MS at the mg m-3 level. 

Journal of Environmental Monitoring (2003) 5 (4), 574-577. 

Sanusi, Astrid; Montury, Michel; Ferrari, Federico; Millet, Maurice 

PDMS GC-MS 

A solid-phase microextraction-gas chromatography-mass spectrometry 

approach for antivarroa acaricides and pesticide residues in honey. 


Volante, M.; Galarini, R.; Miano, V.; Cattaneo, M.; Pecorelli, I.; Bianchi, M.; 

Marinoni, M. T.; Cossignani, L.; Damiani, P 


Application of solid-phase microextraction for the determination of 

organophosphorus pesticides in aqueous samples by gas chromatography 

with flame photometric detector. 

Talanta (2001) 55(4), 807-814. 

Yao, Z. W.; Jiang, G. B.*; Liu, J. M.; Cheng, W. 

Various GC-FID 

Focused microwave assistance for extracting some pesticide residues from 

strawberries into water before their determination by SPME/HPLC/DAD. 

Journal of Agricultural and Food Chemistry (2001) 49(11). 

Falqui-Cao, C.; Wang, Z.; Urruty, L.; Pommier, J. -J.; Montury, M. * 

60 um PDMS/DVB HPLC 

Analysis of acidic pesticides using in situ derivatization with 

alkylchloroformate and solid-phase microextraction ( SPME ) for GC-MS. 

Chemosphere (2001) 44(7), 1531-1539. 

Henriksen, T.; Svensmark, B.; Lindhardt, B.; Juhler, R. K. 

PDMS GC-MS 

Formation of volatile halogenated by-products during chlorination of 

isoproturon aqueous solutions. 

Chemosphere (2001) 45(3), 269-274. 

Lopez, A.; Ciannarella, R.; Mascolo, G.; Tiravanti, G. 


Factors affecting multiresidue determination of priority herbicides when 

using solid-phase microextraction. 

Journal of AOAC International (2002) 85(2), 486-493 

Albanis, Triantafyllos A.; Konstantinou, Ioannis K.; Lambropoulou, Dimitra 

A. 

Determination of organochlorine pesticides in water using microwave 

assisted headspace solid-phase microextraction and gas chromatography 


Jen, Jen-Fon; Li, Gwo-Chen; Li, Hong-Ping 

Field study for degradation of methyl parathion in apples cultivated with 

integrated crop management system. 

Bulletin of Environmental Contamination and Toxicology (2002) 69(6), 771- 

778 

Tsatsakis, A. M.; Danis, T. G.; Nikitovic, D. P.; Stratis, I. A.; Toutoudaki, M.; 

Tsakiris, I. N. 

Solid-phase microextraction and gas chromatography-mass spectrometry 

for the rapid screening of triazole residues in wine and strawberries. 


Zambonin, C. G.; Cilenti, A.; Palmisano, F. 

Determination of organochlorine pesticides in ground water using solidphase 

microextraction followed by dual-column gas chromatography with 

electron-capture detection. 


Tomkins, Bruce A.; Barnard, Angela R. 


100um PDMS and 85um 

Polyacrylate 

GC-FID, GC-MS 

Various fibers compared GC-ECD 

30um PDMS GC-ECD

1495 




Pesticides in bee 

products 

1505 Dimethylchloroarsine 

1522 

1531 

1554 

1551 

Analytical methods for pesticide residue determination in bee products. 

Journal of Food Protection (2002) 65(9), 1502-1511 

Fernandez, M.; Manes, J.; Pico, Y. 

Identification of dimethylchloroarsine near a former herbicide factory by 

headspace solid-phase microextraction gas chromatography-mass 

spectrometry. 

Chemosphere (2002) 48(9), 1003-1008 

Aldstadt, Joseph H., III; Killelea, Daniel R. 

85um Carboxen PDMS 

Stableflex 

GC-MS 

Chlorinated pesticides in 

Determination of chlorinated pesticides in water by SPME/GC. 

water 

Water Research (2002) 36(7), 1909-1911 

Boussahel, R.; Baudu, M.; Bouland, S.; Montiel, A.; Moussaoui, K. M. 

100um PDMS GC-ECD 

Organophosphorus 

pesticides in cherry and 

strawberry juice 

Pesticides in water and 

food 

Pesticides in human 

blood 

1386 Herbicides 

1384 

Tebufenpyrad and 

oxadiazon. 

1558 Polyphenols in wine. 

Headspace solid phase microextraction applied to the analysis of 

organophosphorus insecticides in strawberry and cherry juices. 



Evaluation of Solid Phase Microextraction-gas chromatography in the 

analysis of some pesticides with different mass spectrometric techniques: 

Application to environmental waters and food samples. 


Benfenati, E.; Natangelo, M.; Tavazzi, S. 

Headspace solid-phase microextraction in combination with gas 

chromatography and tandem mass spectrometry for the determination of 

organochlorine and organophosphorus pesticides in whole human blood. 


Hernandez, F.; Beltran, J.; Lopez, F. J.; Pitarch, E. 


GC-ITMS 

GC-MS 

Applications of solid-phase microextraction ( SPME ) in the determination of 

residues of certain herbicides at trace levels in environmental samples. 

Journal of Environmental Monitoring (2001) 49(9), 505-508. 

Ramesh, A.; Ravi, P. E. 

65 um Carobwax/DVB GC-ECD 

Determination of tebufenpyrad and oxadiazon by solid-phase 

microextraction and gas chromatography-mass spectrometry. 

Chromatographia (2001) 54(5-6), 377-382. 

Navalon, A.; Prieto, A.; Araujo, L.; Vilchez, J. L.* 


Gas phase post derivitization following SPME for rapid analysis of 

polyphenols in wine by GC-MS. 

Zhongshan Daxue Xuebao, Ziran Kexueban 40(1) 54-57. Chinese 

Luan, Tian-gang; Li, Gong-ke; Zhang, Zhan-xia. 

2078 Pesticides Fast screening determination of some ubiquitous 85µm polyacrylate GC-MS 

in water pesticides with SPME in water samples immersion sampling 

Analytical Letters, 37, #7, 1427-1436 

Moreira Vaz, J.; Komatsu, E. 

2079 Pesticides in Multiresidue method using SPME for the determination 100µm PDMS GC-MS 

air of various peticides with different volatility in 40min 

confined atmospheres dynamic air sampling 

Anal and Bioanal Chemistry, 379, #3, 476-483 

Ferrari, F; Sanusi, Ad; Millet, M; Montury, M 

2080 Chlorpyrifos Interactions of chlorpyrifos with colloidal materials GC 

from water in aqueous systems 

J of Environmental Quality, 33., #5, 1765-1770 

Wu, Jigang; Laird, David A. 





2081 Pesticides in SPME-GC-(tandem) MS as a tool for pesticide residue 65µm PDMS-DVB GC-MS-MS 

water analysis in water samples at high sensitivity and immersed fiber 

selectivity w/ confirmation capabilities 

J Chromatogr A, 1026, #1-2, 239-250 

Goncalves, C.; Alpendurada, M. F. 

2082 Dieldrin in Transport and fate of dieldrin in poplar and willow headspace GC 

trees trees analyzed by SPME 

Chemosphere, 61, #1,, 85-91 

Anderson, Larry G.; Ramaswami, Anu; Skaates, S. 

2083 Pesticides Pesticide residue analysis in waters by SPME 100µm PDMS GC-MS-MS 

in water coupled to GC-tandem mass spectrometry. 65µm PDMS-DVB 

Analytical Letters, 37, 1, 99-117 

Arrebola, F. ; Cortes Aguado, S.; Sanchez-Morito, N.; 

Garrido Frenich, A.; Martinez Vidal, J. 

2084 Pesticides Determination of pesticides and some metabolites in headspace/ immersed GC-MS-MS 

in milk different kinds of milk by SPME and low-pressure GC-MS-MS acidified sample 


Frenich, A. Garrido; Gonzalez-Rodriguez, M.J.; Liebanas, F. J. 

Arrebola; Lopez, F. J. Sanchez; Vidal, J. L. Martinez 

2085 Organo- Comparison of SPME and stir bar sorptive 100µm PDMS LC-MS 

phosphorus extraction for determining six organophosphorus 

insecticides insecticides in honey by LC-MS 

in honey J Chromatogr A, 1030, #1-2, 77-85 

Blasco, C.; Fernandez, M.; Pico, Y.; Font, G. 

2086 Pyrethroid Application of SPME for the determination of pyrethroid immersion sampling GC/MS 

In vegetables residues in vegetable samples by GC-MS 


Beltran, J.; Hernandez, F.; Lopez, F.J.; Peruga, A.; Pitarch, E. 

2087 Pesticides in Water quality and presence of pesticides in a immersion sampling GC 

water tropical coastal wetland in southern Mexico 

Mar. Pollut. Bull., 48, #11-12, 1130-1141 

Bello-Mendoza, R; Hernandez-Romero, A.; Malo, E.; Tovilla-Hernandez, 

C 

2088 p,p'-DDT Determination of dichlorodiphenyltrichloroethane in 100µm PDMS GC-ECD 

in water water using automated SPME-GC-ECD immersion sampling 

Fenxi Huaxue, 32, #4, 500-502 

Luan, T. G.; Lan, C. Y.; Zhou, H. L.; Wong, M. H. 

2089 Fluazifop Evaluation of an SPME and GC-MS method for 100µm PDMS GC-MS 

in water analysis of fluazifop in water. stirring 

Acta Chromatographica, 14, #1, 231-236 

Olszewska, E. 

2090 Pesticides Cost analysis of ELISA, solid-phase extraction, and comparison of cost GC 

in water SPME for the monitoring of pesticides in water 

Environmental Research, 98, #1, 143-150 

Dalvie, M.; Sinanovic, E.; London, L; Cairncross, E; 

Solomon, A.; Adam, H. 

2091 Prethroid Advanced method using microwaves and SPME 100µm PDMS GC-MS 

residue on coupled w/GC-MS for the determination of pyrethroid 30min immersed 

strawberries residues in strawberries water/acetornitrile 

J. Chromatogr. A, 1046, #1-2, 35-40 preextraction 

Guillet, Valerie; Montury, Michel; Sanusi, Astrid 

2092 Pesticides in Analysis of pesticide residues in juice and beverages "review" Review article GC-MS 

beverages Crit. Rev. Anal. Chem., 34, #2, 121-131 

Albero, B; Gonzalez, L; Sanchez-Brunete, C; Tadeo, J. 

2093 Pesticides Combining SPME and on-line preconcentration-capillary CE-UV 

in water electrophoresis sensitive analysis of pesticides in foods 

Electrophoresis, 26, #4-5, 980-989 

Hernandez-Borges, J.; Cifuentes, A.; 

Garcia-Montelongo, F.; Rodriguez-Delgado, M. 





2094 Pesticides in Highly sensitive analysis of multiple pesticides in foods NH 2HCO 3 buffer CE-MS 

food combining SPME, capillary electrophoresis-MS & chemometrics pH 4 CE-UV 

Electrophoresis, 25, #13, 2065-2076 

Hernandez-Borges, Javier; Rodriguez-Delgado, M.; 

Garcia-Montelongo, Francisco J.; Cifuentes,A. 

2095 Pesticides Application of SPME to the study of the photochemical 100µm PDMS GC-MS 

in water behaviour of five priority pesticides: "On-fiber" 30min extract 

and aqueous photodegradation immersion sampling 

J. Chromatogr. A, 1047, #2, 271-279 

Sanchez-Prado, Lucia; Llompart, Maria; Lores, Marta; 

Garcia-Jares, Carmen; Cela, Rafael 

2096 Pesticides in Applicability of headspaceSPME to the determination 30µm polyacrylate GC-MS 

water of multi-class pesticides in waters. 30° to 100°C 


Sakamoto, Mitsushi; Tsutsumi, Taizou 

Soil 

36 Hexachlorocyclohexane Application of SPME and GC with Electron-Capture and Mass 100µm PDMS GC-ECD, 

in soil Mass Spectrometric Detection for the Determination of 20-30 min GC-MS 

Hexachlorocyclohexanes in Soil Solutions immersion 

J. Chromatogr. 687: 133-140 (1994) 

Popp, P., Kalbitz, K., Opperman, G. 

stirring 

74 Diesel fuel Solid Phase Microextraction-GC for Analysis of Diesel Fuel 100µm PDMS GC-FID 

in soil Residues in Soil 55°C, 30 min 

Request from Dept. Soil Science, University of Manitoba 

Winnipeg, MB, Canada R3T 2N2. 

Graham, K., Webster, B., Sarna, L. 

headspace 

716 THF, methanol Analysis of THF and methanol in distillation residue 65µm PDMS/DVB GC-FID 

in distillate samples by automated headspace SPME-GC with FID 9min. 

J Chromatogr. Sci. (2000), 38(3), 117-121 

Gavlick, W. 

headspace 

870 PAHs in The use of SPME and GC-MS for the chemical characterization 

environmental and assessment of PAH pollution in aqueous 

samples environmental samples 

Int. J. Environ. Anal. Chem (2000) 78(3-4) 205-221 

Havenga, Willem J.; Rohwer, Egmont R 

717 PAHs Solid Phase Microextraction of PAHs from soil 

in soil Chem. Ana., 2000 (45 No.6) 835-842 

Sedukiene, I., Vickackaite, V., Kazlauskas, R. 

567 PAHs Chemical characterization and screening of hydrocarbon 100µm PDMS GC-MS 

in soil pollution in industrial soils by headspace SPME 40 min 

J-Chromatogr,-A. 2 Jul 1999; 848(1-2): 279-295 

Havenga,-WJ; Rohwer,-ER 

headspace 

865 PAHs Solid phase microextraction of PAHs from soil 

in soil Chemia Analityczna (Warsaw) (2000) 45(6) 835-842 30min @ 60°C 

Seduikiene, I.; Vickackaite, V.; Kazlauskas, R. heaspace 

75 Pesticides Extraction of Pesticides by Solid Phase Microextraction 100µm PDMS GC-ECD, -NPD 

in soil (from Soil) immersed, 

Request from: Dept. Environmental Assessment, Swedish 

University of Agricultural Sciences, PO Box 7050, 

Uppsala, Sweden 

Bengsson, S., Berglof, T. 

water solution 





855 Triazine, amides Determination of triazines and amides in water using GC-MS 

in water solid-phase microextraction coupled with GC-MS. 


Hu, R.; Elia, D.; Berthion, J. -M.; Poliak, S. 

529 Triazines, Determination of polar pesticides in soil by SPME couple to 85µm polyacrylate HPLC-MS 

carbamates HPLC-MS salt added 

in soil leachates Fresenius'J. Anal. Chem. (1999), 363(7), 680-685 

Moder, M., Popp, P., Eisert, R., Pawliszyn, J. 

718 Triazines, Determination of triazines in soil leachates by SPME 85µm polyacrylate GC-MS 

in soil leachates coupled to GC-MS 30min @ 20°C 

J. Chromatogr. A 2000, 874(2), 247-255 

Zambonin, C.., Palmisano, F. 

aggitation 

530 Organophosphorus Determination of organophosphorus pesticides in soil 85µm polyacrylate GC-FID 

pesticides in by headspace SPME 1 hr @ 80°C 

soil Fresenius'J. Anal. Chem (1999), 363(7), 673-679 

Ng, W., Teo, M., Lakso, H. 

headspace over soil 

76 Lindane Analysis of Lindane in Water and Soil by Solid Phase 30µm & 100µm PDMS GC-ECD 

in water and soil Microextraction 58°C 

Request from: Dept. Soil Science, University of Manitoba, 40 min (headspace) 

Winnipeg MB, Canada R3T 2N2. 

