SPME Applications Guide - Overbrook Scientific

SPME Applications Guide 

The SPME Applications Guide is a bibliographic resource of published technical articles about solid phase microextraction. With the 

continued growth of SPME, and its expansion into environmental, food, forensic, and other fields, we recognize the need for an organized 

bibliography. This guide should serve a useful purpose in your SPME research and analyses. 

This guide is for general information only. We have made every attempt to make the information as complete and accurate as possible. 

Where entries are missing, information was not available at the time of printing. 

NOTE: Because of copyright restrictions, Supelco cannot provide copies of the articles listed. If you desire copies, please refer to the 

publications cited. 

Using This Guide 

This guide is organized in an easy-to-use format. The references are 

grouped into application areas (see the Table of Contents) with the 

over 600 new references placed at the end of each area in bold. The 

Analyte/Matrix column identifies the class of analytes and the 

sample matrix. The Literature Reference column provides the title of 

the article, journal reference, and authors. The next column describes 

the SPME fiber and conditions used in the sample extraction. 

The last column indicates the instrument used in the analysis. 

Key to Abbreviations 

Abbrev. Description 

AED atomic emission detection 

DVB divinylbenzene 

ECD electron capture detection 

FID flame ionization detection 

FPD flame photometric detection 

FTD flame thermonic detection 

GC gas chromatography 

HPLC high pressure liquid chromatography 

ICP inductive coupled plasma 

MS mass spectrometry 

MSD mass selective detection 

NPD nitrogen/phosphorus detection 

PAD photodiode-array detection 

PDMS polydimethylsiloxane 

PICI positive ion chemical ionization 

SIM selective ion monitoring 

TCD thermionic-selective detection 

TED thermal energy detection 

VIS visible spectrophotometry 

sigma-aldrich.com 

Table of Contents 


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Tel: (800) 247-6628 (814) 359-3441 Fax: (800) 447-3044 (814) 359-3044 

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Application Area 

Books .................................................................... 2 

Foods .................................................................... 2 

Polymers and Coatings .......................................... 68 

Natural Products .................................................... 72 

Pharmaceuticals .................................................... 91 

Biological Matrices ................................................. 94 

Toxicology ........................................................... 109 

Forensics ............................................................. 128 

Environmental ..................................................... 135 

Water .......................................................... 140 

Pesticides ..................................................... 184 

Soil .............................................................. 195 

Air ............................................................... 204 

Theory and Technique ......................................... 211 

Supelco SPME Literature ...................................... 231 

SPME Products .................................................... 232

Books 

Foods 

SPME Application Guide 7th Edition 

(New references added to the 7th edition are in bold) SPME Fiber / 

Analyte / Extraction 

Matrix Literature Reference Conditions Instrument 

Techniques for Analyzing Food Aroma, Supelco Cat. # 26589-U 

Marcel Decker ISBN: 0-8247-9788-4, Marsili, R. 

Solid Phase Microextraction: A Practical Guide Supelco Cat. # 26610-U 

Edited by SueAnn Scheppers Wercinski 

Marcel Decker 15BN: 0-8247-7058-7 

Solid Phase Microextraction: Theory and Practice Supelco Cat. # 26591-U 

Edited by Janusz Pawliszyn 

VCH, New York, 275pp (1997) 

Applications of Solid Phase Microextraction Supelco Cat. # 26611-U 

Edited by Janusz Pawliszyn 

RSC Chromatography Monographs ISBN 0-85404-525-2 

Royal Society of Chemistry 1999 

Applied SPME, 1999, 364-371 Royal Society of 

Chemistry, Cambridge, UK Coden: 67TUA8 

Talon, R, Montel, M. 

601 Aroma compounds Developments in extraction techniques and their Review article GC 

in food application to analysis of volatiles in foods 

Trends-Anal-Chem, May 2000, 19(5), 322-329 

Sides, S., Robards, K., Helliwell, S. 

602 Contaminants Application of SPME in Food Analysis Review article GC, LC, MS 

in Food J. Chromatogr. A (2000), 880(1+2), 35-62 

Kataok, H., Lord, H., Pawliszyn, J. 

2593 PAHs in Use of headspace SPME coupled to LC for the analysis of PAHs 60µM PDMS/DVB LC-fluorimetric 

tea infusion in tea infusions 60 min @ 90 °C 

J Chromatogr A 1164, #1-2, 10-17 (2007) headspace 

Vinas, P.; Campillo, N.; Aguinaga, N.; Perez-Canovas, E.; 

Hernandez-Cordoba, M. 

784 Catechins, cafeine Automated in-tube solid phase microextraction coupled polypyrrole capillary LC-ES-MS 

in tes with HPLC-ES-MS for the determination of catechins 

and caffeine in tea 

Analyst (Cambridge, U. K.) (2000) 125(12), 2216-2222 

Wu, J. C.; Xie, W.; Pawliszyn, J. 

2557 Sorbic, benzoic Simultaneous determination of sorbic and benzoic acids in food 85µm polyacrylate GC-FID 

acids in food dressing by headspace SPME and gas chromatography headspace 

dressing J. Chromatogr., A 1117, #1, 109-114 (2006-06-02) 

Dong, C. Z.; Mei, Y.; Chen, L. 

2199 Sorbic, benzoic Headspace SPME applied to the simultaneous determination of 65µm PDMS-DVB GC-FID 

acids in sorbic and benzoic acids in beverages headspace 

beverages Anal. Chim. Acta (2006) 562. #1, 23-29 

Dong, Chunzhou; Wang, Wenfang 

834 Caffeine Caffeine determination in beverages by SPME and GC-MS 

in beverages Ind. Bevande (2000) 29(170) 595-597, 605 

Guidotti, Maurizio; Panzironi, Laura 

8 Caffeine and flavors Solventless Determination of Caffeine in uncoated fiber GC-MS 

in coffee/tea/cola Beverages Using SPME with Fused Silica Fibers 

J. Chromatogr. 603: 185-191 (1992) 

Hawthorne, S., Miller, D., Arthur, C., Pawliszyn, J. 

5 min 

2461 Phthalic acid esters Headspace SPME of phthalic acid esters from vegetable oil 100µm PDMS GC/ECD 

Ambient temperature, unless otherwise indicated. 2




in vegetable oil employing solvent based matrix modification 

Anal. Chim. Acta 582, #1,24-33 (1-16-2007) 

Holadova, K.; Prokupkova, G.; Hajslova, J.; Poustka, Jan 

headspace 

2751 Volatiles from free Headspace-(HS-SPME) analysis of oxidized volatiles from free headspace GC 

Fatty acids fatty acids (FFA) and application for measuring hydrogen 

donating antioxidant activity 

FOOD CHEM. 105, #1, 414-420 (2007) 

JaeMin Lee; Dong-Hwan Kim; Pahn-Shick Chang; JaeHwan Lee 

2875 Alcohol Reaction design for evaluation of the substrate range of hydrolases headspace GC-MS 

hydrolases Biocatalysis and Biotransformation 26, #3, 228-234 (2008) 

Antoniotti, Sylvain; Fernandez, Xavier; Dunach, Elisabet 

2471 Fatty acids Physicochemical and volatiles characterization of trans-free solid headspace GC 

in solid fats fats produced by lipase-catalyzed interesterification. 

J Food Sci 72, #6, E368-74 (2007 Aug) 

Lee, J H; Akoh, C C; Lee, K-T 

2209 Volatiles in Identification of volatile degradants in formulations containing sesame headspace GC-MS 

Sesame oil oil using SPME/GC/MS 

J. PHARM. BIOMED. ANAL. 44, #2, 450-455 (28 JUN 2007) 

Chen, W.; Zhou, P.; Wong-Moon, K. C.; Cauchon, N. S. 

2671 Off-flavours SPME-GC and sensors as rapid methods for monitoring headspace GC-FID 

in nuts lipid oxidation in nuts. 

Food Additives and Contaminants 24, #11, 1219-1225 (2007) 

Pastorelli, S; Torri, L; Rodriguez, A; Valzacchi, S; Limbo, S; Simoneau, C. 

2726 Flavors in Endogenous biophenol, fatty acid and volatile profiles of selected oils headspace GC 

camellia oil FOOD CHEM. 100, #4, 1544-1551 (2007) 

Haiyan, Z.; Bedgood, Jr D. R.; Bishop, A. G.; Prenzler, P. D.; Robards, K. 

2275 Flavors in Sensory evaluation of butterfat-vegetable oil blend spread prepared headspace 

canola oil and with structured lipid containing canola oil and caprylic acid 

caprylic acid J Food Science 70 #7, S406-S412 (2005) 

Kim, B.; Shewfelt, Robert L.; Lee, Hyoungil; Akoh, Casimir C. 

2158 Volatile oxidative Evaluation of oxidative stability of canola oils by headspace analysis headspace GC 

products of JAOC, 82, #12, 869-874 (2005) 

canola oil Richards, Amy; Wijesundera, Chakra; Salisbury, Phil 

2157 Volatile flavors Sensory and oxidative quality of screw-pressed flaxseed oil headspace GC 

in flaxseed oil JAOC, 82, #12, 887-892 (2005) 

Wiesenborn, D.; Kangas, N.; Tostenson, K.; Hall, C.; Chang, K. 

2305 Volatiles in Analysis of volatile compounds and triglycerides of seed oils DVB/Car 50/30µm GC/MS 

Poppy seed oil extracted from different poppy varieties (Papaver somniferum L.) headspace 

J Ag Food Chem 53, #21, 8310-8316 (2005) 

Krist, S.; Stuebiger, G.; Unterweger, H.; Bandion, F.; Buchbauer, G. 

2693 Hexanal & pentane A headspace SPME method of use in monitoring hexanal and pentane headspace GC/MS 

in liquid during storage: Applications to liquid infant foods and powdered 

infant foods infant formulas. 

Food Chem. 101, #3, 1078-1086 (2007) 

Garcia-Llatas, G.; Lagarda, M. J.; Romero, F.; Abellan, P.; Farre, R. 

32 Flavors in Solid Phase Microextraction for Flavor Analysis 100µm PDMS GC/GC-MS 

coffee/fruit juice/ J. Agric. Food Chem, 42: 1925-1930 (1994) 10 min 

vegetable oil Peppard, T., Yang, X. 

603 Volatiles Analysis of volatile contaminants in vegetable oils by 75µm Carboxen/PDMS GC-MS 

in vegetable oil headspace SPME with Carboxen-based fibers. 30-45 min @ 100°C 

J. Chromatogr. 873 (2000): 79-94 

Page, B., Lacroix, G. 

headspace 





39 Halogenated volatiles Application of SPME to the Headspace GC Analysis of GC 

in food Halogenated Volatiles in Selected Foods 

J. Chromatogr. 648 (1): 199-211 (1993) 


41 Fatty acids C2-C10 Determination of Fatty Acids Using SPME 85µm polyacrylate GC/GC-MS 

in water Anal. Chem: 67(23): 4396-4403 (1995) Low pH, salt 

Pan, L., Adams, M., Pawliszyn, J. derivative: 1-pyrenediazomethane 

2646 Volatiles from Chemical composition and volatile constituents of Anthyllis barba-jovis headspace GC-MS 

flavonol NAT. PROD. RES. 21, #5, 418-425 (01 MAY 2007) 

glycosides Pistelli, L.; Noccioli, C.; Bertoli, A.; Scapecchi, G.; Potenza, D. 

2176 Volatile organics Headspace solid-phase microextraction analysis of artificial flavors headspace GC-MS 

from artificial J Sci of Food and Agri., (2005) 85, #25, 2645-2654 30 min 

flavors Coleman, William M.; Dube, Michael F. 

42 Flavors in Measuring Flavors Using SPME 100µm PDMS GC-MS 

corn oil Food Quality January/February 1995, pp40-41 

Mindrup, R. 

40°C, 45 min 

925 Flavors, off-flavors Sample preparation for the analysis of flavors and Review article 

in food off-flavors in foods 

J. Chromatogr A, 2000, 873(1), 3-11 

Wilkes, J., Conte, E., Kim, Y., Holcomb, M., Sutherland, J. 

Miller, D. 

883 Flavors in Recent application of SPME for monitoring flavor 75µm Carboxen/PDMS GC-MS 

food components in foods 

Food Testing & Analysis Feb./March 2000, 17-20 

Mindrup, R. 

65µm DVB/PDMS 

181 Flavors in SPME Associated with Microwave Assisted 100µm PDMS SIM GC-MS 

coffee, potato Extraction of Food Products pH 2, salt 

chip J. High Res. Chromatogr. 20 (4): 213-216 (1997) headspace 

Wang, Y., Bonella, M., Khaled, M., McNair, H. 10 min 

60 Sulfur volatiles in Headspace SPME Analysis of Volatile Organic Sulfur 

truffle aroma Compounds in Black and White Truffle Aroma 

J. Agric. Food Chem, 43 (8): 2138-2143 (1995) 

Pelusio, F., Nilsson, T., Tino, R., Larsen, B., Montnarell, L. 

830 Sulfur compounds Changes of aroma in shell eggs 

from egg shell Czech J. Food Sci (2000) 18, 231-233 

Adamiec, J.; Dolezal, M.; Mikova, K.; Davidek, J 

831 Sulfur compounds Limitations to the use of SPME for quantitation 

of mixtures of volatile organic sulfur compounds 

Anal. Chem (2001) 73(7) 1646-1649 

Murray, R. A. 

2245 Aroma Aroma active compounds of Bulgogi GCO 

compounds Journal of Food Science (2005) 70 #8, C517-C522 

of Bulgogi Ko, H.; Kim, T.; Cho, I.; Yang, J; Kim, Y.; Lee, H. 

604 Aroma compounds Determination of major aroma impact compounds in 75µm Carboxen/PDMS GC-MS 

in fermented fermented cucumbers by SPME-GC-MS- 20min @50°C 

cucumbers Olfactometry detection 

J. Chromatogr. Sci. (2000), 38(7), 307-314 

Marsili, R., Miller, N. 

NaCl added 

61 Flavors in SPME of Flavor Compounds -- A Comparison of Two Fiber 100µm PDMS, GC-FID 

cinnamon bark Coatings and Discussion of the Rules of Thumb for Adsorption 85µm polyacrylate 

LC-GC 13 (11): 882-886 (1995) 120°C 

Yang, X., Peppard, T. headspace 





62 Flavors in SPME and Chiral Gas Chromatography Separations 100µm PDMS GC-FID 

apple essence, LC-GC 13 (9): 734-740 (1995) 30°C or 40°C 

seeds, candy Mani, V., Woolley, C. headspace 

2544 Aroma compounds HS-SPME analysis of the volatile compounds from spices as a source 65µm PDMS/DVB GC-MS 

from spices of flavour in 'Campo Real' table olive preparations 

Flavour and Fragrance J. 22, #4, 265-273 (JUL-AUG 2007) 

Perez, R. A.; Navarro, T.; de Lorenzo, C. 

headspace 

2578 Volatiles in Analysis of volatile components during potherb mustard (Brassica headspace GC-MS 

potherb mustard juncea, Coss.) pickle fermentation using SPME-GC-MS 

LWT - Food Science and Technology 40, #3, 439-447 (2007) 

Zhao, Dayun; Tang, Jian; Ding, Xiaolin 

772 Volatiles in Analysis of volatile constituents of mustard paste by GC/MS 100µm PDMS GC-MS 

mustard paste w/SPME and simultaneous distillation and extraction 

Fenxi Huaxue (2000) 28(12) 1489-1492 

30min @ 70°C 

Liu, B. in Chinese 

2437 Volatiles in Comparison of headspace-SPME-GC-MS and LC-MS for the detection headspace GC-MS 

vanilla extracts and quantification of coumarin, vanillin, and ethyl vanillin in 

vanilla extract products 

Food Chem 107, #4, 1701-1709 (15 APR 2008) 

De, Jager L. S.; Perfetti, G. A.; Diachenko, G. W. 

854 Volatiles in Analysis of the volatile components in vanilla extracts and 85µm polyacrylate GC-MS 

vanilla extracts flavourings by SPME and gas chromatography 

J Ag Food Chem (2000) 48(12), 5802-5807 

Sostaric, T.; Boyce, M. C.; Spickett, E. E. 

40min @ 20°C 

829 Volatiles of Analysis of headspace compounds of distillers grains using 75µm Carboxen/PDMS GC-MS 

distillers grains SPME in conjunction with GC/MS and TGA. 60min 

J Cereal Sci. (2001) 33(2), 223-229 

Staff, C., Biswas, S. 

headspace 

2211 Essential oil of Comparison of essential oil of Xanthogalum purpurascens GC-MS 

Xanthogalum Lallem. Obtained via different isolation techniques 

purpurascens J. Essent. Oil Res. 18 #2, 181-184 (2006) 

Lallem Baser, K.H.C.; Duran, A.; Ozek, G.; Ozek, T.; Sagiroglu, M. 

878 Essential oils in SPME of hop volatiles Potential use for determination and 100µm PDMS GC-MS 

hops verification of hop varieties 30min @ 70°C 

J. Chromatogr A 918 (2001) 159-167 

Kovacevic, M., Kac, M. 

headspace 

63 Essential oils in Determination of Essential Oils in Hops by Headspace SPME 100µm PDMS GC-FID 

hops J. Agric. Food. Chem, 44: 1768-1772 (1996) 

Field, J., Nickerson, G., James, D. Heider, C. 

50°C, 4 hr 

2860 Volatiles from 

Comparison of liquid-liquid extraction with headspace methods for the 

characterization of volatile fractions of commercial hydrolats from 

typically Mediterranean species GC-MS 

Essential oils J. Chromatogr A 1193, 1-2, 37-49 (Jun 6 2008) 

Barboni, T.; Costa, J.; Desjobert, J.; Leandri, C.; Paolini, J. 

605 Essential oils Production of Yarrow (Achillea millefolium L.) in Norway: 100µm PDMS GC-MS 

in yarrow Essential Oil Content and Quality 40min @ 50°C 

J. Agric. Food Chem, (2000) 48 No,12, 6205-6209 

Rohloff, J., Skagen, E., Steen, A., Iversen, T. 

headspace 

2917 Volatiles from Inheritance of aroma compounds in a model population of Fragaria headspace GC-MS 

plants Plant Breeding 127, #1, 87-93 (FEB 2008) 

Olbricht, K.; Grafe, C.; Weiss, K.; Ulrich, D. 





2679 Essential oils in Comparison of different extraction methods for the determination of headspace GC-MS 

aromatic plants essential oils and related compounds from aromatic plants and 

optimization of solid-phase microextraction/gas chromatography. 

Anal Bioanalyt Chem 387, #6, 2207-2217 (2007 ) 

Richter, J.; Schellenberg, I. 

221 Essential oils in A Comparison of Selected Analytical Approaches to the 100µm PDMS GC-MS 

Virginia cedar oil Analysis of an Essential Oil 10-120 sec 

Flavour and Fragrance Journal 12 (1): 1-8, (1997) 

Coleman, W., Lawrence, B. 

headspace 

396 Essential oils in Automatic Injection SPME-Chiral-GC-MSD Analysis of 7µm PDMS GC-MS 

Virginia cedar oil Essential Oils 6 sec 

J.Chromatographic Sci., Vol. 36, Dec. 1998, 575-578 headspace 

Coleman, W., Perfetti, T., Lawrence, B. stirring 

444 Volatiles in Identification of Volatile Compounds in Sunflower Oil 100µm PDMS GC-MS 

sunflower oil by Headspace SPME and Ion-Trap GC/MS 

J. High Resolut. Chromatgr. (1998), 46(7), 2744-2747 

Keszler, A., Heberger, K., Gude M. 

841 Volatiles in Mechanism of volatile compound production during storage 100µm PDMS GC-MS 

sunflower oil of sunflower oil 40 min @ 25°C 

J Ag Food Chem. (2000) 48(12), 5981-5985 

Keszler, A., Kiska, T. Nemeth, A.. 

headspace 

2832 pentachlorophenol A preliminary feasibility study for pentachlorophenol column GC-MS 

in water sorption by almond shell residue 

Chem. Eng. J. 136, #2-3, 188-194 (Mar 1 2008) 

Alves, A.; Estevinho, B.N.; Ribeiro, E.; Santos, L. 

2658 Aldehydes in Determination of some aldehydes by using SPME-HPLC w/ UV detection. 65µm PDMS/DVB LC-UV 

bitter almonds & J AOAC Int 90, #6, 1689-94 (2007 Nov-Dec) 

cinnamon bark Kumar, Ashwini; Singh, Baldev; Malik, Ashok Kumar; Tiwary, Dhananjay K 

2184 Volatiles from Analysis of volatile aldehydes in oat flakes by SPME-GC/MS headspace GC-MS 

oat flakes Polish J Food and Nutrition Sci. (2005) 14, #4, 389-395 DVB/Carboxen 

Klensporf, Dorota; Jelen, Henryk H. 

569 12 Aldehydes Influence of extraction parameters and medium on 100µm PDMS GC-MS 

in sunflower oil/water efficiency of SPME sampling in analysis of aliphatic aldehydes 30 min @ 40°C 

J-Chromatogram-A. 11 Jun 1999; 845(1-2): 337-347 

Keszler,-A; Heberger,-K 

headspace 

447 Xylene Determination of trace xylene in contaminated palm 100µm PDMS GC-FID 

in palm oil oil by SPME and capillary GC 1 min. 60°C 

Fenxi Huaxue (1999), 27(6), 676-678 headspace 

Chen, W., Guo, C., Hu, C. 

2757 Aroma volatiles A 3-year study on quality, nutritional and organoleptic evaluation GC/MS 

in olive oil of organic and conventional extra-virgin olive oils 

JAOCS 85, #2, 151-158 (2008) 

Ninfali, P.; Bacchiocca, M.; Biagiotti, E.; Esposto, S.; Servili, M.; 

Montedoro, G.; Rosati, A. 

2672 Aroma volatiles Aromagrams - Aromatic profiles in the appreciation of food quality review article 

in food FOOD CHEM. 101, #2, 845-872 

Plutowska, B.; Wardencki, W. 

2147 Aroma volatiles Analysis of single-cultivar extra virgin olive oils by means of an headspace GC/MS 

in olive oil Electronic Nose and HS-SPME/GC/MS methods 

Sens Actuators, B Chem, (2006) 114, #2, 674-680 

Cimato, A.; Dello Monaco, D.; Distante, C.; Epifani, M.; Sani, G.; 

Siciliano, P.; Taurino, A.M.;Zuppa, M. 

803 Volatiles Volatile compounds of virgin olive oil evaluated by SPME 





in olive oil An application in the discrimination of virgin olive oils 

according to the cultivar and area 

Proceedings of the Phytochemical Society of Europe 

(2000) Vol. 46, 211-220 

Servili, M; Montedoro, G; Selvaggini, R; Taticchi, A 

577 Dimetyl disulfide & Volatile reduced sulfur compounds in butter by SPME 85µm polyacrylate GC-EID 

methanethiol J-Dairy-Res. Feb 1999; 66(1): 115-123 10 min. @ 30-35°C 

in butter Shooter,-D; Jayatissa,-N; Renner,-N 

338 Benzene, toluene Determination of benzene & toluene in vegetable HPLC 

in vegetable oil oil by SPME/HPLC headspace 

J. Commod. Sci. (1999), 38(1), 3-14 

Giuffrida, R., Clasadonte, M., Zerbo, A. 

606 Volatiles Headspace SPME use for the Characterization of volatile Carboxen/DVB/PDMS GC-FID 

in vegetable oil compounds in vegetable oils of different sensory quality 20-60°C 

J. Agric Food Chem, (2000), 48(6), 2360-2367 headspace 

Jelen, H., Obuchowska, M., Zawirska-Wojtasiak, R. 

885 Steroisomers Different stereoselectivity in the reduction of pulegone GC-MS 

Pulegone enantiomers by Mentha species 

Planta Medica (2001) 67(3) 260-262 

Mosandl, A.; Beck, T.; Fuchs, S. 

2724 Aldehydes in Determination of stale aldehydes in beer by headspace SPME and 65µm PDMS/DVB GC-MS 

beer automatic precolumn derivatization. headspace 

Fenxi Shiyanshi 26, #4, 38-41(2007) 60min @ 60°C 

Wu, Q. -J.; Chen, H. -L.; Yang, Z. -X. PFBOA derivative in Chinese 

2393 NDMA in Solid-phase microextraction of N-nitrosodimethylamine in beer 65µm PDMS/DVB GC-MS 

beer Food Chemistry 107, #3, 1348-1352 (2008) headspace 

Perez, D. M.; Alatorre, G. G.; Alvarez, E. B.; Silva, E. E.; Alvarado, J. F. J 

2219 Aroma High gravity fermentations for low calories beer production GC 

from Beers Journal of Biotechnology (2005) 118 Suppl. 1, S152 

Piddocke, Maya; Sorensen, Thomas; Pedersen, Sven; Olsson, Lisbeth 

2558 Flavors in Method optimization by SPME in combination with GC-MS for 75µm Carboxen GC-MS 

beer analysis of beer volatile fraction headspace 

J. Chromatogr., A 1121, #2, 145-153 (2006-07-21) 

Pinho, O.; Ferreira, M.; Santos, L. 

106 Flavors in Characterization of Beer Samples Using SPME-GC Analysis 100µm PDMS GC-FID 

beer Supelco Reporter Vol. 16, #4, pg. 7 

Vas, G. 

10 min 

2716 Sulfur compounds Comparison of headspace and direct single-drop microextraction headspace GC-FPD 

in beer and headspace SPME for the measurement of volatile sulfur 

compounds in beer and beverage by GC-FPD 

J. Chromatogr. A. 1125, #1, 133-137 (2006-08-25) 

Xiao, Q.; Yu, C. H.; Xing, J.; Hu, B. 

607 Sulfur compounds Determination of sulfur compounds in beer using headspace 65µm Carboxen/PDMS GC-FPD 

in beer SPME and GC analysis with pulsed FPD detector 32min @45°C 

J. Chromatogr. A. (2000), 872(1+2), 203-213 

Hill, P., Smith, R. 

headspace 

100 Flavors Characterization of Commercial Vodkas by SPME-GC/MS 100µm PDMS GC-MS 

in vodka J. Sci. Food Agric. 70: 380-388 (1996) 

Ng, L., Hupe, M., Harnois, J., Moccia, D. 

1 hr 

202 Methylcyclopendienyl Determination of Methylcyclopendienyl Manganese Tricarbonyl 

manganese in Beverages by SPME 

tricarbonyl Food Addit. Contam. 14 (3): 301-307 (1997) 

in beverages Forsyth, D., Dusseault, L. 

2538 Attractants of Onion aphid (Neotoxoptera formosana) attractants, in the headspace of headspace GC-MS 

onion aphids Allium fistulosum and A-tuberosum leaves 

J Applied Entomology 131, #1, 8-12 (FEB 2007) 





Hori, M. 

395 Aroma volatiles Determination of Fresh Onion (Allium Cepa L) Volatiles 100µm PDMS GC-MS 

in onion by SPME Combined with GC/MS 1 min 

Z Lebedsm Unters Forsch A (1998) 207: 39-43 

Jarvedpaa, E., Zhung, Z., Huopalahti, R., King, J. 

headspace 

Possible advantage of various sample transfer techniques 

799 Aroma volatiles for fast GC-MS analysis of true onion volatiles 100µm PDMS, GC-MS 

in onion J. Chromatogr. A. (2000), 896(1+2), 117-124 85µm polyacrylate 

Arnault, I.; Mondy, N.; Cadoux, F.; Auger, J. 2min, headspace 

Analysis of free fatty acids in whey products by SPME 

954 Fatty acids, J Agric Food Chem, 2001, 49, 3993-3998 30µm PDMS GC-FID 

in whey products Tomaino, R., Parker, J., Larick, D. 40 min @ 110°C 

headspace 

Determination of free fatty acids and lactones in cheese 

816 Fatty acids, lactones by solid phase microextraction (SPME) 

in cheese Aust. J. Dairy Technol.,(1998), 53(2), 140 

Wijesundera, C., Drury, L., Walsh, T. 

Traceability of Asiago mountain cheese: A rapid, low-cost analytical 

2298 Sesquiterpenes procedure for its identification based on solid-phase microextraction PDMS GC/MS 

in cheese Journal of Dairy Science (2005) 88 #10, 3426-3434 headspace 

Favaro, G.; Magno, F.; Boaretto, A.; Bailoni, L.; Mantovani, R. 

Application of SPME GC-MS and multivariate analysis for resolving 

2256 Flavors from flavor problems with cheese-based products headspace GC/MS 

cheese-based Abstracts of Papers Am Chem Society (2004) 228, #1, U74 

products Marsili, Ray T. 

Application of SPME-GC method for analysis of the aroma of 

2689 Aroma from white surface mould cheeses headspace GC 

white surface J Food Nutrition Research 46, #2, 84-90 (2007) 

mould cheeses Vitova, E.; Loupancova, B.; Stoudkova, H.; Zemanova, J. 

101 Flavors 

SPME for Cheese Volatile Compound Analysis 

J. Food Sci. 61: 1118-1129 (1996) 100µm PDMS, GC, GC-MS 

in cheese J. Food Sci. 61: 1118-1129 (1996) polyacrylate 

60°C, 20 min 

788 Volatilse 

Solid-Phase Microextraction-Mass Spectrometry: A New 

Approach to the Rapid Characterization of Cheeses GC-MS 

in cheese Anal. Chem (2001) 73(5), 1030-1036 

Peres, Christophe; Viallon, Christine; Berdague, Jean-Louis 

826 Volatiles in 

Use of preconcentration techniques applied to a Mass 

Spectrometer based "Electronic Nose". GC-MS 

Emmital cheese Analusis (2000) 28(8), 743-749 

Bosset, J.; Escher, F.; Schaller, E.; Zenhausern, S.; Zesiger, T. 

Cooperation between wild lactococcal strains for cheese 

2294 Aromas in aroma formation headspace GC/MS 

cheese Food Chemistry 94 #2, 240-246 (2006) 

Amarita, F.; de la Plaza, M.; Fernandez de Palencia, P.; Requena, T.; . 

Pelaez, C 

380 Aroma volatiles 

Pattern Recognition of Swiss Cheese Aroma Compounds by 

SPME/GC and an Electronic Nose 85µm polyacrylate GC-FID 

in cheese Milchwissenscaft (1998) 53 (5) 259-263 40°C, 30 min 

Jou, K., Harper, W. headspace 


Cryo-trapping/SPME/GC analysis of cheese aroma 

Talanta (1999) 48(4), 747-753 100µm PDMS GC-FID, EMS 

in cheese Jaillais, B., Bertrand, V., Auger, J. 

A Study of Volatile "Trapping" in Spray-Dried Whey Protein 

4 min @ 20°C 

headspace 

187 Volatiles in Concentrate by Crushing and/or Vacuuming and Detection GC-MS 

whey protein by SPME/GC-MS 

Food Res. Int. 29: 495-504 (1996) 

Stevenson, R., Chen, X. 






Use of SPME of Volatile Compounds in Whey Protein 

Concentrates 85µm polyacrylate GC-MS 

whey protein Milchwissenschaft (1998) 53 (4) 209-212 40°C, 30 min 

Yang, J., Li, W., Harper, W. headspace, stirring 

Headspace sampling of whey protein concentrate 

450 Volatiles in solutions using SPME GC-MS 

whey protein Food Res. Int. (1999), 31(5), 371-379 headspace 

Le Quanch, M., Chen, X., Stevenson, R. 

422 Flavors in 

Isolation of Flavor Compounds from Protein Material 

ACS Symp. Ser. (1998), 705 (Flavor Analysis), 107-115 

protein Mills, O., Broome, A. 


Qualitative and Quantitative Analysis of Flavor 

Additives on Tobacco Products Using SPME-GC-MS Carbowax/DVB GC-MS 

tobacco J. Agric. Food Chem. 45: 844-849 (1997) 95°C, 15 min 

Clark, J., Bunch, J. headspace 

137 Phenols in 

Quantitative Determination of Phenols in Mainstream Smoke 

with SPME-GC Selected Ion Monitoring MS Polyacrylate GC-MS 

tobacco smoke J. Chromatogr. Sci. 34: 272-275 (1996) 

Clark, J., Bunch, J. 

Buffer, 1 hr 

608 Acetates 

Quantitative analysis of acetates in cigarette tobacco 

using SPME and GC-MS 75µm Carboxen/PDMS GC-MS 

in Cigarette tobacco J. Chromatogr. Sci. (2000), 38(4), 137-144 

Watxon, C., Ashley, D. 

5min. Headspace 

Derivatization of SPME GC-MS Determination of 

369 Carboxylic acid esters Organic Acids in Tobacco 85µm polyacrylate GC-MS 

in tobacco J. Chromatographic Science, Vol. 35, (1997) 209-212 15 min, stirring 

Clark, J., Bunch, J. MeOH-HCl derivatives 

2216 Volatiles of 

Comparison of simultaneous distillation extraction and SPME for 

determination of volatile constituents in tobacco flavor headspace GC-MS 

tobacco flavor J Cent South Univ Technol Eng 12 #5, 546-551 (2005) 

Guo, Fang-Qiu; Huang, Lan-Fang; Wei, Wan-Zhi; Zhong, Ke-Jun 

822 Alkenylbenzenes 

SPME of alkenylbenzenes and other flavor-related 

compounds from tobacco for analysis by selected ion 65µm Carbowax/DVB GC-MS 

flavor compounds monitoring GC-MS 2min @ 95°C 

in tobacco J. Chromatogr.A, 858 (1999) 79-89 

Stanfill, S., Ashley, D. 

SPME and GC w/ atomic emission detection for multiresidue 

2200 Pesticides in determination of pesticides in honey Atomic 

honey Anal. Chim. Acta(2006) 562. #1, 9-15 emission 

Aguinaga, N.; Campillo, N.; Hernandez-Cordoba, M.; Penalver, R. 

931 Pesticide residues 

SPME applied to the analysis of pesticide residues 

in honey using GC with ECD 100µm PDMS, GC-ECD 

in honey J. Chromatogr. A (1998), 829(1-2), 269-277 60min @ 70°C 

Jiméniz, J., Bernal, J., del Nozal, G., Martin, M., Mayorga, A. 

Application of SPME in Determination of Phenol in Honey 

immersed 

agitated 

431 Phenols in Riv. Sci. Aliment, (1997) 26(3/4), 97-102 

honey Conte, L., Botolomeazzi, R., Moret, S., Sibaini, A., Marcazzan, G. 


Determination of volatile organic compound patterns characteristic of 

five unifloral honey by SPME-GC-MS coupled to chemometrics. headspace GC-MS 

from multifloral J. Agric. Food Chem. 54, #19, 7235-7241 (2006-09-20) 

honey Baroni, M. V.; Nores, M. L.; Diaz, M. P.; Chiabrando, G. A.; Fassano, J. P.; 

Costa, C.; Wunderlin, D. A. 




Matrix Literature Reference 

Screening of volatile composition from Portuguese multifloral honeys 

Conditions Instrument 

2520 Aroma volatiles using headspace SPME-GC-quadrupole mass spectrometry 50/30µm DVB/CAR GC-MS 

from multifloral Talanta 74, #1, 91-103 (NOV 15 2007) 45 min @ 60°C 

honey Pontes, M.; Marques, J. C.; Camara, J. S. headspace 


Aroma investigation of unifloral Greek citrus honey using SPME-GC-MS 

Food Chem. 100, #1, 396-404 ( 2007) headspace GC-MS 

from citrus honey Alissandrakis, E.; Tarantilis, P. A.; Harizanis, P. C.; Polissiou, M 

Headspace volatiles from unifloral honeys of Satureja montana L. and 

2918 Volatiles from Salvia officinalis L.of Croatian origin isolated by SPME 

unifloral honey Planta Medica 3, #9, 896 (AUG 2007) 

Jerkovic; Marijanovic, Z.; Jelic, M. 


Volatile profile of Croatian lime tree (Tilia sp.), fir honeydew (Abies alba) 

and sage (Salvia officinalis) honey headspace GC-MS 

sage honey Food Technology and Biotechnology 45 # 2, 156-165 ( APR-JUN 2007) 

Lusic, D.; Koprivnjak, O.; Curic, D.; Sabatini, A..; Conte, L.. 

433 Volatile organics 

Identification of Volatile Organic Compounds Present 

in Different Honeys Through SPME and GC/MS GC-MS 

in honey Ind. Alimenti., (1998), 37(368), 351-356 

Guidotti, M., Vitali, M. 

109 Aroma volatiles in 

Comparison of Dynamic Headspace Concentration 

on Tenax with SPME for Analysis of Aroma Volatiles 100µm PDMS, GC-MS 

carbonated cola J. Agric. Food Chem. 45: 2638-2641 (1997) 85µm polyacrylate 

beverages Elmore, S., Erbahdir, M., Mottram, D. 60°C, 30 min 

headspace 

2433 Aroma volatiles in 

Discrimination between defective and non-defective Brazilian coffee 

beans by their volatile profile 50/30µm DVB/CAR GC-MS 

brewed coffee FOOD CHEM. 106, #2, 787-796 (15 JAN 2008) 

Mancha, Agresti P. D. C.; Franca, A. S.; Oliveira, L. S.; Augusti, R. 

headspace 

SPME Applications in Gas Chromatography Olfactometry 

349 Aroma volatiles in Dilution Analysis 

100µm, 30µm, 7µm 

PDMS GC-FID 

brewed coffee J. Agric. Food Chem. 1999, 47, 1616-1618 1-90 min 

Deibler, K., Acree, T., Lavin, E. headspace, stirring 

119 Aroma in 

Solid Phase Microextraction: A Valuable Problem Solver 

Food Product Design December 1996, pp 73-77 various fibers & 

food products Marsili, R. extraction conditions 

128 Flavor volatiles in 

Analysis of Flavor Volatiles Using Headspace SPME 

J. Agric. Food Chem. 44: 2187 (1997) 85µm polyacrylate GC-FID 

fruit juice Steffen, A., Pawliszyn, J. 

Screening of Brazilian fruit aromas using SPME-GC-MS 

60 min, salt added 

headspace, stirring 

609 Aroma compounds J. Chromatogr. A.,873(1), 117-127 various fibers GC-MS 

in Brazilian fruit Augusto, F., Valenta, A., dosSantos, T., Rivellino, S. headspace 

425 Volatiles 

Analysis of Volatile Fruit Components by Headspace 

Solid Phase Microextraction 100µm PDMS GC-MS 

in fruit Food Chem. (1998), 63(2), 281-286 30 min @ 30°C 

Ibanez, E., Lopez-Sebastian, S., Ramos, E., Tabera, J., Reglero, G. headspace 

Sample preparation in the determination of phenolic 

872 Phenolics compounds in fruits review article 

in fruits Analyst (Cambridge, U. K.) (2000) 125(5) 989-1009 

Antolovich, M.; Prenzler, P.; Robards, K.; Ryan, D. 


Flavor Volatiles in Fruit Beverage with Automated SPME 

Food Test. Anal, 2(3), pp16-18 (1996) 100µm PDMS, GC-FID 

fruit beverage Penton, Z. 85µm polyacrylate 

20 min, headspace 





Changes in Citrus Hystrix Oil During Autoxidation 


424 Oxidative byproducts Dev. Food Sci. (1998), 40 (Food Flavors: Formation, 

in citrus hystrix oil Analysis and Packaging Influences), 707-718 

Pudil, F., Wijaya, H., Janda, V., Volfova, J., Valentova, H., 

Porkorny, J. 

893 Monoterpenes 

Degradation of monoterpenes in orange juice 

by gamma radiation 100µm PDMS GC-MSD 

in orange juice J. Ag Food Chem. (2001) 49(5) 2422-2426 60°C, 20 min 

Fan, Xuetong; Gates, Robert A headspace, stirring 

Effect of pulp reduction and pasteurization on the release of 

2632 Aroma compounds aroma compounds in industrial orange juice. headspace GC-MS 

orange juice J Food Sci 72, #8, S535-43 (2007 Oct) 

Berlinet, C; Guichard, E; Fournier, N; Ducruet, V 

2472 Flavor compounds 

SPME for headspace analysis of key volatile compounds in orange 

beverage emulsion. 75µm Carboxen GC 

orange beverage Food Chemistry 105, #4, 1659-1670 (2007) Headspace 

emulsion Mirhosseini, H.; Salmah, Y.; Nazimah, S. A. H.; Tan, C. P. 

Optimization of SPME Analysis for Headspace 

15 min @ 45°C 

15% NaCl 

358 Flavor compounds Flavor Compounds of Orange Juice 100µm PDMS GC-FID 

in orange juice J. Agric. Food Chem. 1998, 46, 2744-2747 60°C, 20 min 

Jia, M., Zhang, H., Min, D. headspace, stirring 

Pulsed electric field processing effects on flavor 

451 Flavor compounds compounds and microorganism of orange juice 

in orange juice Food Chem (1999), 65(4), 445-451 

Jia, M., Zhang, Q, Min, D. 

Volatiles from Unpasteurized and Excessively 

561 Flavor compounds heated orange juice with SPME and 75µm Carboxen/PDMS GC-MS 

in orange juice GC Olfactometry 30 min Headspace 

J. Food Science, Vol.64, N0.5, 1999, 800-803 40°C 

Bazemore, R., Goodner, K. Rouseff, R. 


Comparison of Gas-Sampled and SPME-Sampled Static 

Headspace for the Determination of Volatile Flavor Compounds 65µm PDMS/DVB GC-MS 

fruit juices Anal. Chem. Vol. 71, No. 1, January 1, 1999, pg 23-27 40°C, 30 min 

Miller, M., Stuart, J. headspace 

131 Flavor volatiles 

Solid Phase Microextraction for Quantitative 

Headspace Sampling of Apple Volatiles 100µm PDMS GC-MS 

in apples Anal. Chem. 68: 4114 (1996) 30 min 

Matich, A., Rowan, D., Banks, N. headspace 


Rapid Analysis of Volatile Flavor Compounds in 

Apple Fruit Using SPME & GC-Time-of-Flight Mass Spec 100µm PDMS GC-FID 

In apples J. Agric. Food Chem. 45: 1801-1807 (1997) 2-8 min 

Song, J., Gardner, B., Holand, J., Beaudry, R. headspace 


Volatile Production and Fruit Quality During Development 

of Superficial Scald in Red Delicious Apples 

red delicious apples Food Res. Int. (1997), 30(2), 95-103 

Paliyath, G., Whiting, M., Stasiak, M., Murr, D., Clegg, G. 

899 Aroma compounds 

Influence of packaging on the aroma stability of strawberry 

syrup during shelf life 100µm PDMS GC-FID 

in strawberries J. Agric. Food Chem. 49(5): 2290-2297 (2001) 60 min @ 50°C 

Ducruet, V Feigenbaum, A; Fournier, N; Guichard, E; Saillard, P. 

Application of SPME and GC/Time-o-Flight Mass 

headspace 

agitated 

383 Flavor volatiles in Spectrometry for Rapid Analysis of Flavor Volatiles 65µm PDMS/DVB GC-MS 

tomato, strawberry in Tomato and Strawberry Fruits 23°C, 12 min 





J. Agric. Food Chem. 46: 3721-3726 (1998) 

Song, J., Fan, L., Beaudry, R. 

headspace 

A new concept for the measurement of total 

452 Flavor volatiles in volatile compounds of food 

tomato, strawberry, Z. Lebenam. Unters, Forsch A, 1999, 208(4), 254-258 

raspberries, apples Azodanlou, R., Darbellay, c., Luisier, J., 

Villettaz,J., Amode, R. 

2797 Fungicides in 

Pesticide analysis in tomatoes by solid-phase microextraction 

and micellar electrokinetic chromatography 65µm PDMS/DVB 

tomatoes J. Chromatogr., A 1185, #1, 151-154 (MAR 21 2008) 

Ravelo-Perez, L.; Hernandez-Borges, J.r; Borges-Miquel, T.; Angel 

Rodriguez-Delgado, Miguel 

immersed 

Study of the volatile composition of tomato during storage by a 

2839 Aroma volatiles combination sampling method coupled with GC-MS headspace GC-MS 

from tomato J Science of Food and Agriculture 88, #1, 116-124 (Jan 2008) 

Zhang, Zhuo-Min; Zeng, Dan-Dan; Li, Gong-Ke 

Aroma volatiles of tomatoes and tomato products evaluated by SPME 

2684 Aroma volatiles Flavour and Fragrance J. 22, #5, 395-400 (2007) headspace GC-MS 

from tomato Markovic, K.; Vahcic, N.; Kovacevic Ganic, K.; Banovic, M. GC-FID 

A preliminary study of plant aroma profile characteristics by a 

2478 Aroma volatiles combination sampling method coupled with GC-MS headspace GC-MS 

from tomato Microchemical Journal 86, #1, 29-36 (JUN 2007 

Zhang, Zhuo-Min; Li, Gong-Ke 

SPME method for in vivo measurement of allelochemical uptake 

2357 Allelochemical J Chem Ecol 34, #1, 1-6, 70-75 (Jan-2008) GC 

compounds in Loi, Rebecca X; Solar, Marissa C; Weidenhamer, Jeffrey D 

tomato plants 

Aroma-active compounds of Elsholtzia splendens using AEDA and 

2820 Volatiles from HS-SPME-GC-O dilution analysis headspace GC-MS 

aromatic plant Flavour and Fragrance J. 23, #1, 58-64 (JAN-FEB 2008) 

Choi, Hyang S.; Min, Kyung C. 


Comparison of Three Sample Preparation Techniques for the 

Determination of Fresh Tomato Aroma Volatiles 100µm PDMS GC-MS 

in tomato Book: Flavor Science: Recent Developments, Buttery & 30°C, 10 min 

Shadhidi, Washington, DC, 1998 p. 289-292 headspace 

Krumbein, A., Ulrich, D. salt added 

766 Volatiles 

Volatile emissions of tomato 

Mededelingen Faculteit Landbouwkundige en Toegepaste 

in tomato Biologische Wetenschappen Universiteit Gent 

(1999) 64(4), 159-161 

Maes, K; Debergh, P; Sandra, P; Vercammen, J 

headspace 

933 Volatiles 

Critical aspects for the reliable headspace analysis of plants 

cultivated in vitro 

in tomato Phytochemical Analysis (2001) 12(3), 153-158 

Maes, K; Debergh, P; Sandra, P; Vercammen, J 

Pham-Tuan, Hai 

headspace 


Effect of Thermal Treatment in the Headspace Volatile 

Compounds of Tomato Juice 65µm Carbowax/DVB GC-MS 

in tomato juice Istituto di Indstrie Agrarie, University of Perugi, via S. 35°C, 30 min 

Costnazo I-06126, Pergia-Italy 

Servili, M., Selvaggini, R., Begliomini, A., Montedoro, G. 

CaCl added 


Relationships between the volatile compounds evaluated by 

SPME and the thermal treatment of tomato juice: 65µm Carbowax/DVB GC-EIMS 

in tomato juice optimization of the blanching parameters 

Food Chemistry (2000) 71(3), 407-415 

Servili, M.; Selvaggini, R.; Taticchi, A.; 

Begliomini, A. L.; Montedoro, G. 

29°C, 15 min 





Solid-Phase Microextraction: Artifact Formation and Its 


214 Strawberries & apples Avoidance 85µm polyacrylate GC-MS 

in fruit homogenate Chromatographia 46: 63-66 (1997) 30 sec 

Verhoeven, H., Beuerle, T., Schwab, W. immersion 


Analysis of Strawberry Aroma by SPME 

Dtsch. Lebesm - Rundsch. 91: 349 (1995) 

in strawberry Ulrich, D., Eunert, S., Hober, E., Rapp, E. 

A new concept for the measurement of total volatile 

590 Aroma volatiles compounds of food. 

PDMS, CW/DVB, 

PDMS/DVB GC-FID 

in strawberries Z-Lebensm-Unters-Forsch-A. Apr 1999; 208(4): 254-258 polyacrylate 

Azodanlou-R; Darbellay,C; Luisier,JL; Villettaz,JC; Amado,R 30 min @ 25°C 

headspace 

Comparison of volatiles of banana powder dehydrated by vacuum 

2496 Aroma volatiles belt drying, freeze-drying and air-drying headspace GC-MS 

from dried Food Chemistry 104, #4, 1516-1521 (2007) 

banana powder Wang, J.; Li, Yuan Zhi; Chen, Ren Ren; Bao, Jin Yong; Yang, Gong 


Evaluation of the Solid Phase Microextraction of 

Aroma Compounds in Banana 

in banana Collog.-Inst. Nat. Rech. Agron. 75 (Bioflavour 95) 117 (1995) 

Picque, D., Normand, A., Corrieu, G. 


Identification of volatile coumpounds in cantaloupe at 

various developmental stages using SPME 100µm PDMS GC-MS 

in cantaloupe J Agric Food Chem 2001, 49(3), 1345-1352 12.5 min headspace 

Beaulieu, J., Grimm, C. sat. salt, agitated 

150 Pyrazines 

SPME of Pyrazines in Model Reaction Systems 

J. Sci. Food Agric. 72: 91 (1996) 

Ibanez, E., Bernhard, R. 

2895 Pyrazines 

Formation of pyrazines and a novel pyrrole in Maillard model systems 

of 1,3-dihydroxyacetone and 2-oxopropanal 

J Agric Food Chem 56, #6, 2147-2153 (MAR 26 2008) 

Adams, An; Polizzi, Viviana; van Boekel, Martinus; De Kimpe, N. 

headspace GC-MS 

934 Pyrazines 

Solid-phase microextraction with aqueous immersion for 

analysis of Maillard-generated pyrazines in model reaction 

system 

Diss. Abstr. Int., B 2000, 61(5), 2287 

Cai, Yanxuan 

356 Menthol 

SPME-GC-Mass Selective Detection Analysis of Selected 

Sources of Menthol 65µm Carboxen/PDMS GC-MS 

(natural) J. Chromatogr. Sci. (1998), 36(8) 401-405 50°C, 20 sec 

Coleman, W., Lawson, S. headspace 

Determination of menthol and menthone in food and 

453 Menthol, menthone pharmaceutical products by SPME-GC ethoxy dimethylsiloxane GC-FID 

food/pharmaceutical J. Chromatogr., A 1999, 847 (1+2), 161-169 15 min @ 30°C 

Ligor, M., Buszewski, B. immersed 

Measurement of gas-liquid partition coefficient and 

610 Aroma headspace concentration profiles of perfume materials 7µm PDMS GC-MS 

in perfume by SPME and capillary GC-MS 10 min headspace 


Liu, Z. Wene, M. 

Contribution of volatiles to the flavor of oatmeal 

611 Flavor compounds J. Sci Food Agric.1/15/2000, 80(2);, 247-254 100µm PDMS GC-MS 

in oatmeal Zhou, M, Robards, K., Helliwell, S., Glennie-Hommes, M. water solution @ 100°C 





Changes in the volatile profile of oats induced by processing 

Conditions 

headspace 

Instrument 

894 Flavor compounds J. Agric. Food Chem. 49 (5): 2125-2130 (2001) 100µm PDMS GC-MS 

in oats Robards, Kevin; An, Min; Helliwell, Stuart; Sides, Alasdair 

SPME for the Analysis of Flavors 

30SEC @ 25°c 

headspace 

309 Flavors in Techniques for Analyzing Food Aroma, pp81-112, various fibers 

food products Food Sci. Technol., New York (1997) 

Harmon, A. 

& conditions 


Analysis of Volatile Fragrance and Flavor Compounds by 

Headspace SPME Combined with Gas Chromatography/ 100µm PDMS GC-MS 

consumer products Mass Spectrometry 30 min 

J. Chem. Educ. 1999, 76(2), 245-248 

Galipo, R., Canhoto, A., Walla, M., Morgan, S. 

headspace 


Solid Phase Microextraction for the enantiometric analysis of 

Flavors in Beverages 85µm Polyacrylate GC-MS 

in beverages J. AOAC Intl, Vol. 84, No. 2, 2001, 479-485 60 min., headspace 

Ebeler, S., Sun, G., Datta, M., Stremple, P., Vicker, A. salt added 

2771 Rose oxide 

Stereoselective formation of the varietal aroma compound rose oxide 

during alcoholic fermentation headspace GC/MS 

in white wine J. AOAC Intl, Vol.56, No. 4, 1371-1375 (FEB 27 2008) 

Koslitz, Stephan; Renaud, Lauren; Kohler, Marcel; Wuest, Matthias 

Monitoring of the principal carbonyl compounds involved in 

2233 Carbonyls malolactic fermentation of wine by SPME and positive ion chemical 65um DVB GC/MS 

in wine ionization GC/MS analysis (PFBOA) 

J. Mass Spectrom. 40 #12, 1558-1564 (2005) derivatives 

Dalla Vedova, A.; Flamini, R.; Ongarato, S.; Panighel, A.Perchiazzi,N.; 5min @ 50C 

2904 Carbonyls 

Analysis of carbonyl compounds via headspace SPME with on-fiber 

derivatization and GC-ion trap tandem MS determination GC-ITMS 

biological samples of their O-(2,3,4,5,6-pentafluorobenzyl)oxime derivatives PFBHA 

and foodstuffs, Anal. Chim. Acta 617, #1-2, 119-131 (Jun 9 2008) 

Bokuz, U.; Fischer, Ulrich; Ganss, S.; Kopp, B.; Potouridis, T.; 

derivatives 

891 Volatile carbonyls 

Comparison of extraction techniques for GC 

determination of volatile carbonyl compounds in alcohols. GC-ECD 

in alcohols Fresenius' J.Anal Chem. (2001) 369(7-8) 661-665 

Wardencki, W; Namiesnik, J; Orlita, J. 

PFBHA derivatives 

903 Carbonyls 

Determination of carbonyl compounds in water by 

derivatization SPME and GC analysis GC 

in water J. Chromatography A 1998, 809, 1-2, 75-87 

Bao,M., Pantani,F.,Griffini,O.,Burrini,D.,Santianni, D., Barbieri, K. 

Development of a dynamic headspace SPME procedure coupled to 

2817 Organic content GC-qMSD for evaluation the chemical profile in alcoholic beverages various fibers GC-qMSD 

in alcoholic Analytica Chimica Acta 609, #1, 82-104 (FEB 18 2008) headspace 

beverage Rodrigues, F.; Caldeira, M.; Camara, J. S. 

Research on alcoholic beverages at Alko's control Lab 

454 Organic content Kem.-Kemi, 1999, 26(2), 95-97 GC-MS 

in alcoholic Lehtonen, P. 

beverage Finnish 

Analysis of free fatty acids, higher alcohols and 

455 Alcohols, esters, free esters in sake by headspace-SPME 

fatty acids Nippon Jozo Kyokaishi (1999), 94(3), 252-257 

in Sake Utsunomiya, H. Japanese 

Solid-phase microextraction for the GC-MS determination of 





2867 Oxazole fungicide oxazole fungicides in malt beverages 100µm PDMS GC-MS(SIM) 

in malt beverages Anal. Bioanal. Chem. 391, #3, 1425-1431 (2008) 70µm CW-DVB 

Aguinaga, N.; Campillo, N.; Hernandez-Cordoba, M.; immersion 

Martinez-Castillo, N.;Vinas, Pilar 60°C, 30 min 


Headspace Gas Chromatography Profiles of Fruit-Flavored 

Malt Beverages, Using SPME 100µm PDMS GD-FID 

malt beverages J. Am. Soc. Brew. Chem. 55 (3): 112-118 (1997) 45°C, 45-60 min 

Constant, M., Collier, J. headspace 


Optimisation of a complete method for the analysis of volatiles 

involved in the flavour stability of beer by SPME-GC-MS headspace GC-MS 

beer wort J. CHROMATOGR. A 1190, #1-2, 342-349 (May 9 2008) 

De Schutter, D.; Delvaux, F.; Delvaux, F.; Saison, D. PFBHA derivative 


Optimisation of wort volatile analysis by headspace SPME in 

combination with gas chromatography and mass spectrometry headspace GC-MS 

beer wort J. CHROMATOGR. A 1179, #2, 75-80 (01 FEB 2008) 

De, Schutter D. P.; Saison, D.; Delvaux, F.; Derdelinckx, G.; Rock, J.; . 

Neven, H.; Delvaux, F. 

313 Alcohols, esters 

Solid Phase Microextraction for the Analysis of Some 

Alcohols and Esters in Beer: Comparison with Static 85µm polyacrylate GC-FID 

in beer Headspace Method 50°C, 30 min 

J. Agric. Food Chem. 46 (4): 1469-1473 (1998) headspace 

Wasowicz, E., Kaminski, E., Jelen, H., Wlazly, K. salt added 

2818 Dimethyl sulfide 

Laboratory inter-comparison of dissolved dimethyl sulphide 

(DMS) measurements using purge-and-trap and SPME GC-MS 

in water techniques during a mesocosm experiment 

Marine Chemistry 108, #1-2, 32-39 (JAN 1 2008) 

Vogt, M.; Turner, S.; Yassaa, N.; Steinke, M.; Williams, J.; Liss, P. 

headspace 

Headspace SPME for the analysis of dimethyl 

456 Dimethyl sulfide sulfide from beer 65µm Carboxen/PDMS GC-FPD 

in beer J. Agric. Food Chem. 1999, 47(7), 2505-2508 15 min @ 30°C 

Scarlata, C. Ebeler, S. headspace 

1.5gm NaCl 

Characterization of whiskIes using SPME with GC-MS 

612 Volatiles in J.Chromatogr. A (2000) 896, 351-359 85µm polyacrylate GC-MS 

whiskies Fitzgerald, G., James, K., MacNamara, K., Stack, M. 35 min 

headspace 

Changes in volatile compounds of palm sap (Arenga pinnata) 

2368 Volatiles in during the heating process for production of palm sugar headspace GC-MS 

palm sap Food Chemistry 102, # 4, 1156-1162 (2007) 

Ho, C. W.; Aida, W. M. Wan; Maskat, M. Y.; Osman, H. 

A headspace SPME method for the determination of some 

953 Volatiles in secondary compounds of Brazilian sugar cane spirits by GC 85µm polyacrylate GC-FID 

sugar cane spirits J Agric Food Chem, 2001, 49, 3533-3539 25 min @ 60°C 

Nonato, E., Carazza, F., Silva, C. Carvalho, C., Cardeal, Z headspace 

2.5g NaCl 

Determination of volatile fatty acid ethyl esters in raw spirits using 

2765 Fatty acid ethyl SPME and GC headspace GC-FID 

esters in spirits Anal. Chim. Acta 613, #1, 64-73 (Apri 14 2008) 

Plutowska, Beata; Wardencki, Waldemar 

Characterization of rum using solid-phase microextraction with GC-MS 

2732 Aroma volatiles Food Chemistry 104, # 1, 421-428 (2007) 100µm PDMS GC-MS 

in rum Pino, J. A 35 min @ 35°C 

headspace 

Comparison of two extraction methods for evaluation of volatile 

2502 Aroma volatiles constituents patterns in commercial whiskeys. Elucidation of the 75µm Carboxen GC-MS 

in whiskeys main odour-active compounds 

Talanta 74, #1, 78-90 ( Nov 15 2007) 

Caldeira, M.; Camara, J.S.; Marques, J.C.; Perestrelo, R.; Rodrigues, F. 

headspace 





Aroma of dehydrated pear products 

2621 Aroma volatiles LWT - Food Sci. Technol. 40, #9, 1578-1586 (November 2007) headspace GC-MS 

in pear products Komes, Drazenka; Kovacevic Ganic, Karin; Lovric, Tomislav 

Changes in odor of Bartlett pear brandy influenced by 

595 Aroma volatiles sunlight irradiation. 100µm PDMS GC-EIMS 

in Brandy Chemosphere. Mar 1999; 38(6): 1299-1303 15 min @ 40°C 

Kralj-Cigic,-I; Zupancic-Kralj,-L 

Analysis of brandy aroma by SPME and liquid-liquid extraction 

613 Aroma compounds J. Sci. Food Agric. Apr 2000, 80(5), 625-630 100µm PDMS GC-FID 

in brandy Ebeler, S., Terrien, M., Butzka, C. 30 min @ 50°C 

Headspace 

A comparison of SPME and stir bar sorptive extraction coupled to 

2830 Resveratrol HPLC for the rapid analysis of resveratrol isomers in wines, 50 µm CW/TPR LC-Fluorimetric 

isomers in musts and fruit juices immersion 

wine, musts, Anal. Chim. Acta 611, #1, 119-125 (Mar 17 2008) 30 min @ 40°C 

fruit juices Campillo, N.; Hernandez-Cordoba, M.; Hernandez-Perez, M.; Vinas, P. 

Differentiation of "claret", Rose, Red and Blend wines based 

2780 Aroma volatiles on the content of volatile compounds by headspace SPME-GC 65µm CW/DVB GC-FID 

in wine Eur. Food Res. Technol. 226, #6, 1317-1323 (April 2008) Headspace 

Cabredo-Pinillos, S.; Cedron-Fernandez, T.; Saenz-Barrio, C. 

Rapid headspace SPME-GC-MS assay for the quantitative determination 

2410 Off-flavors of some of the main odorants causing off-flavours in wine headspace GC-MS 

in wine J. Chromatogr., A 1141,#1, 1-9 (2007-02-02) 

Boutou, S.; Chatonnet, P. 

Analysis of aromatic components in kiwifruit wine by GC-MS with SPME 

2514 Aroma volatiles J Northwest A & F University - Natural Science Ed. 35, #6, 89-93 (2007) headspace GC-MS 

in wine Guo Jing; Yue TianLi; Yuan YaHong; Gao ZhengPeng 

Optimization of headspace SPME for analysis of wine 

827 Aroma volatiles aroma compounds 

in wine Am Journal Enology and Viticul (2000) 51(4), 379-382 

Zoecklein, B. W.; Whiton, R. S headspace 


Use of an array of metal oxide sensors coupled with SPME for 

characterisation of wines. Study of the role of the carrier gas headspace GC-MS 

in wine Sens Actuators, B Chem 132, #1, 125-133 (May 28 2008) 

de Saja, J.; Guadarrama, A.; Rodriguez-Mendez, M.; Villanueva, S. 

Discrimination of wine aroma using an array of conducting 

901 Aroma volatiles polymer sensors in conjunction with SPME technique 

in wine Sens Actuators, B Chem (2001) 77(1-2), 401-408 

De Saja, J.A.; Fernandez, J.A.; Guadarrama, A.; Iniguez, M.; Souto, J 

Effect of cultural practices and environmental factors on 

896 Aroma volatiles fruit and wine quality GC-MS 

in wine Agriculturae Conspectus Scientificus 2001 66(1) 13-20 

Bravdo, Ben Ami 


Systematic Optimization of the Analysis of Wine Bouquet 

Components by SPME 85µm polyacrylate GC-FID 

in wine J. High Res. Chromatogr. 19: 257-262( 1996) 15 min 

Garcia, D., Magnaghi, S., Danzer, K. immersion, stirring 

pH 4, salt added 

Rapid headspace SPME-GC-TOF/MS method for qualitative profiling of 

2340 Aroma volatiles ice wine volatile fraction I. Method development and optimization. 50/30µm DVB/CAR GC-TOF/MS 

in ice wine J Chromatogr A 1147 # 2, 213-223 (2007) 5 min @ 45 C 

Setkova, Lucie; Risticevic, Sanja; Pawliszyn, Janusz headspace 

3 mL, 1gm salt added 


Rapid headspace SPME-GC-TOF/MS method for qualitative profiling 

of ice wine volatile fraction. II: Classification of Canadian and 50/30µm DVB/CAR GC-TOF/MS 

in ice wine Czech ice wines using statistical evaluation of the data 5 min @ 45 C 

J Chromatogr A 1147 # 2, 224-240 (2007) headspace 





Setkova, Lucie; Risticevic, Sanja; Pawliszyn, Janusz 


Rapid headspace SPME-GC-TOF/MS method for qualitative 

2411 Aroma volatiles profiling of ice wine volatile fraction. III: Relative characterization 

in ice wine of Canadian and Czech ice wines using self-organizing maps. 

J Chromatogr A 1147 # 2, 241-253 (2007) 

Setkova, Lucie; Risticevic, Sanja; Pawliszyn, Janusz 

2564 Organotin 

Optimization of the SPME procedure for the ultra-trace determination of 

organotin compounds by GC-inductively coupled plasma-MS Car/DVB 30/50µm GC-ICP-MS 

compounds J. Anal. At. Spectrom. 21, #9, 970-973 (2006-08-25) 

Bianchi, F.; Careri, M.; Maffini, M.; Mangia, A.; Mucchino, C. 

2 cm length 

2421 Organotin in 

Organotin speciation in French brandies and wines by 

SPME-GC-Pulsed flame photometric detection 100µm PDMS GC-FPD 

brandies and wines J. CHROMATOGR. A 1180, #1-2, 122-130 (08 FEB 2008) 30 min 

Heroult, J.; Bueno, M.; Potin-Gautier, M.; Lespes, G. 

Gas-phase post-derivatization following SPME for rapid 

headspace 

ethylated derivative 

798 trans-ResverAtrol determination of trans -resveratrol in wine by GC-MS GC-MS 

in wine Analytica Chimica Acta (2000) 424(1), 19-25 22°C 

Luan, T. G.; Li, G. K.; Zhang, Z. X. 

Comparison of Two Recent Solventless Methods for the 

headspace 

silyl derivative 

201 Procymidone residue Determination of Procymidone Residues in Wines: 100µm PDMS GC-MS 

in wine Solid-Phase Microextraction-GC-MS and ELISA Tests 30 min 

J. Agric. Food Chem. 45: 1519-1522 (1997) immersion 

Urruty, L., Montury, M., Braci, M., Fournier, J., Dournel, J. stirring 

Reveal the diversity of commercial spontaneously-fermented plum 

2242 Favor wines in their components by using single strain yeast-fermented HPLC 

compounds plum wine 

in plum wine Taiwanese J Agr Chem Food Sci. 43 #3, 162-170 (2005) 

Lin, Shih-Bin; Wu, Yo-Ping; Shen, Fang-Ling 


Qualitative and quantitative analyses of volatile organic 

compounds in wines using SPME-GC 

in wine Chem. Anal. (Warsaw, Pol.) (2001) 46(2) 215-224 

Buszewski, B; Ligor, M. 


Investigation of Wine Bouquet Components by SPME- 

Capillary GC, Using Different Fibers 85µm polyacrylate GC-FID 

in wine J. High Resolut. Chromatogr. 20 (12): 665-668 (1997) 30 min 

De La Calle Garcia, D., Feller, K., Reichbacher, M., immersion 

Danzer, K., Hurlbeck, C., Bartzech, C. stirring 


Analysis of Wine Bouquet Components Using Headspace 

SPME-Capillary Gas Chromatography 85µm polyacrylate GC-MS 

in wine J. High Resolut. Chromatogr. (1998), 21(7), 373-377 60 min 

De La Calle Garcia, D., Feller, K., Reichbacher, M., Danzer, K., headspace 

Hurlbeck, C., Bartzech, C. stirring 


Classification of wine samples according to origin and 

grape varieties on the basis of inorganic and organic 85µm polyacrylate GC-MS 

in wine trace analysis 60 min 

American Lab, Oct. 1999, Vol. 31(20) 26-33 headspace 

Danzier, K., De La Calle Garcia, D., Thiel, G., Reichbacher, M., 

Determination of 2,4,6-trichloroanisole & 2,4,6-tribromoanisole 

stirring 

salt added 

2145 2,4,6-Trichloro- on ng /L to pg/L levels in wine by SPME-GC-MS headspace GC-HRMS 

anisole,2,4,6- J. Chromatogr. A, 1111, #1, 71-75 (2006) 

tribromoanisole Gustafsson, I.-B.; Jonsson, S.; Lindstrom, G.; Uusitalo, T.; 

in wine Van Bavel, B. 

Analysis of Cork Taint in Wine and Cork Material at 





94 Trichloroanisole Olfactory Sub-Threshold Levels by SPME 100µm PDMS SIM-GC-MS 

in wine J. Agric. Food Chem. 45: 1995-1997 (1997) 20°C, 30 min 

Fisher, C., Fischer, U. salt added 

385 Trichloroanisole 

Detection of Cork Taint in Wine Using Automated SPME in 

Combination with GC-MS-SIM 100µm PDMS, GC-MS-SIM 

in wine Book chapter 15: ACS Symposium Series 1999, Oxford 85µm polyacrylate 

University Press, "Flavor Analysis Development in 45°C, 25 min 

Isolation and Characterization" 

Butzke, C., Evans, T., Ebeler, S. 

headspace 

Protection of some aroma volatiles in a model wine medium by sulphur 

2821 Aroma volatiles dioxide and mixtures of glutathione with caffeic acid or gallic acid GC-MS 

in model wine Flavour and Fragrance Journal 23, #1, 35-39 (JAN-FEB 2008) 

Roussis, Ioannis G.; Sergianitis, Spyros 

2384 Sulfur volatiles 

Concurrent quantification of light and heavy sulphur volatiles in wine 

by headspace SPME-GC-MS CAR/DVB 30/50µm GC-MS 

in wine Rapid Commun. Mass Spectrom. 21,#5, 707-714 (2007-03-15) 2 cm length 

Fedrizzi, B.; Magno, F.; Moser, S.; Nicolini, G.; Versini, G. headspace 

377 Sulfides, disulfides 

Headspace SPME Analysis of Volatile Sulfides and 

Disulfides in Wine Aroma 100µm PDMS, GC-FPD 

in wine J. Chromatogr. A 808 (1998) 211-218 85µm polyacrylate 

Mestres, M., Busto, O., Guasch, J. 

Headspace SPME of Sulfides and Disulfides Using 

30°C, 15 min, salt 

headspace 

406 Sulfides, disulfides Carboxen/PDMS Fibers in the Analysis of Wine Aroma 75µm Carboxen/PDMS GC-FPD 

in wine J. Chromatogr. A, 835 (1999) 137-144 25°C, 30 min 

Mestres, M., Sala, C., Marit, M., Busto, O., Guasch, J. 

Analysis of benzothiazole in Italian wines using 

headspace 

stirring, salt added 

614 Benzothiazoles SPME-GC-MS 65µm Carbowax/DVB GC-MS 

in wine J. Agric. Food Chem. (2000), 48(4), 1239-1242 15min @ 50°C 

Bellavia, V., Natangelo, M., Fanelli, R., Rotilio, D. headspace 


Similarities in the Aroma Chemistry of Gewurztraminer 

Variety of Wines and Lychee (Litchi chinesis Sonn.) Fruit 100µm PDMS GC-MS 

in wine J. Agri. Food Chem. 1999, 47, 665-670 15 min 

Ong, P., Acrees, T. headspace 

427 Volatiles 

Fast Screening Method for Wine Headspace Compounds 

Using SPME and Capillary GC Technique headspace 

in wine Am. J. Enol. Vitic. (1998), 49(1), 100-104 

Vas, G., Koteleky, K., Farkas, M., Ddobo, A., Vekey, K. 


Determination of Volatile Aroma Compounds of 

Blaufrankisch Wines Extracted by SPME 100µm PDMS GC-MS 

in wine J. Chromatographic Sci., Vol. 36, Oct. 1998, 505-510 10 min (headspace) 

Vas, G., Gal, L., Harangi, J., Dobo, A., Vekey, K. 1 hr (immersion) 

Classification of wine samples according to origin 

457 Flavor volatiles and grape varieties on the basis of inorganic and 85µm polyacrylate GC-FID 

in wine organic trace analysis 60-90 min 

Am. Laboratory, Oct. 1999, Vol. 31, No. 20, 26-34 headspace 

Danzier, K, DeLaCalle Garcia, D, Thiel, G., Satr.salt 

Reichenbacher, M 


Examination of aroma production kinetics of 

different commercial wine yeast in fermenting 100µm PDMS GC-FID 

in wine muscat ottonel wines with the help of SPME 10 min 

headspace sampling and fast GC analysis 

Acta Aliment, (1999), 28(2), 133-140 

Vaes, W., Blechschmidt, I., Kovacs, T., Vekey, K. 

headspace 





Improvement of the chemometric variety characterization of 


582 Aroma volatiles wines by improving the detection limit for aroma compound 85µm polyacrylate GC-EMIS 

in wine J-High-Resolut-Chromatogr. Jun 1999; 22(6): 322-326 3 hr. , headspace 

Weber,-J; Beeg,-M; Bartzsch,-C; Feller,-K-H; 

De-la-Calle-Garcia,-D; Reichenbaecher,-M; Danzer,-M 

NaCl added 


Determination of volatiles from red wines made 

by carbonic maceration using SPME technique 100µm PDMS GC-EIMS 

in wine Acta Aliment, 1999, 28(1), 95-101 

Vas, G., Loerincz, G. 

10 min headspace 


A comparison of the volatiles compounds from Pinus massoniana 

twigs extracted by SPME and steam distillation headspace GC/MS 

from Pinus J Nanjing Forestry University (Natural Sciences Edition) 

massoniana twigs 31, #1, 78-80 (2007) 

Wang Yan; Ye JianRen 

2634 Phenolic content 

Determination of the alkyl- and methoxy-phenolic content in wood 

extractives by micellar solid-phase microextraction and GC-MS headspace GC/MS 

in wood Talanta 73, #3, 505-513 (SEP 30 2007) 

Pino, Vernica; Ayala, Juan H.; Gonzalez, Venerando; Afonso, Ana M. 

Induction of sesquiterpenoid production by methyl jasmonate 

2295 Fragrances in aquilaria sinensis cell suspension culture headspace GC/MS 

from woody J. Essent. Oil Res. (2005) 17 #2, 175-180 

material Honda, G.; Ito, M.; Kiuchi, F.; Okimoto, K.; Shimada, Y.; Yagura, T. 


Analysis of French and American oak chips with different toasting 

degrees by headspace SPME-GC-MS Car/DVB 30/50µm GC/MS 

from oak chips Journal of Chromatography A 1173, #1-2, 10-17 (2007) 

Bozalongo, R.; Carrillo, J.; Fernandez-Torroba, M.; Tena, M. 

headspace 

Monitoring Toasting Intensity of Barrels by 

559 Aroma volatiles Chromatographic Analysis of Volatile 100µm PDMS GC-FID 

from toasted oak compounds from Toasted Oak Wood 30 min @ 22°C 

J. Agric. Food Chem, 1999, 47, 4310-4318 

Chatonnet, P., Cutzach, I., Pons, M., Dubourdieu, D. headspace 

Application of SPME for determining residues of chlorpyrifos and 

2663 Chlorpyrifos in chlorpyrifos-methyl in wine with gas chromatography (GC). headspace GC-ECD 

wine J Institute of Brewing 113, #2, 213-218 (2007) 

Anli, E.; Vural, N.; Vural, H.; Gucer, Y. 

Assembly tests of "Nero d'Avola" with wines 

460 Polyphenolics derived from an allocthonous cultivar: GC-MS 

in red wine study of polyphenolic and aromatic profiles. headspace 

Ind. Bevande (1999), 28(160), 119-126 Italian 

Papucci, A, Monte, L., D'Agostino, S, 

Aozzino, P., Avellone, G 

Sample preparation optimization in wine and grapes. Dilution and 

2885 Volatiles from sample/headspace volume equilibrium theory for headspace SPME headspace GC-MS 

wine and grapes J Chromatogr A 1192, #1, 25-35 (May 23 2008) 

Boss, Paul K.; Kalua, Curtis M. 

Comprehensive two-dimensional gas chromatography with TOF-MS 

2635 Monoterpenoids of monoterpenoids as a powerful tool for grape origin traceability headspace GC-ToF-MS 

from white grapes J Chromatogr A 1161, #1-2, 292-299 (AUG 17 2007) 

Rocha, S.; Coelho, E.; Zrostlikova, J.; Delgadillo, I.; Coimbra, M. 

Distinction and identification of lignins based on their volatile 

2763 Volatiles from headspace composition headspace GC-MS 

ligins Talanta 75, #2, 594-597 (Apr 15 2008) 

Delgadillo, Ivonne; Evtuguin, D.; Goncalves, V.; Rocha, S. 

Monitoring ester formation in grape juice fermentations 

775 Esters using SPME coupled with GC-MS 100µm PDMS GC-MS 





in grape juice J. Agric. Food Chem (2001) 49(2), 589-595 1 hr. 

Vianna, E; Ebeler, S. headspace 

315 Styrene 

Determination of Styrene in Wine by SPME and GC-MS 

Mitt. Klosterneuburg 47 (4): 117-123 (1997) GC-MS 

in wine Flak, W., Tscheik, G. 

311 Methylisocyanate 

SPME Analysis of Methyl Isothiocyanate in Wine 

J. Agric. Food Chem. 45 (8): 3092-3094 (1997) 65µm Carbowax/DVB GC-FID, NPD 

in wine Gandini, N., Riguzzi, R. 

Analysis of Diacetyl in Wine Using SPME -GC-MS 

30 min 

headspace 

salt added 

366 Diacetyl J. Agric Food Chem. 1999, 47, 612-617 60µm Carbowax/DVB GC-MS 

in wine Hayasaka, Y., Bartowsky, E. 

Multiple pesticide analysis in wine by MEKC combined with 

24°C, 5 min 

headspace 

salt added 

2465 Pesticides SPME and sample stacking 60µm PDMS/DVB micellar EKC 

in Wine Electrophoresis 28, #22, 4072-4081 (NOV 2007) diode-array 

Borges-Miquel, T.; Hernandez-Borges, J.; Ravelo-Perez, L.; 

Rodriguez-Delgado, M. 

detection 

2362 Pesticides 

Pesticide analysis in rose wines by micellar 

electrokinetic chromatography 60µm PDMS/DVB micellar EKC 

in Wine J. Sep. Sci. 30, #18, 3240-3246 (Dec. 2007) 

Borges-Miquel, T.; Hernandez-Borges, J.; Ravelo-Perez, L.; 

Rodriguez-Delgado, M. 


Determination of Pesticide Residues in Wine by SPME and 

GC/MS for Consumer Risk Assessment GC-MS 

in Wine Food Addit. Contam. 15 (3): 280-287 (1998) 

Vitali, M., Guidotti, M., Giovinazao, R., Cendrone, O. 

2611 Pesticide residue 

Removal of residual pesticides on vegetable using ozonated water 

Food Control (UK) 18, #5, 466-72 (May 2007) headspace GC-MS 

on vegetables Tiangang Luan; Gilbert Yuk Sing Chan; Jiguo Wu; Chongyu Lan; 

Thomas Wai Hung Lo 


Applications of SPME to the Analysis of 

Pesticide Residues in Vegetables 100µm PDMS, GC-ECD 

on vegetables Pest. Manag Sci 56: 618-636 (2000) 60µm Carbowax/DVB GC-NPD 

Volante, M.,Pontello, M., Volante, L. Cattaneo, M., Bianchi, M., 

Bianchi, M., Colzani, L. 

50 min 


Study on the method of SPME coupled to GC for 

determination of organophosphorus pesticide residue 

on vegetables in vegetables. 

Ziran Kexueban (2000) 39(4), 509-515 

Chen, W; Hou, X; Zhang, L; Lin, H; Pan, Ji 

432 Pesticides in 

Some Applications of SPME in the Analysis of 

Pesticide Residues in Food 

food J. Environ. Sci. Health, Part B (1998), B33 (3), 279-292 

Volante, M.,Cattaneo, M., Bianchi, M., Zoccola, G. 

(in Chinese) 

SPME of pesticide residues from strawberries 

461 Pesticides Food Addit. Contam. (1999), 16(3), 111-117 100µm PDMS 

on strawberries Hut, R., Henniont, B., Urrutyt, L., Monturyt, M. 45 min @ 25°C 

SPME coupled with HPLC: a complementry technique to SPME 

783 Pesticides GC for the analysis of pesticide residues in strawberries 60µm PDMS/DVB LC-UV 

on strawberries Food Addit. Contam. (2000), 17(11), 915-923 45 min @ 25°C 

Wang, Z.; Hennion, B.; Urruty, L.; Montury, M. headspace 

Analysis of carbamate and phenylurea pesticide residues in fruit 

2439 Pesticides in juices by SPME-LC-MS.Analysis of carbamate and phenylurea 50µm CW/TPR LC-MS 





fruit juices pesticide residues in fruit juices by SPME-LC-MS 60µm PDMS/DVB 

J. Chromatogr., A 1147, #2, 135-143 (2007-04-20) 

Sagratini, G.; Manes, J.; Giardina, D.; Damiani, P.; Pico, Y. 