Anderson, K., Sarna, L., Webster, B. 

15-20 min (immersion) 

880 Organochlorine Determination of organochlorine pesticides and their 100µm PDMS, GC-ECD 

pesticides in metabolities in soil samples using headspace SPME 65µm DVB/PDMS 

soil J.Chromatogr. A (2001) 918(1), 177-188 60min@70C 

Doong, R., Liao, P. heahspace 

stirred 

881 Fipronil in Determination of fipronil by SPME and GC-MS 85µm polyacrylate GC-MS 

water, soil, urine J chromatogr. A 919(2001) 215-221 30min. @ 60°C 

Vilchez, J., Prieto, A., Araujo, L., Navalon, A. stirred 

9.5 pH 

857 Metochlor Determination of metolachlor volatile flux from 

from soil soil using SPME 

Prepr. Ext. Abstr. ACS (2001) 41(1) 307-311 

McConnell, L.; Kim, H; Nochetto, C; Gish, T; Prueger, J 

833 Halobenzenes Gas chromatography/ion-trap tandem mass spectrometry 100µm PDMS GC-MS 

in soil and water for the analysis of halobenzenes in soils by SPME 

Rapid Commun Mass Spectrometry (2000) 14(23) 2271-2281 

Sarrion, M. N.; Santos, F. J.; Galceran, M. T. 

45min 

92 Chlorobenzenes Analysis of Chlorobenzenes in Soils by Headspace SPME 100µm PDMS GC-Ion Trap 

in soil and water and GC-Ion Trap MS 

J. Chromatogr. A 771: 181-189 (1997) 

Santos, F., Sarrion, M., Galceran, M. 

headspace MS 

921 Chlorobenzenes Strategies for the analysis of chlorobenzenes in soils using GC-Ion Trap 

in soil SPME coupled with GC-ion trap mass spectrometry 

J. Chromatogr. A (1998), 819(1-2), 197-209 

Sarrión, M., Santos, F., Galceran, M. 

MS 

238 Chlorobenzenes, Analysis of Chloro- and Nitroanilines and Benzenes in Soil 85µm polyacrylate GC-ECD 

nitrobenzenes, by Headspace Solid-Phase Microextraction headspace 

anilines in soil, water J. Chromatogr. A 746: 71-81 (1996) 

Fromberg, A., Nilsson, T., Larsen, R., Montanarella, L., 

Facchetti, S., Madsen, J. 

50°C, 30 min 





97 Semivolatiles Coupled Subcritical Water Extraction with SPME for 100µm PDMS GC-MS 

in solids Determining Semivolatile Organics in Environmental Solids 15 min 

Anal. Chem. 68: 3892-3898 (1996) 

Hageman, K., Mazeas, L., Grabanski, C., Miller, D., Hawthorne, S. 

immersion 

793 Phenols Fast determination of phenols in contaminated soils 85µm polyacrylate GC-FID 

in soil J. Chromatogr., A (2001) 911(1), 135-141 60min. @20°C 

Baciocchi, R.; Attina, M.; Lombardi, G.; Boni, M. R immersion, pH 1 

719 Chlorophenols Determination of chlorophenols in soil using accelerated 85µm polyacrylate GC-MS 

in soil solvent extraction combined with SPME 20min. @20°C 

Anal. Chem. (2000), 72(3), 46-551 immersion, pH 2 

Wennrich, L, Popp, P., Moeder, M. satr NaCl 

531 Volatiles and Headspace SPME for the determination of volatile and 100µm PDMS GC-MSD 

semivolatiles semivolatile pollutants in soils 30 min @ 20°C 

in soils/water Talanta (1999), 48(2), 451-459 

Llompart, M., Li, K., Fingas, M. 

headspace 

532 PAHs, hydrocarbons Investigation by SPME and GC-MS of organic films on GC-MS 

in pollutant crust stone monuments 

Rapid. Commun. Mass Spectrom. (1999), 13(10), 895-900 

Angelis, F., Di Tullio, A., Mellerio, G., Quaresima, R, Volpe, R 

533 Aldehydes, acids Degradation of palmitic (Hexadecanoic) acid deposited on 

from palmitic acid TiO2 coated self cleaning glass: kinetics of disappearance, 

intermediate products and degradation pathways 

New J. Chem (1999), 23(4), 365-374 

Romeas, V., Pichat, P., Guillard, C., Chopin, T., Lehaut, C. 

534 PAHs in Interaction between natural organic matter (NOM) and 85µm polyacrylate GC-MS 

organic matter polycyclic aromatic compounds, Comparison of 30 min 

fluorescence quenching and SPME pH3, immersed 

Fresenius'J. Anal. Chem. (1999), 364(4), 313-319 

Myung, S., Kim, M., Min, H., Yoo, E. Kim, K. 

alkyl formate derivative 

172 Elemental analysis Elemental and Organometallic Analysis of Soil Using 100µm PDMS GC-MS 

of soil Glow-Discharge MS and GC-MS 50°C, 10 min 

Rapid Commun. Mass Spectrom. 10: 341-346 (1996) 

Barshick, C., Barshick, S., Mohill, M., Britt, P., Smith, D. 

salt added 

174 Mercury species in Performance Improvements in the Determination of Mercury GC-ICP 

natural gas condensate Species in Natural Gas Condensate Using Online 

Amalgamation Trap or SPME with Capillary GC-Microwave- 

Induced Plasma Atomic Emission Spectrometry 

Analyst 121: 1055-1060 (1996) 

Snell, J., Frech, W., Thomassen, Y. 

535 Organomercury SPME and GC-MIP-AED for the speciation analysis of GC-MIP-AED 

in soil and water organomercury compounds 

J. High Resolut. Chromatogr. (1999), 22(3), 181-182 

Mothes, S., Wennrich, R. 

239 BTEX, chlorinated The Determination of Volatile Organic Compounds in Soils 100µm PDMS GC-MS 

hydrocarbons Using SPME with Gas Chromatography-Mass Spectrometry 5 min 

in soil J. High Res. Chromatogr. 19: 515-519 (1996) 

James, K., Stack, M. 

headspace 





197 VOCs in Environmental Analysis of Volatile Organic Compounds in overview 

water and sediment Water and Sediment by GC 

J.Chromatogr. A 733A 733: 119-141 (1996) (review) 

Kuran, P., Sojak, L. 

article 

536 VOCs in Determination of VOC contamination in borehole sediments 

sediment by headspace SPME-GC analysis water solution 

Fresenius' J. Anal. Chem 1999, 364(7), 645-647 

Dermietzel, Jurgen, Strenge, G. 

headspace 

768 Tributyltin Determination of tributyltin by automated in-tube In-tube SPME LC-ES-MS 

in water SPME with HPLC-ES-MS 

J Anal At Spectrom (2001) 16(2), 159-165 

Wu, J; Mester, Z; Pawliszyn, J. 

Supel-Q PLOT 

720 Butyltin Determination of butyltin compounds in aqueous GC-FID 

in water samples by GC w/FPD and headspace SPME after 

in-situ hydride derivatization 

Aanl. Sci. 2000, 16(6), 585-588 

NaBEt4 

Jiang, G, Liu, J. Japanese 

771 Butyltin Determination of butyltin compounds in sediments GC-FPD 

in sediment by headspace SPME and capillary GC w/FPD using quartz 

surface induced luninescence 

Fenxi Huaxue (20001) 29(2), 158-160 KBH-4 

Liu, J; Jiang, G. in Chinese 

721 Butyltin Determination of butyltin species in water and GC-FID 

in water sediment by SPME-GC-FID 

J.Chromatogr. A (2000), 873(1), 61-71 

Millan, E., Pawliszyn, J. 

NaBEt4 

888 Solid phase microextraction as a tool for trace 

element speciation 

Spectrochim. Acta, Part B (2001) 56B(3), 233-260 

Mester, Z.; Sturgeon, R.; Pawliszyn, J. 

852 Butyltin Speciation of butyltin compounds in marine sediments with 100µm PDMS GC-MS 

in marine sediment headspace SPME and gas chromatography: MS 

Fresenius' J. Anal. Chem 2001, 369(6), 510-515 headspace 

Cardellicchio, N.; Decataldo, A.; Di Leo, A.; Giandomenico, S. NaBEt4 derivative 

722 Butyl-, phenyltin SPME: a new procedure for the control of butyl- 100µm PDMS GC-FID 

in water and phenyltin pollution in the environment by GC-FID 60 min, immersed 

Analyst (Cambridge, UK) 2000, 125(2), 263-268 

Aguerre, S., Montigny, C, Lespes, G., Gaultier, M. 

NaBEt4 

199 Organotin Solid Phase Microextraction to Study the Sorption of 100µm PDMS GC-MS 

in humic organic matter Organotin Compounds onto Particulate and Dissolved 30 min 

Humic Organic Matter 


Poerschmann, J., Kopinke, F., Pawliszyn, J. 

immersion 

343 Methylmercury Development of a Technique for the Analysis of Inorganic 100µm PDMS, GC-MS 

derivative Mercury salts in Soils by GC-MS 65µm PDMS/DVB 

in soil Intl. J. Mass Spectrometry 178 (1998) 31-41 50°C, 5 min 

Barshick, C., Barshick, S., Britt, P., Lake, D., Vance, M., stirring, salt added 

Walsch, E. methyl bis(dimethylgloximate) 

pyridinecobalt (III) 





723 Methylmercury Determination of methylmercury by SPME-ICP-MS: a new ICP-MS 

derivative sample introduction method for volatile metal species 

in soil J. Anal. AT. Spectrom (2000) 15(7), 837-842 

Mester, Z., Lam, J., Sturgeon, R, Pawliszyn, J. 

209 Applications of Sorbent Extraction in Environmental Analysis 

Chem. Anal. (Warsaw) 42 (3): 297-314 (1997) 

Gorlo, D., Namiesnik, J., Zygmunt, B. 

303 PAHs, amines, aromatic Coupled Subcritical Water Extraction with SPME for 100µm PDMS GC-ECD 

from soil & particulate Determining Semivolatile Organics in Environmental Solids 15 min 

Anal. Chem. (1996) 68, 3892-3898 

Hageman, K., Mazeas, L., Grabanski, C, Miller, D., 

Hawthorne, S. 

immersion 

884 Phenyl compounds Determination of phenyl compounds in drinking water by 

in water solid phase microextraction coupled with capillary GC/MS 

Huanjing Huaxue (2001) 20(2) 191-195 

920 PCBs Simple method for estimating PCH concentratons on soils 

in soil and sediments using subcritical water extraction coupled 

with SPME 

J. Chromatogr. A (1998), 814(1-2) 151-160 

Hawthorne, S., Grabanski, C., Hageman, K. Miller, D. 

304 PCBs Solid-Phase Microextraction of Polychlorinated Biphenyls 100µm PDMS GC-ECD 

in soil J. Chromatogr. A 800 (2): 257-266 (1998) 15 min 

Yang, Y., Miller, D., Hawthorne, S. immersion 

370 PCBs Adsorption versus Absorption of PCBs onto SPME Coatings 7µm PDMS GC-ECD 

in soil Anal. Chem. 1998, Vol. 70, 1866-1869 5 hr 

Yang, Y., Hawthorne, S., Miller, D. immersion 


537 PCBs in Headspace SPME for the determination of PCBs in soils 100µm PDMS GC-MS 

soil & sediment and sediments 30 min @ 100°C 

water slurry J. Microcolumn Sep. (1999), 11(6), 307-402 

Llompart, M., Li, K., Fingas, M. 

headspace 

724 PAHs Determination of PAHs in sediment using SPME w/GC-MS 100µm PDMS GC-MS 

in sediment J. Chromatogr. Sci. (2000), 38(2), 55-60 

Cam, D., Gagni, S., Meldolesi, L., Galletti, G. 

538 Bisphenol A An attempt by SPME with on-column silylation for a rapid GC-MS 

in water and highly sensitive determination of bisphenol A BSTFA derivative 

Bunseki Kagaku (1999) 48(6), 589-593 

Takao, Y. Lee, H., Arizono, K. 

Japanese 

305 Organics SPME of Semivolatile Organic Compounds from 

from odoriferous Odoriferous Samples 

samples Hazard. Ind. Wastes (28th) 734-738 (1996) 

Wojtowicz, C., Clifton, A., Willy, D. 

1014 

Tin and butyltin in 

sediment 

Assessment of tin and butyltin species in estuarine superficial sediments 

from Gipuzkoa, Spain 

Chemosphere (2003) 51 (8), 643-649. 

Arambarri, I.; Garcia, R.; Millan, E. 

PDMS GC-FID 


1028 

1040 

1068 

1108 




Methylmercury and 

butyltin in sediments 

Bis(2-chloroethyl) sulfide 

in soil. 

Chlorophenols in landfill 

leachates 

Musk compounds in 

sludge. 

1193 VX in soil 

1220 Triazines in soil. 

1240 PAHs in sediment 

1255 VX nerve agent in soil. 

1297 Isocarbophos in soil. 

1320 

Determination of methylmercury and butyltin compounds in marine biota 

and sediments using microwave-assisted acid extraction, solid-phase 

microextraction, and gas chromatography with microwave-induced plasma 

atomic emission spectrometric detection. GC-MIP-AES 


Tutschku, S.; Schantz, M. M.; Wise, S. A.* 

Application of headspace solid-phase microextraction and gas 

chromatography-mass spectrometry for detection of the chemical warfare 

agent bis(2-chloroethyl) sulfide in soil. Polyacrylate GC-MS 


Kimm, G. L.; Hook, G. L.; Smith, P. A.* 

Direct determination of chlorophenols in landfill leachates by solid-phase 

micro-extraction-gas chromatography-mass spectrometry. GC-MS 


Ribeiro, A.; Neves, M. H.; Almeida, M. F.; Alves, A.; Santos, L. * 

Determination of musk compounds in sewage treatment plant sludge 

samples by solid-phase microextraction 


Cela, Rafael; Garcia-Jares, Carmen; Llompart, Maria; Polo, Maria; Salgado, 

Carmen 

Various GC-MS 

Detection of VX contamination in soil through solid-phase microextraction 

sampling and gas chromatography/mass spectrometry of the VX 

degradation product bis(diisopropylaminoethyl)disulfide. 


Smith, Philip A.; Ding, Bangwei; Hook, Gary L.; Kimm, Gregory; Koch, 

David; Savage, Paul B. 

PDMS GC-MS 

Determination of triazines in soil by microwave-assisted extraction followed 

by solid-phase microextraction and gas chromatography-mass 



Shen, G.; Lee, H. K.* 

Micellar microwave-assisted extraction combined with solid-phase 

microextraction for the determination of polycyclic aromatic hydrocarbons in 

a certified marine sediment. 


Pino, V.; Ayala, J. H.; Afonso, A. M.; Gonzalez, V. * 

PDMS, polyacrylate. GC-MS 

Detection of O -ethyl- S -(2-diisopropylaminoethyl) methylphosphonothiolare 

(VX) contamination in soil through solid-phase microextraction sampling and 

gas chromatography/mass spectrometry of the VX degradation product 

bis(diisopropylaminoethyl)disulfide. GC-MS 


Hook, G. L.; Kimm, G.; Koch, D.; Savage, P. B.; Ding, B. W.; Smith, P. A.* 

Determination of isocarbophos in soil samples by gas chromatographymass 

spectrometry with combination of microwave-assisted extraction and 

solid-phased microextraction. GC-MS 


Yang, Y.; Li, G. K.* 

Determination of antifouling compounds in marine sediments by solid-phase 

microextraction coupled to gas chromatography-mass spectrometry. GC-MS 




1363 




Petroleum hydrocarbons 

in soil 

1385 n-alkanes in soil. 