90 min @ 20 C 


Fast screening of pesticide residues in fruit juice by SPME 

Food Chemistry 107, #3, 1314-1325 (2008) GC-MS 

fruit juices Cortes-Aguado, S.; Sanchez-Morito, N.; Arrebola, F. J.; 

Frenich, A. G.; Vidal, J. L. M 

10 min 


Screening method for the determination of parts per trillion levels 

of pesticide residues in vegetables combining SPME-GC-MS 65µm PDMS/DVB GC-MS 

vegetables Anal. Lett. 40, #13-15, 2886-2914 (2007-12) 10 min @ 20 C 

Cortes Aguado, S.; Sanchez-Morito, N.; Garrido Frenich, A.; 

Martinez Vidal, J. L.; 

immersed 

Validation of a SPME method for the 

462 Organophosphorus determination of organophosphorus pesticides 100µm PDMS GC-FPD 

pesticides in in fruits and fruit juice 3 min 

fruit/fruit juices J. Chromatogr. A (1999), 843(1), 35-42 immersed 

Simplicio, A, Vilas Boas, L. 

SPME-HPLC-MS applied to the analysis of insecticides in honey. 

2358 Insecticides in Food Addit Contam 25, #1, 59-69 (2008 Jan ) HPLC-MS 

honey Blasco, C; Font, G; Picoo, Y 

Determination of organophosphorus pesticides in honeybees 

929 Organophosphorus after solid phase microextraction 85µm Polyacrylate GC-NPD 

pesticides in J. Chromatogr. A (2001), 922(1-2) 257-265 45min @ 25°C 

honeybees Fernandez, M., Padron, C., Marconi, L., Colombo, R. Ghinie, S. immersed 

Sabatini, A, Girotti, S. stirred 

463 Organochlorine & 

A Systematic Approach to Optimize SPME 

determination of Pesticides in Ethanol/Water 

organophosphorus mixtures used as Food Simulates 

in water/ethanol Anal. Chem. (1999), 71(13), 2417-2422 

Batlle, R, Sanchez, C., Nerin, C. 

616 Volatiles 

Evidence for selectivity of absorption of volatile organics 

compounds by PDMS SPME fiber 30µm PDMS GC-MS 

in water J. Chromatogr. A,(2000) 885, 457-464 60min 

Niedziella, S., Rudkin, S., Cooke, M. headspace 


Analysis of Aroma Release During Microwave Heating 

J. Agric. Food Chem. 45 (11): 4388-4392 (1997) 60µm Carbowax/DVB GC-FID 

in water traps Roberts, D., Pollien, R. 10 min 


SPME Associated with Microwave Assisted Extraction of 

Food Products 

in food products J. High Resolut. Chromatogr. (1997), 20(4), 213-216 

Wang, Y., Bonilla, M., McNari, H., Khaled, M. 

immersion, stirring 

2400 1-naphthlamine 

Application of microwave-assisted desorption/headspace SPME as 

pretreatment step in the gas chromatographic determination of 65µm PDMS/DVB GC-FID 

from silica gel 1-naphthylamine in silica gel adsorbent 

Talanta 71, # , 1993-1997 (2007-03-30) 

Yan, C. T.; Jen, J. F.; Shih, T. S. 

headspace 


Analysis of volatile compounds of Iberian dry-cured loins with 

different intramuscular fat contents using SPME-DED headspace GC/MS 

dry-cured Meat Science 79, #1, 172-180 (MAY 2008) 


Effect of salt content and processing conditions on volatile compounds 

formation throughout the ripening of Iberian ham headspace GC/MS 

dry-cured Eur. Food Res. Technol. 225, #5-6, 677-684 (September 2007) 

Iberian ham Andres, Ana I.; Cava, Ramon; Muriel, Elena; Ruiz, Jorge; Ventanas, S. 

318 N-nitrosamines 

Rapid Semi-Quantitative Estimation of N-Nitrosodibulylamine 

and N-Nitrosodibenzylamine in Smoked Hams by SPME 85µm polyacrylate GC-thermal 





in smoked hams Followed by GC-Thermal Energy Analysis 10 min energy or MS 

J. Chromatogr. A 788(1+2): 131-140 (1997) headspace 

Sen, N., Seaman, S., Page, B. 

Application of spme for analysis of volatile flavors produced by 

stirring 

salt added 

2639 Volatiles from traditional fermented meat headspace GC/MS 

fermented meat J. Hunan Agric. Univ. (China) 33, #2, 232-4 (2007) 

Yu Bing; Zhou Hong-li; Li Zong-jun 

GC-MS techniques for characterization of meat products 

2234 Volatiles from Annu. Int. Meet., p 7271-7293 (2004) 75µm Carboxen GC/MS 

raw beef Balasubramanian, S.; Chen, Q.; Gu, H.; Jelen, H.; Logue, C.; headspace 

Marchello, M.; Nord, R.; Panigrahi,S. 


Application of SPME to the Analysis of Warmed 

Over Flavor in Beef 100µm PDMS GC-MS 

in beef Poster Paper, IFT 1999 35°C, 10 min 

Gruen, I., Fernando, L., Mobley, S. headspace 

890 Atrazine in 

Ethanol-modified subcritical water extraction combined 

with SPME for determining atrazine in beef kidney. 60µm Carbowax/DVB GC-MS 

beef J.Ag Food Chem (2001) 49(5) 2175-2180 

Curren, Meredith S. S.; King, Jerry 

30min @ 25°c 


Two-fiber SPME combined with GC-MS for the analysis of 

volatile aroma compounds in cooked pork Carboxen/PDMS. GC-MS 

in cooked pork J. Chromatogr. A 905(2000), 233-240 Carboxen/DVB/PDMS 

Elmore, J. Mottram, D., Hierro, E. 30 min @ 60°C 

618 Hexanal, pentanal 

A comparison of SPME fibers for measurement of hexanal 

and pentanal in cooked turkey Carboxen/DVB/PDMS 

20 min, headspace @ 

GC-FID 

in cooked turkey Food Chem Feb. 2000, 68(3), 339-345 

Brunton, N., Cronin, D, Durcan, R., Monahan, F. 

40°C 

924 Volatiles 

SPME as a tool for studying volatile compounds in frog skin 

Chemistry and Ecology 2000 

in frog skin Smith, B, Zini, C., Pawliszyn, J. Tyler, M., Hayasaka, Y, 

Williams, B., Caramao, E. 

423 Volatiles 

Comparison of Volatile Analysis of Lipid-Containing and 

Meat Matrices by SPME and SFE 

in meat ACS Symp. Ser. (1998), 705 (Flavor Analysis), 107-115 

Snyder, J., King, J., Zhang, Z. 

Mass spectrometry based sensor strategies for the authentication 

2826 Volatiles of oysters according to geographical origin GC-MS 

from oysters J Agric Food Chem, 56, #2, 321-327 (JAN 23 2008) 

Ratel, J.; Berge, Philippe; B., Jean-Louis; Cardinal, Mireille; Engel, E. 

Development of an SPME-GC-MS/MS procedure for the 

2892 2-phenoxyethanol monitoring of 2-phenoxyethanol in anaesthetised fish CAR/DVB 30/50 GC-MS 

in fish Talanta 75, #4, 1082-1088 (May 30 2008) headspace 

Hajslova, Jana; Klimankova, Eva; Kocourek, Vladimir; Kolarova, J.; 60 min at 30 °C 

Poustka, Jan; Riddellova, Katerina 

Fish and food safety: Determination of formaldehyde in 12 

2587 Formaldehyde fish species by SPME extraction and GC-MS analysis headspace GC-MS 

in fish FOOD CHEM. 100, #3, 1049-1053 (2007) pentafluorobenzyl 

Bianchi, F.; Careri, M.; Musci, M.; Mangia, A. hydroxyamine 

derivative 

Analysis of volatile compounds in bighead carp by microwave. 

2539 Flavor volaitles Distillation and SPME-GC-MS and olfactometry headspace GC-MS 

in carp fish Se Pu 25, #2, 267-71 (2007 Mar) 

Zhao, Qingxi; Xue, Changhu; Xu, Jie; Sheng, Wenjing; Xue, Yong; Li, Z. 





New method for the rapid determination of volatile 

786 Volaitle amines substances: The SPME-direct method. Part II. Determination GC-FID, NPD 

in fish of the freshness of fish 

Sens Actuators, B Chem (2001) 72(3), 204-207 headspace 

Bene, A.; Hayman, A.; Luisier, J.L.; Reynard, E.; Villettaz, J 

SPME-GC-MS integrated with chemometrics for detection of 

2468 Volatiles from Salmonella typhimurium contamination in a packaged fresh vegetable headspace GC-MS 

salmonella Anal. Chim. Acta 581, #1, 63-70 (2 Jan. 2007) 

infected 

alfalfa sprouts 

Siripatrawan, Ubonrat; Harte, Bruce R 

SPME/GC of Salmonella-Infected Beef 

619 Volatiles from J Agric Food Chem, 2000, 48, 2253-2259 75µm Carboxen/PDMS GC-FID 

salmonellas infected Ogihara, H., Horimoto, Y., Hai, Z., Skura, B., Nakai, S. 10 min 

beef 

Use of Digital Aroma Technology and SPME GC-MS to 

25% NaCl 

393 Volatiles from compare Volatile compounds Produced by Bacteria 100µm PDMS GC-MS 

processed poultry isolated from Processed Poultry 30 min @ 37°C 

J. Sci. food Agric. 1998, 78, 343-348 headspace 

Arnold, J., Senter, S. stirred 

862 Allyl isothiocyanate 

Formation of allyl isothiocyanate from sinigrin in the 

digestive tract of rats monoassociated with a human colonic GC-MS 

in rats strain of Bacteroides thetaiotaomicron 

FEMS Microbiology Letters (2001) 197(1) 99-103 

Rabot, S; Duguay, A; Elfoul, L; Khelifa, N; Quinsac,A; Rimbault, A 

headspace 

253 Putrescine, 

An Electrodeposition Device for the Determination of 

Putrescine and Cadaverine by High-Resolution GC carbon fibers HPLC 

cadaverine in J. High Resolut. Chromatogr. 19 (5): 294-297 (1996) 0-60 min, immersion (C18 column) 

borate buffer solution Conte, E., Miller, D. 

Measurement of volatile oxidation products from milk using . 

stirring 

pH 8 

2727 Oxidative products solvent-assisted flavour evaporation and SPME headspace GC-MS 

from milk Intl Dairy Journal 17, #7, 746-752 (2007) 

Havemose, M. S.; Justesen, P.; Bredie, W. L. P.; Nielsen, J. H. 

40°C 

620 Hexanal, pentanal 

Shelf-life prediction of processed milk by SPME -MS and 

multivariate analysis 75µm Carboxen/PDMS GC-MS 

metabolites in milk J. Agric Food chem (2000), 48(8), 3470-3475 20min. @ 50°C 

Marsili, R. headspace 

Comparison of SPME and Dynamic Headspace Methods for 

386 Oxidative byproducts the GC-MS Analysis of Lighted Induced Lipid Oxidation 75µm Carboxen/PDMS GC-MS 

in milk Products in Milk 45°C, 15 min 

J. Chromatogr. Sci. 1999, 37, 17-23 headspace 

Marsili, R. salt added 

Influence of flavor variability in skim milk powder on consumer 

2274 Off-flavors acceptability of ingredient applications headspace GC/MS 

in skim milk powder J Food Science 70 #7, S427-S431 (2005) 

Caudle, Alissa D.; Yoon, Youngmo; Drake, Maryanne 

Quantitative determination of thermally derived off-flavor 

2301 Off-flavor compounds in milk using SPME-GC headspace GC/MS 

compounds J Dairy Science 88 #11, 3764-3772 (2005) 

in milk Vazquez-Landaverde, P. A.; Velazquez, G.; Torres, J. A.; Qian, M. 

372 Off-flavors 

SPME-MS-MVA as an Electronic Nose for the Study of 

Off-Flavors in Milk 75µm Carboxen/PDMS GC-MS 

in milk J. Agric. Food Chem. 1999, 47, 648-654 45°C, 12 min 

Marsili, R. headspace 

2627 Volatile flavors 

Research advances: Squeezing more shelf life out of milk 

J Chem Educ 84, #4, 572-574 (April 2007) headspace GC/MS 

in milk King, Angela G. 





2148 Odors from 

Removal of odours from milk prepared from peanut 

J Food Sci Technol, 43, #2, 205-209 (2006) headspace GC/MS 

peanut milk 

powder 

Bangoura, Mamadouba; Nong, Zhang Guo 

SPE/SPME-GC/MS approach for measuring musk compounds in . 

2369 Musk compounds serum and breast milk GC/MS 

in breast milk Food Chemistry 102, #4,1156-1162 ( 2007 ) 

Ho, C. W.; Aida, W. M. Wan; Maskat, M. Y.; Osman, H. 

621 Chlorinated organics 

Application of SPME for the rapid analysis of chlorinated 

organics in breast milk GC-ECD 

in breast milk Fresenius, J. Anal.Chem, Jan 2000, 366(1), 106-111 

Rohrig, L., Meisch, H. 

749 Acetaldehyde 

Flavor threshold for acetaldehyde in milk, chocolate milk, and 

spring water using SPME-GC for quantification 75µm Carboxen/PDMS GC-FID 

in milk & water J.Agric.FoodChem 2001, 49(3), 1377-1381 45°C, 15 min 

vanAardt, M., Duncan, S., Bourne, D., Marcy, J., Long, T., headspace 

Hackney, C., Heisey, C., salt added 

364 Off-flavors 

Off Flavor and Malodors in Food: Mechanism of Formation 

and Analytical Techniques various fibers GC 

in food Book-Techniques for Analyzing Food Aroma, 

Marcel Decker ISBN: 0-8247-9788-4 

Marsili, R. 

and conditions 

376 Volatile metabolites 

Evaluation of SPME for Analysis of Volatile Metabolites 

Produced by Staphylococci 85µm polyacrylate GC-FID 

in water J. Agric. Food Chem. 1998, 46, 228-234 80°C, 15 min 

Vergnais, L., Masson, F., Montel, M., Berdague, J., Talon, R. headspace, stirring 

365 Volatiles 

Determination of Volatile Organic Compounds in Tea 

Industrie de la Bevande XXVI (1997) febbralo, 19-22 100µm PDMS GC-MS 

in tea Guidotti, M. 

Analysis of vitamin K in green tea leafs and infusions by SPME-GC-FID 

50°C, 15 min 

headspace 

2699 Vitamine K from FOOD CHEM. 100, #1, 405-411 (2006) 7µm PDMS GC-FID 

green tea leafs Reto, M.; Figueira, M. E.; Filipe, H. M.; Almeida, C. M. M. immersion 

40°C, 45 min 


Application of head-space SPME coupled to comprehensive 

two-dimensional GC-TOF-MS for the determination of multiple headspace GC-TOF-MS 

tea samples pesticide residues in tea samples 

Analytica Chimica Acta 611, #2, 163-172 (MAR 24 2008) 

Schurek, J.; Portoles, T.; Hajslova, J.; Riddellova, K.; Hernandez, F. 

2378 Aromatic 

Analysis of aromatic components in Wuzi green tea by SPME/GC/MS 

Xibei Zhiwu Xuebao 27, #2, 371-376 ( FEB 2007) GC-MS 

compounds Liu La-ping; Shi Ya-ge; Zhang Rui-ming; Li Lan; Yang Rong 

in green tea in Chinese 

622 Polyphenols 

Comparative Study and Partial characterization of Azorean 

green Tea Polyphenols 

in green tea J. Food Compos. Anal. (1999), 12(4), 273-287 

Baptista, J., da P Tavares, J., Carvalho, R. 

319 Caffeine 

Quantitative Determination of Caffeine in Beverages, 

Using a Combined SPME-GC-MS Method bare fiber GC-MS 

in tea, coffee J. Chem. Educ. 74 (9): 1130-1132 (1997) 

Yang, M., Orton, M., Pawliszyn, J. 


Characterization of Roasted Coffee and Coffee Beverages 

by SPME-GC and Principal Component Analysis 100µm PDMS, GC-MS 

in coffee J. Agric. Food Chem. 1997, 45: 4680-4686 7µm PDMS 





Bicchi, C., Panero, O., Pellegrino, G., Vanni, A. 

Obtention of a Brewed Coffee Aroma Extract by an 

60°C, 5 min 

headspace 

302 Volatile aroma Optimized Supercritical CO2-Based Process 100µm PDMS GC-MS 

in brewed coffee J. Agric. Food Chem. 1998, 46, 4011-4016 60°C, 10 min 

Ramos, E., Valero, E., Ibanez, E., Reglero, G., Tabera, J. headspace 


SPME Method Development for Headspace analysis of 

volatile flavor compounds PDMS/DVB GC-MS 

in coffee J. Agri. Food Chem 2000, 48, (6) 2430-2437 60 min headspace 

Roberts, D., Pollien, P., Milo, C. pH 2 

Screening for 2-Acetyl-1-pyrroline in the Headspace of Rice 

624 2-Acetyl-1-pyrroline using SPME/GC-MS 

80µm 

Carboxen/DVB/PDMS GC-MS 

in rice J. Agric. Food Chem 2001, 49, 245-249 80°C, 15 min 

Grimm, C, Bergman, jC., Delgado, J., Bryant, R. 

Removal of geosmin and 2-methylisorboneol (2-MIB) in water from 

headspace 

.75gm in 100µl H20 

2642 2-MIB, geosmin Zuikerbosch Treatment Plant (Rand Water) using β-cyclodextrin headspace GC-MS 

in water polyurethanes 

Water SA 33, #2, 223-227 (April 2007) 

Krause, R.; Malefetse, T.; Mamba, B.; Mhlanga, S.; Nxumalo, E.; 

Salipira, K.L.; Sithole, S. 

Microwave mediated distillation with SPME 

464 2-MIB, geosmin determination off-flavors, geosmin and 100µm PDMS GC-MS 

in water methylisoborneol, in catfish tissue 25 min 

J. Chromatogr. A (1999), 833(2), 223-230 immersed 

Zhu, M., Aviles, F., Conte, E., Miller, D., salt added 

Perschbacher, P. 

Microwave Distillation-SPME-GC Analysis of 

625 2-MIB, geosmin 2-methylisoboreneol and Geosmin in Catfish 

80µm 

Carboxen/DVB/PDMS GC-IC-MS 

in water Am-Lab Feb 2000: 32(3), 40-48 60°C, 20 min 

Lloyd, S., Grimm, C. heaspace 

Analysis of 2-Methylisoboreneol and Geosmin in Catfish 

2-MIB, geosmin by Microwave Distillation-SPME 100µm PDMS GC-MS 

in water J. Agri. Food Chem., 47, No. 1, pg. 164-169, 1999 40°C, 15 min 

Lloyd, S., Grimm, C. saturated salt 

stirring 

362 MIB & geosmin 

Determination of Geosmin and 2-Methylisoboreneol in Water 

Using SPME and GC-Chemical Ionization/Electron Impact Carboxen/DVB/PDMS GC-MS 

in water Ionization Ion Trap MS 60°C, 30 min 

Analyst (Cambridge, U.K.) (1998), 123 (10), 2155-2160 headspace 

McCallum, R., Pendleton, P., Scumann, R., Trinh, M. stirring 

salt added 

2429 MTBE in 

Evaluating peats for their capacities to extract methyl tertiary 

butyl ether from contaminated water using SPME-GC headspace GC-MS 

drinking water J Environ Sci Health A 43, #2, 132-43 (2008 Feb) 

Rizzuti, Anthony M; Cohen, Arthur D; Nguyen, Dung D 

Evaluating peats for their capacities to extract methyl tertiary 

2871 MTBE in butyl ether from contaminated water using SPME-GC headspace GC-MS 

drinking water J EnviSci and Health Part A 43, #6, 672-673 (2008) 

Rizzuti, Anthony 

Evaluation of zeolite for control of odorants emissions from 

2531 VOCs from simulated poultry manure storage headspace GC-MS 

poultry manure J. ENVIRON. QUAL. 36, #1,184-193 (2007) 

Cai, L.; Koziel, J. A.; Liang, Y.; Nguyen, A. T.; Xin, H. 

Evaluating Peats for their capacities to remove 

465 C2-C10 acid, odorous compounds from liquid swine manure 85µm polyacrylate GC-MS 

aldehydes, phenols using headspace SPME 20 min @ 72°C 





in swine manure J. Environ. Sci.Health, B34(4), 709-748 (1999) headspace, pH 2 

Rizzuti, A., Cohen, A., Hunt, P., Vanotti, M. 

Headspace-SPME-GC as a tool to define an index that establishes the 

2722 Ethyl esters retention capacity of the wine polymeric fraction towards ethyl esters headspace GC 

in wine J.Chromatogr. A 1150, #1-2, 155-161 (2007) 

Rocha, S. M.; Coutinho, P.; Delgadillo, I.; Coimbra, M. A. 

Analysis of esters in wines 

966 Esters in wine J.Chromatogr. A (2002) 963(1-2), 213-223 Various GC 

Rodriguez-Bencomo, J.J.; Conde, J.E.; Rodriguez-Delgado, M.A.; Garcia- 

Montelongo, F.; Perez-Trujillo, J.P. 

Flavor and odor differences between fresh and preserved onions 

967 Aroma in onions J.Chromatogr. A (2002) 963(1-2), 89-93 Polyacrylate GC-MS 

Mondy, N.; Duplat, D.; Christides, J.P.; Arnault, L.; Auger, J. 

Influence of crushing technique on composition of volatiles in olive oil 

968 Volatiles in olive oil European Journal of Lipid Science and Technology (2002) 104(8), 483-489 65 um Carbowax/DVB GC-MS 

Servili, M.; Piacquadio, P.; de Stefano, G.; Taticchi, A.; Sciancalepore, V. 30 mins. 

Monitoring volatile compounds during the dry-cured ham ripening process 

969 

Volatiles in dry-cured 

ham J.Chromatogr. A (2002) 963(1-2), 83-88 

Andres, A.I.; Cava, R.; Ruiz, J. 

Bisphenol type contaminants from food packaging materials in aqueous foods. 

970 

Bisphenol in food 

packaging J.Chromatogr. A (2002) 963(1-2), 375-380 

Nerin, C.; Philo, M.R.; Salafranca, J.; Castle, L. 

HPLC 

992 

996 

Development of headspace SPME, GC-MS method for the identification of 

odour causing volatile compounds in packaging materials. 

Odour compounds in 

food packaging 

materials J.Chromatogr. A (2002) 963(1-2), 381-392 75 um carboxen/PDMS GC-MS 

Ezquerro, O.; Pons, B.; Tena, M.T. 

Response surface models used for prediction of photooxidative quality changes 

of havarti cheese. 

Photooxidative quality 

changes of havarti 

cheese. European Food Research and Technology (2003) 216 (2), 93-98. GC-MS 

Stapelfeldt, Henrik; Mortensen, Grith; Sorensen, John. 

Solid phase micro-extraction technique and its applications in medical analysis. 

997 Yaoxue Xuebao (2003) 38 (2), 153-158. 

Liu Zhen-ling; Wu Cai-ying. 

999 

Volatile compounds recovered by solid-phase microextraction from fresh 

adductor muscle and total lipids from sea scallop ( Placopecten magellanicus ) 

from Georges Bank (Nova Scotia). 

Volatile compounds 

from scallops Journal of Food Science (2002) 67 (6), 2032-2037. PDMS/DVB GC-MS 

Linder, M.; Ackman, R. G. 250 C, 2 minutes 

Headspace solid-phase microextraction in combination with gas 

chromatography-mass spectrometry for the rapid screening of 

organophosphorus insecticide residues in strawberries and cherries 

1007 Insecticides in fruit J.Chromatogr. A (2003) 993(1-2), 197-203. GC-MS 

Albanis, Triantafyllos A.; Lambropoulou, Dimitra A. 

Solid phase microextraction capillary gas chromatography combined with 

furnace atomization plasma emission spectrometry for speciation of mercury in 

fish tissues 

1012 Mercury in fish Spectrochmica Acta - Part B Atomic Spectroscopy (2003) 58 (3), 427-441. GC-FAPES 

Campos, Reinaldo C.; Grinberg, Patricia; Mester, Zoltan; Sturgeon, Ralph E. 





Headspace volatiles of Scutellaria californica A. Gray flowers 

2781 Volatiles in J. Essent. Oil Res. 20, #2, 169-171 (March/April 2008) headspace GC-MS 

gray flowers Dao, Lan; Patterson, Robert; Rodriguez, David; Takeoka, G. 

Analysis of the volatile compounds of flowers and essential 

2768 Volatiles in oils from Lavandula angustifolia cultivated in northeastern Italy Carboxen/DVB GC-MS 

lavender flowers by headspace SPME -GC-MS headspace 

Planta Medica 74, #2, 182-187 (FEB 2008) 50 min. 

Da Porto, Carla; Decorti, Deborha 

Use of SPME as a sampling technique for the characterization of 

2470 Volatiles in volatile compounds emitted from Chinese daffodil flowers. headspace GC-MS 

daffodil flowers. J. Anal. Chem. (Transl. Zh. Anal. Khim.) 62, #7, 674-679 (2007-07) 

Song, G.; Xiao, J.; Deng, C.; Zhang, X.; Hu, Y. 

Volatile constituents of the leaves and flowers of Hypericum triquetrifolium Turra 

1016 Volatiles in flowers Flavour and Fragrance Journal (2003) 18 (2), 91-94. GC-MS 

Bertoli, Alessandra; Mazzetti, Michele; Menichini, Francesco; Morelli, Ivano; 

Spinelli, Guido 

Evolution of volatile byproducts during wine fermentations using immobilized 

cells on grape skins. 

Volatile byproducts in 

1017 wine Journal of Agricultural and Food Chemistry (2003) 51 (8), 2402-2408. 

Komaitis, Michael; Kanellaki, Maria; Koutinas, Athanasios; Mallouchos, 

Athanasios 

Analysis of terpenoids from hemlock (Tsuga) species by solid-phase 

microextraction/gas chromatography/ion-trap mass spectrometry. 

Terpenoids from 

1018 hemlock Journal of Agricultural and Food Chemistry (2003) 51 (8), 2115-21120. 

Lagalante, Anthony F.; Montgomery, Michael E. 

GC-MS 

Volatile components associated with freshly cooked and oxidized off-flavours in 

turkey breast meat. 

1027 Volatiles from meats Flavour and Fragrance Journal 2002) 17 (5), 327-334. GC-MS 

Brunton, N. P.; Cronin, D. A.*; Monahan, F. J. 

Analysis of volatile and semivolatile composition in cut tobacco and total 

particulate matter of cigarettes with SPME-GC-MS. 

Volatiles and semi- 

1044 volatile in cigarettes. Fenxi Shiyanshi (2002) 21 (5), 31-35. 

Li, R.; Wang, L.; Li, Q.; Tong, X. D. 

85 um Polyacrylate GC-MS 

Survey of 2-ethylhexanoic acid in baby food 

2376 2-ethylhexanoic Food Additives and Contaminants 24, #7, 792-797 (JUL 2007) 

acid in baby food Ezerskis, Z.; Pastorelli, S.; Contini, C.; Simoneau, C. 

1052 

Comparison of mass spectrometry-based electronic nose and solid phase 

microextraction gas chromatography-mass spectrometry technique to assess 

infant formula oxidation. 

Oxidation of infant 

formula Journal of Agricultural and Food Chemistry (2003) 51 (9), 2790-2796. GC-MS 

Guy, Philippe A.; Fenaille, Francois; Fumeaux, Rene; Milo, Christian; Visani, 

Piero 

Formation of aroma compounds from ribose and cysteine during the maillard 

reaction. 

1053 Aroma compounds Journal of Agricultural and Food Chemistry (2003) 51 (9), 2714-2721. GC-MS 

Cerny, Christoph; Davidek, Tomas 

A headspace-SPME-MS method for monitoring rapeseed oil autoxidation 

2497 Volatile compounds J Am Oil Chemists' Society 84, #6, 509-517 (JUN 2007) headspace GC-MS 

rapeseed oil Jelen, H. H.; Mildner-Szkudlarz, S.; Jasinska, I.; Wasowicz, E 

Solid-phase microextraction for studies on the enantiomeric composition of 

filbertone in hazelnut oils. 

1055 Volatile compounds Journal of Agricultural and Food Chemistry (2003) 51 (9), 2496-2500. 

hazelnut oil. Ruiz del Castillo, M. L.; Blanch, G. P.; Flores, G.; Herraiz, M. 




Matrix 


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Simultaneous headspace SPME analysis of off-flavour compounds 

from Quercus suber L. cork. headspace GC-MS 

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Neto, P. V.; Rocha, S. M.; Silvestre, A. J. D. 

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Fast and sensitive method to determine chloroanisoles in cork using 

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Optimization of headspace sampling using solid-phase microextraction for 

chloroanisoles in cork stoppers and gas chromatography-ion-trap tandem mass 

spectrometric analysis. 

Chloroanisoles from 

1065 cork. Journal of Separation Science (2003) 26 (5), 369-375. 

Musci, Marilena; Bianchi, Federica; Careri, Maria; Mangia, Alessandro 

75 um Carboxen/PDMS GC-MS-MS 

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Volatile free fatty acids 

in ewe cheese. Analytical Chemistry (2002) 74 (20), 5199-5204. 

Pinho, O.; Ferreira, I. M. P. L. V. O.*; Ferreira, M. A. 

85 um polyacrylate GC-MS 

Determination of pyrimethanil and kresoxim-methyl in green groceries by 

headspace solid-phase microextraction and gas chromatography-mass 

spectrometry. 

Pyrimethanil and 

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green groceries. Journal of Chromatography, A (2002) 975 (2), 355-360. 

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Distribution of aroma volatile compounds in different parts of mango fruit. 

Aroma compounds in 

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Singh, Zora; Lalel, H. J. D.; Tan, S. C. 

GC-MS 

Identification of odors from overripe mango that attract vinegar flies, Drosophila 

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Odors from overripe 

1081 mango. Journal of Chemical Ecol (2003) 29 (4), 899-909. 

Zhu, Junwei; Baker, Thomas C.; Park, Kye-Chung 

GC-EAD 

1083 Methyl jasmonate 

Prediction correlation of vapor pressure for methyl jasmonate 

Journal of Food Engineering (2003) 59 (4), 431-433. 

Acevedo, C.; Sanchez, E.; Simpson, R.; Young, M.E. 

GC-MS 

Analysis of volatile chemical composition in mulberry leaves using 





2545 Volatiles from microwave assisted extraction associated with SPME headspace GC-MS 

mulberry leaves Chemistry and Industry of Forest Products 27, #3, 107-110 (2007) 

Li JieHong; Chen DaiWu 

2436 Fenitrothion in 

Quantification of fenitrothion and its main metabolites in poplar leaves 

by isotope dilution GC-MS coupled with SPME GC-MS 

poplar leaves J. Chromatogr. A 1177, #1, 170-174 (Jan 4 2008) 

Barrio, R.; Goicolea, M.; Millan, S.; Rodriguez, E.; Sampedro, M.; 

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Changes in volatile compounds of small gamma -irradiated fresh cilantro leaves 

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1085 from cilantro Journal of Agricultural and Food Chemistry (2002) 50 (26), 7622-7626. 

Fan, X. T.; Sokorai, K. J. B. 

GC-MS 

1086 Ethanol in Tequila 

Tequila authenticity assessment by headspace SPME-HRGC-IRMS analysis of 

carbon-13/carbon-12 and oxygen-18/oxygen-16 ratios of ethanol. 

Journal of Agricultural and Food Chemistry (2002) 50 (26), 7520-7523. GC-MS 

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Aguilar-Cisneros, B. O.; Lopez, M. G.; Richling, E.; Heckel, F.; Schreier, P. * 

Survey on the presence of butyltin compounds in Chinese alcoholic beverages, 

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chromatography-flame photometric detection. 

Butyltin compounds in 

alcoholic beverages Journal of Agricultural and Food Chemistry (2002) 50 (23), 6683-6687. 

Liu, J. Y.; Jiang, G. B.* 

GC-MS 

Synthesis and stable isotope dilution assay of ethanethiol and diethyl disulfide 

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Ethanediol and diethyl 

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Majcenovic, A. B.; Schneider, R.; Lepoutre, J. -P.; Lempereur, V.; Baumes, R. * 

Differential effects of tomato ( Lycopersicon esculentum Mill) matrix on the 

volatility of important aroma compounds. 

Aroma compounds 

1089 from tomatoes. Journal of Agricultural and Food Chemistry (2003) 51 (3), 722-726. 

Bezman, Y.; Mayer, F.; Takeoka, G. R.; Buttery, R. G.; Ben-Oliel, G.; 

Rabinowitch, H. D.; Naim, M. 

Stale flavour volatiles in Australian commercial UHT milk 

2246 Flavour volatiles during storage headspace GC-FiD 

in milk Australian J Dairy Technology 60, #3, 231-237 (2005) 

Perkins, M.; Elliott, A.; D'Arcy, B.; Deeth, Hilton C. 

Volatile fraction of milk: comparison between purge and trap and solid phase 

microextraction techniques. 

1090 Volatile fraction of milk Journal of Agricultural and Food Chemistry (2002) 50 (25), 7350-7355. 

Contarini, G.; Povolo, M. 

SPME applied to the study of volatile organic compounds emitted by three 

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1091 eucalyptus. Journal of Agricultural and Food Chemistry (2002) 50 (25), 7199-7205. 

Zini, C. A.; Augusto, F.; Christensen, E.; Caramao, E. B.; Pawliszyn, J. * 

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1105 Volatiles in mango 

Headspace solid-phase microextraction and gas chromatography-mass 

spectrometry analysis of free volatile compounds in Mango. 

Chromatographia (2002) 55(11-12), 737-741 

Shang, C. Q.; Deng, C. H.; Zhang, X. Y.; Chen, Z. F.; Hu, Y. M. 

GC-MS 

Optimization of headspace SPME-GC-AED analysis 





2524 Methylmercury of monomethylmercury 65 µm PDMS/DVB GC-AED 

J Chromatogr A 1174, #1-2, 7-12 (2007 Dec 7) 100 µm PDMS 

Geerdink, Renoe Bernard; Breidenbach, Rembert; Epema, O. 

Certification of methylmercury content in two fresh-frozen 

NaBPh4 derivative 

headspace 

2612 Methylmercury reference materials: SRM 1947 Lake Michigan fish tissue and 100 µm PDMS GC-MS 

in mussel tissue SRM 1974b organics in mussel tissue (Mytilus edulis). NaBPh4 derivative GC-ICP-MS 

Anal Bioanal Chem 387, #7, 2335-41 (2007 Apr) 

Davis, W .; Christopher, S.; Pugh, R.; Donard, O.; Krupp, E.; Point,D.; 

Horvat, M.; Gibicar, D; Kljakovic-Gaspic, Z; Porter, B.; Schantz, M. 

headspace 

2676 Methylmercury 

Comparison of extraction procedures for methylmercury 

determination by a SPME-GC-AFS system immersion GC 

in marine fish Microchemical Journal 85, #1, 122-126 (JAN 2007) 

Abranko, Laszlo; Kmellar, Bela; Fodor, Peter 

SPME-GC-pyrolysis-AFS determination of methylmercury in 

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2286 Methylmercury marine fish products by alkaline sample preparation and aqueous immersion GC 

in marine fish phase phenylation derivatization 

J Ag Food Chem 53, #14, 5499-5505 (2005) NaBPh4 

Jokai, Zsuzsa; Abranko, Laszlo; Fodor, Peter derivative 

Determination of methylmercury in fish tissues by isotope dilution SPME-GC- 

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1106 Methylmercury in fish. Journal of Analytical Atomic Spectrometry (2003) 18 (5), 431-436. 

Mester, Zoltan; Sturgeon, Ralph E.; Yang, Lu 

PDMS GC-ICP-MS 

2444 Acetates in wine 

GC-MS determination of 3-mercaptohexan-1-ol and 3-mercaptohexyl 

acetate in wine: A comparison of headspace SPME and 

solid phase extraction methods 

Anal. Chim. Acta 596, #2, 291-297 (2007-07-23) 

Fedrizzi, B.; Versini, G.; Lavagnini, I.; Nicolini, G.; Magno, F. 

headspace GC/MS 

Determination of major compounds in sweet wines by headspace solid-phase 

microextraction and gas chromatography. 

Alcohols, acetates in 

1127 sweet wines. Journal of Chromatography, A (2003) 991 (1), 13-22. 

Rodriguez-Bencomo, J. J.; Conde, J. E.; Garcia-Montelongo, F.; Perez-Trujillo, 

J. P.* 

GC 

Detection of 2-aminoacetophenone off-flavor in wine by SPME- 

2226 Off-flavors and SIM GC-MS headspace SIM GC-MS 

in wine American Journal of Enology and Viticulture 56 #3, 302A (2005) 

Qian, Michael; Fan, Wenlai 

Determination of 2,4,6-trichloroanisole in wines by headspace solid-phase 

microextraction and gas chromatography-electron-capture detection. 

2,4,6-trichloroanisole in 

1128 wine. Journal of Chromatography, A (2002) 977 (1), 1-8. 

Riu, M.; Mestres, M.; Busto, O. *; Guasch, J. 

GC-ECD 

Contribution to the characterisation of wines from the grape 

2312 Volatiles from cultivars 'Rotgipfler' and 'Zierfandler' from the winegrowing headspace GC/MS 

wine region Thermenregion in Austria. 

Mitteilungen Klosterneuburg 55 #5-6, 129-139 (2006) (German) 

Flak, W.; Krizan, Rudolf; Sturm, Paul; Tscheik, Gabriele; Wallner, Erich 


Analysis of volatile composition of siriguela (Spondias purpurea L.) 

by SPME DVB/CAR 50/30µm 

siriguela fruit Food Sci. Technol. 39 #4, 436-442 (2006) 

Antunes, O.; Bizzo, H.; Carvalho, C.; Ceva-Antunes, P.Silva, A. 

1129 VOC's in fruit 

Analysis of volatile compounds of tapereba ( Spondias mombin L.) and caja ( 

Spondias mombin L.) by simultaneous distillation and extraction (SDE) and 

solid phase microextraction (SPME). 

Journal of Agricultural and Food Chemistry (2003) 51 (5), 1387-1392. 

Ceva-Antunes, P. M. N.; Bizzo, H. R.; Alves, S. M.; Antunes, O. A. C.* 

DVB/CAR/PDMS 





Volatile organic compounds in human milk: methods and measurements 


2353 Volatile organics Envl Sci & Tech 41, # 5, 1662-1667 (2007) headspace GC/MS/SIM 

in human milk Kim, S. R.; Halden, R. U.; Buckley, T. J. 

Study of light-induced volatile compounds in goat apostrophe s milk cheese. 

Volatile compounds in 

1130 goat's milk cheese. Journal of Agricultural and Food Chemistry (2003) 51 (5), 1405-1409. 

Kim, G. Y.; Lee, J. H.; Min, D. B.* 

GC-MS 

Optimization of solid phase microextraction analysis for the headspace volatile 

compounds of Parmesan cheese. 


1131 parmesan cheese. Journal of Agricultural and Food Chemistry (2003) 51 (5), 1136-1140. 

Lee, J. H.; Diono, R.; Kim, G. Y.; Min, D. B.* 

Influence of bleaching by ultrasound on fatty acids and minor 

2877 Aroma volatiles compounds of olive oil. Qualitative and quantitative analysis headspace GC/MS 

in olive oil of volatile compounds (by SPME coupled to GC/MS) 

Ultrason. Sonochem. 15, #4, 590-597 (April 2008) 

Adams, A.; De Kimpe, N.; Frikha, M.H.; Jahouach-Rabai, W.; 

Trabelsi, M.; Van Hoed, V.;Verhe, R. 

2841 Volatile from 

Characterization of monovarietal virgin olive oils from six 

crossing varieties headspace GC/MS 

virgin olive oil. Scientia Horticulturae (Amsterdam) 115, #3, 252-260 (FEB 1 2008) GC/FID 

Manai, H.; Mahjoub-Haddada, F.; Oueslati, I.; Daoud, D.; Zarrouk, M. 


Application of SPME to the analysis of volatile compounds in virgin 

olive oils from five new cultivars. headspace GC/MS 

virgin olive oil. Food Chemistry 102, #3, 850-856 (2007) 

Baccouri, B.; Temime, S.; Campeol, E.; Cioni, P.; Daoud, D.; Zarrouk, M. 


Characterization of virgin olive oil from Southern Tunisia 

European J. Lipid Science and Tech. 110, #1, 81-88 (JAN 2008) headspace GC/MS 

virgin olive oil. Zarrouk, W.; Haddada, F.; Baccouri, B.; Oueslati, I.; Taamalli, W.; 

Fernandez, X.; Lizzani-Cuvelier, L.; Daoud, D.; Zarrouk, M. 


Profiles of volatile compounds from some monovarietal Tunisian 

virgin olive oils. Comparison with French PDO headspace GC/MS 

virgin olive oil. Food Chemistry 103, #2, 467-476 (2007) 

Haddada, F.; Manai, H.; Daoud, D.; Fernandez, X.; Zarrouk, M. 

Lizzani-Cuvelier, L.; 

GC-FID 

Volatiles from leaves, fruits, and virgin oil from Olea europaea cv. Olivastra 

Seggianese from Italy. 

Volatile from virgin olive 

1132 oil. Journal of Agricultural and Food Chemistry (2003) 51 (5), 1382-1386. 

Flamini, G.; Cioni, P. L.; Morelli, I. 

2325 Hexanal in beef 

Accurate determination of hexanal in beef bouillons by headspace 

SPME-GC-MS headspace GC/MS 

bouillons European J Lipid Sci Technology 107 #11, 792-798 (2005) 

Giuffrida, F.; Golay, P.; Destaillats, F.; Hug, B.; Dionisi, F. 

Quantitation of hexanal by automated SPME for studying dietary influences on 

the oxidation of pork. 

1140 Hexanal from pork. Journal of Food Composition and Analysis (2003) 16 (2), 179-188. Carboxen/PDMS GC 

Grun, Ingolf U.; Berg, Eric P.; Fernando, Lakdas N. 

Aroma compound analysis of Piper nigrum and Piper guineense essential oils 

from Cameroon using solid-phase microextraction-gas chromatography, solidphase 

microextraction-gas chromatography-mass spectrometry and 

olfactometry. 

Aroma compounds 

1145 from pepper. Journal of Chromatography, A (2002) 976 (1-2), 265-275. 

Jirovetz, L.; Buchbauer, G.; Ngassoum, M. B.; Geissler, M. 

GC-MS 





Experimental and modelling studies showing the effect of lipid type and level on 

flavour release from milk-based liquid emulsions. 

1146 Flavours from milk Journal of Agricultural and Food Chemistry (2003) 51 (1), 198-195. GC-MS 

Roberts, D. D.; Pollien, P.; Watzke, B. 

Headspace solid-phase microextraction method for the study of the volatility of 

selected flavour compounds. 

Volatile flavor 

1147 compounds Journal of Agricultural and Food Chemistry (2003) 51 (1), 200-205. 

Jung, D. M.; Ebeler, S. E.* 

GC-MS 

Comparison of comprehensive two-dimensional GC-TOF-MS and 

2338 Volatiles from GC-MS for the qualitative characterisation of roasted barley by SPME headspace GC-TOF-MS 

roasted barley J. Sep. Sci. 30 #4, 527-533 (2007-03 ) 

Bianchi, F.; Careri, M. ; Conti, C.; Musci, M.; Vreuls, R. 

Analysis of volatile compounds from various types of barley cultivars 

2302 Volatiles from J Ag Food Chem 53, #19, 7526-7531 (2005) headspace GC/MS 

barley flour Cramer, A.; Mattinson, D.; Fellman, J.Baik, B. 

Optimisation of HS-SPME to study representativeness of partially 

2584 Aroma volatiles baked bread odorant extracts 75µm Carboxen GC 

from baked Food Research Intl. 40, #9, 1170-1184 (2007) 65µm PDMS/DVB 

breads Poinot, P.; Grua-Priol, J.; Arvisenet, G.; Rannou, C.; Semenou, M.; headspace 

Le Bail, Al.; Prost, C. 30 min @ 35°C 

Evolution of aroma volatiles during storage of sourdough breads made 

2420 Aroma volatiles by mixed cultures of Kluyveromyces marxianus and Lactobacillus headspace GC/MS 

from sourdough delbrueckii ssp. bulgaricus or Lactobacillus helveticus 

breads FOOD CHEM. 107, #2, 883-889 (15 MAR 2008) 

Plessas, S.; Bekatorou, A.; Gallanagh, J.; Nigam, P.; Koutinas, A.; 

Psarianos, C 

Effect of carrot (Daucus carota) antifreeze proteins on texture 

2760 Aroma volatiles properties of frozen dough and volatile compounds of crumb headspace GC/MS 

in bread crumbs Food Sci. Technol. 41, #6, 1029-1036 (July 2008) 

Guo, Xiaona; Wang, Li; Zhang, Chao; Zhang, Hui 

Solid-phase microextraction method for headspace analysis of volatile 

compounds in bread crumb. 


1160 bread crumb Cereal Chemistry (2003) 80 (3), 255-259. 

Ruiz, J. A.; Guasch, J.; Mestres, M.; Quilez, J. 

Carboxen/PDMS 

Accurate determination of 2,4,6-trichloroanisole in wines at low parts per trillion 

by solid-phase microextraction followed by GC-ECD. 

2,4,6-trichloroanisole in 

1161 wine. Journal of Agricultural and Food Chemistry (2003) 51 (12), 3509-3514. 

Alzaga, Roberto; Bayona, Josep Maria; Marco, M.-Pilar; Ortiz, Laura; Sanchez- 

Baeza, Francisco 

PDMS GC-MS 

Coupling solid-phase microextraction and high-performance liquid 

chromatography for direct and sensitive determination of halogenated 

fungicides in wine. 

Halogenated 

1174 fungicides in wine. Journal of Chromatography A (2003) 995 (1-2), 135-142. 

Barrio, R. J.; Goicolea, M. A.; Millan, S.; Rodriguez, E.; Sampedro, M. C.; 

Unceta, N. 

PDMS/DVB HPLC-DAD 

Characterization of aroma compounds in apple cider using 

2532 Aroma compounds solvent-assisted flavor evaporation and headspace SPME headspace GC/MS 

in apple cider J Ag Food Chem 55, #8, 3051-3057 (2007) 

Yan Xu; Wenlai Fan; Qian, M. C 

1178 

Effects of processing treatment and sorbate addition on the flavor 

characteristics of apple cider. 

Flavor characteristics in 

apple cider. Journal of Agricultural and Food Chemistry (2003) 51 (7), 1924-1931. 

Boylston, T. D.; Wang, H.; Reitmeier, C. A.; Glatz, B. A. 




Matrix 

Trans-resveratrol in 


Solid-phase microextraction long dash on-fibre derivatization with 

comprehensive two-dimensional gas chromatography analysis of trans - 

resveratrol in wine. 


1179 wine. Chromatographia (2003) 51 (Supp), S349-S353. 

Shao, Y.; Marriott, P. *; Hugel, H. 

GC 

Identification and quantification of the rice aroma compound, 2-acetyl-1pyrroline, 

in bread flowers ( Vallaris glabra Ktze). 

2-acetyl-1-pyrroline in 

1180 bread flowers. Journal of Agricultural and Food Chemistry (2003) 51 (2), 457-462. 

Wongpornchai, S.; Sriseadka, T.; Choonvisase, S. 

GC-FID 

Factors affecting solid phase microextraction (SPME) to concentrate 

2681 Volatiles of the odorants of Chinese white salted noodles for GC-MS analysis. 75µm Carboxen GC-MS 

Chinese noodles Flavour and Fragrance J. 22, #4, 274-279 (2007) 65µm DVB/PDMS 

Li-Yun Lin; Chiung-Huei Peng; Hui-Er Wang; Tsung-Han Wu; 16 min @ 30°C 

Cheng-Chang Chen; Tung-Hsi Yu; Cheung-May Wu; Peng, R. Y. headspace 


Electronic nose and GC-MS to investigate the volatile component of 

an Italian traditional pasta headspace GC-MS 

Italian pasta Cereal Foods World 52, #3, 138-143 (MAY-JUN 2007) 

Baiano, A.; Siciliano, P.; Taurino, M.; Presicce, D.; Gambacorta, G.; 

Lamacchia, C.; Pati, S.; La Notte, E. 


Analysis of the headspace volatiles of freshly brewed arabica coffee 

using solid-phase microextraction DVB/car 50/30µm GC-MS 

brewed arabica J Food Science 72, #7, C388-C396 (Sept. 2007) headspace 

coffee Akiyama, M.; Murakami, K.; Ikeda, M.; Iwatsuki, K.; Wada, A.; Tokuno, K.; 

Onishi, M.; Iwabuchi, H. 

2861 Volatiles 

Headspace SPME-GC-TOF-MS methodology for geographical origin 

verification of coffee DVB/car 50/30µm GC-TOF-MS 

in coffee Anal. Chim. Acta 617, #1-2, 72-84 (Jun 9 2008) headspace 

Carasek, Eduardo; Pawliszyn, Janusz; Risticevic, Sanja 12 min and 55 °C 

Analysis of volatile compounds released during the grinding of roasted coffee 

beans using solid-phase microextraction. 


1185 ground coffee. Journal of Agricultural and Food Chemistry (2003) 51 (7), 1961-1969. 

Akiyama, M.; Murakami, K.; Ohtani, N.; Iwatsuki, K.; Sotoyama, K.; Wada, A.; 

Tokuno, K.; Iwabuchi, H.; Tanaka, K. 

PDMS/DVB GC-MS 

1190 

Singlet oxygen oxidation for 2-pentylfuran and 2-pentenylfuran formation in 

soybean oil. 

2-pentylfuran and 2pentenylfuran 

in 

soybean oil. Journal of Food Science (2003) 68 (4), 1175-1178. 

Min, D. B.; Callison, A. L.; Lee, H. O. 

GC-MS 

SPME for on-line volatile organo-selenium speciation. 

Organo-selenium in 

1191 garlic Journal of Analytical Atomic Spectrometry (2003), 18 (5), 467-473. 

Dietz, C.; Camara, C.; Madrid-Albarran, Y.; Perez-Corona, T. 

PDMS ICP-MS 

Aroma compounds of an Italian wine ( Ruche ) by HS-SPME analysis coupled 

with GC-ion trap MS. 


1197 wine. Food Chemistry (2003) 80 (1), 125-133. 

Bonino, M.; Schellino, R.; Rizzi, C.; Aigotti, R.; Delfini, C.; Baiocchi, C. * 

Various GC-MS 

The electronic nose applied to dairy products: A review 

1208 Dairy products. Sensors and Actuators, B: Chemical (2003) 94 (1), 1-12. 

Ampuero, Silvia; Bosset, J.O. 


Study of phenolic and volatile composition of white wine during 

fermentation and a short time of storage headspace GC/FID GC/MS 





white wine Vitis 46, # 2, 77-84 ( 2007) 

Komes, D.; Ulrich, D.; Ganic, K. Kovacevic; Lovric, T. 

Isolation of white wine volatiles using different sample preparation 

2321 Volatiles from methods 

white wine Vitas 44 #4 187-193 (2005) 

Komes, D.; Ulrich, D.; Lovric, T.; Schippel, K. 


Differentiation of certified brands of origins of Spanish white wines by 

HS-SPME-GC and chemometrics Microfluidics in Cell Analysis GC-MS 

white wine Anal. Bioanal. Chem. 390, #3, 961-970 (February 2008) 

Alcazar, A.; Ballesteros, O.; Jurado, J.M.; Martin, M.J.; Navalon, A.; 

Pablos, F.; Vilchez, J.L. 

headspace 

Flavour analysis of Greek white wine by solid-phase microextraction-capillary 

gas chromatography-mass spectrometry. 

1215 Flavor analysis in wine. Journal of Chromatography, A (2003) 985 (1-2), 233-246. Various GC-MS 

Demyttenaere, J. C. R.; Dagher, C.; Sandra, P.; Kallithraka, S.; Verhe, R.; de 

Kimpe, N. 


Comparative study of the whisky aroma profile based on headspace . 

solid phase microextraction using different fibre coatings 75um Carboxen GC- IT MS 

whisky J. Chromatogr., A 1150, # 1-2, 198-207 (2007-05-25) headspace 

Camara, J.; Marques, J. C.; Perestrelo, R.; Rodrigues, F.; Oliveira, L.; 60 min @ 40°C 

Andrade, P.; Caldeira, M sat. salt 

Analysis of volatiles of malt whisky by solid-phase microextraction and stir bar 

sorptive extraction. 

Volatiles in malt 

1216 whisky. Journal of Chromatography, A (2003) 985 (1-2), 221-232. 

Demyttenaere, J. C. R.; Sanchez Martinez, J. I.; Verhe, R.; Sandra, P.; de 

Kimpe, N. 

Various compared 

Comparison of solid-phase microextraction and purge-and-trap methods for the 

analysis of the volatile fraction of butter. 

Volatile fractions in 

1217 butter. Journal of Chromatography, A (2003) 985 (1-2), 117-125. 

Povolo, M.; Contarini, G. * 

Analysis of virgin olive oil volatile compounds by headspace solid-phase 

microextraction coupled to gas chromatography with mass spectrometric and 

flame ionization detection. 

Volatile components in 

1218 virgin olive oil. Journal of Chromatography, A (2003) 983 (1-2), 19-33. 

Vichi, S.; Castellote, A. I.; Pizzale, L.; Conte, L. S.; Buxaderas, S.; Lopez- 

Tamames, E. * 

DVB/carboxen/PDMS GC-MS 

A SPME-GC procedure for monitoring peppermint flavour in tablets. 

Peppermint flavor in 

1224 tablets. Journal of Pharmaceutical and Biomedical Analysis 2003) 30 (5), 1469-1477. 

Yeung, D. Y. H.; Lee, T.; Grant, G.; Ma, M. H.; Kwong, E. * 

GC 

Determination of the disproportionation products of limonene used for the 

catalytic hydrogenation of castor oil. 

1226 Limonene in castor oil Journal of Chromatography, A (2003) 985 (1-2), 313-319. GC-MS 

Schneider, R. C. S.; Baldissarelli, V. Z.; Martinelli, M.; von Holleben, M. L. A.; 

Caramao, E. B.* 

Effect of Penicillium chryso genum and Debaryomyces hansenii on the volatile 

compounds during controlled ripening of pork loins. 


1231 from pork loins. International Journal of Food Microbiology (2003) 84 (3), 327-338. 

Cordoba, Juan J.; Aranda, Emilio; Asensio, Miguel A.; Benito, Maria J.; Martin, 

Alberto 

GC-MS 

Release of limonene from polysaccharide matrices: Viscosity and synergy effect 


1232 




Limonene from 

polysaccharide 

matrices. Food Chemistry (2003) 82 (2), 227-234. 

Grisel, Michel; Decroix, Bernard; Malhiac, Catherine; Secouard, Sebastien 

Oxidative stability of walnut oils extracted with supercritical carbon dioxide 

1236 Walnut oils Journal of the American Oil Chemists' Society (2003) 80 (6), 575-578. 

Crowe, Tammy D.; White, Pamela J. 

1237 

Evaluation of headspace solid-phase microextraction for the analysis of volatile 

carbonyl compounds in spirits and alcoholic beverages. 

Volatile carbonyl 

compounds from 

spirits. Journal of Chromatography, A (2003) 984 (1), 89-96. 

Wardencki, W.; Sowinski, P.; Curylo, J. 

GC-ECD 

1238 Truffle aroma 

Truffle aroma analysis by headspace solid phase microextraction. 


Diaz, P.; Senorans, F. J.; Reglero, G.; Ibanez, E. * 

GC-MS 

Headspace solid-phase micro-extraction gas chromatography method for the 

determination of methanol in aspartame sweeteners. 

1246 Methanol in aspartame Food Additives and Contaminants 92003) 20 (6), 519-523. 

de Lourdes Cardeal, Z.; Sales, J. A. 

85 um polyacrylate. GC-FID 


Volatiles emission patterns of different plant organs and pollen 

of Citrus limon headspace GC/MS 

Citrus limon Analytica Chimica Acta 589, #1, 120-124 (APR 18 2007) 

Flamini, Guido; Tebano, Marianna; Cioni, Pier Luigi 

Determination of limonene oxidation products using SPME and GC-MS. 

Limonene oxidation 

1248 products Journal of Chromatographic Science (2003) 41 (1), 31-35. 

Marine, S. S.; Clemons, J. 

7 um PDMS 

1249 Geosmin in red beet. 

Biosynthetic origin of geosmin in red beets ( Beta vulgaris L.). 


Lu, G. P.; Edwards, C. G.; Fellman, J. K.; Mattinson, D. S.; Navazio, J. 

GC-MS 

1250 Geosmin in red beet. 

Quantitative determination of geosmin in red beets ( Beta vulgaris L.) using 

headspace solid-phase microextraction. 


Lu, G. P.; Fellman, J. K.; Edwards, C. G.; Mattinson, D. S.; Navazio, J. 

GC 

2447 Tetracycline 

On-line coupling of SPME to commercial CE-MS equipment 

Electrophoresis 28, #9,1312-1318 (2007-05-09) CE-MS 

antibiotic 

in soil 

Santos, B.; Simonet, B. M.; Rios, A.; Valcarcel, M. 

Off-line solid-phase microextraction and capillary electrophoresis mass 

spectrometry to determine acidic pesticides in fruits. 

1251 

Acidic pesticides in 

fruit. Analytical Chemistry (2003) 75 (3), 452-459. 

Rodriguez, R.; Manes, J.; Pico, Y. * 

CE-MS 

Application of solid-phase microextraction for the determination of pyrethroid 

residues in vegetable samples by GC-MS. 

Pyrethroid in 

1252 vegetables. Analytical and Bioanalytical Chemistry (2003) 376 (4), 502-511. 

Beltran, J.; Peruga, A.; Pitarch, E.; Lopez, F. J.; Hernandez, F. 

GC-MS 

Determination of daidzein and genistein in soybean foods by automated on-line 

in-tube solid-phase microextraction coupled to high-performance liquid 

chromatography. 


1253 




Daidzein and genistein 

in soybean foods. Journal of Chromatography, A (2003) 986 (2), 169-177. 

Mitani, K.; Narimatsu, S.; Kataoka, H. * 

HPLC 

Development of a rapid and sensitive method for the simultaneous 

2862 Volatiles from determination of 1,2-dibromoethane,1,4-dichlorobenzene and 100µm PDMS GC-MS 

dried honey naphthalene residues in honey using HS-SPME coupled with GC-MS headspace 

Anal. Chim. Acta 617, #1-2, 64-71 (Jun 9 2008) 

Dimotikali, D.; Hiskia, A.; Triantis, T.M.; Tsimeli, K. 

Preparation of dry honey by microwave-vacuum drying 

2510 Volatiles from J. Food Eng. (UK) 84, #4, 582-90 (Feb. 2008) headspace GC-MS 

dried honey Zheng-Wei Cui; Li-Juan Sun; Wei Chen; Da-Wen Sun 

Analysis of volatile composition of honey by solid phase microextraction and gas 

chromatography-mass spectrometry 

1266 Volatiles from honey Journal of Separation Science (2002) 26 (9-10), 793-801. GC-MS 

Martinez-Castro, Isabel; Sanz, Jesus; Soria, Ana Cristina 

Rebuttal on truffle aroma analysis by headspace solid phase microextraction 

(wrong information or wrong interpretation?). 

1271 Aroma from truffles Journal of Agricultural and Food Chemistry (2003) 51 (15), 4484. 

Ibanez, Elena; Diaz, Paloma; Reglero, Guillermo; Senorans, F. Javier 

Solid phase microextraction-gas chromatography for quantifying headspace 

hexanal above freeze-dried chicken myofibrils. 

1272 Hexanal from chicken Journal of Agricultural and Food Chemistry (2003) 51 (15), 4185-4190. GC-MS 

Goodridge, Carolyn F.; Beaudry, Randolph M.; Pestka, James J.; Smith, Denise 

M. 

Optimization of solid-phase microextraction coupled to gas chromatography for 

determination of phenolic compounds in smoked herring. 

Phenolic compounds 

1275 in smoked herring. Food Chemistry (2003) 82 (4), 513-519. 

Serot, T.; Lafficher, C. 

85 um polyacrylate, 50 C, 55 minutes. 

1282 

Changes in aromatic components of banana during ripening and air-drying. 

Aromatic components 

in bananas. Lebensmittel-Wissenschaft & Technologie (2003) 36 (6), 633-642. 

Bonazzi, C.; Boudhrioua, N.; Giampaoli, P. 

GC-MS 

Studies of selenium-containing volatiles in roasted coffee. 

Selenium in roasted 

1283 coffee. Journal of Agricultural and Food Chemistry (2003) 51 (17), 5116-5122. 

Caruso, Joseph A.; Bryson, Joshua M.; Meija, Juris; Montes-Bayon, Maria; 

Vonderheide, Anne P. 

GC/ICP-MS 

2909 Aroma from 

Pungent and aroma substances of Koreigusu sauce from Okinawa 

Nippon Shokuhin Kagaku Kogaku Kaishi 55, #4, 129-136 (2008) headspace GC/MS 

Koreigusu Takahashi, Kyoko; Nishime, Anzu; Kakinuma, Mirei; Koitabashi, Y.; 

hot sauce Sugaya, Asuka; Tanifuji, Fukuko; Miyamoto, Tomoko 

Determination of 1,3-dichloro-2-propanol and 3-chloro-1,2-propandiol in 

2442 1,3-dichloro- soy sauce by headspace derivatization SPME combined with GC-MS 85µm polyacrylate GC/MS 

propan-2-ol Anal. Chim. Acta 591,#2, 167-172 (2007-05-22) 50°C, 15 minutes 

in soy sauce Lee, M. R.; Chiu, T. C.; Dou, J. P. headspace trifluoroacetamide 

Determination of 1,3-dichloropropanol in soy sauce and related 

0.36g/mL NaCl derivative 

2251 1,3-dichloro- products by headspace GC with MS detection: Interlaboratory study headspace GC/MS 

propan-2-ol Journal of AOAC International 88, #5, 1404-1412 (2005) 

in soy sauce Hasnip, S.; Crews, C.; Potter, N.; Brereton, P.; Diserens, H.; Oberson,J. 

2551 Volatile sulfur 

Identification of volatile sulfur compounds produced by Shigella 

sonnei using gas chromatography-olfactometry headspace GC-MS 





compounds from Food Control (UK) 18, #2, 179-82 (Feb. 2007) 

tryptic soy agar Schneider, K. R.; Warren, B. R.; Rouseff, R. L.; Parish, M. E. 

Effect of soybean lipoxygenase on volatile generation and 

2186 Volatiles from inhibition of aspergillus flavus mycelial growth headspace GC-MS 

soybean J Ag Food Chem, 53, #12, 4778-4783 (2005) 

A.Boue, S.; Shih, B..; Carter-Wientjes, C.H.; Cleveland, T.. 


Influence of irradiating bulk soybeans on their future functional 

and sensory properties in soyfood processing headspace GC-MS 

in soybeans AIChE Annu. Meet. Conf. Proc. (2005) p 12298-12305 

Boylston, T Chia, C; French, S; Perchonok, M; Wilson, Lester 

Identification of volatile compounds in soybean at various developmental stages 

using solid phase microextraction. 


1284 soybeans. Journal of Agricultural and Food Chemistry (2003) 51 (17), 4873-4876. 

Boue, Stephen M.; Carter-Wientjes, Carol H.; Cleveland, Thomas E.; Shih, 

Betty Y. 

GC-MS 

Enantiomeric distribution of chiral compounds in orange juices according to 

their geographical origins. 

Chiral compounds in 

1285 orange juice. Journal of Food Protection (2003) 66 (8), 1448-1454. 

Herraiz, M.; Blanch, G. P.; Caja, M. M.; Ruiz del Castillo, M. L. 

GC-MS 

Analysis of microvolatiles in brandy: Relationship between methylketone 

concentration and Cognac age. 

Methylketone in 

1289 cognac. Journal of the Science of Food and Agriculture (2003) 83 (11), 1143-1149. 

Watts, Vivian A.; Butzke, Christian E. 

1290 

Distribution of the volatile (flavour) compounds in Raclette cheese produced 

with different staphylococci in the smear. 

Volatile (flavour) 

compounds in Raclette Mitteilungen aus Lebensmitteluntersuchung und Hygiene (2003) 94 (3), 192cheese. 

211. 

Bosset, Jacques Olivier; Imhof, Miroslava; Place, Raymond B.; Teuber, Michael 


Isolation and identification of Physalis philadelphica Lam. volatiles 

Agrociencia 41, #3, 337-346 (APR-MAY 2007) GC-MS 

husk tomato Calyecac-Cortero, H.; Cibrian-Tovar, J.; Soto-Hernandez, M.; 

Garcia-Velasco, R. 

in Spanish 

Volatiles emitted from in vitro grown tomato shoots during abiotic and biotic 

stress. 

Volatiles from tomato 

1291 shoots. Plant Cell Tissue and Organ Culture (2003) 75 (1), 73-78. 

Debergh, Pierre C.; Maes, Katrien 

The role of ethylene in mango fruit aroma volatiles biosynthesis. 

Ethylene in mango 

1292 fruit. Journal of Horticultural Science & Biotechnology (2003) 78 (4), 485-496. 

Singh, Zora; Lalel, H. J. D.; Tan, S. C. 

GC-MS 

Solid-phase microextraction liquid chromatography-tandem mass spectrometry 

to determine postharvest fungicides in fruits. 

Postharvest fungicides 

1295 in fruits. Analytical Chemistry (2003) 75 (14), 3606-3615. 

Blasco, C.; Font, G.; Manes, J.; Pico, Y. * 

50 um carbowax/templateLC-MS-MS 

Volatile components of Grana Parmigiano-Reggiano type hard cheese. 

Volatile components in 

1296 cheese. Food Chemistry (2003) 83 (1), 55-61. 

Bellesia, F.; Pinetti, A. *; Pagnoni, U. M.; Rinaldi, R.; Zucchi, C.; Caglioti, L.; 

Palyi, G. 

GC-MS 

2559 PCBs in 

Neuro-genetic multioptimization of the determination of PCBs 

cogeners in human milk by headspace SPME-GC-ECD headspace GC-ECD 

human milk Anal. Chim. Acta 585, #1, 66-75 (2007-02-28) 60 min @ 90C 





Kowalski, C. H.; da Silva, G. A.; Poppi, R.; Godoy, H.; Augusto, F sat. NaCl 

Application of Strategically Designed Sample Composition to the Rapid 

Analytical Screening of Milk Samples for Polychlorinated Biphenyls 

1306 PCBs in milk. Journal of AOAC International (2003) 86 (4), 846-855. 

Carro, Antonia M.; Cela, Rafael; Llompart, Maria; Martinez, Elena; Pazos, 

Manuel 

Mass spectrometry in grape and wine chemistry. Part I: Polyphenols 

Polyphenols in 

1307 grapes/wine. Mass Spectrometry Reviews (2003) 22 (4), 218-250. 

Flamini, Riccardo 

LC-MS 

1315 

Simultaneous determination of ochratoxin A and cyclopiazonic, mycophenolic, 

and tenuazonic acids in cornflakes by solid-phase microextraction coupled to 

high-performance liquid chromatography. 

Ochratoxin A, 

cyclopiasonic acid in 

cornflakes. Journal of Agricultural and Food Chemistry (2003) 51 (18), 5232-5237. PDMS/DVB LC-UV/DAD 

Palmisano, Francesco; Aresta, Antonella; Cioffi, Nicola; Zambonin, Carlo G. 

Challenges and prospects of Iberian pork products: Verification of the sensorial 

and nutritional quality of Iberian ham. 

1319 Iberian ham Alimentaria (2003) 40 (345), 45-58. 

Ventanas, S.; Ventanas, J.; Petron, M. J.; Jurado, A.; Carrapiso, A. 

1323 

Application of polyphenylmethylsiloxane coated fiber for solid-phase 

microextraction combined with microwave-assisted extraction for the 

determination of organochlorine pesticides in Chinese teas 

Organochlorine 

pesticides in Chinese 

teas. Journal of Chromatography, A (2003) 1015 (1-2), 11-21. polyphenylmethylsiloxane GC-ECD 

Cai, Lingshuang; Dong, Li; Wu, Caiying; Xing, Jun 

Analyses of pesticides and their metabolites in foods and drinks. 

1325 Pesticides in foods Trends in Analytical Chemistry (2002) 20(11), 649-661 LC-MS 

Ahmed, Farid E. 

1330 

Chemotaxonomical analysis of the essential oil aroma compounds of four 

different Ocimum species from southern India. 

Oil aroma compounds 

in Ocimem species. European Food Research and Technology (2003) 217 (2), 120-124. GC-MS 

Jirovetz, Leopold; Buchbauer, Gerhard; Kaniampady, Molikutty M.; Shafi, 

Mohamed 

Solid-phase microextraction of volatile compounds in left dbl quote Terrincho 

right dbl quote ewe cheese: comparison of different fibres. 


1338 ewe cheese. Journal of Chromatography, A (2003) 1011 (1-2), 1-9. 

Pinho, O.; Peres, C.; Ferreira, I. M. P. L. V. O.* 

CAR-PDMS GC-MS 

Application of isotope dilution to the determination of methylmercury in fish 

tissue by solid-phase microextraction gas chromatography-mass spectrometry. 

1339 Methylmercury in fish. Journal of Chromatography, A (2003) 1011 (1-2), 135-142. 

Yang, L.; Colombini, V.; Maxwell, P.; Mester, Z.; Sturgeon, R. E. 

PDMS GC-MS 

1347 

Comparison of two SPME fibres for differentiation of coffee by analysis of volatile 

compounds. 


coffee Chromatographia (2001) 54(9-10), 647-652. 

Costa Freitas, A. M.; Parreira, C.; Vilas-Boas, L. 

Carbowax/DVB, PDMS GC-MS 

Solid-phase microextraction-gas chromatographic-mass spectrometric method 

for the determination of the fungicides cyprodinil and fludioxonil in white wines. 

1348 Fungicides in wine Journal of Chromatography A (2002) 942(1-2), 41-52 

Simal Gandara, J.; Cancho Grande, B.; Rial Otero, R.; Yague Ruiz, C. 

Ambient temperature, unless otherwise indicated. 38 

50/30um DVB/Carboxen 

PDMS 

GC-MS




1356 Volatiles in wines 

Classification of Nebbiolo-based wines from Piedmont (Italy) by means of solidphase 

microextraction-gas chromatography-mass spectrometry of volatile 

compounds. 

Journal of Chromatography A (2002) 943(1), 123-137 

Aceto, Maurizio; Marengo, Emilio; Maurino, Valter 

GC-MS 

Determination of cyclopiazonic acid in cheese samples using solid-phase 

microextraction with high performance liquid chromatography. 

Cyclopiazonic acid in 

1362 cheese. Food Chemistry (2001) 75(2), 249-254. 

Zambonin, C. G.; Monaci, L.; Aresta, A. * 

Carbowax/TPR HPLC 

2-Methyl-3-furanthiol and methional are possible off-flavours in stored orange 

juice: aroma-similarity, NIF/SNIF GC-Olfactometry, and GC analyses. 

Off flavours in orange 

1367 juice. Journal of Agricultural and Food Chemistry (2001) 49(11), 5425-5432. 

Bezman, Y.; Rouseff, R. L.; Naim, M. * 

GC-O 

Headspace solid phase microextraction ( SPME ) analysis of flavour compounds 

in wines. Effect of the matrix volatile composition in the relative response factors 

in a wine model. 

Flavour compounds in 

1368 wine. Journal of Agricultural and Food Chemistry (2001) 49(11), 5142-5151. 

Rocha, S.; Ramalheira, V.; Barros, A.; Delgadillo, I.; Coimbra, M. A. 

GC 

New device for direct extraction of volatiles in solid samples using SPME 

1370 Volatiles in solid foods. Journal of Agricultural and Food Chemistry (2001) 49(11), 5115-5121. GC-MS 

Ruiz, J.; Ventanas, J.; Cava, R. 

The use of an electronic aroma-sensing device to assess coffee differentiation. 

Comparison with SPME gas chromatography-mass spectrometry aroma 

patterns. 

1372 Coffee aroma Journal of Food Composition and Analysis (2001) 14(5), 513-522. 100 um PDMS GC-MS 

Costa Freitas, A. M.; Parreira, C.; Vilas-Boas, L. 

1377 PAH in rice. 

Dynamics analysis for the distribution of PAH in rice. 

Journal of Health Science (2001) 47(5), 446-451. 

Liu, X. X.; Korenaga, T. 

GC-MS 

1378 Fatty acids in milk. 

Quantitative determination of short-chain free fatty acids in milk using solidphase 


Journal of Agricultural and Food Chemistry (2001) 49(10), 4603-4608. 

Gonzalez-Cordova, A. F.; Vallejo-Cordoba, B. * 

Polyacrylate GC 

Comparison of simultaneous distillation extraction and solid-phase 

microextraction for the determination of volatile flavour components. 

Volatile flavour 

1382 compounds. Journal of Chromatography, A (2001) 930(1-2), 1-7. 

Cai, J. B.; Liu, B. Z.; Su, Q. D.* 

GC-MS 

Solid-phase microextraction ( SPME ) technique for measurement of generation 

of fresh cucumber flavour compounds. 

Cucumber flavour 

1387 compounds Journal of Agricultural and Food Chemistry (2001) 49(9), 4203-4207. 

Palma-Harris, C.; McFeeters, R. F.*; Fleming, H. P. 

PDMS GC 

Characterization of volatiles in different dry gins 

2330 Volatile fraction of J Ag Food Chem 53, #26, 10154-10160 (2005) headspace GC/MS 

distilled gins Vichi, S.; Riu-Aumatell, M.; Mora-Pons, M.; Buxaderas, S.; 

Lopez-Tamames, Elvir 

1389 Scotch whiskies 

Headspace congeners of blended scotch whiskies of different product 

categories from SPME analysis. 

Journal of the Institute of Brewing (2001) 107(5), 315-332. 

Lee, K. -Y. M.; Paterson, A. *; Birkmyre, L.; Piggott, J. R 

PDMS, polyacrylate GC-FID 


1390 




Volatile fingerprinting (SPME-GC-FID) to detect and discriminate diseases of 

potato tubers. 


Volatiles in potato 

tubers 

Plant Disease (2002) 86(2), 131-137 

Kushalappa, A. C.; Chen, C. R.; Lee, B.; Lui, L. H. 

GC-FID 

Fast extraction, clean-up and detection methods for the rapid analysis and 

screening of seven indicator PCBs in food matrices. 

1399 PCBs in food. Trends in Analytical Chemistry (2002) 21(1), 39-52 

Anklam, E.; von Holst, Christoph; Bjorklund, E. 

Optimization of solid phase microextraction analysis of aroma compounds in a 

Portuguese muscatel wine must. 

1401 Aroma from wine must. Journal of Microcolumn Separations (2001) 13(6), 236-242. 85 um polyacrylate 

Relva, A. M.; Freire, Luis M. T. Vaz; Freitas, A. M. Costa 

Monitoring of lipid degradation products by solid-phase microextraction 

Lipid degeneration 

1402 products in oils Journal of Microcolumn Separations (2001) 13(6), 215-220. 

Doleschall, Fruzsina; Kemeny, Zsolt; Kovari, Katalin; Recseg, Katalin 

100 um PDMS GC-FID 

Optimization of solid-phase microextraction analysis for studying change of 

headspace flavor compounds of banana during ripening. 

1403 Volatiles in bananas Journal of Agricultural and Food Chemistry (2002) 50(4), 653-657 

Liu, Tai-Ti; Yang, Tsung-Shi 

Solid phase microextraction and gas chromatography-olfactometry analysis of 

internal volatiles from intact citrus fruits and their aroma activity 

1414 Volatiles from fruit. Abstracts of Papers American Chemical Society (2001) 222(1-2), AGFD142. GC-O 

Rouseff, Russell L.; Lin, Jianming 

SPME GC-MS-based testing for monitoring off-flavor development in processed 

milk. 

1415 Off-flavors from milk Abstracts of Papers American Chemical Society (2001) 222(1-2), AGFD27. 

Marsili, Ray T. 

1418 

1420 

1421 

Volatiles in soybean 

and corn oils 

Solid phase microextraction of volatile soybean oil and corn oil compounds. 

Journal of Food Science (2002) 67(1), 71-76 Various fibers compared GC-MS 

Min, D. B.; Lee, J. H.; Steenson, D. F. 

Polydimethylsiloxane solid-phase microextraction-gas chromatography method 

for the analysis of volatile compounds in wines. Its application to the 

characterization of varietal wines. 


wine. Journal of Chromatography A (2001) 922(1-2), 267-275. PDMS GC 

Polo, M. C.; Martin-Alvarez, P. J.; Pozo-Bayon, M. A.; Pueyo, E. 

Determination of organochlorine pesticides and chlorobenzenes in strawberries 

by using accelerated solvent extraction combined with sorptive enrichment and 

gas chromatography/mass spectrometry. 

Pesticides in 

strawberries. Journal of AOAC International (2001) 84(4), 1194-1201. 

Wennrich, Luise; Breuste, Juergen; Koeller, Gabor; Popp, Peter 

Analysis of volatile compounds released from embryogenic cultures and somatic 

embryos of sweet oranges by head space SPME 


1422 from oranges. Plant Cell Tissue and Organ Culture (2001) 66(1), 31-34. 

Del Bosco, S. Fatta; Alonzo, G.; Saiano, F.; Tusa, N. 

GC-MS 

The effects of temperature and pressure on the performance of 

Carboxen/PDMS fibres during solid phase microextraction ( SPME ) of 

headspace volatiles from cooked and raw turkey breast. 

Volatiles from turkey 

1423 breast. Flavour and Fragrance Journal (2001) 16(4), 294-302. Carboxen/PDMS 





Cronin, D. A.; Brunton, N. P.; Monahan, F. J. 


Headspace-SPME analysis of volatiles of the ridge gourd (Luffa acutangula) and 

bitter gourd (Momordica charantia) flowers. 

Volatiles of gourd 

1424 flowers. Flavour and Fragrance Journal (2001) 16(4), 289-293. 

Grun, I. U.; Fernando, L. N. 

GC-MS 

Changes in the aroma of a strawberry drink during storage. 

Aroma of strawberry 

1426 drink. Journal of Agricultural and Food Chemistry (2001) 49(7), 3244-3252. 

Siegmund, Barbara; Derler, Karin; Pfannhauser, Werner 

Truffle aroma characterization by headspace solid-phase microextraction 

1440 Truffle aroma Journal of Chromatography A (2003) 1017(1-2), 207-214 

Diaz, P.; Ibanez, E.; Reglero, G.; Senorans, F.J 

Analysis of total propionic acid in feed using headspace solid-phase 

microextraction and gas chromatography 

1441 Propionic acid in feed Journal of Chromatography A (2003) 1017(1-2), 161-166 

Ibanez, Carlos 

1442 

1448 

Volatiles in Italian 

Vinegars 

Garlic flavor 

components 

Quantitative analysis of 2-furfural and 5-methylfurfural in different Italian 

vinegars by headspace solid-phase microextraction coupled to gas 

chromatography-mass spectrometry using isotope dilution 

Journal of Chromatography A (2003) 1017(1-2), 141-149 

Calabrese, Roberto; Davoli, Enrico; Giordano, Lucia; Rotilio, Domenic 

Comparative study of extraction techniques for determination of garlic flavour 

components by gas chromatography-mass spectrometry. 