1394 Hydrocarbons in soil. 

1411 

Butyltin species in 

sediment. 

1446 Chlorophenols in soil 

1461 Organophosphorus 

pesticides in soil 

1462 

Tributyltin in water and 

soil 

1464 Aromatic acids in soil 

1486 Monoaromatic 

hydrocarbons in soil 

1490 Tributyltin in sediment 

1491 Organometallics in soil 

Determination of petroleum hydrocarbons in contaminated soils using solidphase 

microextraction with gas chromatography-mass spectrometry. 100 um PDMS GC-MS 

Journal of Chromatographic Science (2001) 39(11), 481-486. 

Cam, D.; Gagni, S. 

A new PVC-activated charcoal fibre coated on silver wire: application in 

determination of n-alkanes in the headspace of soil samples by SPME-GC. 

Analytical Sciences (2002) 18(1), 77-81. 

Farajzadeh, M.; Matin, A. A. 

Activated charcoal/PVC GC 

Determination of hydrocarbons in old creosote contaminated soil using 

headspace solid-phase microextraction and GC-MS. 

Chemosphere (2001) 44(7), 1641-1648. 

Eriksson, M.; Faeldt, J.; Dalhammar, G.; Borg-Karlson, A. -K. 


Headspace solid-phase microextraction of butyltin species in sediments and 

their gas chromatographic determination. 100 um PDMS 

Journal of Separation Science (2001) 24(6), 459-464. 

Gui-bin, Jiang; Ji-yan, Liu; Ke-wu, Yang; Qun-fang, Zhou 

Determination of chlorophenols in soil samples by microwave-assisted 

extraction coupled to headspace solid-phase microextraction and gas 

chromatography - Electron-capture detection 


Jen, Jen-Fon; Wei, Ming-Chi 

Solid-phase microextraction coupled to gas chromatography- mass 

spectrometry for the study of soil adsorption coefficients of 

organophosphorus pesticides 

Journal of Environmental Monitoring (2002) 4(4), 477-481 

Zambonin, C. G.; Palmisano, F.; Losito, I.; Cilenti, A. 

Gas phase detection of tributyltin chloride arising from aqueous and solid 

matrices. 


Bancon-Montigny, Chrystelle; Lam, Joseph W.; Maxwell, Paulette; Mester, 

Zoltan; Sturgeon, Ralph E.; Yang, Lu 

Separation and identification of aromatic acids in soil and the Everglades 

sediment samples using solid-phase microextraction followed by capillary 

zone electrophoresis. 


Deng, Yiwei; Fan, Xiaofang 

Solid-phase microextraction-gas chromatographic determination of volatile 

monoaromatic hydrocarbons in soil. 


Zygmunt, Bogdan; Namiesnik, Jacek 

Improvement in measurement precision with SPME by use of isotope 

dilution mass spectrometry and its application to the determination of 

tributyltin in sediment using SPME GC-ICP-MS. 


Yang, Lu; Mester, Zoltan; Sturgeon, Ralph E. 

Gas phase sampling of volatile (organo)metallic compounds above solid 

samples. 


Mester, Zoltan 


85um Polyacrylate, 1g soil in 

6mL water, pH 2, 9mins. 

Headspace 

GC-ECD 

GC-MS 

GC-MS 

85um Polyacrylate CZE 


100um PDMS, sodium 

tetraethylborate derivative 

GC-IDMS 

ICP-MS




1150 Tributyltin in sediment 

1326 

Polycyclic musks in 

sewage. 

Determination of tributyltin compounds in surface sediments of harbour by 

gas chromatography with headspace solid-phase microextraction GC-FPD 


Lei, Z.; Huang, C. J.; Jia, L.; Shi, H. H. 

Removal of two polycyclic musks in sewage treatment plants: freely 

dissolved and total concentrations. GC-MS 


Artola-Garicano, E.; Borkent, I.; Hermens, J. L. M.; Vaes, W. H. J. 

2097 Chloro- SPME as a tool to predict internal concentrations 30µm PDMS GC 

benzenes of soil contaminants in terrestrial organisms after 1 day sample 

in soil exposure to a laboratory standard soil. headspace 

Chemosphere, 54, #4, 561-568 

van der Wal, L.; van Gestel, C.; Hermens, J. 

2098 Butyltin in Applicability of SPME combined with GC-MIP AED for the ethylated derivative GC-MIP AED. 

sediment determination of butyltin compounds in sediment samples. headspace 

Analytical and Bioanalytical Chemistry, 380, #5-6, 853-857 sonication 

Carpinteiro, J.; Rodriguez, I. *; Cela, R. 

2099 Hydrocarbons Surface geochemical results complement headspace GC 

in soil conventional development approaches 

World Oil, 225, #12, 54-65 

Quinlan, W.; Wood, James; Wylie, Albert 

2100 Phenanthrene Plant-assisted degradation of phenanthrene as headspace GC-FID 

in soil assessed by solid-phase microextraction (SPME) 

Intl J of Phytoremediation, 6, #3, 253-268 

Hynes, Russell K.; Farrell, Richard E.; Germida, James J. 

2101 Prometryn Determination of prometryn in soil by GC-MS using microwave heated GC-MS 

in soil microwave-assisted extraction associated with SPME 

Fenxi Huaxue, 32, #6, 775-778 

Yang, Y.; Luan, W.; Luo, X. J.; Li, G. K.* 

2102 Fungistasis Soil volatile fungistasis and volatile fungistatic compounds Headspace GC-MS 

in soil Soil Biol. Biochem.,36, #12, 1997-2004 

Chuankun, Xu; Keqin, Zhang; Leming, Zhang; Minghe, Mo 

2103 BTEX Determination of benzene, toluene, ethylbenzene 75µm Carboxen GC-FID 

in soil and xylenes in soils by multiple headspace SPME 30min @ 30°C 

J. Chromatogr. A, 1035, #1, 17-22 headspace over soil 

Ezquerro, O; Ortiz, G; Pons, B; Tena, M suspended in water 

2104 Fungicides in Determination of the fungicides vinclozolin and 85µm polyacrylate GC-MS 

soil dicloran in soils using ultrasonic extraction coupled 5% acetone/water 

with SPME 

Anal. Chim. Acta, 514, #1, 125-130 


2105 Fungicides in Determination of pyrimethanil and kresoxim-methyl 85µm polyacrylate GC-MS, SIM 

in soil in soils by headspace SPME and GC-MS headspace 


Araujo, L; Navalon, A; Prieto, A; Vilchez, J 

2106 Tetracyclic The moss Physcomitrella patens releases a headspace GC-MS 

diterpene tetracyclic diterpene 

from moss Plant Cell Rep., 22, #10, 780-786 

Kassner, H.; Schultze, W.; VonSchwartzenberg, K. 

2107 Chlorinated Static headspace versus head space SPME for the headspace GC-MS 

solvents in for the determination of volatile organochlorine 

compounds in landfill leachates by GC 

Talanta, 63, #4, 809-814 

Fernandez Martinez, E.; Fernandez Sanchez, M.; 

Florez Menendez, J.; Sanchez Uria, J.;Sanz-Medel, A. 





2108 Organics Optimization of microwave-assisted extraction GC-MS 

in sebum followed by SPME-GC-MS detection for the assay 

of some semi-volatile organic 

J. Chromatogr.B, 825, #1, 11-20 

Diaz-Vazquez, Liz; Garcia, Oscar; Marrero, I.; 

Rosario, Osvaldo; Velazquez, Zorangelys 

2109 Organic Sediment dilution method to determine sorption Immersed extract from GC 

chemicals in coefficients of hydrophobic organic chemicals sediment in water 

sediment Environ. Sci. Technol., 39. #11, 4220-4225 

Busser, F; Hermens, J.; Klamer, H.; Mayer, P; Ter Laak, T 

2110 PCDDs/PCDF Simple device for the SPME screening of 100µm PDMS GC-MS 

in soil polychlorodibenzo-p-dioxins and polychlorodibenzo- headspace 

furans in heavily contaminated soil samples. sonicated 


Chia, K. J.; Lee, T. Y.; Huang, S. D.* 

Air 

725 Organic vapors Application of SPME for determination of organic vapors in review article 

in gaseous matrices gaseous matrices 

J. Chromatogr. A, 885(2000) 405-418 

Namiesnik, J., Zygmunt, B., Jastrzebska, A. 

846 Solvent vapors Solvent vapour monitoring in work space by SPME 100µm PDMS 

in air J Hazardous Materials (2001) 83(1-2), 83-91 

Li, K.; Fingas, M.; Goldthorp, M.; Lambert, P.; 

Santilli, A.; Whiticar, S. 

75µm Carboxen/PDMS 

726 Volatiles Airflow Rate in the Quantitation of Volatiles in Air Streams 100µm PDMS GC-FID 

in air by Solid Phase Microextraction 

Anal. Chem 2000, 72, 3949-3955 

Bartelt, R., Zilkowski, B. 

30 min 

727 Volatile organic Sorbent trapping of volatile organic compounds from air 75µm Carboxen/PDMS GC-FID 

in air J. Chromatogr. A, 885 (2000) 120-151 

Harper, M. 

review article 

758 Volatile organic Air sampling with porous SPME fibers compounds 75µm Carboxen/PDMS GC-FID 

in air Anal. Chem. 2000, 72, 5178-5186 65µm DVB/PDMS 

Koziel, J., Jia, M., Pawliszyn, J. 5-10 sec air sampling 

754 Volatile organic Air sampling and Analysis of Volatile Organic compounds 100um PDMS GC-FID 

in air with Solid Phase Microextraction 

J. Air & wasteManage. Assoc 51: 173-184 

Koziel, J., Pawliszyn, J. 

55 BTEX Analysis of Environmental Air Samples by Solid Phase 100µm PDMS GC-MS 

in air microextraction and GC/Ion Trap Mass Spectrometry 3 min 


Chai, M., Pawliszyn, J. 

gas sampling 

226 Petroleum Estimation of Air-Coating Distribution Coefficients for SPME 100µm PDMS, GC-FID 

hydrocarbons Using Retention Indexes from Linear Temperature-Programmed 30µm PDMS 

in air Capillary Gas Chromatography. Application to the Sampling 

and Analysis of Total Petroleum Hydrocarbons in Air 

Anal. Chem. 69: 402-408 (1997) 

Martos, P., Saraullo, A., Pawliszyn, J. 

30-480 min 

375 Formaldehyde Sampling and Determination of Formaldehyde Using SPME 65µm PDMS/DVB GC-MS 

derivatives with On-Fiber Derivatization 10-150 sec 

in air Anal. Chem. 198, 70, 2311-2320 gas sampling 

Martos, P., Pawliszyn, J. PFBHA derivatives 





110 Amines Determination of Amines in Air and Water Using Derivatization 65µm Carbowax/DVB GC-FID 

in air Combined with SPME 30 min 

J. Chromatogr. A 773: 249-260 (1997) gas sampling 

Pan, L., Chong, M., Pawliszyn, J. DPTFA derivatives 

539 Thiol and sulfides Evaluation of SPME for sampling of volatile organic sulfur 75µm Carboxen/PDMS GC-AED 

in air samples compounds in air for subsequent GC analysis with 

atomic emission detection 

J. Chromatogr., A 1999, 848(1+2), 305-315 

Haberhauer-Troyer, C., Rosenberg, E., Grasserbauer, M 

540 Sulfur compounds Studies on the application of SPME for analysis of volatile 100µm PDMS FPD-GC 

in water/ N2 & organic sulfur compounds in gaseous and liquid samples 10 min 

propane Chem. Anal. (Warsaw), 1999, 44(3A), 485-493 

Wardencki, W., Namiesnik, J. 

233 C5-C11 hydrocarbons, Calibration of Solid-Phase Microextraction for Air Analyses 30µm & 100µm PDMS GC-FID 

BTEX Based on Physical Chemical Properties of the Coating 15-450 sec 

in air Anal. Chem. 69: 206-215 (1997) 

Martos, P., Pawliszyn, J. 

gas sampling 

541 Chlorobenzen and On Calibration of SPME-GC-MS system for analysis of Optimization of sampling GC-MS 

p-xylene organic air contaminants using gaseous standard mixtures 

in air Chem. Anal. (Warsaw) (1999), 44(2), 201-213 

Namiesnik, J., Gorlo, D, Wolska, L, Zygmunt, B. 

308 Organic vapors Calibration Procedure for SPME-GC Analysis of Organic 

in air Vapors in Air 

Talanta 44 (9): 1543-1550 (1997) 

Gorlo, D., Wolska, L., Zygmunt, B., Namiesnik, J. 

756 Organic vapors Diffusion-Based Calibration for SPME Analysis of Carboxen/PDMS 

in air Aqueous samples DVB/PDMS 

Anal. Chem. 2001, 73 (1), 13-18 

Sukola, K., Koziel, J., Augusto, F., Pawliszyn, J. 

10sec. Passive sampling 

828 Determination of absolute amount extracted by SPME 

different approaches under examination 

J.Microcolumn Separations (2000) 12(10), 550-557 

Tuduri, L.; Desauziers, V.; Fanlo, J. L 

757 Aerosols, particulate Sampling and Analysis of Airbourne Particulate matter 7um PDMS GC-MS 

in air and aerosols using In-Needle Trap and SPME fiber devices 

Anal. Chem., 2001, 73(1), 47-54 

Koziel, J., Odziemkowski, M., Pawliszyn, J. 

10 sec 

739 Aerosols, particulate Sampling and Raman Confocal Microspectroscopic Analysis PDMS Raman 

in air of Airborne Particulate Matter Using Poly(dimethylsiloxane 

Solid-Phase Microextraction Fibers 

Anal. Chem (2001) 73(13), 3131-3139 

Odziemkowski, M.; Koziel, J.; Irish, D.; Pawliszyn, J. 

574 Solvents Application of SPME to monitoring indoor air quality. 100µm PDMS GC-MS 

in air Fresenius'-J-Anal-Chem. Apr 1999; 363(7): 696-699 15 min 

Gorlo,-D; Zygmunt,-B; Dudek,-M; Jaszek,-A; Pilarczyk,-M; Namiesnik,-J 

542 Organic pollutants Application of SPME to monitoring indoor air quality 100µm PDMS GC-MS 

in air Fresenius' J. Anal. Chem. (1999), 363(7), 696-699 

Gorlo, D., Zygmunt, B., Dudek, M., Jaszek, A, Pilarczyk, M., 

Maniesnik, J. 





543 Organic vapors Time-Weighted Average Sampling with SPME Device; 100µm PDMS 

in Air Implications for Enhanced Personal Exposure Monitoring to 

Airborne Pollutants 

Anal. Chem. (1999), 71(8), 1513-1520 

Martos, p. Pawliszyn, J. 

932 Organic vapors Time-weighted average sampling of volatle and semiin 

Air volatile airborne organic compounds by the SPME device 

J. Chromatogr. A (2000), 892(1-2), 455-467 

Khaled, A, Pawliszyn, J. 

306 VOCs Application of Solid Phase Microextraction for Determination 

in water and air of Volatile Halogenated Hydrocarbons in Air and Water 

of an Indoor Swimming Pool 

Fresenius’ Environ. Bull. 5 (1+2): 55-60 (1996) 

Czerwinski, J., Zygmunt, B., Namiensnik, J. 

307 Pollution A Case Study of Indoor Pollution by Chinese Cooking 

in air Toxicol. Environ. Chem. 65 (1-4): 217-224 (1998) 

Benfenati, E., Pierucci, P., Niego, A. 

347 VOCs Nonequilbrium Quantitation of Volatiles in Air Stream by SPME 7µm, 30µm, 100µm GC-FID 

in air Anal. Chem. Vol. 71, January 1, 1999, pg. 92-101 PDMS 

Bartelt, R., Zilkowski, B. 27°C, 30 min 

gas sampling 

544 Volatiles in The sampling and analysis of volatile organic compounds 

atmosphere in the atmosphere 

React. Hudrocarbons Atmos. (1999), 119-157 

Boob, Academic, Coden: 67ERAQ 

Cao, X, Hewitt, C. 

851 Toluene diisocyanate Determination of gaseous toluene diisocyanate by use of 65µm DVB/PDMS LC-MS-MS 

solid-phase microextraction with on-fibre derivatisation. 60min. 

Fresenius' J. Anal. Chem. (2001), 369(6), 524-529 

Nilsson, U.; Batlle, R.; Colmsjo, A. 

dibutylamine derivative 

752 VOC, formaldehyde Field air analysis with SPME device varied fibers GC-FID 

in air Analytica Chimiera Acta 400 (1999) 153-162 1-75 min 

Koziel, J., Jia, M., Khaled, A., Noah, J., Pawliszyn, J. air samples 

753 VOC, formaldehyde Field Sampling and Determination of Formaldehyde in Indoor 65µm DVB/PDMS GC-FID 

in air Air with SPME and On-Fiber Derivatization 10min. Headspace 

Environ Sci Technol 2001, Vol 35, pg. 1481-1486 

Koziel, J., Noah, J., Pawliszyn, J. 

PFBHA Derivative 

755 Aromatic VOCs Design of Validation of Portable SPME devices for 65µm DVB/PDMS GC-FID 

in Indoor air rapid field air sampling and diffusion-based calibration 

Anal. Chem. 2001,73(3), 481-486 

Augusto, F., Koziel, J., Pawliszyn, J. 

30 sec air sampling 

759 VOCs Fast field sampling/sample preparation and quantification 65µm DVB/PDMS GC-FID 

in Indoor air of volatile organic compounds in indoor air by SPME 

and portable GC 

Field Analytical Chem. And Tech 4(2-3): 73-84,2000 

Jia, M., Koziel, J., Pawliszyn, J. 

1min. Headspace 

545 Volatile organics Analysis of volatile organic compounds in the ambient air of 

in air Algiers by GC with a beta-cyclodextrine capillary column 

J. Chromatogr A, 1999, 846(1+2), 287-293 

Yassaa, N., Meklati, B., Cecinato, A. 





984 VOC's in air Dynamic versus static sampling for quantitative analysis of VOC's in air. 

J.Chromatogr. A (2002) 963(1-2), 49-56 

Tuduri, L.; Desauziers, V.; Fanlo, J.L. 

PDMS/carboxen 

1062 

Volatile organics from 

steel. 

1070 Hydrogen cyanide in air 

1114 

Malodorous sulphur 

compounds in effluents 

1144 Smoke plumes 

1175 VOCs in air 

1187 

1194 PAHs 

1200 Benzene in air 

1305 

1313 

Volatile aliphatic amines 

in air. 

Chemical warfare 

agents 

Analysis of airborne volatile organic compounds of a steel industry by solid 

phase microextraction and gas chromatography/mass spectrometry. GC-MS 

Bulletin of Environmental Contamination and Toxicology (2003) 70 (5), 957- 

963. 

de Lourdes Cardeal, Z.; de Carvalho, C. R.; Parreira, F. V. 

Solid phase microextraction with analysis by gas chromatography to 

determine short term hydrogen cyanide concentrations in a field setting. GC-NPD 


Smith, P. A.; Sheely, M. V.; Kluchinsky, T. A, Jr. 

Development of a quantification method for the analysis of malodorous 

sulphur compounds in gaseous industrial effluents by solid-phase 

microextraction and gas chromatography-pulsed flame photometric 

detection 


Desauziers, Valerie; Fanlo, Jean-Louis; Lestremau, Francois; Roux, Jean- 

Claude 

PDMS/carboxen GC-PFPD 

Discrimination of combustion fuel sources using gas chromatography-planar 

field asymmetric-waveform ion mobility spectrometry GC-MS 


Eiceman, Gary A.; Funk, Paul A.; Hughs, S. Edgar; Miller, Raanan A.; 

Nazarov, Erkijon G.; Tarassov, Alexander 

Potential of solid-phase microextraction fibers for the analysis of volatile 

organic compounds in air. 


Tuduri, Ludovic; Desauziers, Valerie; Fanlo, Jean Louis 

Sampling and sample-preparation strategies based on solid-phase 

microextraction for analysis of indoor air. 

Trends in Analytical Chemistry (2002) 21 (12), 840-850. 

Koziel, J. A.; Novak, I. 

Screening direct analysis of PAHs in atmospheric particulate matter with 

SPME PDMS 

Talanta (2003) 60 (4), 687-693. 

Vaz, Jorge Moreira 

Determination of benzene at trace levels in air by a novel method based on 

solid-phase microextraction gas chromatography/mass spectrometry. 


Salvadori, Piero; Cuzzola, Angela; Pucci, Sergio; Raffaelli, Andrea; Saba, 

Alessandro 

Various fibers compared 

GC-ITMS 

Determination of volatile aliphatic amines in air by solid-phase 

microextraction coupled with gas chromatography with flame ionization 

detection GC-FID 


Jastrzebska, Anna; Namiesnik, Jacek; Zygmunt, Bogdan 

Solid phase microextraction sampling and gas chromatography/mass 

spectrometry for field detection of the chemical warfare agent O-ethyl S-(2diisopropylaminoethyl) 

methylphosphonothiolate (VX) 


Betsinger, Geoffrey; Hook, Gary L.; Kimm, Gregory; Logan, Tom; Savage, 

Paul B.; Smith, Philip A.; Swift, Austin 

Various GC-MS 


1334 

1342 




Odorant emissions from 

landfills. 

1373 Sarin in air and water. 

1186 

1141 

Perfume oil in household 

products. 

Characterisation of odorants emissions from landfills by SPME and GC/MS 

Chemosphere (2003) 51 (5), 357-368. 

Davoli, E.; Gangai, M.L.; Morselli, L.; Tonelli, D. 

DVB/Carboxen/PDMS GC/MS 

A simple calibration procedure for volatile organic compounds sampling in 

air with adsorptive solid-phase microextraction fibres. 

Analyst (2003) 128 (9), 1028-1032. 

Tuduri, L.; Desauziers, V. *; Fanlo, J. L. 

PDMS/CAR GC-FID 

Screening for sarin in air and water by solid-phase microextraction-gas 


Journal of Chromatographic Science (2001) 39(10), 420-424. 

Schneider, J. F.; Boparai, A. S.; Reed, L. L. 

Determination of perfume oil in household products by headspace solidphase 

microextraction and fast capillary gas chromatography. Various FCGC 

Chromatographia (2003) 57 (Supp), S199-S206. 

Bothe, F.; Dettmer, K.; Engewald, W. * 

VOC's from irradiated 

mail. Volatile organic compounds produced during irradiation of mail. 

AIHA Journal (2003) 64 (2), 189-195. 

Smith, Philip A.; Hakspiel, Shelly J.; Miller, Stephen; Sheely, Michael V. 

1126 Sulfur compounds 

1098 Ethylene oxide 

1447 


air 

1476 Isocyanates in air 

1478 Volatiles in air 

1479 VOCs in air 

Evaluation of solid-phase microextraction for time-weighted average 

sampling of volatile sulfur compounds at ppb concentrations Carboxen/PDMS 


Andersson, Fras Annika T.; Desauziers, Valerie; Fanlo, Jean-Louis; 

Lestremau, Francois 

Determination of low-level residual ethylene oxide by using solid-phase 

microextraction and gas chromatography. 


Ayoub, K.; Harris, L.; Thompson, B. 

Characterization of volatile effluents of livestock buildings by solid-phase 


Int. J. Environ. Anal. Chem. (2003) 83(10), 837-849 

Begnaud, Frederic; Berdague, Jean-Louis; Peres, Christophe 

Development of a personal isocyanate sampler based on DBA derivatization 

on solid-phase microextraction fibers. 


Nilsson, Ulrika; Batlle, Ramon; Colmsjo, Anders 

Traditional sampling with laboratory analysis and solid phase 

microextraction sampling with field gas chromatography/mass spectrometry 

by military industrial hygienists. 

AIHAJ (2002) 63(3), 284-292 

Thomas, Richard J.; Smith, Philip A.; Lee, Arthur P.; Kluchinsky, Timothy A., 

Jr.; Erickson, Richard P.; Savage, Paul B.; Stevens, Michael; Williams, 

Kenneth 

Solid phase microextraction : Measurement of volatile organic compounds 

(VOCs) in Dhaka City air pollution. 

Journal of Environmental Science and Health Part A Toxic-Hazardous 

Substances & Environmental Engineering (2002) A37(7), 1223-1239 

Hussam, A.; Alauddin, M.; Bhattacharjee, M.; Bibi, H.; Chowdhury, D.; Khan, 

A. H.; Sultana, S. 



65um PDMS/DVB, dibutylamine 

(DBA) derivative 

HPLC-MS 

GC-MS




1523 Glutaraldehyde in air 

1524 

Valeraldehyde in air 

(TWA) 

Gas chromatographic determination of glutaraldehyde in the workplace 

atmosphere after derivatization with O-(2,3,4,5,6pentafluorobenzyl)hydroxylamine 

on a solid-phase microextraction fibre. 


Pieraccini, Giuseppe; Bartolucci, Gianluca; Boccalon, Pierpaolo; Dugheri, 

Stefano; Focardi, Leonardo; Pacenti, Marco 

Time-weighted average sampling of airborne n-valeraldehyde by a solidphase 

microextraction device. 


Tsai, S.-W.; Chang, T.-A. 

1543 Nicotine in air Trace analysis of nicotine in indoor air by a SPME method. 

Bulletin of Environmental Contamination and Toxicology (2002) 68(4), 485- 

489 

Shuokui, H.; Huali, Y.; Jianfang, F.; Songting, G. 

1528 

1547 

VOCs in air (dynamic 

sampling) 

Volatiles in air (passive 

sampling) 

1388 Perfumes 

Dynamic air sampling of volatile organic compounds using solid phase 


Journal of Environmental Science and Health Part B Pesticides Food 

Contaminants and Agricultural Wastes (2002) B37(4) 365-378 

Razote, Edna; Chobpattana, Wannee; Jeon, Ike; Maghirang, Ronaldo 

Evaluation of indoor exposition to benzene, toluene, ethylbenzene, xylene, 

and styrene by passive sampling with a solid-phase microextraction device. 


Cardeal, Zenilda de L.; de Carvalho, Ciomara R.; Parreira, Fabricio V. 

On-fiber derivatization with 

PFBHA 

65um DVB PDMS, on-fiber 

derivatization with PFBHA 

GC 

GC-FID 


100um PDMS, 65um DVB 

PDMS 

Atmospheric lifetimes and fates of selected fragrance materials and volatile 

model compounds. 

Environmental Science and Technology (2001) 35(18), 3595-3600. 

Aschmann, S. M.; Arey, J.; Atkinson, R. *; Simonich, S. L 

PDMS GC-MS 

2111 Hydrocarbons Measuring the effect of photocatalytic purifiers on 15 min sampling GC 

in air indoor air hydrocarbons and carbonyl pollutants 

J. Air Waste Manage. Assoc., 55, #1, 88-96 

Disdier, Jean; Mas, Denis; Pichat, Pierre 

2112 BTEX Air sampling of aromatic hydrocarbons in the 100µm PDMS GC-FID, GC-MS 

in air presence of ozone by SPME headspace 

J Chromatogr A, 1025, #1, 57-62 

Xiong, G; Koziel, J.; Pawliszyn, J. 

2113 PCBs in Sampling and analysis of PCBs in indoor air by headspace GC-MS 

indoor air sorbent enrichment followed by headspace 

SPME and GC-MS 

J. Chromatogr. A,1072, #1, 99-106 

Ares, S; Barro, R; Cela, R; Garcia-Jares, C; Llompart, M 

2114 Organo- Air sampling of organophosphate triesters using 100µm PDMS GC 

phosphate SPME under non-equilibrium conditions. 1 hr. sampling 

triesters in Anal & Bioanalytical Chem, 378, #7, 1847-1853 

air Isetun, S.; Nilsson, U.; Colmsjo, A.; Johansson, R. 

2115 Organo- Evaluation of SPME w/ PDMS for air sampling of 100µm PDMS GC 

phosphate gaseous organophosphate flame-retardants 8 hrs. sampling 

triesters in and plasticizers 

Air Anal & Bioanalytical Chem, 380, #2, 319-324 

Isetun, Sindra; Nilsson, Ulrika; Colmsjo, Anders 

2116 Volatile Investigation of artefact formation during analysis 75µm Carboxen GC 

sulfur of volatile sulfur compounds "in air" using SPME direct air sample 

compounds Chromatographiam 59, #9-10, 607-613 

in air Lestremau, F.; Andersson, F.; Desauziers, V. * 





2117 BTEX in Determination of benzene, toluene, ethylbenzene and 75µm Carboxen GC-MS 

air xylenes in air by SPME-GC-MS 30 min sampling 

Analytical & Bioanalytical Chem, 380, #5-6, 824-830 

Tumbiolo, S.; Gal, J. -F.*; Maria, P. -C.; Zerbinati, O. 

2118 Acetic acid Use of SPME for the detection of acetic acid by ion-trap GC-ITMS 

in air GC-MS and application to indoor levels in museums 

J. Chromatogr. A, 1067, #1-2, 331-336 

Godoi, Ana F.L.; Van Grieken, Rene; Van Vaeck, Luc 

2119 Chloro- Development of a sensitive methodology for the 65µm PDMS-DVB GC-MS 

benzenes analysis of chlorobenzenes in air bycombination of 65µm CW GC-ECD 

in air SPE and headspace SPME headspace 

J. Chromatogr. A, 1045, #1-2, 189-196 

Ares,S; Barro,R; Cela,R; Garcia-Jares,C; Llompart,M 

2120 Sarin in Air Dynamic SPME for sampling of airborne sarin with Direct sampling of air GC-MS 

GC-MS for rapid field detection and quantification 

J. Sep. Sci., 27,#12, 1017-1022 

Hook, G.; Lepage, C; Miller, S.; Smith, P. 

2121 Sulfur compd Analysis of sulfur-containing compounds in ambient air direct sampling GC-FPD 

in air using SPME-GC with pulsed FPD 

Int. J. Environ. Anal. Chem., 84, #10, 749-760 

Li, Kwong-Chi; Shooter, David 

2122 Aniline Determination of aniline in silica gel sorbent by one-step 65µm PDMS-DVB GC-FID 

in air in situ microwave assisted desorption coupled to headspace 

headspace SPME and GC-FID 3 min extraction 

Talanta, 64, #3, 650-654 

Jen, Jen-Fon; Shih, Ton-Sheng; Yan, Cheing-Tong 

2123 Popylene Propylene glycol vapor contamination in controlled headspace MD-GC-MS 

glycol in environment growth chambers: Toxicity to corn and 

air soybean plants 

J. Environ. Sci. Health Part B, 40, #3, 443-448 

McConnell, Laura; Niu, Genhua; Reddy, Vangimalla R. 