Analytical and Bioanalytical Chemistry (2003) 377(4), 749-756 

Lee, S. N.; Kim, N. S.; Lee, D. S. 


PDMS headspace 13.6 

mins. 

85um Polyacrylate 

headspace 


PDMS headspace 


PDMS, headspace 

GC-MS 

GC-FID, GC-MS 

GC-MS 

GC-MS 


Comparative study of different extraction techniques for the analysis 

of virgin olive oil aroma headspace GC-MS 

Olive Oil Food Chemistry 105, #3, 1171-1178 (2007) 

Vichi, S.; Guadayol, J.; Caixach, J.; Lopez-Tamames, E.; Buxaderas, S. 

1451 Volatiles in Olive Oil 

Solid-phase microextraction in the analysis of virgin olive oil volatile fraction: 

Characterization of virgin olive oils from two distinct geographical areas of 

northern Italy. 

Journal of Agricultural and Food Chemistry (2003) 51(22), 6572-6577 

Lopez-Tamames, Elvira; Buxaderas, Susana; Conte, Lanfranco S.; Pizzale, 

Lorena; Vichi, Stefania 

GC-FID, GC-MS 

Solid-phase microextraction in the analysis of virgin olive oil volatile fraction: 

Modifications induced by oxidation and suitable markers of oxidative status. 

1452 Volatiles in Olive Oil Journal of Agricultural and Food Chemistry (2003) 51(22), 6564-6571 

Lopez-Tamames, Elvira; Buxaderas, Susana; Conte, Lanfranco S.; Pizzale, 

Lorena; Vichi, Stefania 

GC-FID, GC-MS 

1453 

Free fatty acids in ewe 

cheese 

Quantification of short-chain free fatty acids in "Terrincho" ewe cheese: 

Intravarietal comparison. 

Journal of Dairy Science (2003) 86(10), 3102-3109 

Ferreira, I. M. P. L. V. O.; Ferreira, M. A.; Pinho, O. 

Evaluation of two commercial solid-phase microextraction fibres for the analysis 

of target aroma compounds in cooked beef meat 


85um Polyacrylate 65 

degrees C, 45 mins. 

Headspace 

GC-FID




1454 Aroma volatiles in beef Talanta (2003) 61(4), 529-537 

Istasse, Louis; Machiels, David 


PDMS, Carboxen PDMS, GC-MS 

headspace 


Volatile profiles of sparkling wines obtained by three extraction 

methods and gas chromatography-mass spectrometry 50/30µm DVB/Car GC-MS 

sparkling wine Food Chemistry 105, #1, 428-435 (2007 ) headspace 

Bosch-Fuste, J.; Riu-Aumatell, M.; Guadayol, J. M.; Caixach, J.; 

Lopez-Tamames, E.; Buxaderas, S. 

30 min @ 35 C 


Volatile compounds by SPME-GC as age markers of sparkling wines. 

American Journal of Enology and Viticulture (2003) 54(3), 158-162 GC-MS 

1463 

sparkling wine 

Long chain alcohols 

from 

food-borne bacteria 

Buxaderas, Susana; Francioli, Sonia; Lopez-Tamames, Elvira; Riu-Aumatell, 

Montserrat; Torrens, Jordi 

Comparison of long-chain alcohols and other volatile compounds emitted from 

food-borne and related Gram positive and Gram negative bacteria. 

Journal of Basic Microbiology (2002) 42(6), 373-380 GC-MS 

Hamilton-Kemp, T. R.; Archbold, D. D.; Collins, R. W.; Elgaali, Hesham; 

Newman, M. C.; Yu, Keshun 

Application of solid phase microextraction to evaluate traces of thymol in honey. 

1465 Thymol in honey Apidologie (2002) 33(6), 545-552 

Conte, Lanfranco S.; Bogdanov, Stefan; Gracco, Luisa; Piasenzotto, Lara 

Analysis of Riesling wine volatiles by a novel headspace solid-phase 

microextraction gas chromatography method. 

1471 VOCs in Riseling wine American Journal of Enology and Viticulture (2002) 53(3), 251A 

1472 

Volatiles in dry-cured 

ham 

Optimisation of solid phase microextraction ( SPME ) for the analysis of volatile 

compounds in dry-cured ham. 

Journal of the Science of Food and Agriculture (2002) 82(14), 1703-1709 

Flores, Monica; Gianelli, Maria Pia; Toldra, Fidel 

Estimation of the main dill seeds odorant carvone by solid-phase 


1473 Carvone in dill seeds Nahrung (2002) 46(5), 357-359 

1474 

1481 

1482 

Zawirska-Wojtasiak, Renata; Wasowicz, Erwin 


PDMS 

85um Polyacrylate, 

100um PDMS 

GC-FID 

Clean recovery and HRGC-MS/HRGC-FTIR identification of volatiles from 

soybean (Glycine max). 

Volatiles from soybean 

Italian Journal of Food Science (2002) 12(2), 175-182 

leaves 

Damiani, P.; Bin, F.; Castellini, M.; Cossignani, L. 

GC-MS 

Binding properties of 2-pentyl pyridine to soy protein as measured by solid 

phase microextraction 

2-pentyl pyridine 

Journal of Food Science (2002) 67(1), 142-145 

binding to soy proteins 

Boatright, W. L.; Johnson, L. A.; Reuber, M.; Zhou, A. 


Vinegar 

Headspace solid-phase microextraction analysis of aroma compounds in 

vinegar. Validation study. 

Journal of Chromatography A (2002) 967(2), 261-267 75um Carboxen/PDMS 

Castro Mejias, Remedios; Garcia Barroso, Carmelo; Garcia Moreno, Ma. de 

Valme; Garcia Rowe, Fernando; Natera Marin, Ramon 


1496 

1499 

1500 




Mycophenolic acid in 

cheese 

Characterization of 

flavors in coffee 

Volatiles in orange 

juice 

Solid-phase microextraction-high performance liquid chromatography and diode 

array detection for the determination of mycophenolic acid in cheese. 

Food Chemistry (2002) 78(2), 249-254 

Zambonin, C. G.; Aresta, A.; Monaci, L. 

50um Carbowax TPR HPLC-PAD 

Characterization of flavor compounds during grinding of roasted coffee beans. 

Abstracts of Papers American Chemical Society (2002) 224(1-2), AGFD 68 

Sotoyama, Kazuyoshi; Ohtani, Noboru; Murakami, Kazuya; Iwatsuki, Keiji; 

Akiyama, Masayuki; Iwabuchi, Hisakatsu; Tanaka, Kiyofumi; Tokuno, Katsuya; 

Wada, Akira 

Variables affecting SPME headspace analysis of orange juice volatiles 

Abstracts of Papers American Chemical Society (2002) 224(1-2), AGFD 49 

Goodrich, Renee M.; Bryan, Charles R.; Braddock, Robert J. 

Volatile compounds in hydrolyzed pineapple (Ananas comosus L. Merryl) perola 

variety and clarified pasteurized juices obtained by solid-phase microextraction 

1516 Voltiles in pineapple Alimentaria (2002) 39(333), 129-132 65um PDMS DVB GC-MS 

de Carvalho, Lucia Maria Jaeger; da Silva, Carlos Alberto Bento; de Oliveira 

Godoy, Ronoel Luiz; Abadio, Fernanda Dias Bartolomeu; Figueira, Jose 

Americo A. 

1517 


wine 

Headspace solid-phase microextraction gas chromatography/mass 

spectrometry in the analysis of the aroma constituents of 'Cannonau of Jerzu' 

wine. 

Rapid Communications in Mass Spectrometry (2002) 16(11), 1086-1091 GC-MS 

Podda, Gianni; Begala, Michela; Corda, Luciana; Fedrigo, Maria Anna; Traldi, 

Pietro 

2405 Volatile flavors 

Analysis of volatile flavor compounds of sardine (Sardinops 

melanostica) by solid phase microextraction. headspace GC-MS 

of sardine J Food Sci 73, #1, S83-88 (2008 Jan) 

Ganeko, N; Shoda, M; Hirohara, I; Bhadra, A; Ishida, T; Matsuda, H; 

Takamura, H; Matoba, T 

2548 MIB and 

Natural origins of off-flavours in fish related to feeding habits 

Water Science and Technology 55, #5, 301-309 (2007) headspace GC-MS 

geosmin 

in fish 

Papp, Zs. Gy.; Kerepeczki, E.; Pekar, F.; Gal, D. 

Patterns in volatile components over heated fish powders 

2173 Volatiles from Food Research International 39, #2, 190-202 (2006) headspace GC-MS 

fish powder Mjos, Svein A.; Solvang, Marianne 

Headspace volatile components of smoked swordfish (Xiphias 

0.5-4 h at 40° 

to 140°C 

2299 Volatiles from gladius) and cod (Gadus morhua) detected by means of spme-gc-ms headspace GC/MS 

smoked fish Food Chemistry 94 #1, 151-156 (2006) 

Guillen, M. D.; Errecalde, W. C.; Salmeron, J.; Casas, C. 

1520 

Volatiles in smoked 

fish 

Volatile components of raw and smoked black bream (Brama raii) and rainbow 

trout (Oncorhynchus mykiss) studied by means of solid phase microextraction 

and gas chromatography/mass spectrometry. 

Journal of the Science of Food and Agriculture (2002) 82(9), 945-952 

Guillen, Maria D.; Errecalde, Maria C. 

Characterization and semiquantitative analysis of volatiles in seedless . 

2567 Aroma volatiles watermelon varieties using solid-phase microextraction 50/30µm DVB/Car GC/MS 

in watermelon J. Agric. Food Chem. 54, #20, 7789-7793 (2006-10-04) headspace 

Beaulieu, J. C.; Lea, J. M. 

Effect of cutting and storage on acetate and nonacetate esters in 

2311 Volatile Esters in convenient, ready-to-eat fresh-cut melons and apples headspace GC/MS 

melons & apples HortScience 41 #1, 65-73 (2006) 

Beaulieu, John C. 

Effect of storage on some volatile aroma compounds in fresh-cut cantaloupe 

melon. 


1521 

1525 




Aroma volatiles in 

cantaloupe 


Lamikanra, Olusola; Richard, Olga A. 


Fatty acid ethyl ethers 

in rum 

Headspace solid-phase microextraction of higher fatty acid ethyl esters in white 

rum aroma. 


Guasch, J.; Busto, O.; Marti, M. P.; Mestres, M.; Perez, J.; Pino, J. 

Screening of variety- and pre-fermentation-related volatile compounds 

2466 Volatiles from during ripening of white grapes to define their evolution profile headspace GC-MS 

white grapes ANAL. CHIM. ACTA 597, #2, 257-264 (10 AUG 2007) 

Coelho, E.; Rocha, S. M.; Barros, A. S.; Delgadillo, I.; Coimbra, M. A. 

Applications of GCxGC-TOF-MS to targeted analyses of volatiles 

2803 Volatiles from in grapes during berry development headspace GCxGC-TOF-MS 

grapes American J Enology and Viticulture 59, #1, 115A (2008) 

Sacks, Gavin L.; Pan, Bruce S.; Ryona, Imelda 

Effect of vertical shoot-positioned, smart-dyson, and Geneva double- 

2810 Volatiles from curtain training systems on Viognier grape and wine composition headspace GC-MS 

grapes American J Enology and Viticulture 59, #1, 11-21 (2008) 

Zoecklein, B.; Wolf, T.; Pelanne, Lisa.; Miller, M. ; Birkenmaier, S. 

1526 

Investigation of volatiles evolution during the alcoholic fermentation of grape 

must using free and immobilized cells with the help of solid phase 

microextraction ( SPME ) headspace sampling. 

Volatiles in alcoholic 


fermentation of grapes 

Komaitis, Michael; Kanellaki, Maria; Koutinas, Athanasios; Mallouchos, 

Athanasios 

Optimization of headspace solid-phase microextraction ( SPME ) for the odor 

analysis of surface-ripened cheese. 

1527 Odors in cheese Journal of Agricultural and Food Chemistry (2002) 50(13), 3810-3817 headspace 

Ducruet, Violette; Feigenbaum, Alexandre; Gratadoux, Jean Jacques; 

Jouquand, Celine; Lecanu, Laurent 

1534 Butyltin in wines 

Headspace solid-phase micro-extraction gas chromatography-mass detection 

method for the determination of butyltin compounds in wines. 

Analytica Chimica Acta (2002) 458(1), 231-239 

Azenha, Manuel; Vasconcelos, Maria Teresa 


Determination of ethylphenol compounds in wine by headspace solid-phase 

microextraction in conjunction with gas chromatography and flame ionization 

detection. 

1535 Ethylphenol in wine Analytica Chimica Acta (2002) 458(1), 111-117 

Nepveu, Francoise; Gastine, Valerie; Monje, Marie-Carmen; Privat, Christelle 

Changes in quality parameters and volatile aroma compounds in 

2347 Aroma compounds fairtime-peach during fruit development and ripening 

in peach Italian Journal of Food Science 19, #1, 3-13 (2007) 

Agozzino, P.; Avellone, G.; Filizzola, F.; Farina, V.; Lo Bianco, R. 

85um Polyacrylate, NaCl 

added, 40mins. 

GC- 

OLFACTOMETRY 

GC-FID 


Automated determination of ethyl carbamate in stone-fruit spirits 

2317 Ethyl carbamate using headspace SPME-GC-MS 65µm CW/DVB GC/MS 

in fruit spirits J. Chromatogr. A 1108 #1, 116-120 (2006) headspace 

Kuballa, Thomas; Lachenmeier, Dirk W.; Nerlich, Uta 30 min at 70 

1537 

Ethyl carbamate in 

wine 

Determination of ethyl carbamate in wine by solid-phase microextraction and 

gas chromatography/mass spectrometry. 

American Journal of Enology and Viticulture (2002) 53(1), 60-63 

Zoecklein, B. W.; Whiton, R. S. 


65um Carbowax DVB, 

30mins, headspace 

GC-MS




Quantitative analysis of 3-alkyl-2-methoxypyrazines in juice and wine 

2907 3-alkyl-2-methoxy using stable isotope labelled internal standard assay 50/30µm DVB/CAR GC-MS 

pyrazines in J. Chromatogr., A 1190,#1-2, 294-301 (May 9 2008) Headspace 

in wine and juice Blake, A.J.; Brindle, I.D.; Chen, X.; Inglis, D.; Kotseridis, Y.S.; pH 6 

Pickering, G.J.; Sears, M.; Soleas, G.; Spink, M. 

Implementation of headspace SPME-GC-MS/MS methodology 

2901 3-alkyl-2- for determination of 3-alkyl-2-methoxypyrazines in wine 75µm Carboxen GC-MS 

methoxypyrazines Eur. Food Res. Technol 227, #2, 449-461 (June 2008) 30-80 min 

in wine Godelmann, Rolf; Kuballa, Thomas; Limmert, Susanne 30-80 °C 

Determination of 3-alkyl-2-methoxypyrazines in lady beetle-infested 

2806 3-alkyl-2- wine by SPMEheadspace sampling headspace GC 

methoxypyrazine J of Agri and Food Chemistry 56(3), 1065-1071 (FEB 13 2008) 

in wine Galvan, Tederson Lutz; Kells, Stephen; Hutchison, William Dale 

1539 

1541 

1542 

1546 

3-alkyl-2methoxypyrazines 

in 

wine 

Butyltin in Portuguese 

wines 

Volatiles in Spanish 

honey 

Short-chain fatty acids 

in cane and beet 

sugars 

Headspace solid-phase microextraction analysis of 3-alkyl-2-methoxypyrazines 

in wines. 


Guasch, J.; Busto, O.; Marti, M. P.; Mestres, M.; Sala, C. 

Butyltin compounds in Portuguese wines. 

Journal of Agricultural and Food Chemistry (2002) 50(9), 2713-2716 GC-MS 

Azenha, Manuel; Vasconcelos, Maria Teresa 

Analysis of volatiles from Spanish honeys by solid-phase microextraction and 



Tadeo, Jose L.; Calvo, Rosa M.; Perez, Rosa A.; Sanchez-Brunete, Consuelo 

Semiquantitative determination of short-chain fatty acids in cane and beet 

sugars. 

Journal of Chromatographic Science (2002) 40(3), 127-132 

Grimm, Casey C.; Batista, Rebecca B.; Godshall, Mary An 

75um Carboxen PDMS, 

70 degrees C, 30mins. GC-MS 

2415 Sulfur compounds 

Quantitative determination of wine highly volatile sulfur 

compounds by using automated headspace SPME-GC-pulsed FPD: 75µm Carboxen 

GC-FPD 

in wines Critical study and optimization of a new procedure 20 MIN @ 35°C 

J. Chromatogr., A 1143, #1-2, 8-15 (-2007-03-02) headspace 

Lopez, R.; Lapena, A. C.; Cacho, J.; Ferreira, V. 

Volatile sulfur compounds in oregon wines determined by SPMEsaturated 

NaCl 

2225 Sulfur compounds pulsed flame photometric detection headspace GC-FPD 

in wines American Journal of Enology and Viticulture 56 #3, 309A (2005) 

Fang, Yu; Qian, Michael 

1555 

Sulfur compounds in 

wines 

Application of headspace solid-phase microextraction to the determination of 

sulphur compounds with low volatility in wines. 


Mestres, M.; Busto, O.; Guasch, J. 


PDMS 

GC-MS 

1196 

Analysis of chemical constituents of capsicol by GC-MS. 

Fenxi Ceshi Xuebao (2003) 22 (1), 67-70. 

Zhu, X. L.; Liu, B. Z.; Zong, R. W.; Yun, G. O. 

GC-MS 

1211 

Identification of 2-bromo-3,4,5,6-tetrachloroaniline and its quantification in the 

color additives D&C Red Nos. 27 and 28 (phloxine B) using solid-phase 

microextraction and gas chromatography-mass spectrometry 

Journal of Chromatography A (2003) 1005 (1-2), 143-153. 

Andrzejewski, Denis; Weisz, Adrian 

GC-MS 





Determination of nicotine and other minor alkaloids in international cigarettes by 

solid-phase microextraction and gas chromatography/mass spectrometry. 

1243 Nicotine in cigarettes Analytical Chemistry (2003) 74 (19), 4878-4884. GC-MS 

Wu, W. J.; Ashley, D. L.; Watson, C. H.* 

Determination of the volatile constituents of Chinese Coriandrum sativum L. by 

gas chromatography-mass spectrometry with solid-phase microextraction. 

1274 Chromatographia (2003) 57 (5-6), 357-361. 100 um PDMS, 250 C, 3 mGC-MS 

Deng, C. H.; Song, G. X.; Hu, Y. M.*; Zhang, X. M. 

1314 

Aroma dilution method using GC injector split ratio for volatile compounds 

extracted by headspace solid phase microextraction. 

Food Chemistry (2003) 83 (1), 151-158. 

Lee, Hyong Joo; Kim, Kyoung Heon; Kim, Tae Hwan; Kim, Young-Suk; Lee, 

Sang Mi; Oh, Sangsuk 

GC-O 

Flavor-protein binding: Disulfide interchange reactions between ovalbumin and 

volatile disulfides. 

Disulfide flavors from 

1409 proteins Journal of Agricultural and Food Chemistry (2001), 49(9), 4333-4336. 

Mottram, Donald S.; Adams, Rachel L.; Brown, Helen M.; Parker, Jane K. 

Analysis of esters in wines 

1559 Esters J.Chromatogr. A (2002) 963(1-2), 213-223 Various GC 

in wine Rodriguez-Bencomo, J.; Conde, J.; Rodriguez-Delgado, M.A.; 

Garcia-Montelongo, F.; Perez-Trujillo, J.P. 

Contribution of dimethyl sulfide to the aroma of Syrah and 

1560 Dimethyl Grenache Noir wines and estimation of its potential in grapes headspace GC-MS 

sulfide in of these varieties 

wine J Agr Food Chem, 52, #23, 7084-7093 

Segurel, M.; Razungles, A.; Riou, C; Salles, M; Baumes, R 

Hydrolysis of glycosidically bound volatiles from apple leaves 

1561 Volaitles in (cv. Anna) by Aspergillus niger beta-glucosidase affects headspace GC-MS 

apple leaves the behavior of codling moth (Cydia pomonella L.) 

J Agril and Food Chem, 52, #26, 6212-6216 

Wei, Shu; Reuveny, Haim; Bravdo, Ben-Ami; Shoseyov, Oded 

Genetic diversity of volatile components in Xinjiang Wild 

2547 Volaitles in Apple (Malus sieversii) Headspace GC-MS 

apples Journal of Genetics and Genomics 34, #2, 171-179( FEB 2007) 

Chen, X.; Feng, T.; Zhang, Y.; He, T.; Feng, Jianrong; Zhang, Chunyu 

Monitoring seasonal variation in apple fruit volatile 

1562 Volaitles in emissions in situ using SPME in situ GC 

apples Phytochemical Analysis, 14, No 4, 232-240 

Hern, Alan; Dorn, Silvia 

Ester variability in apple varieties as determined 

1563 Esters in by SPME-GC-MS PDMS fiber GC-MS 

apples J Agril and Food Chem, 52, #26, 8086-8093 Headspace 

Young, J. C.; Chu, C. L. G.; Lu, X. W.; Zhu, H. H. 

Potential of SPME-GC and chemometrics to detect 

1564 Volaitles in adulteration of soft fruit purees. Headspace GC-FID 

stawberry vs J Agr Food Chem, 52, #3, 421-427 GC-MS 

a puree Reid, L.; Oapostrophe Donnell, C.; Downey, G. 

Development of headspace SPME-GC method for the 

1565 Solvents in determination of solvent residues in edible oils various fibers GC-FID 

edible oils, and pharmaceuticals headspace GC-ECD 

pharmaceutics J. Chromatogr. A, 1071, #1-2, 119-124 

Michulec, M.; Wardencki, W. 

Rapid determination of volatile constituents in safflower by microwave 

2701 Volatiles in distillation and simultaneous SPME-GC-MS 65µm PDMS/DVB GC/MS 

safflower oil Annali di Chimica 97, #10, 1075-1084 (OCT 2007) headspace 

Yu, Yingjia; Yang, Bei; Zhou, T.; Zhang, H.; Shao, Luping; Duan, G. 

Identification of volatile compounds in structured lipid of 





1566 Volatiles in safflower oil using electronic nose and SPME-GC-MS headspace GC-MS 

safflower oil Agr Chem&Biotechnogy, 46, #4, 152-155 

Shin, Jung-Ah; Lee, Jong-Ho; Lee, Ki-Teak 

Monoterpene and sesquiterpene hydrocarbons of virgin olive oil by . 

2708 Terpenes headspace SPME coupled to gas chromatography/mass spectrometry headspace GC/MS 

in olive oil J. Chromatogr., A 1125, #1, 117-123 (2006-08-25) 

Vichi, S.; Guadayol, J.; Caixach, J.; Lopez-Tamames, E.; Buxaderas, S. 

Determination of halogenated solvents content in olive oil by two 

2248 Halogenated completely automated headspace techniques coupled to GC-MS headspace GC/MS 

solvents in Analytica Chimica Acta (2005) 552 #1-2, 60-66 

olive oil Arrebola, F. ; Gonzalez-Rodriguez, M.; Garrido Frenich, A.; 

Marin-Juan, A.; Martinez Vidal, J.; 

Characterization of olive paste volatiles to predict the sensory quality 

2515 Volatiles from of virgin olive oil headspace GC/MS 

Virgin olive oil European J Lipid Sci Tech 109, #7, 663-672 (JUL 2007) 

Garcia-Gonzalez, Diego L.; Tena, Noelia; Aparicio, Ramon 

Effect of the matrix volatile composition in the headspace SPME 

2300 Volatiles from analysis of extra virgin olive oil 65µm PDMS/DVB GC/MS 

Virgin olive oil Food Chemistry 94 #1, 143-150 (2006) headspace 

Contini, Marina; Esti, Marco 

Comparative study on volatile analysis of extra virgin 

1567 Volatiles in olive oil by dynamic headspace and SPME 100µm PDMS GC-MS-TOF 

olive oils Food Chemistry, 90, #1-2, 69-79 65µm PDMS-DVB 

Kanavouras, A.; Kiritsakis, A.; Hernandez, R. J. headspace 

Application of SPME to virgin olive oil quality control 

2738 Volatiles in J Chromatogr A, 1121, #1, 140-144 (2006-07-14) 65µm PDMS/DVB GC/MS 

olive oils Jimenez, A.; Aguilera, M. P.; Beltran, G.; Uceda, M. headspace 

30 min @ 40°C 

Application of SPME in the analysis of volatile oils 

1568 Volatiles in compounds in virgin olive oils. 100µm PDMS GC 

olive oils J Chromatogr A, 1028, #2, 321-324 15 min @ 45°C 

Jimenez, A.; Beltran, G.; Aguilera, M. P. headspace 

Analysis of virgin olive oil volatiles by a novel electronic 

1569 Volatiles in nose based on a miniaturized SAW sensor array headspace SAW 

olive oils coupled with SPME enhanced headspace enrichment GC 

J AgriFood Chem, 52, #25, 7475-7479 

Garcia-Gonzalez, D.; Barie, N; Rapp, M; Aparicio, R 

A chemical investigation by headspace SPME and 

1570 Terpenes GC-MS of volatile and semi-volatile terpenes in headspace GC-MS 

in olibanum various olibanum samples 

Phytochemistry (Amsterdam), 66, #12,1499-1514 

Hamm, S; Bleton, J; Connan, J; Tchapla, A 

2450 Terpenes from 

Quantifying sesquiterpene and oxygenated terpene emissions from 

live vegetation using solid-phase microextraction fibers. 65µm PDMS-DVB GC-MS 

live branches J. Chromatogr., A 1161, #1-2, 113-120 (2007-08-17) headspace 

Bouvier-Brown, N. C.; Holzinger, R.; Palitzsch, K.; Goldstein, A. H. 10-45 min 

Simultaneous distillation-extraction of high-value volatile compounds 

2522 Volatiles from from Cistus ladanifer L 85µm Polyacrylate GC-FID 

Rock-rose Anal. Chim. Acta 584, #2, 439-446 (Feb 19 2007) 60 min @ 40°C 

Alves, Arminda; Mendes, Adelio; Santos, Lucia; Teixeira, Salome headspace 

20% NaCl 

Simultaneous determination of phytohormones in plant extracts 

2479 Phytohormones using SPME and HPLC 50µm CW GC, HPLC 

from plants Chromatographia 66, #7/8, 515-520 (2007) 

Liu HongTao; Li YanFen; Luan TianGang; Lan ChongYu; Shu WenSheng 

Volatile profiling of Arabidopsis thaliana - Putative olfactory 

2288 Volatiles from compounds in plant communication headspace GC/IMS 

plants Phytochemistry (Amsterdam) 66 #16, 1941-1955 (2005) 

Rohloff, Jens; Bones, Atle M. 

Evaluation of extracts and oils of mosquito (Diptera : Culicidae) 

2202 Volatiles from repellent plants from Sweden and Guinea-Bissau headspace GC-MS 

plants J Medical Entomology 43, #1, 113-119 (2006) 

Jaenson, Thomas G. T.; Palsson, Katinka; Borg-Karlson, Anna-Karin 





Characterization of three Agave species by GC 

1571 Terpenes & and SPME-GC-MS headspace GC, GC-MS 

fatty acids in J Chromatogr A, 1027, #1-2, 131-136 steam distillation 

plants Pena-Alvarez, A.; Diaz, L.; Medina, A.; Labastida, C.; 

Capella, S.; Vera,L.. 

Analysis of volatile compounds of camu-camu (Myrciaria dubia (HBK) 

2628 Volatiles in Mcvaugh) fruit isolated by different methods headspace GC-MS 

camu-camu fruit J. Essent. Oil Res. 19, #6, 527-533 (Nov/Dec 2007) 

Pino, Jorge A.; Quijano, Clara E. 

Analysis of volatile secondary metabolites 

1572 Volatiles from Colombian Xylopia ronatica (Lamarck) by headspace GC-MS 

in fruit different extraction and headspace methods and GC 

J Chromatogr A, 1025, #1, 105-113 

Stashenko, E.; Jaramillo, B.; Martinez, J 

Comparison of volatile compounds of corn oil and 

1573 Volatiles modified corn oil by electronic nose and SPME-GC-MS headspace GC-MS 

in corn oil Agri Chem and Biotechnology, 47, #3, 153-156 

Vu, Phuong-Lan; Shin, Jung-Ah; Lee, Ki-Teak 

Application of the SPME and in food analysis 

1574 Review Polish J Food and Nutrition Sci, 13, #4, 355-361 100µm PDMS GC-MS 

Ligor, Magdalena; Wojcik, Jan; Buszewski, Boguslaw 85µm polyacrylate 

headspace 

Essential oil in fruits of Peucedanum alsaticum L. and Peucedanum 

2812 Volatiles from cervaria (L.) Lap.Composition and antibacterial activity 

essential oils Planta Medica 73, #9, 883-884 (AUG 2007) 

Skalicka-Wozniak, K.; Los, R.; Glowniak, K.; Malm, A. 

Use of SPME in diffusive sampling of the atmosphere generated 

2318 Volatiles from by different essential oils headspace GC/MS 

essential oils Anal. Chim. Acta 559 #2, 97-104 (2006) 30 min @ 20°C 

Batlle, R.; Huerga, M.A.; Lopez, P.; Nerin, C. 

High-throughput analysis of bergamot essential oil by fast SPME 

2222 Volatiles in capillary GC-FID 30 and 7µm PDMS GC-FID 

essential oils J. Chromatogr. A, 1103, #1, 162-165 (2006) headspace 

Costa, R.; Dugo, G.; Dugo, P.; Mondello, L.; Presti, M.; Tranchida, P. 

Steam distillation-SPME for the detection of 

1575 Volatiles from Ephedra sinica in herbal preparations headspace GC-MS 

essential oils J Chromatogr A, 1025, #1, 51-56 

Tellez, M.; Khan, I.; Schaneberg, B.; Crockett, S.; 

Rimando, A.; Kobaisy,M 

Testing of microencapsulated flavours by electronic 

1576 Volatiles from nose and SPME-GC headspace GC-MS 

essential oils Food Chem, 92, #1, 45-54 

Baranauskiene, R; Venskutonis, P, Galdikas,A., 

Senuliene, Daiva; Setkus, Arunas 

SPME-GC-MS a fast and simple screening method 

1577 Organo- for the assessment of organophosphorus headspace GC-MS 

phosphorus pesticides residues in wine and fruit juices. 

pesticides Food Chemistry, 86,#2, 269-274 

in wine/juice Zamabonin, C; Quinto, M; deVietro, N; Palmisano, F 

Metabolites of lesser grain borer in grains. 

1578 Volatiles J Agrl Food Chem, 52, #4, 898-908 headspace GC-MS 

from wheat Seitz, L. M.; Ram, M. S. 0-240min @ 20°-40°C 

Headspace SPME-GC-Mass spectrometric 

1579 Volatiles of analysis of the essential oils of two traditional headspace GC-MS 

essential oils Chinese medicines, Angelica pubescens and 

Angelica sinensis. 

Chromatographia, 59, #5-6, 343-349 

Song, G. X.; Deng, C. H.; Wu, D.; Hu, Y. M.* 

Comparative study on volatile components of Nardostachys Rhizome 

2853 Volatiles from Journal of Natural Medicines 62, #1, 112-116 (JAN 2008) headspace GC-MS 

chinese grandiflora Tanaka, Ken; Komatsu, Katsuko 

Fast determination of curcumol, curdione and germacrone in three 





2704 Active ingredients species of Curcuma rhizomes by microwave-assisted extraction 100 µm PDMS GC-MS 

from chinese followed by headspace SPME-GC-MS 20min @ 80°. 

medicine J. Chromatogr., A 1117, #2, 115-120 (2006-06-09) headspace 

Deng, C. H.; Ji, J.; Li, N.; Yu, Y. J.; Duan, G. L.; Zhang, X. 30% NaCl 

Analysis of the volatile compounds in Ligusticum chuanxiong Hort. 

2589 Volatiles from using HS-SPME-GC-MS 65µm PDMS-DVB GC-MS 

chinese medicines J. PHARM. BIOMED. ANAL. 44, #2, 464-470 (28 JUN 2007) headspace 

Zhang, C.; Qi, M.; Shao, Q.; Zhou, S.; Fu, R. 

GC-MS following microwave distillation and headspace SPME for fast 

2570 Essential oils analysis of essential oil in dry traditional Chinese medicine headspace GC-MS 

in Chinese J. Chromatogr., A 1133, #1-2, 29-34 (2006-11-10) 

medicine Li, N.; Deng, C. H.; Li, Y.; Ye, H.; Zhang, X. M. 

Rapid determination of essential oil compounds in Artemisia 

2166 Essential oils Selengensis Turcz by GC-MS with microwave distillation and headspace GC-MS 

in Chinese simultaneous SPME 

medicine Anal. Chim. Acta, 556, #2, 289-294 (2006) 

Deng, Chunhui; Xu, Xiuqin; Yao, Ning; Li, Ning; Zhang, Xiangmin 

Headspace SPME-GC-MS for analysis of volatile components 

2553 Volatiles from from Atractylodes macrocephala Koidz 65µm PDMS-DVB GC-MS 

chinese medicines Sepu 25, #1, 43-47 (2007-01) 30 min @ 70°C 

Guo, F. Q.; Huang, L. F.; Zhou, S. Y. headspace 

Recent developments in sample preparation techniques for 

2500 Review article chromatography analysis of traditional Chinese medicines. 

J Chromatogr A 1153, #1-2, 90-96 (2007 Jun 15) 

Deng, Chunhui; Liu, Ning; Gao, Mingxia; Zhang, Xiangmin 

SPME-multicapillary GC coupled to different 

1580 Organo- detection systems and applied to volatile headspace ICP-MS, MIP-AES, 

selenium in organo-selenium speciation in yeast. AFS 

yeast J Analytical Atomic Spectrometry, 19, #2, 260-266 

Dietz, C.; Sanz Landaluze, J.; Ximenez-Embun, P.; Madrid-Albarran, Y.; 

Camara, C. 

Volatile organoselenium monitoring in production and gastric 

1581 Organo- digestion processes of selenized yeast by SPME-multicapillary headspace MIP-AES 

selenium in GC coupled microwave-induced plasma atomic 

yeast emission spectrometry 

Appl. Organomet. Chem., 18, #12, 606-613 

Camara, C.; Dietz, C.; Madrid, Y.; Sanz Landaluze, J. 

Production of volatile organic sulfur compounds (VOSCs) 

1582 Sulfur compd by basidiomycetous yeasts headspace GC-MS 

in yeast FEMS Yeast Research, 5, #4-5, 379-385 

Buzzini, Pietro; Romano, Sergio; Turchetti, Benedetta; 

Vaughan, Ann; Pagnoni, Ugo Maria; Davoli, Paolo 

Direct coupling of SPME and quartz tube-atomic 

1583 Methyl absortpion spectrometry for selective and sensitive 65µm PDMS-DVB GC-MS, AA 

mercury in determination of methylmercury in seafood: An bare silica fiber 

seafood assessment of chloride & hydride generation headspace 

J Analytical Atomic Spectrometry, 19, #2, 220-254 chloride derivative. 

Fragueiro, S; Lavilla, I; Bendicho, C. 

Volatile changes in cantaloupe during growth, maturation, and in 

2258 Flavor volatiles stored fresh-cuts prepared from fruit harvested at various maturities headspace GC-MS 

in cantaloupe J Am Society for Horticultural Sci. 131, #1, 127-139 (2006) 

Beaulieu, John 

Volatile profile, sensory attributes, and quality of 

1584 Flavor volatiles freshcut cantaloupe is maturity-at-cutting dependent headspace GC-MS 

in cantaloupe Hortscience, 38, #5, 833 

Beaulieu, John C.; Bett, Karen L. 

Fatty acid composition of tomato affects fruit and 

1585 Fatty acids leaf biosynthesis of C6 aldehydes and alcohols GC-MS 

in tomatos Hortscience, 38, #5, 833 

Canoles, M; Li, C; Howe, Gg; Beaudry, R 

Rapid determination of C6-aldehydes in tomato plant emission 

1586 C6 aldehydes by GC-MS and SPME with on-fiber derivatization 65µm PDMS-DVB GC-MS 





in tomatos J Sep Science, 28, #2, 172-176 5 min @ 25ºC 

Deng, Chunhui; Li, Ning; Zhu, Weimin; Qian, Ji; PFBHA derivatives 

Yang, Xiaofeng; Zhang, Xiangmin headspace 

The measurement of sulfur-containing aroma compounds in 

1587 Sulfur aroma samples from production-scale brewery operations headspace GC-FPD 

from Beer JAm Society of Brewing Chemists, 63, #3, 129-134 

Miracle, R. E.; Ebeler, S. E.; Bamforth, C. W. 

Determination of C3-C10 aliphatic aldehydes using PFBHA 

1588 Aldehydes in derivatization and SPME.Application to the analysis of beer PFBHA derivatives GC 

beer Chemia Analityczna, 49, #6, 869-880 20min @ 20°C 

Jelen, H.; Dabrowska, A.; Klensporf, D.; Nawrocki, J.; Wasowicz,E. headspace 

Volatile compounds of Aspergillus strains with different 

1589 Volatiles from abilities to produce ochratoxin A headspace @ GC 

wheat grain J Agri Food Chem, 53, #5, 1678-1683 20° to 27°C 

Jelen, Henryk H.; Grabarkiewicz-Szczesna, Jadwiga 

Quantification of selected aroma-active compounds in strawberries by 

2697 Volatiles from headspace SPME-GC and correlation with sensory descriptive analysis headspace GC-MS 

strawberries J Food Science 72, #7, S487-S496 (2007) 

Jetti, R. R.; Yang, E.; Kurnianta, A.; Finn, C.; Qian, M. C. 

Comparison of methodologies for the identification of aroma 

1590 Volatiles from compounds in strawberry headspace GC-MS 

strawberries Turk. J. Agric. For., 29, #5, 383-390 

Bar, E; Kafkas, E; Kafkas, S; Koch-Dean, M.Larkov, O; Lavid, N 

Lewinsohn, Efraim; Ravid, Uzi; Schwab, Wilfried 

Analysis of strawberry volatiles using comprehensive two 

1591 Volatiles from dimensional gas chromatography with headspace SPME headspace GC-GC 

strawberries J Chromatogr, B:817, # 1, 97-107 

Williams, A.; Ryan, D.; Guasca, A.; Marriott, P.; Pang, E. 

Main compounds responsible for off-odour of strawberries 

1592 Off-odour in infected by Phytophthora cactorum headspace GC-olfactometry 

strawberries Letters in Applied Microbiology, 40, #4, 255-259 

Jelen, H. ; Krawczyk, J.; Larsen, T. ; Jarosz, A.; Golebniak, B. 

Volatile compounds as markers for coliforms 

1593 Volatiles from inoculated on strawberry fruit. 15 min headspace GC 

strawberries Hortscience, 38, #5, 831 

Yu, K; Elgaali, H; Hamilton-Kemp, T; Newman, M; 

Collins, R; Archbold,D. 

SPME-GC-MS analysis of garlic oil obtained 

1594 Sulfur volatiles by hydrodistillation various fibers GC-MS 

from garlic J. Chromatogr. A, 1036, #1, 91-93 headspace 

Calvo-Gomez, O.; Lopez, M.; Morales-Lopez, J. 

Comparative study of extraction techniques for 

1595 Garlic flavor determination of garlic flavor components by GC-MS 50/30µm DVB/CAR GC-MS 

components Anal. Bioanal. Chem., 377, #4, 749-756 headspace 

Kim, Nam-Sun; Lee, Dong-Sun; Lee, Sun-Neo 

SPME and GC-MS of volatile compounds from 

1596 Volatiles from avocado puree after microwave processing headspace GC-MS 

avocado J. Chromatogr. A, 1036, #1, 87-90 30sec microwave 

Dorantes, A.; Guzman, G; Lopez, M. pH 5.5 

Sensory evaluation of the odour of a sunflower oil emulsion 

2462 Oxidative throughout oxidation headspace GC-MS 

byproducts in European J.Lipid Sci. Tech. 109, #1, 38-48 (JAN 2007) 50°C in dark 

sunflower oil Villiere, A.; Rousseau, Florence; Brossard, Chantal; Genot, C. 