Theory / Technique 

856 Volatiles An automated method for the determination of some volatile GC-ECD 

in water organic compounds in water samples after extraction by 

SPME and CGC-ECD analysis 

Rev. Port. Farm (2000) 50(4) 141-149 

Cunha, E.; Goncalves, C.; Alpendrurada, M. F. (Portuguese) 

2 VOCs, BTEX, PAHs Solid Phase MicroExtraction with Thermal Desorption Using 56µm PDMS GC-FID, 

in water Fused Silica Optical Fibers 2 min GC-ECD 


Arthur, C., Pawliszyn, J. salt added 

5 BTEX Solid Phase MicroExtraction: An Attractive Alternative 100µm PDMS GC-FID 

in water Environmental Lab. 11, Dec/Jan 1992/1993 pp 10-15 14 min 

Arthur, C., Killam, L., Chai, M., Buchholdz, K., Potter, D., stirring 

Zhang, Z., Pawliszyn, J. salt added 

9 BTEX Automation and Optimization of Solid Phase MicroExtraction 56µm & 100µm PDMS GC-FID 

in water Anal. Chem. 64: 1960-1966 (1992) 2-40 min 

Arthur, C., Killam, L., Buchholz, K., Pawliszyn, J. stirring, salt added 

820 Jasmine plant A versatile Robotic Arm for Static headspace 85µm Polyacrylate GC-MSN 

beer sampling with SPME 30min. 

LC-GC Europe, April 2001, 215-222 

Pham-Tuan, H., Vercammen, J., Sandara, P. 

headspace 





12 BTEX Solventless Injection Technique for Microcolumn Separations 100µm PDMS GC-MS 

in water J. Microcolumn Sep. 5: 51-56 (1993) 

Arthur, C., Chai, M., Pawliszyn, J. 

13 BTEX, PAHs Headspace Solid Phase MicroExtraction 56µm PDMS GC-FID 

in water Anal. Chem. 65(14): 1843-1852 (1993) 1-5 min 

Zhang, Z., Pawliszyn, J. headspace 

16 Nitroaromatics Practical Use of Automated Solid Phase Extraction 100µm PDMS GC-FID 

in water Amer. Lab. Nov. Vol. 25,1993, p18-24 1-20 min 

Berg, J. immersion 

17 Toluene On-Line Monitoring of Flowing Samples Using SPME-GC 56µm PDMS GC-FID 

in water Anal. Chim. Acta 284: 265-273 (1993) 20 min 

Motlagh, S., Pawliszyn, J. immersion, stirring 

21 Phenols Optimization of Solid Phase MicroExtraction (SPME) Conditions 85µm polyacrylate GC-MS 

in water and air for Phenol Analysis 40 min 

Anal. Chem. 66: 160-167 (1994) immersion & headspace 

Buchholz, K., Pawliszyn, J. pH 2, salt added 

acetate derivatives 

204 Phenols Determination of Phenols by Solid-Phase Microextraction 

J. Chromatogr. A 767: 171-175 (1997) 

Bartak, P., Cap, L. 

391 Phenols, PAHs SPME for Determining the Binding State of Organic Pollutants 7µm PDMS GC-MS 

in water in Contaminated Water Rich in Hujic Organic Matter 50°C, 90-180 min 

J. Chromatogr. A, 816 (1998) 159-167 headspace 

Porschamann, J., Kopinke, F., Pawliszyn, J. stirring 

24 PAHs Silica-Fiber microextraction for Laser Desorption Ion Trap Trimethlysilyl coated fiber MS 

in soil and water Mass Spectrometry 

Anal. Chem. 66: 1897-1901 (1994) 

Cisper, M., Earl, W., Nogar, N., Hemberger, P. 

3 min 

27 PAHs Solid Phase microextraction Coupled to HPLC 15µm PDMS HPLC-UV 

in water Anal. Chem. 67: 2530-2533 (1995) 6-60 min 

Chen, J., Pawliszyn, J. immersion 

222 Potential Applications of Coupled SPME-HPLC 

LaborPraxis 20 (11): 66-68, 71 (1996) 

Haag, I. 

HPLC 

33 Fatty acids, PAHs, Solvent-free Sample Introduction for Supercritical Fluid 15µm PDMS, GC-FID 

pesticides in Chromatography Using Polymer Coated Fibers 85µm polyacrylate 

methanol/water J. Microcolumn Res. 42: 1925-1930 (1994) 5 min 

Hirat, Y., Pawliszyn, J. immersion 

35 BTEX Headspace SPME vs. Purge & Trap for the Determination of 100µm PDMS GC-FID 

in water Substituted Benzenes in Water 40°C, 50 min 

J. Chromatogr. Sci. 32(8): 317-322 (1994) headspace 

MacGillevra, B. stirring, salt 

38 BTEX Quantitative Extraction Using an Internally Cooled Solid 50µm PDMS GC-MS 

in water Phase MicroExtraction Device 22-80°C, 2-5 min 

Anal. Chem. 67(1): 34-43 (1995) 

Zang, Z., Pawliszyn, J. 

headspace 





43 Organophosphorus Element-Selective Detection of Pesticides by Gas 100µm PDMS GC-AED 

pesticides Chromatography Atomic Emission Detection 20 min 

in water and Solid Phase MicroExtraction 

J. Chromatogr. 683: 175-183 (1994) 

Eisert, R., Levser, K., Winsch, G. 

immersion 

44 BTEX Solid-Phase Microextraction: A Solvent-Free Alternative for polyacrylate, PDMS GC-FID 

in water for Sample Preparation 

Anal. Chem. 66(17): 844A-853A (1994) 

Zang, Z., Yang, M., Pawliszyn, J. 

immersion, salt 

45 BTEX New Solvent-Free Sample Preparation Techniques Various fibers and GC-FID,E1858 

in water and air ES &T 28 (13): 569A-574A (1994) 

Boyd-Boland, A., Chai, M., Luo, Y. Zhand, Z. Yang., M., 

Pawliszyn, J. 

extraction conditions GC-MS 

213 A New Separation and Extraction Method -- Solid-Phase 

Microextraction 

Sepu (Chinese) 15 (2): 118-119 (1997) 

Liu, J. 

56 SPME 

GIT Fachz. Lab. 39: 325-362 (1995) 

Popp, P. 

57 BTEX Sample Introduction Approaches for Solid Phase 

in water MicroExtraction-Rapid GC 

Anal. Chem. 67: 3265-3274 (1995) 


GC-FID 

58 BTEX Solid Phase MicroExtraction/Isothermal GC for Rapid 15µm PDMS GC-FID 

in water Analysis of Complex Organic Samples 2 min 

J.High Res.Chromatogr. 18 (2): 161-166 (1995) headspace 

Gorecki, T., Pawliszyn, J. stirring 

59 Semivolatiles SPME as a Method for Estimating the Octanol Water Partition 85µm polyacrylate GC-FID 

in water Coefficient min to 20 hr 

Anal. Chem. 68: 130-133 (1996) 

Dean, J., Tomlinson, W., Makovskaya, V., Cumming, R., 

Hetheridge, M., Comber, M. 


546 PAHs Solubility and partitioning studies with PAHs using an 100µm SPME GC-MS 

in water and optimized SPME procedure stirred 

octanol-water Fresenius' J. Anal. Chem. (1999), 363(4), 426-428 

Paschke, A., Popp, P., Schueuermann, G. 

728 PAHs Determination of PAHs in waste water by off-line coupling 100µm PDMS HPLC 

in waste water SPME with column liquid chromatography 

J. Chjromtogr. A, 897(2000) 153-159 

Popp, P., Bauer, C., Moder, M., Paschke, A. 

60 min fluorescence 

547 Pesticides in Extracted amounts by SPME: a realistic approach to the 

water partition coefficient K. 

J. Chromtogr. Sci. 1999, 37(8), 277-282 

Urruty, L., Montury, M 

548 Volatiles Determination of Henry's law coefficient by combination of 100µm PDMS GC-FID 

in water the equilibrium partitioning in closed systems and 

SPME techniques 

J. Chromatogr, A., (1999), 830(2), 353-363 

Dewulf, J., Van Langenhove, H., Everaert, P 

30 min @ varied temp. 





237 Organics in Partitioning of Organic Chemicals to Polyacrylate-Coated 85µm polyacrylate GC-FID, -ECD 

water and air Solid-Phase Microextraction Fibers: Kinetic Behavior and immersion GC-MS 

Quantitative Structure-Property Relationships 

Anal. Chem. 68: 4458-4462 (1996) 

Vaes, W., Hamwik, C., Ramos, E., Verhaar, H., Hermens, J. 

stirring 

84 Solid Phase Microextracting Using Fused-Silica Fibers Coated 

with Graphitized Carbon Black 


Mangani, R., Cenciarini, R. 

88 Overview New Direction in Sample Preparation for Analysis of 

Organic Compounds 

Trends Anal. Chem. 14 (3): 113-122 (1995) 

Pawliszyn, J. 

Multiple applications 

121 Eugenol, Solid Phase Microextraction for Quantitative Analysis in 85µm polyacrylate GC-MS 

2,4-dimethylphenol, Nonequilibrium Situations 1-160 min 

2-phenylethanol Anal. Chem. 69: 1230-1236 (1997) immersion, stirring 

in water Ali, J. salt added 

360 2-Octanol SPME in Headspace Analysis, Dynamics in Non-Steady State 85µm polyacrylate, GC-MS 

in water Mass Transfer 100µm PDMS 

Anal. Chem., 70: 4822-4826, (1998) 

Ali, J. 

headspace 

214 Strawberries Solid-Phase Microextraction: Artifact Formation and Its 85µm polyacrylate GC-MS 

and apples Avoidance 30 sec 

in fruit homogenate Chromatographia 46: 63-66 (1997) 

Verhoeven, H., Beuerle, T., Schwab, W. 

immersion 

139 McReynolds probes Studying Activity Coefficients of Probe Solutes in Selected 7µm PDMS GC-FID 

in methanol Liquid Polymer Coatings Using SPME 25-100°C, 15 min 

J. Phys. Chem. 100: 17648 (1996) 

Zhang, Z., Pawliszyn, J. 

headspace 

729 Lidocane Multiple solid phase microextraction 100µm PDMS HPLC 

from water J. Chromatogr. A. (2000) 878, 27-33 

Koster, E., de Jong, G. 

45min 

939 Fibers coated with molecularly imprinted polymers for SPME 

Anal. Chem (2001) 73(13) 3140-3145 

Koster, E; Crescenzi, C; den Hoedt, W; Ensing, K; de Jong, G 

579 BTEX and solvents Study of polymer coatings for solid-phase microextraction 88µm PDMS 

in water Sepu. Jan 1999; 17(1): 10-13 

Zhang,-DN; Wu,-CY; Ai,-F 

148 Maillard reaction A Study of the Behavior of Maillard Reaction Products 100µm PDMS GC-MS 

products Analyzed by SPME-GC-Mass Selective Detection 5 min 

in water J. Chromatogr. Sci. 34: 213 (1996) immersion 

Coleman III, W. stirring 

207 Alkyl & alkoxy aroma & A Study of the Behavior of Polar and Nonpolar SPME Fibers 100µm PDMS GC-MSD 

flavor compounds J. Chromatogr. Sci. 35 (6): 245-258 (1997) 5 min 

in water Coleman, W. immersion & 

headspace 






730 Inorganic anions SPME of inorganic anions based on polypyrrole film Polypyrrole film Ion Chrom. 

in water Analyst (Cambridge, UK), 2000, 125(3), 391-394 

Wu, J., Yu, Z, Lord, H., Pawliszyn, J. 

764 Volatile organics Preparation and appplication of polypyrrole films in SPME Polypyrrole film In-tube GC-FID 

PAHs, amines J. Chromatogr. A (2001) 909(1) 37-52 20min. LC-UV 

in water/air mixture Wu, J., Pawliszyn, J. headspave 

163 Mercury, SPME Combined with Electrochemistry 10µm gold on GC-MS 

mercury compounds Anal. Commun. 33(10): 361-364 (1996) carbon steel electrode 

in water Guo, F., Gorecki, T., Irish, D., Pawliszyn, J. 5 min 

gas phase sampling 

stirring, KNO3 added 

182 Use of SPME with Ion Mobility Spectrometry 

Anal. Lett. 30 (7): 20-22 (1997) 

Orzechowsa, G., Poziomek, E., Tersol, V. 

GC-MS 

228 VOCs SPME of Volatile Organic Compounds. Estimation of the 100µm PDMS GC-FID 

in seawater Sorption Equilibrium from the Kovats Index Effect of Salinity 45 min 

and Humic Acids and the Study of the Kinetics by the immersion 

Development of an "Agitated/Static Layer" Model stirring 

J. Chromatogr. A 761: 205-217 (1997) 

Dewulf, J., Everaert, M., Van-Langenhove, H. 

salt added 

840 Squalene Determination of squalene in seawater by SPME-GC-MS and 100µm PDMS GC-MS 

in seawater the concentration variation of squalene in redtide seawater. 45 min 

Fenxi Huaxue (2000) 28(11) 1326-1330 immersion 

Zhao, M. Q.; Li, G. K.; Luan, T. G.; Zhang, Z. X. stirring 

165 Triazines, organic Development of a Prototype System for Quasi-Continuous 85µm polyacrylate GC-ECD, -FID 

pesticides Analysis of Organic Contaminants in Surface or Sewage 10 min 

in sewage water Water Based on In-Line Coupling of SPME to GC 

J. Chromatogr. A 737 (1): 59-65 (1996) 


300mL/min flow 

166 Pesticides Design of Automated SPME for Trace Analysis of 100µm PDMS GC-FID 

in water Organic Compounds in Aqueous Samples 30 min 

J. Chromatogr. A 776: 293-303 (1997) 

Eisert, R., Pawliszyn, J. 

stirring 

184 BTEX, Sample Preparation for GC with SPE & SPME 100µm PDMS GC-FID 

pesticides Chromatogr. 37: 205-236 (1997) 2-20 min 

in water Penton, Z. immersion, stirring 

salt added 

236 Aromatic Porous-Layer Solid-Phase Microextraction Using Silica 30µm C8 silica bonded GC-FID 

hydrocarbons Bonded Phase metal fiber 

in water Anal. Chem. 69: 190-195 (1997) 20 min 

Liu, Y., Shen, Y., Lee, M. stirring 

189 PAHs in High Temperature Water Extraction Combined with SPME 30µm PDMS GC-FID 

water extract Anal. Commun. 33: 421-424 (1996) 70 min 

Daimon, H., Pawliszyn, J. stirring 

220 C6-C11 hydrocarbons Initial Bandwidth Resulting from Splitless and Solid-Phase 100µm PDMS GC-FID 

in water Microextraction Gas Chromatographic Injections 10 min 

J. High Res. Chromatogr. 20 (2): 77-80 (1997) immersion 

Snow, N., Okeyo, P. stirring 





138 PAHs in Optimizing Split/Splitless Injection Port Parameters for SPME 7µm & 100µm PDMS GC-FID 

water J. Chromatogr. A 740 (1): 139-145 (1996) 5 hr 

Langenfeld, J., Hawthorne, S., Miller, D. immersion, stirring 

211 Nitro musk compounds Nitro Musks in Cosmetic Products: Determination by 100µm PDMS GC-AID 

in cosmetic products Headspace SPME and GC with Atomic Emission Detection: 1-60 min 

Dynamics of Organic Compound Extraction from Water, 

Using Liquid-Coated Fused Silica Fibers 

Chromatogrphia 45; 138-144 (1997) 

Struppe, C., Schaefer, B., Engewald, W. 

headspace 

243 Dynamics of Organic Compound Extraction from Water, Using 

Liquid-Coated Fused Silica Fibers 

Anal. Chem. 66: 1186-1199 (1994) 

Arthur, C., Pawliszyn, J. 

437 Review SPME and Its Utilization in Environmental Analysis 

Chem. Listy (1998), 92(8), 633-642 

Sedlakova, J., Matisova, E., Slezackova, M. 

549 Review of 52 refs. Trends in SPME for determining organic pollutants in 

environmental samples 

Trends Anal. Chem. 1999, 18(8), 557-568 

Penalver, A., Pocurull, E., Borrull, F., Marce, R. 

Varied 

550 Proceeding of Extech Advances in Extraction Technology: A report from Extech '99 

LC-GC Current Trends and development in Sample Prep, 

Sept. 1999, Vol. 17., No. 90, S25-S30 


Varied 

551 Overview of SPME Sample Preparation for GC with SPE and SPME 

Advances in Chromatography, Vol. 37, 1966, 205-236 

Book chapter by M. Dekker, New York, 1996 

Penton, Z. 

244 Solid Phase Microextraction -- A Unique Tool for 

Chemical Measurements 

Can. J. Chem. 74: 1297-1308 (1996) 

Gorecki, T., Boyd-Boland, A., Zhang, Z., Pawliszyn, J. 

245 Solvent Free Sample Preparation Techniques Based on Fiber 

and Polymer Technologies 

Environ. Sci. Technol. 28: 569A-574A (1994) 

Boyd-Boland, A., Chai, M., Luo, Y., Zhang, Z., Yang, M., 


246 BTEX, Solid Phase Microextraction 100µm PDMS GC-FID, -ECD 

pesticides Tech. Aquat. Toxicol. 459-477 (1996) 10-30 min 

in water Webster, G., Sarna, L., Graham, K. immersion 

stirring 

247 Solid Phase Microextraction Technique for Gas overview 

Chromatography 

Huaxue 54 (3): 119 (1996) 

Huang, S. 

article 

248 BTEX, Sample Preparation for Gas Chromatography with SPE 100µm PDMS GC-FID 

pesticides and SPME 2-20 min 

in water Adv. Chromatogr. (N.Y.) 37: 205-236 (1997) immersion, stirring 

Penton, Z. salt added 





249 BTEX, Solid Phase Microextraction-SPME, State of the Art 100µm PDMS GC-FID 

pesticides Chromatography Kaiser, O. (Ed.) Incom, Dusseldorf, 2-20 min 

in water pp153-166 (1997) immersion, stirring 

Kern, H., Penton, Z. salt added 

250 Reference book Solid Phase Microextraction: Theory and Practice various fibers 

VCH, New York, 275pp (1997) 

Pawliszyn, J. 


731 Reference book Applications of Solid Phase Microextraction 


RSC Chromatography Monographs 

35 applications described 

732 Overview Theory of solid phase microextraction 


Pawliszyn, J. 

733 Researchers are giving SPME a second look 30:50 Carboxen/DVB/PDMS GC-FID 

R&D Magazine, February 1999, 44-45 headspace 

251 Overview Sample Preparation and Solid-Phase Extraction no fibers or 

LC-GC 15: 1106, 1108, 1110-1113, 1116-1117 (1997) 

Majors, R., Raynie, D. 

conditions shown 

252 Formaldehyde, Recent Advances in Solid Phase Microextraction 65µm PDMS/DVB, GC-MS, 

surfactants in LC-GC May Supplement, ppS41-S46 (1998) Carbowax/TPR fiber HPLC-UV 

air and water Lord, H., Pawliszyn, J. varied conditions 

255 Thiophenes Application of SPME/GC-MS to Characterize Metabolites in 85µm polyacrylate GC-MS 

in water the Biodesulfurization of Organosulfur Model Compounds 20 min 

in Gitumen immersion 

Environ. Sci. Technol. 32 (3): 421-426 (1998) 

MacPherson, T., et al. 

pH 2 

256 Construction of an Interface for SPME-PC-SFC 

J. High Resolut. Chromatogr. 34 (10): 275-277 (1997) 

Medvedovici, A., Sandar, P. 

257 Phenylurea pesticides Automated In-Tube SPME Coupled to HPLC Omegawax 250 HPLC-UV, 

in water Anal. Chem., Vol. 69, No. 16, August 15, 1997, 3140-3147 


25µL, 10 flush cycles 245nm 

258 PAHs Effect of Heating the Interface on Chromatographic 100µm PDMS HPLC-UV, 

in water Performance of SPME Coupled to HPLC 60 min 254nm 

Anal. Commun. 34 (11): 365-369 (1997) immersion 

Daimon, H., Pawliszyn, J. heat desorb 22-180°C 

259 PAHs Effect of Heating the Interface on Chromatographic 100µm PDMS HPLC-UV, 

in water Performance of SPME Coupled to HPLC 60 min 254nm 

Analyst (Cambridge) 122 (11): 365-369 (1997) immersion 

Daimon, H., Pawliszyn, J. heat desorb 22-180°C 

260 Hg (II) ion SPME Combined with HPLC for the Determination of Metal Ions polypropylene hallow HPLC-UV, 

in water Using Crown Ether as Selective Extracting Reagent fiber, 30 min 254nm 

J. Microcolumn Sep. 167-173 (1998) immersion 

Jia, C., Luo, Y., Pawliszyn, J. derivative: 

dibenzo-18-crown-6 

734 Dopamine in Analysis of biogenic amines by SPME and HPLC with Carbowax-TPR HPLC 

biological matrix electrochemical detection 

J. Chromatogr. A, (2000) 873, 396 

Auger, J., Boulay, R., Jaillais, B., Delion-Vancassel, S. 

electrochem 





368 Aromatic amines SPME Coupled with HPLC for the Determination of Aromatic Carbowax/TPR, HPLC-UV, 

in wastewater Amines PDMS/DVB 280nm 

Anal. Chem., Vol. 71, No. 2, January 15, 1999, 310-316 30 min or 20 min 

Wu, Y., Huang, S. Na2SO4 buffer added 

407 Phenylurea pesticides Automated In-Tube SPME Coupled to HPLC Omegawax 250 UV, 245nm 

in water Anal. Chem., Vol. 69, No. 16, August 15, 1997, 3141-3147 


25uL, 10 flush cycles 

735 Carbamate Automated in-tube SPME-HPLC for Carbamate Intube capillaries HPLC 

pesticides pesticide analysis 

in water J. Chromatogr. A, (2000) 873(1), 137-147 

Gou, Y, Eisert, R., Pawliszyn, J. 

736 Carbamate In-tube SPME coupled to capillary LC for Carbamate Intube capillaries HPLC 

pesticides analysis in water samples 

in water Anal. Chem. 2000, 72(13), 2774-2779 

Gou, Y., Pawliszyn, J. 

737 Carbamate On-line coupling of in-tube SPME to HPLC for analysis Intube capillaries HPLC 

pesticides of carbamates in water samples: comparison of 

in water two commercially available autosampler 

J. Microcolumn Sep. (2000), 12(3), 125-134 

Gou, Y., Tragas, C., Lord, H., Pawliszyn, J. 

789 Development of effective sample pretreatment by in-tube 

SPME and its application 

Chromatography (2000) 21(4), 276-279 

Kataoka, Hiroyuki; Wu, Jingcun; Lord, Heather L.; Pawliszyn, J. 

Intube capillaries 

810 Sample preparation technique using fiber-in-tube SPME 

Chromatography (2000), 21(4), 284-285 

Jinno, K; Kawazoe, M; Saito, Y; Hayashida, M 

571 175 references On-line combination of aqueous-sample preparation and various references of 

review capillary gas chromatography 

J-Chromatogr,-A. 21 May 1999; 842(1-2): 391-426 

Louter,-AJH; Vreuls,-RJJ; Brinkman,-UAT 

SPME & SPE 

552 Solid phase microextraction turned inside out 

Che. Aust. 1999, 66(6), 9-11 

Tan, D., Marriott, P., Lee,H., Morrison, P. 

Intube capillaries 

412 Solventless Analytical Separation Method -- 

SPME/Microcolumn LC 

Chromatography (1998), 19(2), 6063 

Jinno, K. 

HPLC 

261 Fatty acid Derivatization/SPME: New Approach to Polar Analytes 85µm polyacrylate GC-FID 

methyl esters Anal. Chem. 69(2): 196-205 (1997) 2 hr 

in air and water Pan, L., Pawliszyn, J. headspace, pH 6 

derivative: 1-pyrenyldiazomethane 

819 Formaldehyde Solid phase analytical derivatization: enhancement of 

sensitivity and selctivity of analysis 

J.Chromatogr. A., 843, 19-27 

Rosenfeld, J. 

On-fiber derivatization 





553 9 references New Gas chromatographic approach to polar compounds 

by derivatization-SPME 

Bunseki, 1999 (7), 595-597 

Takauchi, M. 

Japanese 

262 Alcohol and ketones Strategies for the Analysis of Polar Solvents in Liquid Matrixes Nafion fiber GC-ECD 

in water Anal. Chem. 70 (1): 19-27 (1998) 10 min 

Gorecki, T., Martos, P., Pawliszyn, J. headspace 

stirring 

738 Phenanthrene, PCB Absorption of hydrophobic compounds into the 7µm PDMS GC-MS 

pentachlorobenzene poly(dimethylsiloxane) coating of SPME fibers: high 10min 

in water partition coefficients and fluorescence 

microscopy images 

Anal. Chem. (2000) 72(3), 459-464 

Mayer, P., Vaes,W., Hermens, J. 

739 Hydrophobic Nonequilibrium SPME for determination of the freely 7µm PDMS GC-ECD 

compounds (PCBs) dissolved concentration of hydrophobic organic 0.5-60min @ 37°C 

in water compounds: matrix effects and limitations 

Anal. Chem 2000, 72(13), 2802-2808 

Oomen, A., Mayer, P., Tolls, J. 

263 nC8 to nC14, Methodological Aspects of Headspace SPME. Application various fibers GC-FID 

neat J. High Resolut. Chromatogr. 20 (4): 217-221 (1997) 80°C, 5 min 

Schafer, B. Hennig, P., Engewald, W. headspace 

264 Phenol, alcohols Headspace SPME. Dynamics and Quantitative Analysis Before 85µm polyacrylate GC-MS 

in water Reaching a Partition Equilibrium 1-80 min at 25°C, 

Anal. Chem. 69 (16): 3260-3266 (1997) 1-40 min at 80°C 

Ali, J. headspace 

stirring 

413 Tetraethyllead SPME as a Sample Introduction Technique for Radio Frequency 30µm PDMS radio frequency 

in water Glow Discharge MS 5 min glow discharge 

Anal. Commun. (1997), 34(10), 275-277 

Gorecki, T., Belkin, M., Caruso, J., Pawliszyn, J. 

headspace, stirred MS 

265 Effect of Sample Volume on Quantitative Analysis by SPME, 

Part 1 - Theoretical Considerations 

Analyst (Cambridge) 122 (10): 1079-1086 (1997) 


740 Theory Kinetics of SPE and SPME in thin adsorbent layer with 

saturated sorption isotherm 

J.Chromatogr. A (2000) 873(1), 39-51 

Emenov, S, Koziel, J., Pawliszyn, J. 

769 BTEX The use of polymeric fullerenes as a new coating for SPME GC-FID 

from water Chromatographia (2000) 52(11/12), 803-809 

Xiao, C.; Liu, Z. ; Wang, Z.; Wu, C.; Han, H. 

headspace 

266 Organics SPME as a Tool to Determine Membrane/Water Partition 85µm polyacrylate GC-FID 

in water Coefficients and Bioavailable Concentrations in vitro 9-17 min 

Systems 

Chem. Res. Toxicol. 10 (10): 1067-1072 (1997) 

Vae, W., et al. 






267 PAHs, phenols, Sol-Gel Coating Technology for the Preparation of SPME Fibers Solgel coating GC-FID 

anilines of Enhanced Thermal Stability 30 min 

in water Anal. Chem. 69 (19): 3889-3898 (1997) 

Chong, S. et al. 

stirring 

911 Organometalics Development of new SPME fibers by sol-gel technology 

for SPME-HPLC determination of organometals 

Analytica Chimica Acta 1999, 402(1-2) 67-69 

Gabatu, T., Sutton, K., Caruso, J. 

Solgel coatings HPLC 

741 BTEX, herbicides High-performance polyethylene glycol-coated SPME fibers PAG sol-gel fiber 

in water using sol-gel technology 30°C, headspace 

J. Chromatogr. A 893 (2000) 157-168 

Wang, Z., Xiao, C., Wu, C., Han, H. 

salt added, pH adjusted 

554 Sol-gel method for the preparation of SPME fibers 

Anal. Lett., 1999, 32(8), 1675-1681 

Zhou, Z., Wang, Z., Qu, C., Zhan, W., Xu, Y. 

Solgel coatings 

268 BTEX Field-Portable SPME/Fast GC for Trace Analysis 30µm PDMS GC-FID, -PID 

in soil Field Anal. Chem. Technol. 1 (5): 277-284 (1997) 2 min, 

Gorecki, T., Pawliszyn, J. headspace, stirring 

555 Optimization of the SPME device design for field 

applications 

Fresenius' J. Anal. Chem. 1999, 364(7), 610-616 

Muller, L., Gorecki, T., Pawliszyn, J. 

varied coatings 

742 Equipment design Fiber Conditioners for SPME: Design, Testing, and application 

J.High Resol. Chromatogr. 2000, 23(4) 343-347 

Koziel, J., Shurmur, B., Pawliszyn, J. 

948 Organic pollutants SPME- a convenient tool for the determination of review article 

environmental organic pollutants in environmental matrices 

matrices Anal Chem (2001) 31(1), 1-18 

Zygmunt, B.; Jastrzebska, A.; Namiesnik, J. 

269 Organics in New Trends in SPME various fibers GC, HPLC 

air and water Crate. Rev. Anal. Chem. 27 (2): 103-135 (1997) 



556 Review of technique Solid Phase Microextraction 

TrAC, Trends Anal. Chem. (1999), 18(4), 272-282 

Prosen, H., Zupancic-Kralj, L., 

806 Review of technique Solid-phase microextraction (SPME) with direct detection 

a new analytical dimension 

Mitt. Lebensmittelunters. Hyg (2000) 91(6), 690-699 

Luisier, J; Villettaz, J; Azodanlou, R; Amado, R 

GC 

270 C6-C16 hydrocarbons Optimizing SPME-GC Injections 7µm, 30µm, 100µm PDMS GC-FID 

in water LC-GC 15 (12): 1130-1136 (1997) 10 min 

Okeyo, P., Snow, N. stirring 

403 PAHs Theoretical and Practical Comparison of SPME and overview GC-FID 

in water Liquid-Liquid Extraction with Large Volume Injection for 

Analysis of Aqueous Samples by GC 

Book chapter 

Snow, N. 

article 





743 Semivolatiles Use of bench top photochemical reactor and SPME 

in water to measure semivolatile organic compound-hydroxyl 

radical rate constants 

Environ. Toxicol. Chem 2000, 19(7), 1705-1710 

Bernhard, M., Simonich., S. 