Synergistic Effect of BSA on Antioxidant Activities in 

1597 Oxidative Model Food Emulsions GC+G742 

byproducts in J Am Oil Chem Soc, 81, #3, 275-280 

sunflower oil Almajano, M. Pilar; Gordon, Michael H. 

Evidence of the formation of light PAHs during the oxidation of edible 

2912 Oxidative oft in closed containers at room temperature headspace GC-MS 

byproducts in J Agr& Food Chemistry, 56, #6, 2028-2033 (MAR 26 2008) 

sunflower oil Guillen, M.; Goicoechea, E.; Palencia, Gemma; Cosmes, Nerea 





Study of both sunflower oil and its headspace throughout the 

1598 Oxidative oxidation process. Occurrence in the headsapce of headspace @ 70°C GC-MS 

byproducts in toxic oxygenated aldehydes 

sunflower oil J Agr& Food Chemistry, 53, #4, 1093-1101 

Guillen, Maria D.; Cabo, Nerea; Ibargoitia, Maria L.; Ruiz, A 

Bioavailability of permethrin and cyfluthrin in surface waters 

2847 Permethrin and with low levels of dissolved organic matter GC 

cyfluthrin in J Environmental Quality 36, #6, 1678-1685 (NOV-DEC 2007) 

surface waters Yang, W. C.; Hunter, W.; Spurlock, F.; Gan, J. 

SPME of permethrin residues from cucumber using 

1599 Permethrin a silica-bonded phase-coated stainless steel fibre 75µm Carboxen/PDMS GC 

on cucumbers Food Additives & Contaminants, 21, #3. 222-231 100µm PDMS 

Noroozian, E.; Kazemipour, M.; Tehrani, M.; Mahmoudian, M. headspace 

Application of headspace SPME and comprehensive 

1600 Volatiles in two-dimensional gas chromatography (GC x GC) for the headspace GC-GC 

herbal mixture chemical profiling of volatile oils in complex herbal mixtures 

J. Sep. Sci., 27, #5-6, 451-458 

Di, Xin; Huie, C.; Marriott, P.; Shellie, R. 

Determination of residual solvents content 

1601 Solvents in (hexane residue) in plant oil by headspace SPME headspace GC-FID 

plant oil Fenxi Shiyanshi, 23, #4, 70-72 

Lan, F.; Xie, L. Q.; Yang, Z.; Pan, K. Y.; Wu, C. 

Volatile organic compounds released by the entomopathogenic fungus 

2795 Volatiles from Beauveria bassiana headspace GC/MS 

Fungus Microbiological Research 163, #2, 148-151 (2008) 

Crespo, R.; Pedrini, N.; Juarez, M. P.; Dal Bello, G. M. 

HS-SPME-GC applied to rancidity assessment in bakery foods 

2874 Rancidity in European Food Res Tech 227, #1, 1-6 (May 2008) headspace GC/MS 

backery Purcaro, G.; Moret, S.; Conte, L. S. 

products 

Early detection of fungal growth in bakery products by use 

1602 Fungus of an electronic nose based on mass spectrometry headspace GC/MS 

backery J Agr Food Chem, 52, #20, 6068-6074 

products Vinaixa, M.; Marin, S.; Brezmes, J.; Llobet, E.; 

Vilanova, X.; Correig, X.; Ramos, A.; Sanchis, V. 

Mechanisms of extraction of aroma compounds from foods, using 

2192 Aroma adsorbents. Effect of various parameters headspace GC-MS 

compounds Food Reviews International 22, #1, 51-94 (2006) 

from food Nongonierma, A.; Cayot, P.; Le Quere, J.; Springett, M.; Voilley, A. 

Potential of SPME-GC for quarantine-required detection of wood 

2737 Odors from packaging in shipping containers. headspace GC-FID 

wood packaging J. Sep. Sci.30, #7, 1044-1051 (2007-05) 

More, N. A.; Braggins, T. J.; Goldson, S. L. 

Investigation of the interaction of active packaging 

1603 Odors from material with food aroma compounds headspace GC-MS 

packaging Sens Actuators, B Chem, 106, #1, 83-87 

Pastorelli, S.; Simoneau, C.; Strathmann, S. 

Solid-phase microextraction of N -nitrosamines. 

2566 N-nitrosamines J. Chromatogr., A 1117, #1, 11-18 (2006-06-02) CI-MS, NCD 

from water Grebel, J. E.; Young, C. C.; Suffet, I. H. NPD 

2565 N-nitrosamines 

On-site analysis of volatile nitrosamines in food model systems by 

solid-phase microextraction coupled to a direct extraction device DVB/CAR 50/30µm 

in gelatine system Talanta 70, #5, 1017-1023 (2006-12-15) 75µm Carboxen 

Ventanas, S.; Ruiz, J. 25°C 

A method for the determination of volatile N -nitrosamines 

1604 N-nitrosamines in food by HS-SPME-GC-TEA. 65µm PDMS-DVB GC-TEA 

in sausage Food Chemistry, 91, #1, 173-179 85µm polyacrylate 

Andrade, R.; Reyes, F. G. R.; Rath, S. headspace 

2474 Flavor 

SPME-comprehensive two-dimensional gas chromatography-TOF-MS 

for the analysis of honey volatiles DVB/CAR 50/30µm GC-MS 

Volatiles J. Sep. Sci. 30, #4, 534-546 (2007-03) headspace 

from honey Cajka, T.; Hajslova, J. ; Cochran, J.; Holadova, K.; Klimankova, E. 





SPME/GC/MS and sensory flavour profile analysis for estimation of 

2359 Flavor authenticity of thyme honey headspace GC-MS 

Volatiles Intl J of Food Sci & Tech 42, #2, 133-138 (FEB 2007) 

from honey Mannas, Demet; Altug, Tomris 

SPME-GC-MS analysis of volatile organic compounds in 

1605 Flavor honey from Basilicata. Evidence for the presence of GC-MS 

Volatiles pollutants from anthropogenic activities 

from honey Intl J Food Sci & Tech; 39, #10, 1079-1086 

Bentivenga, G; D'Auria, M; Fedeli, P; Mauriello, G; 

Racioppi, R 

SPME-GC-MS determination of monoterpenes in honey 

1606 Monoterpenes J. Sep. Sci.,27, #17-18, 1540-1544 100µm PDMS GC-MS 

in honey Pena, Rosa M.; Barciela, Julia; Herrero, C; Garcia-Martin, S 15min @ 20°C 

agitated, 25% salt 

Evaluation of four isolation techniques for honey 

1607 Aroma aroma compounds. headspace GC 

Volatiles J Sci of Food and Agriculture, 85, #1,91-97 

from honey Alissandrakis, E.; Tarantilis, P. A.; Harizanis, P.; Polissiou, M. 

Characterization of Spanish unifloral honeys by SPME-GC-MS 

1608 Aroma J. Sep. Sci., 28, #9-10, 1093-1100 headspace GC-MS 

Volatiles de la Fuente, Esther; Martinez-Castro, Isabel; Sanz, Jesus 

from honey 

Estimation of the honeydew ratio in honey samples from 

1609 Aroma their physicochemical data and from their volatile composition headspace GC-MS 

Volatiles obtained by SPME and GC-M 

from honey J Sci of Food and Agriculture, 85, #817-824 

Soria,A; Gonzalez, M; deLorenzo, C; MartinezCastro,I; Sanz, J 

Stir bar sorptive extraction of volatile compounds in vinegar: 

2848 Flavors in validation study and comparison with SPME headspace GC 

vinegars J Chromatogra, A, 1167, #1, 18-26 (OCT 5 2007) 

Duran Guerrero, E.; Natera Marin, R.; Castro Mejias, R.; Garcia Barroso,C. 

Three-way principal component analysis of the volatile fraction by 

2431 Flavors in HS-SPME/GC of aceto balsamico tradizionale of modena headspace GC 

vinegars Talanta 74, #4, 547-554 (Jan 15 2008) 

Cocchi, M.; Durante, C.; Grandi, M.; Manzini, D.; Marchetti, A. 

Vinegar classification based on feature extraction and selection from 

2360 Flavors in headspace SPME/GC volatile analyses: a feasibility study. headspace GC-MS 

vinegars Anal Chim Acta 608, # 1, 38-47 (2008 Feb 4) 

Pizarro, C; Esteban-Doez, I; Soaenz-Gonzoalez, C; Gonzoalez-Soaiz, J 

Profiling flavor compounds of potato crisps during storage 

1610 Flavors in using SPME 65µm PDMS-DVB GC-MS 

potato crisps J Chromatogra, A, 1064, #2, 239-245 20min @ 70°C 

Sanches-Silva, A; Lopez-Hernandez, J; Paseiro-Losada, P headspace 

Fast detection of rancidity in potato crisps using e-noses 

1611 Rancidity in based on mass spectrometry or gas sensors headspace GC-MS 

potato crisps Sens Actuators, B Chem, 106, #1, 67-75 

Badia, C.; Brezmes, J.; Correig, X.; Duran, C.; Llobet, E.; 

Vergara, A.; Vilanova, X.; Vinaixa, M. 

A fuzzy ARTMAP- and PLS-based MS e-nose for the 

1612 Rancidity in qualitative and quantitative assessment of rancidity of crisps headspace GC-MS 

potato crisps Sens Actuators, B Chem, 106, #2, 677-686 

Brezmes, J.; Correig, X.; Llobet, E.; Vilanova, X.; Vinaixa, M. 

2416 Fatty acids 

Flavouring of imitation cheese with enzyme-modified cheeses (EMCs): 

Sensory impact and measurement of aroma active short chain fatty headspace GC 

from cheese acids (SCFAs) 

FOOD CHEM. 106, #3, 905-913 (01 FEB 2008) 

Noronha, N.; Cronin, D. A.; O'Riordan, E. D.; O'Sullivan, M. 

Headspace SPME as a tool to estimate the contamination 

1613 PAHs in of smoked cheeses by polycyclic aromatic hydrocarbons 85µm polacrylate GC-MS 

smoked J of Dairy Science, 88, #1, 13-20 60min @ 70°C 

cheese Guillen, M. D.; Sopelana, P. headspace 





Application of artificial neural network on mono-and 

1614 Terpenes sequiterpenes compounds determined by headspace headspace GC-MS 

from cheese SPME-GC-MS for the Piedmont ricotta cheese traceability 

J Chromatogra, A, 1071, #1-2, 247-253 

Giuseppe, Z; Manuela, G; Marta, Bo; Vincenzo, G 

Calibration of gas chromatography inlet splitting for GC 

1615 Review of olfactometry dilution analysis GC 

technique Flavour Fragrance J., 19, #6, 518-521 

Acree, T.; Deibler, K.; Lavin, E.; Llesca, F. 

Volatile free fatty acids as ripening indicators for Serra 

1616 Volatile free da Estrela cheese headspace GC 

fatty acids in J Dairy Sci, 87, #12, 4064-4072 

cheese Tavaria, F. K.; Ferreira, A. C. Silva; Malcata, F. 

Composition and aroma compounds of Ragusano 

1617 Aroma of cheese: Native pasture and total mixed rations. headspace GC 

cheese J Dairy Sci, 87, #4, 816-830 

Carpino, S.; Mallia, S.; LaTerra, S.; Melilli, C.; Licitra, G.; 

Acree, T.; Barbano, D.; VanSoest, P. 

Comparison of purge and trap and SPME techniques for 

1618 Aroma of studying the volatile aroma compounds of three European headspace GC 

cheese PDO hard cheeses 

International Dairy Journal, 15, #6-9, 741-758 

Mallia, S.; Fernandez-Garcia, E.; Bosset, J. Olivier 

Characterization of "Provola dei Nebrodi", a typical Sicilian 

1619 Aroma of cheese, by volatiles analysis using SPME-GC/MS headspace GC-MS 

cheese International Dairy Journal, 15, #6-9, 585-593 

Ziino, M.; Condurso, C.; Romeo, V.; Giuffrida, D.; Verzera, A. 

Optimization of headspace SPME for the analysis of specific flavors 

2878 Aroma of in enzyme modified and natural Cheddar cheese using factorial 75µm Carboxen GC-MS 

cheese design and response surface methodology headspace 

J Chromatogr A, 1195, #1-2, 16-24 (Jun 27 2008) 50 min at 55 °C 

Azarnia, Sorayya; Januszkiewicz, Julien; Lee, Byong; Sabik, Hassan 3 M NaCl 

SPME and GC-MS for rapid characterisation of 

1620 Aroma of semi-hard cheeses headspace GC-MS 

cheese Anal. Bioanal. Chem., 380, #7-8, 930-936 

Condurso, C.; Romeo, V.; Verzera, A.; Zappala, M.; Ziino, M. 

Volatile sulfur compounds in Cheddar cheese determined 

1621 Sulfur compd by headspace SPME and GC-pulsed FPD 75µm Carboxen GC-PFPD 

in cheese J Chromatogr A, 1066, #1-2, 149-157 headspace 

Burbank, Helen M.; Qian, Michael C. 

Analysis of volatile aroma compounds of fresh chilli 

1622 Aroma of (Capsicum annuum) during stages of maturity using SPME headspace GC-MS 

chilli J Food Composition & Analysis, 18, #5, 427-437 30min @ 60°C 

Mazida, M. M.; Salleh, M. M.; Osman, H. 

SPME Ccmbined with GC and olfactometry-MS 

1623 Volaitles from for characterization of cheese aroma compounds. 75µm Carboxen GC-MS 

cheese Lebensmittel-Wissenschaft & Technologie, 37, #2, 139-154 headspace GC-olfactometry 

Frank, D.; Owen, C.; Patterson, J. 9-16hr extract 

Effect of wild strains used as starter cultures and adjunct cultures 

2879 Volatiles from on the volatile compounds of the Pecorino Siciliano cheese headspace GC/MS 

Siciliano cheese Intl J of Food Microbiology 122, #3, 269-278 (MAR 20 2008) 

Randazzo, C. L.; Pitino, I.; De Luca, S.; Scifo, G. O.; Caggia, C. 

Characterization of the chemistry, biochemistry and volatile profile 

2898 Flavors from of Kuflu cheese, a mould-ripened variety headspace GC/MS 

Kuflu cheese Food Sci. Technol. 41, #7, 1323-1334 (September 2008) 

Brechany, E.Y.; Deegan, K.C.; Hayaloglu, A.A.; McSweeney, P 

1624 Flavors from 

Improved determination of flavour compounds in 

butter by SPME & comprehensive two-dimensional GC headspace GC-GC-TOFMS 

butter J. Chromatogr. A 1086, #1-2, 99-106 

Adahchour, M., Brinkman, U.; Verdel, R., 

Vreuls, R.; Wiewel, J. 

GC-FID 





Effect of thickeners and sweeteners on the release 

1625 Aroma of blended aroma compounds in fat-free stirred headspace GC 

compounds yoghurt during shear conditions 

in yoghurt Intl Dairy Journal, 14, #9, 783-789 

Decourcelle, N.; Lubbers, S.; Vallet, N.; Rondeau, P.; 

Guichard, E. 

Optimization of SPME for the analysis of volatile 

1626 Volaitles from compounds in milk. headspace GC 

milk Journal of Dairy Science, 86, Supplement 1, 294 

Clarkson, H.; Duncan, S.; O'Keefe, S. 

Volatile compounds and chemical changes in 

1627 Volaitles from ultrapasteurized milk packaged in polyethylene headspace @ 5°C GC-MS 

milk terephthalate containers 

J of Food Science, 70. #6, C407-C412 

Solano-Lopez, C.; Ji, T.; Alvarez, V. 

Quality control of raw cows' milk by headspace analysis 

2808 Volaitles from Int. Dairy J. 18, #5, 506-513 (May 2008) headspace GC 

raw cow milk van Hooijdonk, A.C.M.; van Valenberg, H.J.F.; Hettinga, K.A. 

Development of a headspace SPME method combined 

1628 Phthalate w/ GC-MS for the determination of phthalate esters 60min @ 90°C. GC-MS 

esters in in cow milk headspace 

cow milk Analytica Chimica Acta, 538, #1-2, 41-48 NaCl added 

Feng, Yong-Lai; Zhu, Jiping; Sensenstein, R. 

Analytical methods applied to the determination of heterocyclic 

2814 Aromatic aromatic amines in foods Review article 

amines J Chromatogr B, 862, #1-2, 15-42 (FEB 1 2008) 

in food Sanz Alaejos, M.; Ayala, J. H.; Gonzalez, V.; Afonso, A. M. 

SPME coupled with HPLC for the analysis 

1629 Aromatic of heterocyclic aromatic amines. 50µm CW-TPR LC-diode array 

amines J Chromatogr A, 1030, #1-2, 87-93 methanolic NaOH 

in food Cardenes, L.; Ayala, J.; Afonso, A.; Gonzalez, V. 

SPME-GC-MS analysis of horseradish (Armoracia rusticana) 

1630 Isothiocynates Italian J Food Sci, 16, #4,487-490 GC-MS 

in horseradish D'Auria, M.; Mauriello, G.; Racioppi, R. 

Aroma profiles of five basil (Ocimum basilicum L.) cultivars grown 

2451 Volatiles from under conventional and organic conditions headspace GC-ITMS 

basil cultivars FOOD CHEM. 107, #1, 464-472 (01 MAR 2008) GC-TOFMS 

Klimankova, E.; Holadova, K.; Hajslova, J.; Cajka, T.; Poustka, J.; 

Koudela, M. 

Volatile compounds in different cultivars of Apium 

1631 Volatiles from graveolens L. headspace GC-MS 

cultivars Italian J Food Sci, 16, #4, 477-482 

Tirillini, B.; Pellegrino, R.; Pagiotti, R.; 

Pocceschi, N.; Menghini, L. 

Tequila volatile characterization and ethyl ester determination 

1632 Volatiles in by SPME-GC-MS analysis 100µm PDMS GC-MS 

tequila J Agri and Food Chem, 52, #18, 5567-5571 60min @ 40°C 

Vallejo-Cordoba, B.; Gonzalez-Cordova, A.; . immersed 

del Carmen Estrada-Montoya, M. 

Rapid determination of volatile compounds in grapes by 

1633 Volatile aroma HS-SPME coupled with GC-MS 65µm DVB-PDMS GC 

compounds Talanta, 66, #5, 1152-1157 20 min @ 70°C 

in grapes Sanchez-Palomo, E.; Diaz-Maroto, A. ; Perez-Coello, A. headspace 

Stable isotope dilution analysis of wine fermentation products 

1634 Fermentation by HS-SPME-GC headspace GC-MS 

products of Anal. Bioanal. Chem., 381, #4, 937-947 salt addition 

wines Capone, D.; Herderich, M.; Neuwohner, C.; Pardon, K.; 

Pollnitz, A.; Sefton, M; Skouroumounis, G.; 

Smyth, H.; Siebert, T. 

1635 Monoter- 

Comparison of ultrasound-assisted extraction and direct 

immersion SPME method for the analysis of monoterpenoids immersion GC-MS 

penoids in in wine 





wine Talanta, 67, #1, 129-135 

Barciela, J.; Garcia-Martin, S.; Herrero, C.; Pena, R. 


Impact odorants of Chardonnay dry white wine from Changli County 

European Food Res and Tech 227, #1, 287-292 (May 2008) headspace GC/MS 

white wine Li, Hua; Tao, Yong-Sheng; Wang, Hua; Zhang, Li 

Dynamic changes in ester formation during chardonnay juice 

2282 Ester compd in fermentations with different yeast inoculation and initial headspace GC-MS 

Chardonnay brix conditions 

juice. American J Enology and Viticulture 55 #3, 346-354 (2004) 

Lee, Seung-Joo; Rathbone, Da.; Asimont, S.; Adden, R.; Ebeler, S. 

Analytical method for determination of some 

1636 Volatiles in aroma compounds on white wines by SPME-GC 50/30µm DVB/CAR GC 

white wine J of Food Sci, 68, #9, 2817-2820 Headspace 

Ferreira, A.; Guedes de Pinho, P. 

Analysis of methoxypyrazines in wine using 

1637 Methoxy- headspace SPME with isotope dilution and Headspace GC-GC-NPD 

pyrazine comprehensive two dimensional GC GC-GC-TOFMS 

in wine J. Sep. Sci., 28, #9-10, 1075-1082 

Allen, M.; Marriott, P.; Ryan, D.; Smith, J.; Watkins, P. 

GC profile of volatiles in cheese induced by 

1638 Volatiles in different fat globule surface coatings. headspace GC 

cheese J of Dairy Science, 86, Supplement 1, 43 

Everett, D. ; Crownshaw, J.; Ginestet, A.; 

Leus, M.; Dufour, J.. 

Flavor stability of skim and whole milk powder 

1639 Flavors in J of Dairy Science, 86, Supplement 1, 40 GC 

milk products Whetstine, M.; Drake, M..; Karagul-Yuceer, Y.; Avsar, Y. 

GC-MS with SPME method for determination of 

1640 Methyl methyl salicylate and other volatile compounds in 100µm PDMS GC-MS 

salicylate in leaves of Lycopersicon esculentum. Headspace 

tomato leaves Anal. Bioanal. Chem., 378, #2, 518-522 

Deng, C; Zhang, X; Zhu, W; Qian, J 

SPME for flavor analysis in Harari Khat 

1641 Flavors in (Catha edulis) stimulant. 100µm PDMS GC-MS 

Harari Khat J. Zhejiang Univ: Sci, 5, #4, 428-431 30min @ 20°C 

stimulant Abdulsalam, Al-Flahi; Yin, Xue-Feng; Zou, Jian-Kai 

Interactions between volatile and nonvolatile coffee 

1642 Nonvolatiles components. Screening of nonvolatile components headspace GC 

from brewed J Agr Food Chem., 53, #11, 4417-4425 

coffee Charles-Bernard, M.; Kraehenbuehl, K.; 

Rytz, A.; Roberts, D. 

Impact of "ecological" post-harvest processing on the volatile fraction 

2649 Volatiles in of coffee beans: I. Green coffee headspace GC-MS 

coffee beans J. Food Compos. Anal. (UK) 20, #3-4, 289-96 (May 2007) 

Schorr-Galindo, S.; Gonzalez-Rios, O.; Suarez-Quiroz, M. L.; 

Boulanger, R.; Barel, M.; Guyot, B.; Guiraud, J.-P. 

Quality determination and group discrimination of shade grown 

2517 Volatiles in coffee using solid phase microextraction headspace GC-FID 

coffee beans 21st International Conference on Coffee Science, Montpellier, France, 

11-15 September, 2006 PP 306-309 

Jackson, M.; Steiman, S.; Gautz, L.; Bittenbender, H.; Idol, T. 

Comprehensive multidimensional GC for the 

1643 Volatiles in characterization of roasted coffee beans headspace GC-GC 

coffee beans J. Sep. Sci., 27, #5-6, 442-450 

Casilli, A., Costa, R.; Dugo, G., Dugo, P.; Festa, S.; 

Mondello, L.; Tranchida, P. 

Analysis of roasted coffee bean volatiles by using 

1644 Volatiles in comprehensive two-dimensional GC-TOF-MS headspace GC-GC-TOF-MS 

coffee beans J. Chromatogr. A, 1054, #1-2, 57-65 

Casilli, A.; Marriott, P.; Mondello, L.; Ryan, D.; 

Shellie, R.; Tranchida, P. 





Reliable characterization of coffee bean aroma 

1645 Volatiles in profiles by automated headspace SPME-GC-MS with headspace GC-MS 

coffee beans the support of a dual-filter mass a dual-filter spectra library 

J. Sep. Sci., 28, #9-10, 1101-1109 

Casilli, A, Costa, R; Dugo, G, Dugo, P; Festa, S; 

Mondello, L; Tranchida, P. 

Analysis of furan in foods by headspace SPME-GC-IT-MS 

2401 Furan in J. Chromatogr., A 1146, #1,103-109 (2007-03-30) 75µm Carboxen GC-IT-MS 

food Altaki, M. S.; Santos, F. J.; Galceran, M. T. headspace 

Development and validation of a SPME-GC-MS method for the 

2160 Furan in determination of furan in baby-food GC-MS 

baby-food J. Chromatogr. A, (2006) 1102, #1-2, 268-272 

Bianchi, Federica; Careri, Maria; Mangia, Alessandro; Musci, Marilena 

Impact of ionizing radiation and thermal treatments on furan 

2276 Furan in levels in fruit juice headspace GC-MS 

fruit juice J Food Science (2005) 70 #7, E409-E414 

Fan, Xuetong 

Determination of furan levels in coffee using 

1646 Furan in automated SPME-GC-MS headspace GC-MS 

coffee JAOAC Intl, 88, #2,574-576 

Ho, I-Pin; Yoo, Seong-Jae; Tefera, Sebhat 

SPME-GC-MS and multivariate analysis 

1647 Volatiles in for the characterization of roasted coffees headspace GC-MS 

roasted Talanta, 66, #1, 261-265 

coffee Zambonin, C.; Balest, L.; De Benedetto, G.; Palmisano, F. 

Volatile composition of Gutierrezia sarothrae (broom snakeweed) 

2212 Volatiles from as determined by steam distillation and SPME GC-MS 

broom J. Essent. Oil Res.18 #2, 121-125 (2006) GC-FID 

snakeweed Estell, R.; Fredrickson, E.; Lucero, M.; Morrison, A.; Richman, D. 

A direct liquid, non-equilibrium SPME application 

1648 Essential oils for analysing chemical variation of single peltate 100µm PDMS fiber GC-MS 

from leaves trichomes on leaves of Salvia officinalis immersed 

Phytochemical Analysis, 15, #3, 198-203 

Grassi, P.; Novak, J.; Steinlesberger, H.; Franz, C. 

GC-olfactometric characterization of aroma active 

1649 Aroma from compounds in sun-dried and vacuum-dried tarhana Headspace GC-FID 

Tarhana European Food Res &Tech, 218, #6, 573-578 

Goemen, D; Gurbuz, O; Rouseff, R; Smoot, J.; Dagdelen, A 

Lactic acid fermentation of Brassica rapa: 

1650 Aroma from chemical and microbial evaluation of a typical headspace GC-FID 

fermentation Italian product (brovada) 

process European Food Res &Tech, 218, #5, 469-473 

Maifreni, Michela; Marino, Marilena; Conte, L 

Monitoring acetaldehyde concentrations during micro-oxygenation of . 

2687 Acetaldehyde red wine by headspace SPME with on-fiber derivatization headspace GC-FID 

in red wine J Agr Food Chem 55, #14, 5620-5625 (2007) PFBH derivative 

Carlton, W. K.; Gump, B.; Fugelsang, K.; Hasson, A. S. 

Determination of haloanisoles in paper samples for food packaging 

2728 Haloanisoles from by solid-phase microextraction and gas chromatography DVB/CAR 50/30µm GC-MS 

packaging Microchim. Acta 159, #3-4, 229-234 (2007) headspace 

Martendal, E.; Budziak, D.; Debastiani, R.; Carasek, E. 30min @ 70°C 

Comparison of stir bar sorptive extraction and SPME to determine 

2792 Haloanisoles and halophenols and haloanisoles by GC-iontrap MS 

halophenols Talanta 75, #3, 753-759 (May 15 2008) headspace GC-iontrap MS 

in water Alonso, G.; Maggi, L.; Mazzoleni, V.; Salinas, M..; Zalacain, A. 

Multiple headspace solid-phase microextraction for eliminating matrix 

2686 Haloanisoles and effect in the simultaneous determination of haloanisoles and DVB/CAR 50/30µm GC-MS/MS 

halophenols volatile phenols in wines headspace 

in wine J. Chromatogr., A 1166, #1-2, 1-8 (2007) 

Pizarro, C.; Perez-del-Notario, N.; Gonzalez-Saiz, J. M. 





Optimisation of a headspace SPME with on-fiber derivatisation method 

2407 Haloanisoles and for the direct determination of haloanisoles and halophenols in wine. 85µm polacrylate GC-ECD 

halophenols J. Chromatogr., A 1143, #1-2, 26-35 (2007-03-02) 60min @ 70°C 

in wine Pizarro, C.; Perez-del-Notario, N.; Gonzalez-Saiz, J. M. headspace 

MSTFA derivative 

Study of chloroanisoles assay and TCA assay validation in wine and 

2289 Trichloroanisole cork stoppers soaked in dilute alcohol solution using headspace GC-MS/ 

from wine & cork SIDA-HSSPME-GC-MS/EI-SIM EI-SIM 

stoppers J Intl des Scie de la Vigne et du Vin 39 #3, 137-147 (2005) 

Chatonnet, P.; Labadie, Dominique; Boutou, S. 

Matrix effect during the application of a rapid method using HS-SPME 

2542 2,4,6-trichloro followed by GC-ECD for the analysis of 2,4,6-TCA in wine and cork soaks Headspace GC-ECD 

anisole in Food Chemistry 105, #2, 681-690 (2007) 

cork Vlachos, P.; Kampioti, A.; Kornaros, M.; Lyberatos, G. 

Relationship between sensory and instrumental 

1651 2,4,6-trichloro analysis of 2,4,6-trichloroanisole in wine and cork Headspace GC-ECD 

anisole in stoppers 

wine/cork Anal. Chim. Acta, 513, #1, 291-297 

Antico, E.; Garcia Regueiro, J.A.; Guerrero, L.; Insa, S.; . 

Juanola, R.; Salvado, V.; Subira, D 

Determination of fluoride in toothpaste using headspace SPME-GC-FID 

2452 Floride in J. Chromatogr., A 1150, #1-2, 173-177 (2007-05-25) 75µm Carboxen GC/FID 

toothpaste Wejnerowska, G.; Karczmarek, A.; Gaca, J. Headspace 

TMCS derivative 

Assay of stability, free and total concentration of 

1652 Chlloro- chlorhexidine in saliva by solid phasemicroextraction headspace GC 

hexidine in J Pharma and Biomed Analysis, 37, #5, 1015-1024 

saliva Musteata, Florin Marcel; Pawliszyn, Janusz 

Improving headspace-SPME of 3-isobutyl-2- 

1653 Pyrazines methoxypyrazine by experimental design with regard headspace GC-MS 

in wine to stable isotope dilution GC-MS analysis of wine saturated salt 

Anal. Chim. Acta, 513, #1, 223-227 

Lucchese, Y.; Nepveu, F.; Prouteau, C.; Renard, R.; 

Schneider, R.;Vaca-Garcia, C. 

Determination of terpenes in tequila by SPME-GC-MS 

2575 Terpenes in J. Chromatogr., A 1134, #1-2, 291-297 (2006-11-17) 100µm PDMS GC-MS 

tequila Pena-Alvarez, A.; Capella, S.; Juarez, R.; Labastida, C. 30min @ 25°C 

headspace, sat salt 

Optimization of SPME methods for GC-MS 

1654 Terpenes in determination of terpenes in wine 100µm PDMS GC-MS 

wine J Sci of Food and Agr, 85, #7, 1227-1234 15min @ 20°C 

Pena, R.; B, Julia; Herrero, C; Garcia-Martin, S. immersed 

25% NaCl 

Comparative study of sampling systems combined with gas sensors 

2677 Volatiles in for wine discrimination headspace GC 

Spanish wine Sens. Actuators B, Chem. (Switzerland) 126, #2, 616-23 (1 Oct. 2007) 

Lozano, J.; Santos, J.P.; Gutierrez, J.; Horrillo, M.C. 

Sensory profiling of aroma in Greek dry red wines using rank-rating 

2692 Volatiles in and monadic scoring related to headspace composition headspace GC 

Greek wine European Food Res. and Technology 225, #5-6, 749-756 (SEP 2007) 

Koussissi, Elisabeth; Paterson, Alistair; Piggott, John R. 

A survey of Saccharomyces populations associated with wine 

2845 Volatiles in fermentations from the Apulia region (South Italy) headspace GC 

wine yeast Annals of Microbiology 57, #4, 545-552 (2007) 

Tofalo, R.; Torriani, S.; Chaves-Lopez, C.; Martuscelli, M.; 

Paparella,Antonello; Suzzi, Giovanna 

Comparative study of aromatic compounds in young red wines from 

2614 Aromatic volatiles cabernet sauvignon, cabernet franc, and cabernet gernischet headspace GC 

in red wines varieties in China. 

J Food Sci 72, #5, C248-52 (2007 Jun) 

Zhang, M; Xu, Q; Duan, C; Qu, W; Wu, Y 

Factors influencing sensory quality in red wines of the variety 

2419 Volatiles in Aghiorghitiko (Vitis vinifera L.) from Nemea headspace GC-MS 

red wine Eur. Food Res. Technol. 226, #4, 745-753 (February 2008) 

Koussissi, Elisabeth; Paraskevopoulos, Yiannis; Paterson, Alistair 





Characterization of the aroma profile of Madeira wine 

1655 Volatiles in by sorptive extraction techniques headspace GC-MS 

red wine Anal. Chim. Acta, 546, #1, 11-21 

Alves, R.F.; Nascimento, A.M.D.; Nogueira, J.M.F. 

Development of headspace SPME-GC-MS methodology for 

2193 Terpenoids in analysis of terpenoids in Madeira wines 85µm polyacrylate GC-MS 

Madeira wines Anal. Chim. Acta 555. #2, 191-200 (2006) headspace 

Camara, J. S.; Alves, M. Arminda; Marques, J. C. 60-120min @ 

40°C w/salt 

Multivariate analysis for the classification and differentiation of 

2180 Flavors from Madeira wines according to main grape varieties headspace GC-MS 

Madeira wine Talanta 68,#5, 1512-1521 (2006) 

Alves, M. Arminda; Camara, Jose S.; Marques, Jose C. 

Vasconcelos, T. 

Varietal flavour compounds of four grape varieties 

1656 Flavors from producing Madeira wines dynamic headspace GC-MS 

Madeira wine Analytica Chimica Acta, 513, #1, 203-207 

Camara, J.; Herbert, P.; Marques, J.; Alves, M. 

Elimination of matrix effects for headspace SPME of 

1657 Volatiles in important volatile compounds in red wine using a novel coating 65µm PDMS-DVB, GC 

red wine Anal. Chim. Acta, 540, #2, 341-353 85µm polyacrylate 

Liu, Mingming; Tian, Yun; Zeng, Zhaorui 100µm PDMS 

headspace 

Sensitive quantification of sulfur compounds in wine by 

1658 Sulfur headspace solid-phase microextraction technique headspace GC-FPD 

compounds J. Chromatogr. A, 1080, #-2, 177-185 

in wine Fang, Yu; Qian, Michael C. 

Screening of grapes and wine for azoxystrobin, 

1659 Fungicides kresoxim-methyl and trifloxystrobin fungicides headspace GC-MS 

on grapes by HPLC with diode array detection 

Food Additives and Contaminants, 22, #6, 549-566 

Abreu, S.; Correia, M.; Herbert, P.; 

Santos, L.; Alves, A. 

Determination of 2,4,6-tribromoaniline in the color additives 

1660 Tribromo- D&C Red Nos. 21 and 22 (Eosin Y) using SPME-GC-MS headspace GC-MS 

aniline in J. Chromatogr. A, 1057, #1--2, 185-191 

color additives Andrzejewski, Denis; Rasooly, Irit R.; Weisz, Adrian 

Determination of Ochratoxin A in foods: State-of-the-art 

1661 Ochratoxin A and analytical challenges LC-FLD 

in foods Anal. Bioanal. Chem., 378, #1, 96-103 

Monaci, Linda; Palmisano, Francesco 

Comparative analysis of volatile compounds of 

1662 Volatiles in "fino" sherry wine by rotatory and continuous liquid- headspace GC-MS 

sherry wine liquid extraction and SPME in conjunction w/GC-MS 

Anal. Chim. Acta, 513, #1, 141-150 

Barroso, C.G.; Benitez, P.; Castro, R.; Natera, R. 

Application of a wavelet-based algorithm on 

1663 Volatiles in headspace SPME-GC signals for the classification headspace GC-MS 

vinegars of balsamic vinegars. 

Chemometrics and Intelligent Lab Systems, 71, #2, 129-140 

Cocchi, M.; Durante, C.; Foca, G.; Manzini, D.;. 

Marchetti, A.; Ulrici, A. 

Flavour release and rheology behaviour of 

1664 Flavors from strawberry fat-free stirred yogurt during storage. headspace @ 10°C GC 

yogurt J Agri and Food Chemistry, 52, #10, 3077-3082 stirred 

Lubbers, S.; Decourcelle, N.; Vallet, N.; Guichard, E. 

Solid-phase aroma concentrate extraction (SPACE): 

1665 Aroma of a new headspace technique for more sensitive headspace GC-MS 

coffee beans analysis of volatiles 

Flavour & Fragrance Journal, 19, #3, 183-187 

Ishikawa, M.; Ito, O.; Ishizaki, S.; 

Kurobayashi, Y.; Fujita, A. 

Comparison of volatile compounds formed by 

1666 Volatiles from autoxidation and photosensitized oxidation of cod 40°C headspace GC-MS 





cod liver oil liver oil in emulsion systems ferrous chloride added GC-FID 

Fisheries Science (Tokyo), 71, #3, 639-647 foil lined sample vial 

Pan, Xiang-Qing; Ushio, Hideki; Ohshima, Toshiak 

Detection of 2,4,6-trichloroanisole in microorganism- 

1667 2,4,6- free irradiated raisins by SPME-GC-MS 50/30µm DVB/CAR GC-MS 

trichloroanisole J Stored Products Res, 40, #4, 451-459 headspace 

in raisins Aung, L. H.; Jenner, J. F. 

Use of multiple headspace SPME and pervaporation for the 

2283 Haloanisoles determination of off-flavours in wine headspace GC-MS 

in wine J. Chromatogr. A, 1112, #1-2,133-140 (2006) 

Beltran, R.; Garcia-Barrera, T.; Gomez-Ariza, J.L.; Lorenzo, F. 

Simultaneous separation, clean-up and analysis 

1668 Anisoles in of musty odorous compounds in wines by on-line headspace GC-MS-MS 

wines coupling of a pervaporation unit to GC- tandem MS 

Anal. Chim. Acta, 516, #1-2, 165-170 

Garcia-Barrera, T.; Gomez-Ariza, J.L.; Lorenzo, F. 

Optimisation of a two-dimensional on-line coupling 

1669 Anisoles in for the determination of anisoles in wineusing ECD headspace GC-ECD-ICP-MS 

wines and ICP-MS after SPME-GC separation 

Jof AnalyAtomic Spectrometry, 20, #9, 883-888 

Gomez-Ariza, J. L.; Garcia-Barrera, T.; Lorenzo, F. 

Aroma profile of strawberry juice cocktail produced 

1670 Aroma volatile in industrial conditions 100µm PDMS GC-FID and GC-MS 

from Kem Ind, 54, #3, 135-141 headspace 

stawberry Cosic, B.; Ganic, K. Kovacevic; Komes, D.; Lovric, T. 

juice 

Assessment of strawberry aroma through SPME- 

1671 Aroma GC and artificial neuron network methods. Variety headspace GC-MS 

volatiles from Classification versus growing years. 

stawberry J Agri Food Chemistry, 52, #9, 2472-2478 

deBoishebert, V.; Urruty, L.; Giraudel, J.; Montury, M. 