271 PCBs Adsorption versus Absorption of Polychlorinated Biphenyls 100µm & 7µm PDMS GC-ECD 

in water onto SPME Coatings 5 hr 

Anal. Chem. 70 (9): 1866-1869 (1998) 

Yang, Y., Hawthorne, S., Miller, D., Liu, Y., Lee, M. 

stirring 

744 PCBs Response to comments on adsorption versus absorption 100µm PDMS GC-ECD 

in water of polychlorinated biphenyls onto SPME coatings 5 hr 

Anal. Chem. 72 (3): 642-6643 (2000) 

Yang, Y., Hawthorne, S., Miller, D., Liu, Y., Lee, M. 

stirring 

817 Aroclor 1254 Application of SPME-GC-MS to characterize intermediate 85µm polyacrylate GC-MS 

in a joint solar-microbial process for total mineralization 40min. 

of Aroclor 1254 stirring 

J.Chromatogr A 873 (2000) 53-61 2pH w/H3PO4 Rhofr, C., Hawari, J. 

745 Review article Evolution of solid phase microextracton technology 

J. Chromatogr. A 885(2000) 153-193 


various 

557 Benzene, Theory of analyte extraction by selected porous polymer PDMS/DVB, CW/DVB 

4-methylpentan-2one SPME fibers 

in water Analyst (Cambridge, UK) (1999), 124(5), 643-649 

Gorecki, T., Yu, Z., Pawliszyn, J. 

558 Organics New SPME fibers, Not only for aqueous systems PDMS/Carboxen/DVB 

in solvents LaborPraxis (1999), 23(3), 30-32, 34 

Haag, Ingo 

Nafion 

573 BTEX in New coating surfaces of fibers for SPME evaluation of various 

Methanol J-Microcolumn-Sep. May 1999; 11(5): 377-383 

Ligor,-M; Scibiorek,-M; Buszewski,-B 

coatings 

589 Coffee SPME application in GC/olfactometry dilution analysis PDMS fibers GC-FID 

sample J-Agric-Food-Chem. Apr 1999; 47(4): 1616-1618 15 min 

Deibler,-KD; Acree,-TE; Lavin,-EH headspace 

355 Terbutryn SPME with Rotation of the Microfiber 30µm PDMS GC-FID 

in water Anal. Chem 1998, 70, 3981-3982 immersion 

Geppert, H. stirring 

409 Organics Partitioning of Organic Chemicals to Polyacrylate-Coated SPME 85µm polyacrylate GC-FID, -ECD, 

in water Fibers: Kinetic Behavior and Quantitative Structure 35 min MS 

Property Relationship immersion 


Vaes, W., Harnwijk, C., Urreatarazu, R., Verhaar, H. pH 7.5 

408 Methylmercury Application of Isotope Dilution to Ion Trap GC-MS 65µm PDMS/DVB GC-MS 

iodide in Anal. Chem 71, No. 2, Jan. 15, 1999, pg. 483-488 5 min 

soil and water Barshick, C., Barshick, E., Walsch, E., Vance, M., Britt, P. immersion 

stirring 

Anatoxin-a in aqueous Analysis of anatoxin-a in aqueous samples by SPME using on fibre 

974 samples 

derivitization 

J.Chromatogr. A (2002) 963(1-2), 295-302 

Namera, A.; So, A.; Pawliiszyn, J. 

HPLC 


987 




Polychlorinated 

biphenyls Photolysis of polychlorinated biphenyls by SPME 

J.Chromatogr. A (2002) 963(1-2), 37-47 

Lores, M.; Llompart, M.; Gonzalez-Garcia, R.; Gonzalez-Barreiro, C.; Cela, 

R. 

994 Germanium 

995 

1008 

Comparison of chloride- and hydride-generation for quantitation of 

germanium by headspace SPME inductively coupled plasma-mass 

spectrometry. ICP TOF MS 

Analytical and Bioananalytical Chemistry (2002) 373(8), 849-855 

Guo, X.M.; Mester, Z.; Sturgeon, r.e. 

Sample preparation in chromatography for long dash concentration, 

purification and filtration: guide to choice of equipment. 

Laboratorio 2000 (2002) 16 (6), 34-50 

Polesello, A. 

The development of selective and biocompatible coatings for solid phase 



Mullett, Wayne M.; Pawliszyn, Janusz 

1010 Rearrangement of p -menthane terpenes by Carboxen during HS-SPME. 


Zabaras, D.; Wyllie, S. G. 


1030 Review Headspace analysis in modern gas chromatography. 

Trends in Analytical Chemistry (2002) 21 (9-10), 608-617. 

Snow, N. H.; Slack, G. C. 

1045 

Time-weighted average passive sampling with a Solid-Phase 

Microextraction device Various 


Chen, Yong; Pawliszyn, Janusz 

1061 Review article Research progress in solid-phase microextraction. 


Chen, M.; Yuan, D. X.; Xu, P. X.; Chang, D. H. 

1075 

1102 

High concentration 


Static and dynamic 

sampling 

Extending the solid-phase microextraction technique to high analyte 

concentrations: measurements and thermodynamic analysis. 


Gill, K.; Brown, W. A. 

Comparison of different methods: static and dynamic headspace and solidphase 

microextraction for the measurement of interactions between milk 

proteins and flavour compounds with an application to emulsions. 


Fabre, M.; Aubry, V.; Guichard, E. 

1117 On-site calibration method based on stepwise solid-phase microextraction 


Chen, Yong; Pawliszyn, Janusz; Xiong, Guohua 

75 um Carboxen/PDMS 

1118 

Solid-phase microextraction fibre-water distribution constants of more 

hydrophobic organic compounds and their correlations with octanol-water 

partition coefficients Various 


Paschke, A.; Popp, P. 





1134 VOCs Optimization of solid-phase microextraction of volatiles. 

Journal of Chromatography, A (2002) 960(1-2), 159-164 

Matisova, E.; Medved apostrophe ova, M.; Vraniakova, J.; Simon, P. 

1203 Anodized zinc wire as a solid-phase microextraction fiber. 


Djozan, D.; Abdollahi, L. 

GC 

1229 

Monolithic silica column for in-tube solid-phase microextraction coupled to 

high-performance liquid chromatography. HPLC 


Shintani, Y.; Zhou, X. J.; Furuno, M.; Minakuchi, H.; Nakanishi, K. 

1230 PAH's in water Thin-film microextraction. 


Bruheim, I.; Liu, X. C.; Pawliszyn, J. * 

GC-MS 

1245 Review Coupling solid-phase microextraction to liquid chromatography. A review. 


Zambonin, C. G. 

1277 

A new solid-phase microextraction adsorbent of polyphenylethylene-butyl 

acrylate and its application. GC-FID 

Fenxi Shiyanshi (2003) 22 (3, 1-4. 

Shen, S. C.; Wang, W. B.; An, H. 

1288 Copper sulfide wire as a selective fiber in solid-phase microextraction. 


Djozan, D.; Amir-Zehni, M. 

GC-FID 

1303 

1304 

CE in a nonuniform capillary modulated by a cylindrical insert, and zonenarrowing 

effects during sample injection. CE 


Stoyanov, A. V.; Liu, Z.; Pawliszyn, J. * 

Styrene-butyl acrylate copolymer as solid-phase microextraction adsorbent 

and its applications. Styrene-butyl acrylate copolymer 

Sepu (2003) 21 (3), 285-287. 

Xue, H. Y.; Shen, S. C.*; Wang, W. B.; An, H. 

1353 Aliphatic alcohols, BTEX Anodized aluminium wire as a solid-phase microextraction fibre. 


Djozan, D.; Assadi, Y.; Haddadi, S. H. 

GC 

1393 Phenols 

Solid-phase microextraction using fused-silica fibers coated with sol-gelderived 

hydroxy-crown ether. 


Zeng, Z. R.; Qiu, W. L.; Huang, Z. F. 

1433 GC tools Tools simplify GC analysis of trace components 

Research and Development (2001) 43(8), 36-39. 

Marsill, R. 

GC 

1492 

Field sampling with 


Solid-phase microextraction ( SPME ) for rapid field sampling and analysis 

by gas chromatography-mass spectrometry (GC-MS). 


Smith, Philip A.; Hall, Tara; Hook, Gary L.; Kimm, Gregory L. 


GC-MS




1498 Headspace sampling 

1515 

1051 

1073 

Use of SPME with 

complex environmental 

samples 

Organometallic 

arsenobetaine 

Headspace sampling: Critical part in evaluating true gas phase 

concentrations. 


Zehentbauer, Gerhard N.; Eddy, Cindy L.; Pelfrey, Christa S.; Rodriguez, 

Pete A. 

Theoretical considerations on the use of solid-phase microextraction with 

complex environmental samples. 

Environmental Science & Technology (2002) 36(15), 3385-3392 

Zeng, Eddy Y.; Noblet, James A. 

Electrochemical control of solid phase micro-extraction: conducting polymer 

coated film material applicable for preconcentration/analysis of neutral 

species. HPLC-ICP/MS 

Talanta (2002) 58 (4), 739-745. 

Yates, B. J.; Temsamani, K. R.; Ceylan, O.; Oztemiz, S.; Gbatu, T. P.; 

LaRue, R. A.; Tamer, U.; Mark, H. B., Jr.* 

Helical sorbent for fast sorption and desorption in solid-phase 

microextraction-gas chromatographic analysis. 


Ciucanu, I. 

PDMS GC 

1078 Systematic error in automated in-tube solid-phase microextraction 


Raghani, Anil R.; Schultz, Kristin N. 

1097 Flow-sampling system for solid-phase microextraction in situ. 

Fenxi Huaxue (2002) 30 (11), 1394-1398. 

Xu, D. Y.; Liu, M.; Liang, Y. L.; Liu, H. W.; Yin, B. Z.* 


1124 

1125 

1136 Ehtylene oxide 

1137 Amines 

1143 

Physico-chemical approach to study organotin sorption-desorption during 

solid-phase microextraction 


Aguerre, Sandrine; Lespes, Gaetane; Potin-Gautier, Martine 

High extraction efficiency solid-phase microextraction fibers coated with 

open crown ether stationary phase using sol-gel technique Various 


Yun, Lei 

A gas sample pre-concentration device based on solid phase 

microextraction (SPME) and temperature programmed desorption (TPD) Various 

Instrumentation Science and Technology (2003) 31 (2), 155-164. 

Basile, Franco 

Determination of ethylene oxide by solid-phase microextraction device with 

on-fiber derivatization. 


Tsai, S. W.; Wu, K. K. 


Modified copper wire as solid-phase microextraction fibre, selective 

extraction of some amines. GC 


Djozan, D.; Assadi, Y.; Karim-Nezhad, G. 

Modified headspace-SPME-GC device for sampling volatile compounds in 

acidic medium GC-FPD 


Araujo, W.A.; Cappelaro, E.A.; Lacerda, C.A.; Lancas, Fernando M. 


1157 




Hydroxyfullerene as a novel coating for solid-phase microextraction fibre 

with sol-gel technology. GC-ECD 


Yu, J. X.; Dong, L.; Wu, C. Y.*; Wu, L.; Xing, J. 

1212 Novel benzo-15-crown-5 sol-gel coating for solid-phase microextraction 


Peng, Jiagang; Wang, Danhua; Wu, Caiying; Xing, Jun 

GC 

1214 

1247 

1259 

1270 

1281 

1329 

1332 

1337 

New high-performance cryofocalizer injector for in-tube solid-phase 

microextraction and headspace capillary gas chromatographic applications. 


Nardi, L. 

Electrochemically assisted solid phase micro-extraction using L-dopa 

imprinted conducting polymer electrode fibers: Structural aspects. 

Abstracts of Papers American Chemical Society (2003) 225 (1-2), anyl 98. 

Schmiesing, Carla S.; Brooks, Elwood E.; Galal, Ahmed; LaRue, Rebecca 

A.; Mark, Harry B., Jr.; Temsamani, Khalid R. 

Patterns in the precision of quantitative data from multicomponent gas 

chromatographic or gas chromatographic-mass spectrometric analysis GC-MS 


Garcia, M.A.; Martinez-Castro, I.; Sanz, J.; Soria, A.C. 

Solid-phase microextraction from small volumes of sample in a glass 

capillary. 


Zhu, P. L.; Liu, C. L.; Liu, M. C. 

Hydroxycarbonyl products of the reactions of selected diols with the OH 

radical GC-FID 

Journal of Physical Chemistry A (2003) 107 (32), 6200-6205. 

Arey, Janet; Atkinson, Roger; Bethel, Heidi L. 

A comparison of alkyl derivatization methods for speciation of mercury 

based on solid phase microextraction gas chromatography with furnace 

atomization plasma emission spectrometry detection 


Grinberg, P.; Campos, R. C.; Mester, Z.; Sturgeon, R. E.* 

PDMS GC-FAPES 

Spectroscopic Studies of Sorbing Fibers Using Combined Elements with 

Multiple Attenuated Total Internal Reflection 

Optics and Spectroscopy (2000) 89 (3), 413-417. 

Bobasheva, A.S.; Enikeeva, A.G.; Malinin, I.V.; Mamedov, R.K.; Stolyarov, 

B.V.; Volchek, B.Z. 

Negligible depletion solid-phase microextraction with radiolabeled analytes 

to study free concentrations and protein binding: An example with /sup3/H 

estradiol 


Algra, Jon; Heringa, Minne B.; Hermenst, Joop L. M.; Pastor, Dolors; Vaes, 

Wouter H. J. 

1341 Solid phase micro-extraction in a miniature ion-trap mass spectrometer. 

Analyst (2003) 128 (9), 1119-1122. 

Riter, L. S.; Meurer, E. C.; Cotte-Rodriguez, I.; Eberlin, M. N.; Cooks, R. G.* 

PDMS 


1350 




1400 Hydroxy alkyl nitrates. 

1429 Aromatic hydrocarbons 

1430 

1435 VOC's 

1507 

Aliphatic carboxylic 

acids 

Solid-phase microextraction of monocyclic aromatic amines using novel 

fibres coated with crown ether. 


Zeng, Z. R.; Qiu, W. L.; Yang, M.; Wei, X. A.; Huang, Z. F.; Li, F. 

Various GC 

Measurement of octanol-air partition coefficients using solid-phase 

microextraction ( SPME ): Application to hydroxy alkyl nitrates. 

Atmospheric Environment (2001) 35(33), 5843-5854. 

Rudich, Yinon; Shragina, Lea; Treves, Keren 

Application of low-temperature glassy carbon films in solid-phase 

microextraction GC-FID 

Anal. Chem. (2001) 73(24), 5841-5851. 

Giardina, M.; Olesik, S.V. 

Atomic spectrometry update. Industrial analysis: Metals, chemicals and 

advanced materials ICP-MS 


Fairman, B.; Goodall, P.; Hinds, M.W.; Nelms, S.M.; Penny, D.M. 

Application of the polysilicone fullerene coating for solid-phase 

microextraction in the determination of semi-volatile compounds 


Han, S.; Wang, Z.; Wu, C.; Xiao, C.; Xing, J. 

PDMS GC-FID 

Solid-phase microextraction and on-line methylation gas chromatography 

for aliphatic carboxylic acids. 

Analytical and Bioanalytical Chemistry (2002) 373(1-2), 64-69 

Danielson, Neil D.; Cho, Seong R.; Liu, Yaqian 

1502 VOCs from asphalt Effect of masking agents on the emission of VOCs from asphalt. 

Abstracts of Papers American Chemical Society (2002) 223(1-2), CHED 

451 

Smith, Crystal; Hardee, John 

1227 BTEX 

1099 

Chlorohydrocarbon in 

dry cleaning fabrics. 

1257 Formic acid 

Review 

1119 Review article 

1269 Review 

Capillary extractors for left dbl quote negligible depletion right dbl quote 

sampling of benzene, toluene, ethylbenzene and xylenes by in-tube solidphase 

microextraction. 


Nardi, L. 


Method for determining chlorohydrocarbon residues in dry cleaning fabrics 

with gas chromatography-mass spectrometry. 

Sepu (2002) 20 (6), 573-576. 

Chen, J. 


Quantitation of formate by solid-phase microextraction and gas 

chromatography-mass spectrometry utilizing a " 13 C"formate internal 

standard. GC-EIMS 


Kim, J. K.; Shiraishi, T.; Fukusaki, E.; Kobayashi, A. * 

Before the injection - Modern methods of sample preparation for separation 

techniques 


Smith, Roger M. 

Derivatization - solid-phase microextraction techniques and its application to 

analysis of organic compounds. 

Fenxi Huaxue (2003) 31 (4), 496-500. 

Luan, T. G.; Zhang, Z. X. 





1371 Review 

A field guide to instrumentation: modern sample preparation methodology. 

1. Automated SPE. 

Inside Laboratory Management (2001) 5(5), 14-18. 

Sherma, J.; Larkin, J. D.; Larkin, F. H. 

2124 BTX solvents Thermal desorption SPME inlet for differential differential mobilit 

in water mobility spectrometry spectrometry 

Appl Spectrosc, 59, #6, 754-762 

De Harrington, Peter B.; Rainsberg, Matthew R. 

2125 pesticides A review on SPME-HPLC analysis of pesticides in-tube HPLC 

various Crit. Rev. Anal. Chem., 35, #1,71-85 

matrices Aulakh, J.; Kaur, V; Malik, A.; Schmitt-Kopplin, P 

2126 Volatiles & System for the generation of standard gas mixtures headspace GC 

seimivolatiles of volatile and semi-volatile organic compounds for 

in air calibrations of SPME and other sampling devices 

J Chromatogr A, 1025, #1, 3-9 

Koziel, Jacek; Martos, Perry.; Pawliszyn, J 

2127 Sulfur compd Small alpha -Mercaptoketone formation during the headspace GC-MS 

from Mailard Maillard reaction of cysteine and C13 ribose 

reaction J Agrl Food Chem, 52, #4, 958-961 

Cerny, C.; Davidek, T. * 

2128 Review SPME based on polypyrrole films with different counter ions polypyrrole 

Anal. Chim. Acta, 520, #1-2, 257-264 

Pawliszyn, Janusz; Wu, Jingcun 

2129 Review Coupling of dynamic headspace sampling and SPME headspace GC 


Silva, R. C.; Aguiar, P. M. S.; Augusto, F. * 

2130 organics from Extraction techniques comparison w/SFE, GC 

water Anal. Bioanal. Chem., 372, #1, 39-40 microwave, pressure 

Camel, Valerie solvent 

2131 Odors from Study on the method of SPME-GC-MS to quantify GC/MS 

aging material organic gas component. 

Zhipu Xuebao, 25, Suppl, 97-98 

Yang, X. L.; Qin, J. Y.; Kang, B. 

2132 Review Solid-phase microextraction field sampler field sampling 

Anal. Chem., 76, #22, 6823-6828 


2133 BTEX in Kinetics and the on-site application of standards in a preloaded fiber GC 

water solid-phase microextration fiber 

Anal. Chem., 76, #19, 5807-5815 


2134 Review Modelling SPME data from kinetic measurements in GC 

complex samples. 

Analyst (Cambridge, U. K.), 129, #11, 1137-1142 

van Eijkeren, J. C. H.; Heringa, M. B.; Hermens, J. L. M. 

2135 Review Modern extraction techniques. GC 

Analytical Chemistry, 76, #16, 4659-4664 

Raynie, D. E. 

2136 Polar analytes Derivatization and solid-phase microextraction review article GC 

TrAC Trends Anal. Chem., 23, #8, 553-561 

Martinez, Jairo R.; Stashenko, Elena E. 

2137 Review The relationship between elimination rates and GC 

partition coefficients 

Chemosphere, 57, #8, 745-753 

Jager, T.; Kooi, B.W.; Kooijman, S.A.L.M. 





2138 PAHs SPME coupled to GC-MS for determining PAH-micelle GC-MS 

partition coefficients. 

Anal Chem, 76, #15, 4572-4578 

Pino, V.; Ayala, J. H.; Gonzalez, V.; Afonso, A. 

2139 Aromatic Equilibrium in-fibre standardisation technique for SPME headspace GC-FID 

standard on J. Chromatogr. A, 1072, #1, 13-17 

fiber Chen, Y; O'Reilly, J; Pawliszyn, Janusz; Wang, Y 

2140 Review Coupling spme to liquid chromatography. A review HPLC 

Anal. Bioanal. Chem., 375, #1,73-80 

Zambonin, Carlo G. 

2141 Peptides from Approaches for coupling SPME to nanospray Restrictive access MS-nanospray 

tryptic digests J. Chromatogr. A, 1067, #1-2, 197-205 coated fibers 

Dartiguenave, C; Gu, Yu; Lubda, D; Musteata, F; 

Pawliszyn, Janusz; Waldron, Karen; Walles, Markus 

2142 Terpene & Experimental determination and calculation of PDMS fibers GC 

ketones in distribution coefficients between air and fiber with PDMS 

air coating for some groups of organic compounds 

J. Chromatogr. A, 1077, #2, 195-201 

Isidorov, Valery A.; Vinogorova, Vera T. 

2143 Review of A survey on high-concentration-capability headspace headspace GC-MS 

extraction sampling techniques in the analysis of flavors 

techniques and fragrances. 

J Chrom Sci, 42, #8, 402-409 

Bicchi, C.; Cordero, C.; Rubiolo, P. 


SPME Literature 

Literature 

No. Title 

Biochemical / Food and Beverage 

T195869 Solid Phase Microextraction: Solventless Sample Preparation for Monitoring Flavor Compounds 

by Capillary Gas Chromatography (AYM) 

T196901 Solid Phase Microextraction/Capillary GC Analysis of Drugs, Alcohols, and Organic Solvents in Biological Fluids (AYY) 

T396110 SPME Reduces Extraction Time in HPLC Analyses of Food Antioxidants and Preservatives 

T397140 Analysis of Fat Soluble Vitamins from Tablets, Using SPME/HPLC (BKK) 

T398147 

Pharmaceutical 

Solid Phase Microextraction of Odors in Drinking Water, for Analysis by GC-MS (BRG) 

T394062 

Forensic 

Monitor Organic Volatile Impurities (OVIs) in Pharmaceutical Products, Using Solid Phase Microextraction/Capillary GC (AQX) 

T196901 Solid Phase Microextraction/Capillary GC Analysis of Drugs, Alcohols, and Organic Solvents in Biological Fluids (AYY) 

T198922 SPME/GC for Forensic Applications: Explosives, Fire Debris, and Drugs of Abuse (BQS) 

T394061 Solid Phase Microextraction/Capillary GC: Rapid, Sensitive Detection of Gasoline in Fire Debris (AQW) 

T396098 

Environmental 

SPME / HPLC Interface Combines Fast Sample Extraction with Efficient Analysis for Explosives (ASE) 

T394006 Solid Phase Microextraction of Semivolatile Compounds in US EPA Method 625 (AOH) 

T394011 Solid Phase Microextraction of Volatile Compounds in US EPA Method 524.4 (AOM) 

T394017 Polyacrylate Film Fiber for Solid Phase Microextraction of Polar Semivolatiles from Water (AOS) 

T394056 Fast Analysis of Volatile Organic Compounds by Solid Phase Microextraction/Capillary GC (AQL) 

T394058 Fast Screening for Chlorinated Pesticides by Solid Phase Microextraction/Capillary GC (AQN) 

T395081 Monitor BTEX Compounds and Fuels in Water, Using Solid Phase Microextraction and Capillary GC (ARO) 

T395085 Solid Phase Microextraction/Capillary GC Analysis of Nitrogen-Containing Herbicides in Water (ARS) 

T396094 Solid Phase Microextraction of Organophosphate Insecticides and Analysis by Capillary GC/MS (ASB) 

T396099 SPME / HPLC: A Rapid and Sensitive Analysis of Polynuclear Aromatic Hydrocarbons in Water (ASF) 

T396106 Analysis of Surfactants in Water by SPME/HPLC 

T397121 Solid Phase Microextraction for HPLC Analysis of Carbamate and Urea Pesticides (BGU) 

T397141 Air Sampling of VOCs Using SPME for Analysis by Capillary GC (BKF) 

T397143 Field Sampling for Pesticides, Using Solid Phase Microextraction/Capillary GC (BJT) 

T398147 Solid Phase Microextraction of Odors in Drinking Water, for Analysis by GC/MS (BRG) 

Lab Hints and Selection Guides 

T101928 SPME Troubleshooting Guide (EDV) 

T101929 Guide to Quantitation with SPME (EDW) 

T198923 Solid Phase Microextraction: Theory and Optimization of Conditions (BQT) 

T396098 SPME / HPLC Interface Combines Fast Sample Extraction with Efficient Analysis for Explosives (ASE) 

T496037 Solid Phase Microextraction Sampling Stand (AWS) 

T496049 SPME / HPLC Interface (AWV) 

T497105 SPME Portable Field Sampler with Carboxen/PDMS Fiber (BIZ) 

T497174 SPME Portable Field Sampler with 100 µm PDMS Fiber (BKL) 

Free Supelco Literature 

To obtain any of the free literature listed above, to see a complete list of Supelco literature, or to see any new Supelco products, use one 

of the following methods. Some literature is available electronically only. 

● Download from Our World Wide Web Site 


● Contact Our Order Processing Department 

Phone 800-247-6628 (US only) or 814-359-3441 

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181

Ordering Information: 

Sampling and Analysis Mode 

Fiber Core/ Hub Manual Holder Autosampler 

Assembly Type Description (w/ spring) (w/o spring) 

23 Ga* 24 Ga* 23 Ga* 24 Ga* 

Carboxen/Polydimethylsiloxane 

75 µm Carboxen/PDMS Fused Silica/SS Black/plain 57344-U 57318 57343-U 57319 

85 µm Carboxen/PDMS Metal alloy/Metal alloy** Lt. Blue/plain 57906-U 

85 µm Carboxen/PDMS Stableflex/SS Lt. Blue/plain 57334-U 57295-U 57335-U 

Polydimethylsiloxane (PDMS) 

7 µm PDMS Metal alloy/Metal alloy** Green/plain 57919-U 

7 µm PDMS Fused Silica/SS Green/plain 57302 57291-U 57303 

30 µm PDMS Metal alloy/Metal alloy** Yellow/plain 57922-U 

30 µm PDMS Fused Silica/SS Yellow/plain 57308 57289-U 57309 

100 µm PDMS Metal alloy/Metal alloy** Red/plain 57298-U 

100 µm PDMS Fused Silica/SS Red/plain 57342-U 57300-U 57341-U 57301 

Polydimethylsiloxane/Divinylbenzene (PDMS/DVB) 

60 µm PDMS/DVB Stableflex/SS Brown/notched 57317 

65 µm PDMS/DVB Metal alloy/Metal alloy** Blue/plain 57902-U 

65 µm PDMS/DVB Fused Silica/SS Blue/plain 57346-U 57310-U 57345-U 57311 

65 µm PDMS/DVB Stableflex/SS Pink/plain 57326-U 57293-U 57327-U 

Polyacrylate 

85 µm Polyacrylate Fused Silica/SS White/plain 57304 57294-U 57305 

Divinylbenzene/Carboxen/Polydimethylsiloxane 

50/30 µm DVB/CAR/PDMS Metal alloy/Metal alloy (1 cm)** Gray/plain 57912-U 

50/30 µm DVB/CAR/PDMS Metal alloy/Metal alloy (2 cm)** Gray/notched 57914-U 

50/30 µm DVB/CAR/PDMS Stableflex/SS (1 cm) Gray/plain 57328-U 57298-U 57329-U 

50/30 µm DVB/CAR/PDMS Stableflex/SS (2 cm) Gray/notched 57348-U 57299-U 

Polyethylene Glycol (PEG) 

60 µm PEG 

* Ga - Needle gauge. 

Metal alloy/SS Purple/plain 57355-U 57354-U 

** Metal alloy fiber assemblies are provided 1/pk. 

Fiber Assortment Kits 

Automated/HPLC 

Name Description of Fiber Coatings (1 ea.) Recommended Use Manual Std. 23 Ga. 

Needle Needle 

Kit # 1 85 µm polyacrylate, 100 µm PDMS, 7 µm PDMS GC 57306 57307 57285-U 

Kit # 2 75 µm Carboxen/PDMS, 65 µm PDMS/DVB, 85 µm polyacrylate GC 57320-U 57321-U 57286-U 

Kit # 3 60 µm PDMS/DVB, 85 µm polyacrylate, 100 µm PDMS HPLC – 57323-U – 

Kit # 4 100 µm PDMS, 65 µm PDMS/DVB, 75 µm Carboxen/PDMS GC 57324-U 57325-U 57287-U 

StableFlex Kit 65 µm PDMS/DVB, 50/30 µm DVB/Carboxen/PDMS GC 57550-U 57551-U – 

Kit # 5 100 µm PDMS, 65 µm PDMS/DVB, 85 µm Carboxen/PDMS GC 57324-U 57325-U 57287-U 

50/30 µm DVB/Carboxen/PDMS GC 57362-U 

SPME Fiber Holders 

The holder protects the coated fiber, and controls exposure of the 

fiber during analyte adsorption and desorption. The holder is 

reusable indefinitely and accepts the replaceable fiber assembly. 

First time users must order both a holder and a fiber assembly. 

Fiber Holder for Manual Sampling 

An adjustable depth guide positions the fiber for sampling and for 

correct placement in the heated zone of the GC injection port. The 

fiber can be locked in the exposed position. 

Fiber Holder for Automated Sampling or HPLC Analysis 

Use this fiber holder with a Varian 8100/8200 AutoSampler or with 

our SPME/HPLC interface. An SPME upgrade kit is necessary for 

operation with the Varian AutoSampler – contact Varian Instrument 

Division for information concerning system requirements. 

182 

Automated or HPLC Holder 

Manual Holder 

995-0125 

Fiber Holder for CTC, Gerstel, and Thermo Autosamplers ▲▲▲▲▲ 

Use this holder with SPME fiber assemblies that are designed for 

automated sampling. 

Description Cat. No. 

Fiber Holder 

For Manual Sampling 57330-U 

For Varian Autosampler or HPLC Analysis 57331 

For CTC, Gerstel, and Thermo Autosamplers 57347-U 

▲ Autosamplers distributed by Varian, Leap, Gerstel, and Thermo.

SPME Applications Guide - Labicom

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