Hollow fiber membrane-protected SPME of triazine 

1672 Triazine herbicides in bovine milk and sewage sludge samples 65µm PDMS-DVB GC-MS 

herbicides in J. Chromatogr. A, 1047, #2, 189-194 

milk/ sludge Basheer, Chanbasha; Lee, Hian Kee 

2455 Acrylamide 

Determination of acrylamide in food by SPMEGC posittive chemical 

ionization tandem mass spectrometry. 50µm CW/DVB GC-PCI-MS-MS 

in water solutions Anal. Chim. Acta 582, #1, 19-23 (2007-01-16) immersion 

Lee, M. R.; Chang, L. Y.; Dou, J. P. 20 min @ pH 7 

Silylation of acrylamide for analysis by SPME-GC 

1673 Acrylamide ion-trap mass spectrometry 100µm PDMS GC-MS 

in cereals J Agri and Food Chem, 52, #12, 3744-3748 BSTFA derivative 

Lagalante, Anthony F.; Felter, Matthew A. headspace 

Influence of quinoxyfen residues on Saccharomyces 

1674 Quinoxyfen cerevisiae fermentation of grape musts GC 

pesticide in Food Tech and Biotechnology, 42, #2, 89-97 

grape musts Lopez, C; Boselli, E; Piva, A; Ndaghijimana, M; 

Paparella, A; Antonello; S; Mastrocola, D 

Influence of vine training and sunlight exposure 

1675 Pyrazine in on the 3-alkyl-2-methoxypyrazines content in headspace GC 

musts/wines musts and wines from Vitis vinifera variety 

cabernet sauvignon 

J Agri and Food Chemistry, 52, #11, 3492-3497 

Sala, C; Busto, O; Guasch, J; Zamora, Fernando 

The effects of sample preparation and GC injection 

1676 Volatiles from techniques on the accuracy of measuring quaiacol, headspace GC-MS 

oak in wine 4-methylguaiacol and other volatile oak compounds 

in oak extracts by stable isotope dilution analyses 

J Agri and Food Chemistry, 52, #11, 3244-3252 

Pollnitz, A.; Pardon, K.; Sykes, M; Sefton, M. 

Analysis of oak volatiles by GC-MS after ozone sanitization 

1677 Volatiles American J Enology & Viticulture, 56, #1, 46-51 headspace GC-MS 

from Oak Marko, S.; Dormedy, E.; Fugelsang, K.; Dormedy, D.; 5, 10, 15min sampling 





Gump, B.; Wample, Robert 82°C 

Fast screening method for volatile compounds of oak wood 

1678 Volatiles used for aging wines by headspace SPME-GC-MS (SIM) 50/30µm DVB/CAR GC-MS (SIM) 

from Oak J Agri and Food Chemistry, 52, #23, 6857-6861 40min @ 70°C 

wood Diaz-Maroto, M.; Sanchez-Palomo, Eva; Perez-Coello, M. Headspace 

Rapid analysis of flavor volatiles in apple wine 

1679 Volatiles in using headspace SPME 75µm Carboxen GC-MS 

apple wine J Institute of Brewing, 110, #1, 57-65 Headspace 

Wang, L.; Xu, Y.; Zhao, G.; Li, J. 

Markers for irradiated food 

1680 Volatiles from Chem. World, 2, #2, 20 headspace GC 

irradiated food Down, Steve 

Effects of cooking conditions on sensory characteristics of red-cooked 

2833 Flavor compounds beef flavor and identification of the flavor compounds headspace GC/MS 

from red-cooked J Food Process Eng 31, #1, 51-65 (Feb 2008) 

beef Cui, Chun; Wang, Jinshui; Wu, Jinwei; Wu, Xiao; Yang, Bao; Zhao, M. 

Analysis of odor-active components of simulated beef flavor by 

2257 Odor-active SPME-GC-olfactometry GC/MS 

components Abstracts of Papers Am Chem Society (2004) 228, #1, U68 

of beef flavor Moon, Soo Yeun; Cliff, Margaret A.; Li-Chan, Eunice C. Y. 

Development of SPME methodology for analysis 

1681 Volatiles from of headspace volatile compounds in 50/30µm DVB/CAR GC 

Beef simulated beef flavour. 60min @ 60°C 

extract Food Chemistry, 88, #1, 141-149 headspace 

Moon, S. Y.; Li-Chan, E. C. Y.* 

Identification of radiolytic marker compounds in the 

1682 Volatiles from irradiated beef extract powder by volatile analysis headspace @ 30°C GC 

Beef Microchemical Journal, 80. #2, 127-137 

extract Kim, Hun; Cho, Woo-; Ahn, Jun-; Cho, Dooe; Cha, Yong- 

Characterization of volatile compounds of fruit juices 

1683 Volatiles from and nectars by headspace SPMEand GC-MS. headspace GC/MS 

fruit juices Food Chemistry, 87, #4, 627-637 

Riu-Aumatell, M.; Castellari, M.; Lopez-Tamames, E.; 

Galassi, S.; Buxaderas, S. * 

Effect of fat nature and aroma compound hydrophobicity 

1684 Volatiles from on flavor release from complex food emulsions headspace GC-MS 

food emulsions J Agr and Food Chem, 52, #20, 6257-6263 

Relkin, Perla; Fabre, Marjorie; Guichard, Elisabeth 

Characterization of volatile compounds of French 

1685 Volatiles from and Spanish virgin olive oils by HS-SPME: I. headspace GC-RI and GC-MS, 

olive oil identification of quality-freshness markers 

Food Chemistry, 88, #1, 151-157 

Cavalli, J; Fernandez, X.; Lizzani-Cuvelier, L; Loiseau, A 

Oxidation of lipids in food 

1686 Oxidative Polish JFood and Nutrition Sci, 13, #1, 87-100 headspace GC 

byproducts Wasowicz, E; Gramza, A; Hes, M; Jelen, H;Korczak,J; 

from lipids Malecka, M; Mildner-Szkudlarz, S; Rudzinska, M; 

Samotyja, U; Zawirska-Wojtasiak, R 

Photo-oxidation of lipids impregnated on the surface 

1687 Volatiles from of dried seaweed (porphyra yezoensis ueda). headspace @ 45°C GC-FID and GC-MS, 

sea weed Characterization of volatiles 

JAOCS, 81, #8, 773-781 

Ohshima, Toshiaki; Pan, Xiangqing; Ushio, Hideki 

Lipid oxidation in high-pressure processed chicken 

1688 Oxidation breast during chill storage andsubsequent heat 10min @ 80°C GC-MS 

byproducts treatment: effect of working pressure, packaging headspace 

from chicken atmosphere and storage time 

European Food Res and Tech, 219, #2, 167-170 

Wiggers, S.; Kroeger-Ohlsen, M.; Skibsted, L. 


Determination of organic volatile impurities in citric acid 

by SPME-GC GC-MS 

Citric acid Fenxi Shiyanshi, 24, #1, 43-45 





Li, L. H.; Zheng, L.; Guo, W. 

Determination of hexanal as indicator of the lipidic 

1690 Hexanal in oxidation state in potato crisps using GC and HPLC headspace GC-MS 

potato crisps J. Chromatogr. A, 1046, #1-2, 75-81 2,4-dinitrophenyl- HPLC 

Lopez-Hernandez, J.; Paseiro-Losada, P.; Rodriguez- hydrazone derivative. 

Bernaldo De Quiros, A.; Sanches-Silva, A. 

Variation in 4-mercapto-4-methyl-pentan-2-one release 

1691 Volatile thiol by Saccharomyces cerevisiae commercial wine strains headspace GC-AED 

from wine FEMS Microbiology Letters, 240, #2, 125-129 

Howell, K.; Swiegers, J.; Elsey, Go.; Siebert, T.; 

Bartowsky, E.; Fleet, G.; Pretorius, I.; Lopes, M. 

Determination of volatile compounds in wine by 

1692 Volatiles automated SPME-GC headspace GC-FID 

in wine Chromatographia, 59, #11-12, 733-738 

Cabredo-Pinillos, S.; Cedron-Fernandez, T.; 

Parra-Manzanares, A.; Saenz-Barrio, C. 

Evaluation of the antimicrobial activity of citrus 

1693 Off taste of essences on Saccharomyces cerevisiae headspace GC-MS 

soft drink J Agrl and Food Chemis, 52. #23, 6932-6938 

Belletti, Nicoletta; Ndagijimana, Maurice; Sisto, C 

Guerzoni, Maria E.; Lanciotti, Rosalba; Gardini, F. 

Phenylacetaldehyde O-methyloxime: A volatile 

1694 Methyloxime compound produced by grapefruit leaves infected oxime methyl ether GC-MS 

in grapefruit with the citrus canker pathogen, Xanthomonas derivatives 

leaves axonopodis pv. citri headspace 

J Agrl and Food Chemis, 53. #13, 5134-5137 

Zhang, Aijun; Hartung, John S. 

Analysis and characterization of aroma-active compounds 

1695 Aroma of Schizandra chinensis (omija) leaves. headspace GC-MS 

of leaves J Sci of Food and Agriculture, 85, #1, 161-166 

Zheng, C. H.; Kim, K. H.; Kim, T. H.; Lee, H. J.* 

Comparison of three different SPME fibres for analysis of 

1696 Essential oils essential oils in yacon (Smallanthus sonchifolius) leaves 100µm PDMS GC-FID 

from yacon J. Chromatogr. A, 1084, #1-2, 2-6 65µm PDMS-DVB 

leaves Adam, M.; Bajer, T.; Eisner, A.; Juklova, M.; Ventura, K. 50/30µm DVB/CAR 

headspace 

Separation and identification of volatile constituents in Artemisia argyi 

2856 Volatiles from flowers by GC-MS with SPME and steam distillation headspace GC-MS 

argyi flowers J. Chrom. Sci 46, #5, 401-405 (MAY-JUN 2008) 

Li, Ning; Mao, Yu; Deng, Chunhui; Zhang, Xiangmin 

Comparison of essential oil composition of Artemisia 

1697 Essential oils argyi leaves at different collection times by headspace GC-MS 

from argyi headspace SPME-GC-MS 

leaves Chromatographia, 59, #11-12, 729-732 

Zheng, X. H.; Deng, C. H.; Song, G. X.; Hu, Y. M.* 

A SPME method to fingerprint dissolved organic 

1698 Essential oils carbon released from Eucalyptus camaldulensis 100µm PDMS GC 

from Dehnh (River Red Gum) leaves 15min @ 40°C, pH 2 

Eucalyptus Analytica Chimica Acta, 530, #2, 325-333 saturated salt 

leaves Zander, Alek; Bishop, Andrea G.; Prenzler, Paul D. rapid stirring 

Instrumental versus sensory detection of off- 

1699 Off flavors flavors in farm-raised channel catfish headspace GC-MS 

in catfish Aquaculture, 236, #1-4, 309-319 

Grimm, Casey; Lloyd, Steven; Zimba, Paul 

Composition of the essential oils and in vivo emission 

1700 Volaitiles from of volatiles of four Lamium species from Italy: L. headspace GC-MS 

essential oils purpureum, L hybridum , L bifidum & L.amplexicaule. 

Food Chemistry, 91, #1, 63-68 

Flamini, G.; Cioni, P. L.; Morelli, I. 


The use of a non-equilibrated SPME method to 

quantitativelydetermine the off-notes in mint and headspace GC/SIM-MS 

essential oils other essential oil 

J Sci Food & Agri, 84, #10, 1223-1228 

Coleman, W. M., III.; Lawrence, B. M.; Craven, S. H. 





Effect of gamma-irradiated red pepper powder on the chemical 

2277 Volatiles in and volatile characteristics of kakdugi, a Korean traditional headspace 

red pepper fermented radish kimchi 

J Food Science 70 #7, C441-C447 (2005) 

Lee, Jeung Hee; Lee, Ki-Teak; Kim, Mee Ree 

Effect of gamma-irradiation on color, pungency, and 

1702 Volatiles in volatiles of Korean red pepper powder headspace GC-MS 

red pepper Journal of Food Science, 69, #8, C585-C592 

Lee, J. H.; Sung, T. H.; Lee, K. T.; Kim, M. R. 

Analysis of the isothiocyanates present in cabbage 

1703 Isothiocyanate leaves extract and their potential application headspace GC-MS 

in cabbage to controlAlternaria rot in bell peppers 

leaves Food Res Intl., 38, #6, 701-708 

Troncoso, R.; Espinoza, C.; Sanchez-Estrada, A.;S. 

Tiznado, M. E.; Garcia, Hugo S. 

New approach for the detection of organophosphorus 

1704 Organo- pesticide in cabbage using SPME/SnO2 gas sensor: headspace GC 

phosphate Principle and preliminary experiment 

in cabbage Sens Actuators, B Chem, 102, #2, 235-240 

Huang, Xingjiu; Liu, Jinhuai; Meng, Fanli; Sun, Yufeng 

Determination of off-flavour compounds in apple juice caused 

1705 Off flavor by microorganisms using headspace SPME-GC-MS headspace GC-MS 

in apple juice Anal. Chim. Acta, 520, #1-2, 3-11 

Pfannhauser, W.; Siegmund, B.; Zierler, B. 

Study of the effect of different fiber coatings and 

1706 Volatiles from extraction condition on dry cured ham volatile 75µm Carboxen GC 

cured ham compounds extracted by SPME 50/30µm DVB/CAR 

Talanta, 64, #2, 458-466 15, 30, 60min extraction 

Ansorena, D.; Astiasaran, I.; Garcia-Esteban, M.; Ruiz, J. headspace 

saturated NaCl 

Comparison of simultaneous distillation extraction and SPME 

1707 Volatiles in for the analysis of volatile compounds in dry-cured ham. 75µm Carboxen GC-MS 

cured ham J Sci Food and Agri, 84, #11, 1364-1370 headspace 

Garcia-Esteban, M.; Ansorena, D.; Astiasaran, I.; 

Martin, D.; Ruiz, J. * 

Characterization of French and Spanish dry-cured hams: 

1708 Volatiles from influence of the volatiles from the muscles and the headspace GC 

hams subcutaneous fat quantified by SPME-GC 

Meat Science, 69, #4, 635-645 

Sanchez-Pena, C.; Luna, G; Garcia-Gonzalez, D.; Aparicio, R 

Optimisation of a headspace SPME method for the direct 

1709 Chloroanisoles determination of chloroanisoles related to cork taint in red wine headspace GC-ECD 

in wine J. Chromatogr. A, 1056, #1-2, 49-56 

Gonzalez-Saiz, J.; Martinez-Urunuela, A.; Pizarro, C. 

A sensitive SPME-GC-based procedure for determining . 

2485 Pentachlorophenol pentachlorophenol in food headspace MIP-AED 

in food Food Addit Contam 24, #7, 777-83 (2007 Jul) as derivative 

Campillo, Natalia; Peonalver, Rosa; Hernoandez-Coordoba, Manuel 

Multiple SPME in a non-equilibrium situation: Application in 

1710 Chlorophenols quantitativeanalysis of chlorophenols and chloroanisoles headspace GC-MS 

in wine related to cork taint in wine 

J. Chromatogr. A, 1089, #1-2, 31-38 

Gonzalez-Saiz, J.; Martinez-Urunuela, A.; Pizarro, C. 

Ethanol/water extraction combined with SPE and SPME 

2206 Chlorophenols concentration for determination of chlorophenols in cork stoppers 

in cork J Ag Food Chem, 54, #3, 627-632 (2006) 

Insa, S.; Besalu, E.; Iglesias, C.; Salvado, V.; Antico, E. 

Development of solid-phase extraction and SPME 

1711 Chlorophenols methods for the determination of chlorophenols 100µm PDMS GC-ECD 

in cork/wine in cork macerate and wine samples Acetylation derivative 

J. Chromatogr. A, 1047, #1, 15-20 headspace 

Antico, E.; Insa, S.; Salvado, V. 

Migration of 2,4,6-trichloroanisole from cork stoppers to wine 





1712 2,4,6-Trichloro- European Food Research and Tech, 220, #3-4,347-352 headspace GC-ECD 

anisole in wine Juanola, R.; Subira, D.; Salvado, V.; Regueiro, J.; Antico, E. 

Classification of Boal, Malvazia, Sercial and Verdelho wines based 

2668 Monoterpenoids on terpenoid patterns headspace GC-MS 

in wine FOOD CHEM. 101, #2, 475-484, (2007) 

Camara, J. S.; Alves, M. A.; Marques, J. C. 

Inhibition of the decline of volatile esters and terpenols 

1713 Volatile esters during oxidative storage of Muscat-white and Xinomavro- headspace GC-MS 

in wine red wine by caffeic acid and N-acetyl-cysteine 20°C heated sample 

Food Chemistry, 93. #3, 485-492 

Roussis, I.; Lambropoulos, I; Papadopoulou, D 

Volatile compounds of red and white wines by headspace 

1714 Volatiles in SPME using different fibres. 50/30µm DVB/CAR GC 

wine J of Chromatographic Sci, 42, #6, 310-316 40min @ 35°C 

Torrens, J.; Riu-Aumatell, M.; Lopez-Tamames, E.; headspace 

Buxaderas, S. * 

Optimisation of a two-dimensional on-line coupling for 

1715 Haloanisoles the determination of anisoles in wine using ECD headspace GC-ICP-MS 

in wine and ICP-MS after SPME-GC separation GC-ECD 

J Anal At Spectrom, 20, #9, .883-888 

Garcia-Barrera, T.; Gomez-Ariza, J.L.; Lorenzo, F. 

A review of theoretical and practical aspects of SPME 

1716 Impurities in food analysis headspace GC 

constituents IntL J Food Sci & Technology, 39, #7, 703-717 

additives Wardencki, Waldemar; Michulec, Magdalena; Curylo, J. 

flavours 

2432 Flavour from 

Evaluation of SPME-GC-MS for the headspace analysis of 

volatile compounds in cocoa products 50/30μm DVB/CAR GC-MS 

cocoa Talanta 74, #5, 1166-1174 (Feb 15 2008) 60°C for 15 min 

Ducki, S.; Miralles-Garcia, J.; Storey, D..; Tornero, A.; Zumbe, A. headspace 

Characterization of pyrazines in some Chinese liquors and their 

25% NaCl 

2849 Pyrazine in approximate concentrations headspace GC-FTD 

chinese liqours J Agri Food Chemistry, 55, #24, 9956-9962 (NOV 28 2007) 50°C for 30 min 

Fan, Wenlai; Xu, Yan; Zhang, Yanhong 

Satr.NaCl 

Relationship between procyanidin and flavour contents 

1717 Flavour from of cocoa liquors from different origins. headspace HPLC-UV 

cocoa liqours J Agri Food Chemistry, 52, #20, 6243-6249 

Counet, C.; Ouwerx, C.; Rosoux, D.; Collin, S. 

Cocoa quality and processing: A study by SPME and GC 

1718 Methylpyrazine analysis of methylpyrazines headspace GC-MS 

in cocoa Food Bioprod. Process., 82, #4C, 291-297 

Cavicchioli, M.; Del Borghi, M.; Fabiano, B.; Perego, P. 

Optimisation of the derivatisation reaction and 

1719 Chlorophenol subsequent headspace SPMEmethod for the direct headspace GC 

in red wine determination of chlorophenols in red wine acetylated derivaties 

J. Chromatogr. A, 1048, #2, 141-151 

Gonzalez-Saiz, J; Martinez-Urunuela, A; Pizarro, C. 

Headspace SPME-GC-MS analysis of the volatile 

1720 Volatiles compounds of Evodia species fruits 50/30µm DVB/CAR GC-MS 

from dried J. Chromatogr. A, 1087, #1-2, 265-273 18min @ 80°C 

fruit Benvenuti, S; Bertelli, D; Pellati, F; Rossi, M; Yoshizaki, F. headspace 

Comparison of SPME, SFE, steam distillation, and solvent 

1721 Volatiles extraction techniques for analysis of volatile consituents headspace GC-MS 

from dried in Fructus amomi 

ripe fruit J AOAC Intl, 88, #2, 418-423 

Shen, S; Sha, Y; Deng, C; Fu, D; Chen, ; Zhang, Xian 

Rapid analysis of essential oil from Fructus Amomi by 

1722 Volatiles pressurized hot water extraction followed by SPME-GC-MS headspace GC-MS 

from dried J Pharma& Biomedical Analysis, 38, #2, 326-331 15min @ 80°C 





ripe fruit Deng, C; Wang, A; Shen, S; Fu, D; Chen, J; Zhang, X 

Sensory and instrumental evaluation of sweet marjoram 

1723 Volatiles (Origanum majorana L.) aroma headspace GC 

from sweet Flavour Fragrance J., 20, #5, 492-500 

marjoram Baranauskiene, R.; Demyttenaere, J.C.R.; Venskutonis, P. 

Characterization of aroma potential of apricot varieties using 

2688 Arom different extraction techniques headspace GC-MS 

compouonds Food Chem 105, #2, 829-837 (2007) 

apricots Solis-Solis, H. M.; Calderon-Santoyo, M.; Schorr-Galindo, S.; 

Luna-Solano, G.; Ragazzo-Sanchez, J. A. 

Discrimination of eight varieties of apricot (Prunus armeniaca) by 

2629 Arom electronic nose, LLE and SPME using GC-MS and multivariate analysis headspace GC-MS 

compouonds Sens. Actuators B, Chem. (Switzerland) 125, #2, 415-21 (8 Aug. 2007) 

apricots Solis-Solis, H.M.; Calderon-Santoyo, M.; Gutierrez-Martinez, P.; 

Schorr-Galindo, S.; Ragazzo-Sanchez, J.A. 

Trehalose improves flavour retention in dehydrated 

1724 Arom apricot puree headspace GC-FID 

compouonds Intl J Food Science & Tech, 40, #4, 425-435 GC-MS 

apricot puree Komes, D; Lovric, T; Kovacevic G, Karin; 

Gajdos Kljusuric, Jasenka; Banovic, Mara 

Rapid white truffle headspace analysis by proton transfer reaction 

2651 Aroma Volatiles mass spectrometry and comparison with SPME-GC-MS headspace GC-MS 

from white Rapid Comm Mass Spectrometry 21, #6, 2564-2572 (2007) 

truffle Aprea, E.; Biasioli, F.; Carlin, S.; Versini, G.; Maerk, T.; Gasperi, F. 

Aroma characterisation of white truffle by GC-MS and GC-O 

2203 Aroma Volatiles Italian J Food Sci., 17 #4, 463-468 (2005) headspace GC-MS 

from white Piloni, M.; Tat, L.; Tonizzo, A.; Battistutta, F. 

truffle 

Volatile components of truffle species collected in Basilicata 

1725 Volatiles from Micologia Italiana, 30, #3, 11-29 headspace GC-MS 

truffles Mauriello, G.; Marino, R.; D'Auria, M.; Cerone, G.; Rana, G. L. 

Sensitive detection of volatile organic compounds 

1726 Volatiles from (MVOC) produced by mould by means of SPME-GC-MS headspace GC-MS 

mould Naunyn-Schmiedeberg's Archives of Pharmacology 

369, Suppl 1, R145 

Schuetz, E. 

Application of SPME for determining phenylurea herbicides 

1727 Phenylurea and their homologous anilines from vegetables. 85µm polyacrylate GC-NPD 

herbicides on J Chromatogr, A, 1042, #1-2, 9-14 headspace GC-MS-SIM 

vegetables Berrada, H.; Font, G.; Molto, J. C.* 14% salt, pH 11 


Chemical analysis of French beans ( Phaseolus vulgaris L.) by 

headspace SPME and simultaneous distillation/extraction 65µm DVB/PDMS GC-MS 

French beans Food Chem. 101, #3, 1279-1284 (2007) 

Barra, A.; Baldovini, N. ; Loiseau, A.; Albino, L.; Lesecq, C.; Cuvelier, L. 

headspace 

Development of GC-MS with microwave distillation and simultaneous 

2354 Volatiles in SPME for rapid determination of volatile constituents in ginger 65µm DVB/PDMS GC-MS 

ginger J. Pharm. Biomed. Anal. 43, #1, 24-31 (2007-01-04) microwave digested 

Yu, Y. J.; Huang, T. M.; Yang, B.; Liu, X.; Duan, G. L. 

GC-mass Spectrometry coupled with SPME for 

1728 Volatiles in determination of volatile constituents of chinese ginger 100µm PDMS GC-MS 

ginger Fudan Xuebao Zirankexueban, 42, #6, 939-949 headspace 

Song Guo-xin; Deng Chun-hui; Wu Dan; Hu Yao-ming 

Yield effects on 2-methoxy-3-isobutylpyrazine 

1729 MIBP in red concentration in Cabernet Sauvignon using a SPME-GC-MS 50/30µm DVB/CAR GC-MS 

wine J of Agri Food Chemistry, 52, #17, 5431-5435 30min @ 40°C 

Chapman, D. M.; Thorngate, J. H.; Matthews, M. A.; 30% NaCl 

Guinard, J. -X.; Ebeler, S. E.* immersed sampling 

2280 MIBP in red 

Pruning effects on 2-methoxy-3-isobutylpyrazine concentration in 

cabernet sauvignon using a new SPME GC-MS quantification method 

wine American J Enology and Viticulture 55 #3, 296A (2004) 

Chapman, D.; Matthews, M.; Guinard, J.; Ebeler, S. 





Simplified method for detection and quantification of 2-methoxy-3- 

2281 MIBP in isobutylpyrazine in wine headspace GC-MS 

wine American J Enology and Viticulture 55 #3, 276-278 (2004) 

Wampfler, Daniel J.; Howell, G. S. 

Techniques of preparing plant material for chromatographic 

2463 Review article separation and analysis 

J of Biochem Biophysical Methods 70, #2, 253-261 (MAR 10 2007) 

Romanik, G.; Gilgenast, E.; Przyjazny, A.; Kaminski, M. 

Practical approaches to plant volatile analysis 

2198 Volatiles from Plant J. 45, #4, 540-560 (2006) headspace GC-MS 

plants Boland, W.; Hansel, A.; Loreto, F.; Rose, U..; Schnitzler, J.;Tholl, D. 

Volatile constituents of micropropagated plants of 

1730 Essential oils Bupleurum fruticosum L headspace GC and GC-MS 

from plants Plant Science (Oxford), 167, #4, 807-810 

Bertoli, Alessandra; Pistelli, Luisa; Morelli, lvano; 

Fraternale, Daniele; Giamperi, Laura; Ricci, Donata 

Oxidation of lipids and proteins in frankfurters with different fatty acid 

2580 Volatiles in compositions and tocopherol and phenolic contents headspace GC 

frankfurters FOOD CHEM. 100, #1, 55-63 (2007) 

Estevez, M.; Ventanas, S.; Cava, R. 

Influence of the addition of rosemary essential oil on the volatiles 

2304 Volatiles in pattern of porcine frankfurters headspace GC/MS 

porcine J Ag Food Chem 53, #21, 8317-8324 (2005) 

frankfurters Estevez, Mario; Ventanas, Sonia; Ramirez, Rosario; Cava, Ramon 

Effect of pork meat proteins on the binding of volatile compounds 

2896 Volatiles in FOOD CHEM. 108, #4, 1226-1233 (JUN 15 2008) headspace GC/MS 

pork meat Perez-Juan, Maria; Flores, Monica; Toldra, Fidel 

Effect of ionic strength of different salts on the binding of volatile 

2603 Volatiles in compounds to porcine soluble protein extracts in model systems headspace GC/MS 

porcine Food Res. Int. 40, #6, 687-693 (July 2007) 

meats Flores, Monica; Perez-Juan, Maria; Toldra, Fidel 

Analysis of volatiles in porcine liver pates with added sage 

1731 Volatiles from and rosemary essential oils by using SPME-GC-MS headspace GC-MS 

liver pates J Agri Food Chemistry, 52, #16, 5168-5174 

Estevez, Mario; Ventanas, Sonia; Ramirez, R; Cava, R 

Comparative study of volatile compounds in traditional Chinese 

2669 Volatiles in Nanjing marinated duck by different extraction techniques 75µm Carboxen GC-MS 

marinated duck Intl J Food Sci & Tech 42, #5, 543-550 (MAY 2007) headspace 

Liu, Yuan; Xu, Xing-lian; Zhou, Guang-hong 

Relative characterization of rosemary samples according to their . 

2600 Volatiles in geographical origins using microwave-accelerated distillation, . headspace GC-MS 

rosemary oil solid-phase microextraction and Kohonen self-organizing maps. 

Anal Bioanal Chem 389, #2, 631-641 (2007) 

Tigrine-Kordjani, N.; Chemat, F.; Meklati, B. Y.; Tuduri, L.; 

Giraudel, J. L.; Montury, M. 

Determination of volatile compounds in antioxidant 

1732 Volatiles in rosemary extracts by SPME-GC 50/30µm DVB/CAR GC-MS, GC-FID 

rosemary Analytical Letters, 38, #7, 1193-1212 Preheat 15min @ 70C 

Carrillo, Jose David; Tena, Maria Teresa Extract 60min @ 20C 

headspace 

Kinetin enhanced linalool production by in vitro plantlets 

1733 Volatiles from of Lippia alba headspace GC 

plantlets J. Essent. Oil Res., 16, #5, 405-408 

Bizzo, Humberto R.; Lage, Celso L.S.; Leitao, Suzana G.; 

Lopes, Daise; Tavares, Eliana S. 

Optimization of wine headspace analysis by SPME 

1734 Volatiles in capillary GC-w/MS & FID 50/30µm DVB/CAR 

wine Food Chemistry, 93, #2, 361-369 headspace GC-MS 

Tat, L.; Comuzzo, P.; Stolfo, I.; Battistutta, F. 

Determination of chloroanisole compounds in red wine by 





1735 Chloroanisole headspace SPME AND GC-mass spectrometry headspace GC-MS 

in red wine J. Chromatogr. A, 1052, #1-2, 145-149 

Belsue, V; Gonzalez-Penas, E; Irigoyen, A; Lizarraga, E 

Identification of volatile aroma compounds of strawberry wine 

2207 Volatiles from using SPME techniques coupled with GC-MS headspace & GC-MS 

strawberry wine Flavour and Fragrance Journal 21, #1, 68-71 (2006) immersion 

Kafkas, E.; Cabaroglu, T.; Selli, S.; Bozdogan, A.; Kurkcuoglu, M.; 

Paydas, S.; Baser, K. 

Volatile flavour components of mandarin wine obtained 

1736 Flavor volatiles from clementines (Citrus reticula Blanco) extracted by SPME headspace & GC-MS 

in madarin Flavour and Fragrance Journal. 19, #5, 413-416 immersion sampling 

wine Selli, S.; Kurkcuoglu, M.; Kafkas, E.; Cabaroglu, T.; 

Demirci, B.; Baser, K. H. C.; Canbas, A. 

Validation of a SPME method for headspace analysis 

1737 Aroma of wine aroma components 50/30µm DVB/CAR GC-MS 

components Am J of Enology & Viticulture, 56, #1, 37-45 headspace 

in wine Howard, Karen L.; Mike, James H.; Riesen, Roland 

Effect of sample freezing on the SPME performance in the analysis 

2178 Chiral volatiles of chiral volatile compounds in foods headspace GC-MS 

in foods Food Chemistry 96, #2, 334-339 (2006) 

Flores, G.; del Castillo, M.; Blanch, G. Herraiz, M. 

2525 Heterocyclic 

Determination of less polar heterocyclic amines in meat extracts: Fast 

sample preparation method using SPME prior to HPLC-fluorescence 50µm CW-TPR LC-fluorescence 

amines in meat quantification 

Analytica Chimica Acta 582, #2, 259-266 (2007) 

Martin-Calero, A.; Ayala, J. H.; Gonzalez, V.; Afonso, A. M. 

2577 Sulfonamides 

Trace determination of sulfonamides residues in meat with a 

combination of SPME-LC-MS 65µm PDMS-DVB LC-MS 

in meat Talanta 72, #3,1082-1087 (2007-05-15) 

Lu, K. -H.; Chen, C. -Y.; Lee, M. -R. 

Interaction of soluble peptides and proteins from skeletal 

1738 Volatiles from muscle with volatile compounds in model systems as headspace GC 

meat curing affected by curing agents 

agents J Agr Food Chem, 53, #5, 1670-1677 

Gianelli, M. Pia; Flores, Monica; Toldra, Fidel 

Headspace concentration of selected dry-cured aroma compounds 

2590 Volatiles from in model headspace GC-MS 

meat curing FOOD CHEM. 101, #4, 1588-1593 (2007) 

agents Flores, M.; Gianelli, M. P.; Perez-Juan, M.; Toldra, F. 

Optimization of multiple headspace SPME for the quantification 

2179 Volatiles in of volatile compounds in dry fermented sausages headspace GC-MS 

sausages J Agr Food Chem 55, #21, 8688-8695 (OCT 17 2007) 

Flores, Monica; Hernandez, Delia 

Effect of calcium chloride on the volatile pattern and sensory 

2224 Volatiles in acceptance of dry-fermented sausages headspace GC 

sausages European Food Res and Tech 221 #5, 624-630 (2005) 0.05% calcium 

Flores, Monica; Nieto, Pablo; Ferrer, Jose Manuel; Flores, Jose chloride 

Quantitation of selected odor-active constituents in dry fermented 

2503 Volatiles in sausages prepared with different curing salts headspace GC 

sausages J Ag Food Chem 55, #8, 3058-3065 (APR 18 2007) 

Marco, Aurora; Navarro, Jose Luis; Flores, Monica 

Effect of Debaryomyces spp. on aroma formation and 

1739 Volatiles from sensory quality of dry-fermented sausages headspace GC-MS 

sausages Meat Science, 68, #3, 439-446 

Flores, Monica; Dura, M-Asuncion; Marco, Aurora; Toldra, Fidel 

Analysis of volatile components of fermented sausage 

1740 Volatiles from before and after ripeness by SPME-GC-MS headspace GC-MS 

sausages Fenxi Ceshi Xuebao, 23, #6, 40-43 

Zhang, C. H. 





Volatile compounds in Iberian dry-cured loin 

1741 Volatiles from Meat Science, 68, #3, 391-400 headspace GC-MS 

pig loin Muriel, E.; Antequera, T.; Petron, M.; Andres, A.; Ruiz, J. 

Determination of flavor components in Sicilian goat cheese 

2291 Flavors in by automated HS-SPME-GC headspace GC/MS 

goat cheese Flavour Fragrance J. 20 #6, 659-665 (2005) 

Chiofalo, B.; Costa, R.; Dugo, G.; Dugo, P.; Mondello, L.; 

Tranchida, P.; Quinto; Zumbo, Alessandro 

Effects of ultraviolet irradiation on chemical and sensory properties 

2533 Flavors in of goat milk headspace GC/MS 

goat milk J Dairy Sci 90, #7, 3178-86 (2007 Jul) 

Matak, K ; Sumner, S S; Duncan, S E; Hovingh, E; Worobo, R W; 

Hackney, C R; Pierson, M D 

Characterization of Maltese goat milk cheese flavour 

1742 Flavors in using SPME-GC/MS headspace GC-MS 

goat milk South African J of Animal Sci, 34, Suppl. 1, 176-180 

cheese Chiofalo, B.; Zumbo, A.; Costa, R.; Liotta, L.; Mondello, L.; 

Dugo, P.; Chiofalo, V. 

Comparison of efficiency and stability of two 

1743 Volatiles preconcentration techniques (SPME and INDEx) coupled headspace GC-MS 

from cheese to an MS-based "Electronic Nose" 

Mitteilungen aus Lebensmitteluntersuchung und Hygiene 

Hygiene, 95, #1, 85-90 

Pillonel, L; Altieri, D; Tabacchi, R; Bosset, J 

Significance of 2-heptanone in evaluating the effect of 

1744 2-heptanone microfiltration/pasteurisation applied to goats' milk headspace GC-MS 

in goats milk International Dairy Journal, 14, #10, 915-921 

Avalli, Andrea; Povolo, Milena; Carminati, D; Contarini, G 

Qualitative and quantitative composition of the flavour 

1745 Volatiles components of Taiwan calamondin and Philippine Calamansi headspace GC-MS 

from fruit fruit 

European J of Horticultural Science, 69, #3, 117-124 

Yo, S.-P.; Lin, C.-H. 

Properties of soy protein isolate prepared from aqueous 

1746 Off flavors alcohol washed soy flakes headspace GC-MS 

from soy Food Res. Int., 38,#3, 273-279 

protein Hua, Yufei; Huang, Youru; Liu, Xiaoya; Qiu, Aiyong 

SPME analysis of volatile compounds from unfermented 

1747 Volatiles olives sujected to thermal treatment. 65µm PDMS-DVB GC-MS 

from olives Anal & Bioanal Chem, 379, #5, 812-817 headspace 

Navarro, T.; de Lorenzo, C.; Perez, R. A.* 

A multivariate study of the relationship between fatty acids 

1748 Volatiles and volatile flavor components in olive and walnut oils GC-MS 

from olive & J AO C Society, 82, #2, 105-110 

walnut oils Torres, M.; Martinez, M.; Maestri, D. 

Simultaneous determination of volatile and semi-volatile 

1749 Volatiles aromatic hydrocarbons in virgin olive oil by headspace GC-MS 

from olive oil headspace SPME coupled to GC-MS 

J. Chromatogr. A, 1090. #1-2, 146-154 

Buxaderas, S.; Conte, L.; LopezTamames, E.; 

Pizzale, L.; Vichi, S. 

Determination of cannabinoids in hemp food 

1750 Cannabinoids products by use of headspace SPME-GC-MS MSTFA derivative GC-MS 

in food Anal. Bioanal. Chem., 378, #1, 183-189 headspace 

Kroener, L.; Lachenmeier, ; Madea, B.; Musshoff, 

Use of SPME analysis for adsorption of the volatile 

1751 Flavors from compounds in juices clarified by microfiltration. 65µm PDMS-DVB GC-MS 

pineapple Alimentaria, 41, #355, 35-39 headspace 

juice Carvalho, L.; Godoy, R..; Silva, C.; Miranda, R.; 

Figueira, J. 


Analysis of volatile compounds in some typical 

Brazilian fruits and juices by SPME-GC method 100µm PDMS GC-MS 

Brazilian fruits Food Additives and Contaminants, 22, #6, 508-513 20min @ 50°C 





and juices Cardeal, Z.; Guimaraes, E.; Parreira, F. headspace 

Storage and ultraviolet-induced tissue stress 

1753 Flavors from effects on fresh-cut pineapple. headspace GC 

pineapple J Sci Food and Agri, 84, #14, 1812-1816 

Lamikanra, O.; Richard, O. A. 

SPME For the determination of benzoylureas in orange juice 

2355 Benzoylureas in using LC combined with post-column photochemically 60µm DVB/PDMS HPLC 

orange juice induced fluorimetry derivatization and fluorescence detection immersion fluorescence 

J Sep Sci 31, #1, 56-63 (Jan -2008) fluorimetric 

Parrilla Voazquez, Piedad; Mughari, A; Martonez Galera, M. derivative 

High pressure processing of Australian navel orange 

1754 Flavors from juices: Sensory analysis and volatile flavor profiling headspace GC-MS 

navel oranges Innovative Food Sci. Emerg. Tech., 6, #4, 372-387 4°C and 10°C 

Baxter, I.; Easton, K; Schneebeli, K; Whitfield, F 

Evaluation of the thermally dried immobilized cells of Lactobacillus 

2850 Aroma compounds delbrueckii subsp bulgaricus on apple pieces as a potent starter culture headspace GC 

fermented whey J Agr Food Chem 55, #24, 9829-9836 (NOV 28 2007) 

Kopsahelis, N.; Panas, P.; Kourkoutas, Y.; Koutinas, A. 

A sensitive determination method for carbendazim and thiabendazole 

2774 Thiabendazole in apples by SPME-LC with fluorescence detection 60µm DVB/PDMS HPLC 

carbendazim in Food Additives and Contaminants 25, #3, 314-319 (2008) 35min @ 20°C fluorescence 

apples Hu, Yanxue; Yang, X.; Wang, Chun; Zhao, Jin; Li, Weining; Wang, Zhi 

Determination of thiabendazole in orange juice and rind 

1755 Thiabendazole by LC w/fluorescence detection and confirmation by headspace GC-MS-SIM 

in orange GC-MS after extraction by matrix solid-phase dispersion 

juice & rind J AOAC Int, 87, #3, 664-670 

Albero, B; Sanchez-Brunete, C; Tadeo, Jose L. 

Determination of the principal volatile compounds of Turkish Raki 

2842 Volatiles from Journal of the Institute of Brewing 113, #3, 302-309 (2007) headspace GC-MS 

aniseed-flavored Anli, R. Ertan; Vural, Nilufer; Gucer, Yalcin 

spirits 

Characterization of aniseed-flavoured spirit drinks by headspace 

2402 Volatiles from SPME-GC-MS and chemometrics headspace GC-MS 

aniseed-flavored Talanta 72, #2, 506-511 (2007-04-30) 

spirits Jurado, J. ; Ballesteros, O.; Alcazar, A.; Pablos, F. ; Martin, M. ; 

Vilchez, J. L.; Navalon, A. 

Effects of carbohydrate and noncarbohydrate 

1756 Sweetners sweeteners on the orange spirit volatile compounds headspace GC 

in orange Food Sci. Technol., 39, #2, 159-165 

spirits Cordaro, F.; Da Porto, C.; Marcassa, N. 

Comparison of two headspace SPME fibres for the 

1757 Volatiles detection of volatile chemical concentration changes 100µm PDMS GC 

in orange due to industrial processing of orange juice 85µm polyacrylate 

juice J Sci of Food & Agi, 85, #6, 1065-1071 headspace 

Jordan, M.; Goodner, K.; Castillo, M; Laencina, J. 

Studies on the aroma of cupuassu liquor by 

1758 Volatiles in headspace SPME and gas chromatography. 75µm Carboxen GC-MS, GC-AED 

liquor J Chromatogr A, 1025, #1, 115-124 headspace 

de Oliveira, A; Pereira, N; Marsaioli, A; Augusto, F 

Seasonal, populational and ontogenic variation in the 

1759 Volatils from volatile oil content and composition of individuals of headspace GC 

oregano plants Origanum vulgare subsp. Hirtum , assessed by GC 

headspace analysis and by SPME sampling of 

individual oil glands. 

Phytochemical Analysis, 15,#5, 286-292 

Johnson, C; Kazantzis, A.; Skoula, M.; 

Mitteregger, U.; Novak, J. 

Polymers & Coatings 

Application of headspace SPME-GC-MS in characterisation of odorous 

2620 Volatiles from volatile organic compounds emitted from magnetic tape coatings headspace GC 

polyester based on poly(urethane-ester) after natural and artificial ageing 





magnetic tape Polym. Test. (UK) 26, #2, 243-56 (April 2007) 

Thiebaut, B.; Lattuati-Derieux, A.; Hocevar, M.; Vilmont, L.-B. 

Variations in amounts and potential sources of volatile organic 

2643 Odor from chemicals in new cars headspace GC-MS 

new cars Sci. Total Environ. 382, #2-3, 228-239 (Sep 1 2007) 

Chien, Yeh-Chung 

791 Organics in 

The simplest sample treatment techniques to assess the 

quality and safety of food packaging materials. Review article 

packaging materials Reviews in AnalChem (2000) 19(6), 435-465 

Nerin, C.; Rubio, C.; Salafranca, J.; Batlle, R. 

SPME as an Effective Means to Isolate Degradation 

254 Degradation products Products in Polymers 

in polymers J. Environ. Polym. Degrad. 5 (2): 67-73 (1997) 

Hakkarainen, M., Karlsson, S., Albetsson, A. 

2662 Ink solvents on 

Ballpoint pen inks: the quantitative analysis of ink solvents on 

paper by solid-phase microextraction headspace ink solvents on 

paper J Forensic Sci 52, #1, 209-15 (2007 Jan) 

Brazeau, Luc; Gaudreau, Marc 

2489 Volatile in water- 

Comprehensive VOC analysis method for architectural coatings 

JCT CoatingsTech 4, #1, 48-55 (Jan. 2007) headspace GC-MS 

based + solvent 

borne coatings 

Brickweg, Lukas; Guillermo, Audrey; Jones, Dane; Wills, Max 

Direct VOC Analysis of Water-Based Coating by GC and SPME 

GC-FID 

361 Volatile solvents in J. Coating Technology, June 1997 65µm Carbowax/PDMS GC-FID 

water-based coatings Censullo, A., Jones, D., Wills, M. 5 min 

headspace 

salt added 

626 Volatile solvents in 

Analysis of exempt paint solvents by GC using SPME 

J. Coat Technol. (2000), 72(900), 69-74 65µm Carbowax/PDMS GC-FID 

water-based coatings Bodrian, R., Censullo, A., Jones, D., Rashkin, M., Wills, M. 5 min 

headspace 

salt added 


Analysis of volatile varnishes of coated wires by SPME 

Fresenius' J. Anal. Chem. 1999, 364(7), 641-642 GC-MS 

varnished wire Hinz, D., Kwarteng-Acheampong, W., Wenclawiak, B. 

headspace 

426 Acetaldehyde in 

Determination of Residual Acetaldehyde in Polyethylene 

Terephthalate Bottles on SPME 

polyethylene bottles Czech J. Food Sci. (1998), 36(8), 401-405 

Cizkova, H., Voldrich, M., Dobias, J. 

761 Terephthalic acid, 

Determination of plastic monomers in water by SPME 

coupled with liquid chromatography 85µm polyacrylate LC-UV 

vinyl acetate in J.AOAC Intl. Vol 84, No. 2, 2001, 432-436 65µm DVB/PDMS 

water Batlle, R., Sanchez, C., Nerin, C. 

Vinyl chloride analysis with (SPME)-GC-MS 

20min. Immersed 

5% salt, pH 5.7 

853 Vinyl chloride in applied to analysis in materials and aqueous samples. 75µm Carboxen/PDMS GC-MS 

plastic and water Analusis (2000) 28(10) 980-987 

Charvet, R.; Cun, C.; Leroy, P headspace 

Abbreviated analysis of bisphenol A with SPME 

467 Bisphenol A in tableware and food containers 

in plastic Shigen Kankyo Taisaku, 1999, 35(5), 447-451 

Takao, Y., Arizono, K. 

Characterization by SPME-GC-MS of matrix changes of 

876 Poly(L-lactide) poly(L-lactide) exposed to outdoorsoil environment GC-MS 





Polym. Degrad Stab, 71(2000) 147-151 

Gallet, G., Lempianinen, R., Karlsson, S 

Identification of a pharmaceutical packaging off-odor using 

943 Off odors solid phase microextraction GC/MS 100µm PDMS GC-MS 

pharmceutical J Pharm Biomedical Analysis (2001), 25(3-4), 379-386 

packaging Burinsky, D.; Polowy, K.; Sides, S.; Thornquest, A. heaspace 

902 Residual solvents 

Residual solvents determination in pharmaceutical products 

by GC-HS and Gc-MS-SPME 

pharmaceutical J Pharm & Biomedical Analysis 1998, 18(4-5), 623-638 

samples Camarasu, C., Mezei, M., Varga, G. 


Headspace SPME method optimization for 

residual solvent analysis 65µm DVB/PDMS 

pharmaceutical Acta pharm. Hung., 1999, 69(2), 77-84 30 min headspace 

samples Camarasu, C., Mezei, M., Szabo, A 2gm NaCl, 


Improving GC determination of residual solvents in 

pharmaceuticals by the combined use of headspace SPME 100µm PDMS GC-MS 

pharmaceutical and isotopic delution 16min. @ 20°C 

samples J. Chromatogr A, 915 (2001) 209-216 

Coran, S,, Giannellini, S., Massimo, B., Pinzauti, S. 

heaspace 

845 Degradation product 

The use of SPME-GC-MS for the determination of 

degradation products of volatile and semivolatile compounds GC-MS 

of diphenhydramine- J Microcolumn Separations (2001) 13(1), 1-7 

HCl Snow, Nicholas H.; Karaisz, Kenneth 

1035 

New PVC materials for medical applications - The release profile of 

PVC/polycaprolactone-polycarbonate aged in aqueous environments 

Polym Degradation Stab (2003) 80 (3), 451-458. 

Hakkarainen, Minna 

GC-MS 

1084 

Solid-phase microextraction (SPME) in polymer characterization - Long-term 

properties and quality control of polymeric materials 

Journal of Applied Polymer Science (2003) 89 (3), 867-873. 

Albertsson, Ann-Christine; Groning, Mikael; Hakkarainen, Minna 

GC-MS 

Multiple headspace solid-phase microextraction for the quantitative 

determination of volatile organic compounds in multilayer packagings 

VOCs in multi-layer 

1109 packaging. Journal of Chromatography A (2003) 999 (1-2), 155-164. 

Ezquerro, Oscar; Pons, Begona; Tena, Maria Teresa 

Carboxen/PDMS, DVB/carboxen/PDMS 

1176 Polyamide 

thermooxidation 

Headspace solid-phase microextraction with gas chromatography/mass 

spectrometry reveals a correlation between the degradation product pattern and 

changes in the mechanical properties during the thermooxidation of in-plant 

recycled polyamide 6,6 

J. Appl. Polym. Sci (2002) 86(13), 3396-3407 

Groning, Mikael; Hakkarainen, Minna GC-MS 

1321 

Qualitative and quantitative solid-phase microextraction gas chromatographicmass 

spectrometric determination of the low-molecular-mass compounds 

released from poly(vinyl chloride)/polycaprolactone-polycarbonate during 

ageing. 

Journal of Chromatography, A (2003) 1010 (1), 9-16. 

Hakkarainen, M. 

GC-MS 

Determination of poly(dimethyl)siloxane-water partition coefficients . 

2691 Organics from for selected hydrophobic organic chemicals using 14C-labeled analogs PDMS fibers GC-MS 

water J Chromatogr A 1148, #1, 23-30 (2007 Apr 27) 

Yang, Ze-Yu; Greenstein, Darrin; Zeng, Eddy Y; Maruya, Keith A 

immersed 

Effect of polymer concentration on partitioning and molecular recognition in 

plasticized poly(vinyl chloride). 





1345 Analytical Chemistry (2003) 75 (16), 4257-4264. 

Zhang, X.; Zhao, H.; Chen, Z.; Nims, R.; Weber, S. G.* 

Emission of volatiles from polymers - A new approach 

2159 Volatiles from for understanding polymer degradation headspace GC-MS 

polymers J Polymers Environ. 14. #1, 9-13 (2006) 

Albertsson, Ann-Christine; Groening, Mikael; Hakkarainen, Minna 

1366 

Headspace solid-phase microextraction long dash a tool for new insights into 

the long-term thermo-oxidation mechanism of polyamide 6.6. 

Journal of Chromatography, A (2001) 932(1-2), 1-11. 

Groening, M.; Hakkarainen, M. * 

GC-MS 

Direct solid sampling methods for gas chromatographic analysis of 

polymer/additive formulations 

1437 Polymer/additives Polymer Testing (2001) 20(7), 729-740. GC-FTIR-MS 

1518 

Residual styrene 

monomer 

Bart, J.C.J. 

Analysis of residual styrene monomer and other volatile organic compounds in 

expanded polystyrene by headspace solid-phase microextraction followed by 

gas chromatography and gas chromatography/mass spectrometry. 

Journal of Separation Science (2002) 25(8), 539-542 

Kusch, Peter; Knupp, Gerd 

75um Carboxen PDMS, 

headspace 

GC-MS 

1302 

Headspace solid-phase micro-extraction - gas chromatography - mass 

spectrometry applied to quality control in multilayer-packaging manufacture. 


Ezquerro, O.; Pons, B.; Tena, M. T.* 

GC-MS 

TiO/sub2/ reactivation in photocatalytic destruction of gaseous diethyl sulfide in 

a coil reactor 

1209 Diethyl sulfide Applied Catalysis B: Environmental (2003) 44 (1), 25-40. 

Lion, Claude; Savinov, Evgueni N.; Smirniotis, Panagiotis G.; Vorontsov, 

Alexandre V. 

1268 

1434 

A GC-MS method for analysis of volatile monocyclic aromatic compounds in 

heavy fuel oil using headspace-solid phase microextraction. 

Monocyclic aromatic 

compounds in heavy 

fuel oil. Chromatographia (2003) 58 (1-2), 115-117. 

Mangani, G.; Berloni, A.; Maione, M. * 

Determination of methylcyclopentadienyl-manganese tricarbonyl by solid phase 

microextraction-direct thermal desorption-quartz furnace atomic absorption 

spectrometry 

Methylcyclopentadienylmanganese 

tricarbonyl Spectrochim Acta Part B At Spectrosc (2001) 56(2), 215-221. 

Alava-Moreno, Fausto; Bendicho, Carlos; Fragueiro, Maria Sandra; Lavilla, 

Isela 

Thermal stability analysis of organo-silicates, using 

1760 Organo- solid phase microextraction techniques headspace TGA, GC-MS 

silicates from Thermochim Acta, 429, #1, 13-18 

polyurethane Edwards, G.; Halley, P.; Kerven, G.; Martin, D. 

Use of SPME to monitor gases resulting form 

1761 Volatiles thermal plasma pyrolysis. headspace GC 

from polymer Chromatographia, 60, #1-2, 85-88 

pyrolysis Cubas, A.; Carasek, E; Debacher, N. ; de Souza, I. 


Probing the microwave degradation mechanism of phenolcontaining 

polymeric compounds by sample pretreatment heaspace from 20° to GC-MS 

from phenolic and GC-MS analysis 80°C 

polymers Analytica Chimica Acta, 526, #2, 121-129 

Chang, Yu-Cheng; Chu, Tieh-Chi; Ko, Chu-Jung; Ko, Fu 





Use of the SPME-GC-MS technique to study the thermal degradation 

2822 Thermal of isotactic polypropylene: Effects of temperature and reaction time, heaspace GC-MS 

byproducts of and analysis of the reaction mechanism 

polypropylene E-Polymers Jan 30 2008 

Bortoluzzi, J.; Carasek, E.; Cristiano, R.; Gallardo, H..; Soldi, V. 

SPME to concentrate volatile products from thermal 

1763 Thermal degradation of polymers 100µm PDMS, GC-MS 

byproducts of Polym Degradation Stab, 89, #1, 33-37 75µm Carboxen 

polypropylene Bortoluzzi, J.; Carasek, E; Pinheiro, E.; Soldi, V 

2880 Degradation 

Comparison of extraction methods for sampling of low molecular 

compounds in polymers degraded during recycling headspace GC 

products of Eur Polym J 44, #6, 1583-1593 (June 2008) 

polymers Karlsson, Sigbritt; Moller, Johanna; Stromberg, Emma 

Emission of possible odourous low molecular weight 

1764 Odours from compounds in recycled biofibre/polypropylene composites heaspace GC-MS 

polypropylene monitored by head-space SPME-GC-MS 

composites Polym Degradation Stab, 90. #3, 555-562 

De Las Heras, Luis A.; Espert, Ana; Karlsson, Sigbritt 

Development and analytic of odor absorber 

1765 Odor Tenside Surfactants Deterg, 41, #6, 282-286 headspace GC 

removal by Bohmer, Thomas; Muller, Felix; Peggau, Jorg 

Zn ricinoleate 

Headspace-SPME-GC-MS identification of volatile organic 

1766 Volatiles from compounrds released from expanded polystyrene 75µm Carboxen GC-MS 

polystyrene J. Polym. Environ., 12, #2, 83-87 headspace 

Knupp, Gerd; Kusch, Peter 

Correlation between emitted and total amount of 

1767 2-cyclopentyl- 2-cyclopentyl- cyclopentanone in polamide 6.6 headspace GC-MS 

cyclo- allows rapid assessment by Head Space and HS-SPME . GC-RI 

pentanone in under non-equilibrium conditions 

polamide 6.6 J. Chromatogr. A, 1052, #1-2, 151-159 

Groning, Mikael; Hakkarainen, Minna 

Identification and migration of degradation compounds from irradiation 

2864 Degradation of multilayer polyamide 6 films for meat foodstuffs and cheese 100µm PDMS GC-MS 

compounds Anal. Bioanal. Chem. 391, #3, 847-857 (June 2008) 20 min, 80 °C 

of Polamide 6 Felix, J.S.; Manzoli, J.E.; Monteiro, M.; Nerin, C.; Padula, M.; 

Pezo, D.; Romero, J. 

Multiple headspace SPMEof 2-cyclopentyl- cyclopentanone 

1768 2-cyclopentyl- in polyamide 6.6: Possibilities and limitations in the headspace GC-MS 

cyclopentanone headspace analysis of solid hydrogen-bonding matrices 

in polamide 6.6 J. Chromatogr. A, 1052, #1-2, 61-68 

Groning, Mikael; Hakkarainen, Minna 

Chemical characterization of oil-based asphalt release agents 

2308 Volatiles from and their emissions headspace GC/MS 

Asphalt release Fuel 85 #9, 1232-1241 (2006) 

agents Isacsson, Ulf; Tang, Bing 

Determination of aromatic hydrocarbons in asphalt release 

1769 Hydrocarbons agents using headspace SPME-GC-MS headspace GC-MS 

from asphalt J Chromatogra, A, 1069, #2, 235-244 

Isacsson, Ulf; Tang, Bing 

Natural Products 

401 Volatiles 

Analysis of Tobacco Volatiles with SPME 

Dr. W.D. Koller, Federal Research Centre for Nutrition, 100µm PDMS GC-MS 

in tobacco Institute of Process Engineering, Engesserstr. 20, 10 min 

76131 Karlsruhe/Deutschland headspace 


A Simple Screening for Pesticide Residues in Tobacco 

Dr. W.D. Koller, Federal Research Centre for Nutrition, 100µm PDMS GC-MS 

water/MeOH extract Institute of Process Engineering, Engesserstr. 20, 10 min 

76131 Karlsruhe/Deutschland immersion 





102 Flavor additives 

Qualitative and Quantitative Analysis of Flavor Additives 

on Tobacco Products Using SPME-GC-MS 65µm Carbowax/DVB GC-FID 

in tobacco J. Agric. Food Chem. 45: 844-849 (1997) 95°C, 15 min 

Clark, J., Bunch, J. KCl added 

430 Alkaloids 

Determination of Tobacco Alkaloids Using SPME and GC-NPD 

Chromatographia (1998), 47(7/8), 443-448 100µm PDMS GC-NPD 

in tobacco Yang, S., Smetena, I. 12 min, immersed 

627 Acetates 

Quantitative analysis of acetates in cigarette tobacco 

using SPME-GC-MS GC-MS 

in cigarette tobacco J. Chromatogr. Sci (2000), 38(4), 137-144 

Watson, C., Ashley, D. 

headspace 

2554 Volatile Organics 

Analysis of volatile organic compounds in mainstream cigarette smoke 

ENVIRON. SCI. TECHNOL. 41, #4, 1297-1302 (15 FEB 2007) headspace GC-MS 

found in 

cigarette smoke 

Polzin, G. M.; Kosa-Maines, R. E.; Ashley, D. L.; Watson, C. H. 

Identification and determination of mainstream and sidestream 

2434 Organics found in smoke components in different brands and types of cigarettes GC-MS 

cigarette smoke by means of SPME-GC-MS 

J. Chromatogr. A 1180, #1-2,138-150 (Feb 8 2008) 

Bartolucci, G.; Furlanetto, S.; Giannini, I.; Moneti, G.; Orlandini, S.; 

Pieraccini, G.; Pinzauti, S. 

137 Phenols in 

Quantitative Determination of Phenols in Mainstream Smoke 

with SPME-GC-Selected Ion Monitoring Mass Spectrometry 85µm polyacrylate GC-FID 

cigarette smoke J. Chromatogr. Sci. 34: 272-275 (1996) 60 min 

Clark, J., Bunch, J. stirring 

2863 Formaldehyde in 

Determination of particulate-bound formaldehyde from burning 

incense by solid phase microextraction 65µm PDMS/DVB GC-ECD 

incense smoke Bull. Environ. Contam. Toxicol. 80, #4, 324-328 (April 2008) headspace 

Chen, C.Y.; Lin, J.M.; Liou, S.W.; Yang, T.T. PFBHA derivative 


Characterization of incense smoke by SPME - Comprehensive twodimensional 

(GC x GC) 65µm PDMS/DVB GC-GC-FID 

incense smoke Atmospheric Env 41, #27, 5756-5768 (SEP 2007) 

Tran, Tin C.; Marriott, Philip J. 

headspace 

628 Azo dyes 

Study on determination of prohibited azo dyes by SPME 

Fenxi Deshi Xuebao (2000), 19(1), 76-78 GC-MS 

in leather & textiles Xu, H., Tong, H. reduced to aromatic 

amines w/Na2SO4 

Development of a SPME method for detection of the use of 

Azo dyes banned Azo dyes in coloured tectiles and leather 

in leather & textiles Rapid Commun.Mass Spectrom. 13, pp1833-1837 

Cioni, G., Bartolucci, G., Pieraccini, G., Meloni, S., Moneti, G. 

916 Hexachlorobenzene 

Rapid Quantification of hexachlorbenzene in the color 

additives D&C Red Nos. 27 & 28 (phloxine B) using SPME GC-MS 100µm PDMS GC-MS 

in color additives J Chromatogr A (1999) 863(1) 37-46 25min @ 26°C 

Andrezejewski, D., Weisz, A. 

Derivatization Solid-Phase Microextraction Gas 

immersed 

stirred 

210 Solvents in Chromatographic Mass Spectrometric Determination of 65µm Carbowax/DVB GC-FID 

water-based coatings Organic Acids in Tobacco 5 min 

J. Chromatogr. Sci. 35 (5): 209-212 (1997) headspace 

Clark, T., Bunch, J. stirring 

salt added 

836 Biproducts from 

Screening of biotransformation products of carvone 

enantiomers by headspace-SPME/GC-MS headspace GC-MS 





carvone enantiomers Z. Naturforsch., C: J. Biosci(2001) 56(1/2) 58-64 

Demirci, F; Kirimer, N; Demirci, B; Noma, Y; Baser, K 

Analysis of Monoterpenes from Conifer Needles Using SPME 

72 Monoterpenes J. High Res. Chromatogr. 18: 587-592 (1995) 100µm PDMS GC-FID 

in conifer needles Schafer, B., Hennig, P., Engewald, W. 40°C, 5 min 

headspace 


Changes in the Flavor of Monoterpenes During Their 

Autoxidation Under Storage Conditions 65µm Carbowax/DVB GC-MS 

in conifer needles Dept. of Food Chemistry, Prague Institute of Chemical 40°C, 10 min 

Technology, Technicka 5, CZ-16628 Prague 6, Czechia 

Pokorny, J., Pudil, F., Volfova, J., Valentova, H. 

headspace 


SPME for the determination of volatile organics in the 

foliage of Fraser fir 

Vereen, D. A.; McCall, J. P.; Butcher, D. J 


Correlation between the pattern volatiles and the overall aroma of wild 

edible mushrooms 

J. Agric.Food Chem. 56, #5, 1704-1712 (MAR 12 2008), 

De Pinho, P. ; Ribeiro, B.; Goncalves, R.; Baptista, P.; Valentao, P.; 


mushrooms Seabra, Rosa M.; Andrade, Paula B. 

Headspace SPME, Headspace Solid Phase Dynamic Extraction 

2481 Volatiles from (HS-SPDE) and Headspace Sorptive Extraction (HSSE) - comparing headspace GC-MS 

herbs the methods applied to the analysis of volatile components in herbs. 

Zeitschrift fur Arznei- & Gewurzpflanzen 12, #3, 147-153 (2007) 

Wolff, A. C.; Schellenberg, I.; Bansleben, D. 

159 Terpenoids 

Head-Space SPME for the GC-MS Analysis of Terpenoid 

in Herb-Base Formulations GC-MS 

in herbs Fresenius’ J. Anal. Chem. 356: 80 (1996) 

Czerwinski, J., Zygmunt, B., Namiensnik, J. 


SPME of Volatile Components from Natural Grassland Plants 

J. Agric.Food Chem. 2001, 49, 203-209 100µm PDMS GC-MSD 

in plant materials Cornu, A., Carnat, A., Martin, B., Coulon, J., 15 min @ 44°C 

Lamaison, J, Berdague,J 

Monoterpene biosynthesis in Agathosma crenulata (Buchu) 

headspace, 

1 gm in 40mL vial 

848 Monoterpens Flavour and Fragrance Journal (2001) 16(2), 123-135 GC-MS 

in essential oils Mosandl, Armin; Fuchs, Sabine; Sewenig, Sabine 


Head Space SPME for the GC-MS Analysis of Terpenoids in 

Herb-Based Formulations GC-MS 

in herbs J. Anal. Chem. 356 (1): 80-83 (1996) 

Czerwinski, J., Zygmunt, B., Namiesnik, J. 

630 Monoterpens 

Examination of the enatomeric distribution of certain 

monoterpene hydrocarbons in selected essential oils by GC-MS 

in essential oils automated SPME-chiral GC -Mass spectrometry. 

J. Chromatogr. Sci., Mar.2000, 38(3), 95-99 

Coleman, W., Lawrence, B. 

6 se. headspace 

631 Monoterpens & 

Monoterpene composition essential oil from peppermint 

(Mentah x piperita L.) w/regard to Leaf position using 100um PDMS GC-MS 

essential oils SPME and GC-MS Analysis 1 min @ 25°C 

in peppermint J.Agric. Food Chem 1999, 3782-3786 headspace 

632 Monoterpens & 

Biogenesis study of essential oils by SPME enatiomultidimensional 

GC-MS (MDGC/MS) GC-MS 

essential oils GIT Lbor-Gachz (2000), 44(4), 358-362 

in mint plant Fuchs, S., Beck, T., Mosandl, A. 





859 Review article 

Sample preparation for chromatographic analysis 

of plant material 

J Planar Chromatog- Modern TLC (2000) 13(6) 404-413 

Namiesnik, Jacek; Gorecki, Tadeusz 

2513 Trace residue 

Sample preparation techniques for the determination of trace 

residues and contaminants in complex matrices review article 

contaminants J. CHROMATOGR. A 1153, #1-2, 36-53 (15 JUN 2007) 

from food Ridgway, K.; Lalljie, S. P. D.; Smith, R. M. 

863 Volatiles 

Emission of volatile compounds by seeds under 

different environmental conditions GC-MS 

from seeds American Midland Naturalist (2001) 145(2) 419-422 

Jorgensen, Eric 

633 Essential oils 

Chemical composition of the essential oil and headspace 

SPME of the quava fruit GC-MS 

in quava fruit J. Essent. Oil Res (2000), 12(2), 153-158 

Paniandy, J., Chane-Ming, J., Pieribattesti, J. 

headspace 

469 Essential oils 

Rapid GC with resistance heated capillary columns. 

Analysis of essential oils from aromatic plants 

from aromatic plants Git Spez. Sep. (1999), 19(1), 40-43 

Theuerl, T., Kleibohmer,W., Blanke, R. 

2599 Cuticular 

Investigation of cuticular hydrocarbons from Bagrada hilaris 

genders by SPME/GC-MS 85µm polyacrylate GC-MS 

hydrocarbons Anal Bioanall Chem 389, #4, 1259-1265 (OCT 2007) 

from insects De Pasquale, C.; Guarino, S.; Peri, E.; Alonzo, G.; Colazza, S. headspace 

Perception of cuticular hydrocarbons by the olfactory organs in 

2323 Cuticular Periplaneta americana (L.) (Insecta : Dictyoptera) headspace GC 

hydrocarbons Journal of Insect Physiology 51 #12, 1384-1389 (2005) 

from insects Said, Imen; Gaertner, Cyril; Renou, Michel; Rivault, Colette 

389 Cuticular 

Solid Phase Microextraction and Cuticular Hydrocarbon 

Differences Related to Reproductive Activity in the GC-MS 

hydrocarbons Queenless Ant 

in Dinoponera J. Chemical Ecology, 24: 473-490, 1998 

quadriceps ants Monnin, T., Malosse, C., Peeters, C. 

89 Pheromones 

Solid Phase Microextraction, an Alternative Method 

for the Study of Airborne Insect Pheromones 100µm PDMS GC-FID 

in insects (Metamasius hemipterus, Coleoptera, Curculionidae) 5 min 

J. High Res. Chromatogr. 18: 669-670 (1995) 

Malosse, C., Ramirez-Luca, P., Rochat, D., Morin, J. 

headspace 

818 Pheromones 

Use of SPME in the investigation of chemical 

communication in social wasps 7µm PDMS GC-MSD 

in insects J Chromatogr A, 873, (2000), 73-77 

Sldege, M., Moneti, G., Pieraccini, G., Turillazzi, S. 

10min @ 170C 


Identification of the sex pheromone of Sesamia cretica Lederer 

Journal of Chemical Ecology 34, #1, 103-106 (JAN 2008) GC-MS 

in insects Avand-Faghih, Arman; Frerot, Brigitte 


SPME, A New Tool in Pheromone Identification in Lipidoptera 

J High Resolut. Chromtogr. (1997), 20(6), 340-342 7µm PDMS GC-FID or 

in insects Frerot, B., Malosse, C., Cain, A. 5 min GC-FTD 

rubbed on fiber 


(Z)-dodec-3-en-1-ol, a novel termite trail pheromone identified 

after SPME from Macrotermes annandalei. GC-MS 

in termite trail J Insect Physiology (2001) 47(4-5) 445-453 

Bordereau, C; Bonnard, O; Ginies, C; Lettere, M; Peppuy, A; 





Robert, A; Semon, E 


Ethyl 4-methyl heptanoate: A male-produced pheromone of 

Nicrophorus vespilloides headspace 

of male beetles Journal of Chemical Ecology 34, #1, 94-98 (Jan 2008) 

Haberer, Wolf; Schmitt, T.; Peschke, K.; Schreier, P.; Mueller, J. 


1-Tridecene - male-produced sex pheromone of the tenebrionid 

beetle Parastizopus transgariepinus 100µm PDMS GC-MS 

tenebrionid Naturwissenschaften 95, #3 247-251 (MAR 2008) headspace 

beetles Geiselhardt, Sven; Ockenfels, Peter; Peschke, Klaus 


Determination of characteristic odorants from Harmonia axyridis beetles 

using in vivo solid-phase microextraction and multidimensional headspace GC-MS 

Harmonia axyridis gas chromatography-mass spectrometry-olfactometry 

beetles J Chromatogr A, 1147, #1, 66-78, 73-77 (2007), 

Lingshuang Cai; Koziel, J. A.; O Neal, M. E. O 


Detection of Tribolium castaneum (Herbst) volatile defensive 

secretions by SPME-capillary gas chromatography (SPME-CGC). 75µm Carboxen GC-MS 

of red flour J Stored Products Research 43, #4, 540-545 (2007) headspace 

beetles Villaverde, M. L.; Juarez, M. P.; Mijailovsky, S. 15-min 


Role of SPME in the identification of highly volatile 

Pheromones of two Rhinoceros beetles Scapanes australis Carboxen/PDMS GC-MS 

of Rhinoceros and Strategus aloeus (Coleoptera, Scarabaeidae, Dynastinae) 30 min 

beetles J Chromatogr. A, 885 (2000) 433-444, Rochat, D, immersion 

NaCl, borax buffer 

Ramirez-Lucas,P., Malosse,C., Aldana,R. Kakul,T. Morin,J 

(pH9.2) 

Preparation for the analysis of fire ant trail pheromones using 

2262 Pheromones SPME-gas chromatography/mass spectrometry. GC/MS 

from fire ant Abstracts of Papers Am Chem Society 229 #1, U131 (2005) 

Smith, Suncerae I.; Mazitelli, Carolyn; Brodbelt, Jennifer S. 

945 Insecticides 

Measurement of Insecticide Uptake and Effective 

Fraction in a Beneficial Insect Using SPME 

Anal. Chem (2001) 73(13), 3107-3111 

Alix, A.; Collot, D.; Nenon, J.; Anger, J. 

635 Volatiles 

The measurement of volatile compounds in Foray 48B, an 

insecticide prepared from Bacillus thuringiensis var. kurstaki 

in insecticide Sci. Total Env., (2000) Vol. 263, No. 1-3, 155-160 

van Netten, C., Bartlett, K., Chow, Y., Leung, V., Teschke, K. 

120 NH3, putrescine, 

Solid Phase Microextraction Analysis of Static-Air Emissions 

of Ammonia, Methylamine, and Putrescine from a Lure 100µm PDMS FID 

methylamine in for the Mexican Fruit Fly 10 min 

lure cultures J. Agric. Food Chem. 44: 3554-3559 (1996) 

Robacker, D., Bartelt, R. 

headspace 

825 Fly Pheromones 

SPME-GC-direct depostioon infrared spectrometry as 

a convenient method for the determination of volatile 100µm PDMS GC-MS 

in insects compounds from living organisms 

J. Chromatogr. A 819 (1998) 45-50 

Auger, J., Rousset, S., Thibourt, E., Jaillais, B. 

1min. 

937 Chemical attractants 

The use of (SPME) devices in analysis for potential 

mosquito oviposition attractant chemicals from GC-MS 

from cyanobacterial mats. 

cyanobacterial mats. Aquatic Ecology (2000), 34(4), 413-420 

Rejmankova, E.; Lege, M.; Andre, R.; Higashi, .; Roberts, D. 

Chemicals Attractive to Mexican Fruit Fly from 

398 Chemical attractants Klebsiella pneumonia and Citrobacter freundii Cultures 100µm PDMS GC-MS 

in soy broth culture Sampled by SPME 27°C, 30 min 





J. Chemical Ecology, Vol. 23, No., 12, 1997, 2897-2915 headspace 

Robacker, D., Bartelt, R. 

Pheromone analysis using capillary GC techniques 

470 Pheromones J. Chromatogr., A 1999, 843(1+2), 199-236 review of use of SPME GC 

Jones, G., Oldham, N. 


Solid Phase Microextraction Technique Used for Collecting 

Semiochemicals, Identification of Volatiles Released by 100µm PDMS GC-MS 

in insects Individual Signaling Phylionorycter sylvella Moths 1-3 hr 

Z. Nturforsch. C: Giosci. 51: 599 (1996) 

Karlson-Borg, A., Mozuaitis, R. 

headspace 


The scent of the waggle dance 

PLoS Biology 5, #9, 1862-1867 (SEP 2007) headspace GC/MS 

in honey bees Thom, Corinna; Gilley, David C.; Hooper, Judith; Esch, Harald E. 

Use of SDS page, SPME, and GC-MS for chemical analysis of 

2332 Phermones temporal gland secretions from African elephants. GC/MS 

African elephant Abstracts of Papers Am Chem Society (2004) 227 Part1, U443 

Freyaldenhoven, D.; Kopper, R.; Goodwin, T.; Lichti, C.;Rasmussen, L. 

Chemical analysis of urine from male african elephants by SDS PAGE, 

2333 Urine from SPME, and GC-MS. GC/MS 

African elephant Abstracts of Papers Am Chem Society (2004) 227 Part1, U425 

Carver, A.; Davis, B.; Kopper, R.; Goodwin, T.; Lichti, C.; 

Rasmussen, L..; Hollister-Smith, Julie; Alberts, S. 

410 Pheromones in 

Purification, Identification, Concentration and Bioactivity 

of (Z)-7-dodecen-1-yl acetate: Sex Pheromone of the GC-MS 

elephant urine Female Asian Elephant, Elephas maximus 

Chem. Senses 22: 417-437 

Rasmussen, L.E.L., Lee, T.D., Zhang, A., Roelofs, W.L., 

and Daves Jr., G.D. 

773 Fungal volatiles 

Application of SPME for the determination of fungal 

volatile metabolites 

Prog. Biotechnol (2000) 17, 369-377 

Jelen, H.; Wasowicz, E 

394 Free fatty acids 

Sampling Techniques for GC-MS Analysis of Long-Chain 

Free Fatty Acids from Insect Exocrine Glands 100µm PDMS, GC-MS 

in exocrine secretions J. Chromatogr. A 816 (1998) 169-175 65µm Carbowax/DVB 

Maile, R., Dani, F., Jones, G., Morgan, D., Orthius, D. 

Attractants from Stryphylococcus aureus Cultures from 

140°C, 30 min 

headspace 

382 Volatile attractants Mexican Fruit Fly, Anastrepha ludens 100µm PDMS GC-MS 

in cultures J. Chemical Ecology, Vol. 21, No. 11, 1861-1874 (1995) 5 min - 24 hr 

Robacker, D., Flath, R. headspace 

471 Volatile attractants 

Volatiles of bracket fungi Fomtopsis pinicola 

and Fomes fomentarius and their functions as GC-MS 

in bracket fungi insect attractants 

J. Chem. Ecol. (1999), 25(3), 567-590 

Faldt, J., Jonsell, M., Norlander, G., Borg-Karlson, A. 

Volatiles from Fusarium verticillioides (Sacc.) Nirenb. 

584 Alcholols, aldehydes and their attractiveness to Nitidulid beetles. 100µm PDMS GC-FID/MS 

in air J-Agric-Food-Chem. Jun 1999; 47(6): 2447-2454 30 min 

Bartelt,-RJ; Wicklow,-DT 

472 Volatile attractants 

Identification of a new blend of apple volatiles 

attractive to the apple maggot, GC-FID 

from apples Rhagoletis pomonella 

J. Chem. Ecol., 1999, 25(6), 1221-1232 

Zhang, A., Linn, C., Wright, S., Prokopy, R. 

Reissig, W., Roelogs, W. 





Volatiles from apple (Malus domestica) eliciting antennal 


889 Volatile attractants antennal responses in female codling moth Cydia pomonella GC-Electrofrom 

apples (L.) (Lepidoptera: Tortricidae): Effect of plant injury and s 

sampling technique 

Zeitschrift fuer Naturforschung Sec C (2001) 56(3-4) 262-268 

Backman, A; Bengtsson, M; Karlsson, A; Liblikas, I; Witzgall, P 

antennography 

636 Pyrazine 

Headspace SPME method for determining 3-akyl-2 methoxypyrazine 

in musts by PDMS fibers 100µm PDMS/DVB GC-NPD 

in Must J Chromatogr. Sci (2000), 880(1+2), 93-99 4 hr.@30°C 

Sala, C., Mestres, M, Marit, M., Busto, O., Guasch, J. 

Development of a SPME-GC-ECD methodology for 

headspace 

NaCl added 

892 Pesticides selected pesticides in must and wine samples GC-ECD 

in must & wine Fresenius' J Anal Chem) 369(7-8) 647-651 

Alves, A; Correia, M; Delerue-Matos, C 

Headspace SPME and Gas Chromatography with 

211 Musk compounds Atomic-Emission Detection 100µm PDMS GC-AED 

in cosmetic products Chromatographia 45: 138-144 (1997) 80°C, 30 min 

Struppe, C., Schaefer, B., Engewald, W. headspace 

835 Volaitles from 

SPME-GC-MS analyses of hazelnut creams 

Lab. 2000 (2000) 14(7), 86-88 GC-MS 

hazelnut creams Saba, A.; Cuzzola, A.; Raffaelli, A.; Salvadori, P. 

821 Fragrances 

A novel technology to study the emission of 

fragrance from the skin 100µm PDMS GC-MS 

on skin Perfumer& Flavorist, vol. 23 (1998) 1-11 30-60min 

Mookherjee, B., Patel, S., Trenkle, R., Wilson, R. headspace 

637 Volatiles 

Analysis of headspace constituents of Gardenia flower by 

GC-MS with SPME and dynamic headspace sampling 100µm PDMS GC-MS 

in Gardenia flower Sepu, (2000-09) 18(5) 425-455 60 min @ 28°C 

Liu, B., Gao, Y. headspace 

Composition of the volatiles from flowers of Bystropogon 

2811 Volatiles moderensis Webb by SPME 

in flower Planta Medica 73, #9, 949-950 (AUG 2007) 

Castilho, P. C. 

2568 Fragrance in 

Analysis of volatile compounds emitted from fresh Syringa oblata 

flowers in different florescence by headspace SPME-GC-MS 65µm PDMS/DVB GC-MS 

Syringa oblata Anal. Chim. Acta 576, #1, 43-49 (2006-08-18) headspace 

flowers Li, Z. G.; Lee, M. R.; Shen, D. L. 30 min @ 25°C 

882 Fragrance 

On-site field sampling and analysis of fragrance from living 

Lavender (Lavandula angustifolia L.) flowers by SPME 100µm PDMS GC-MS 

in Lavender flowers coupled to GC and io-trap mass spectrometry 10 min @ 28°C 

J. chromatogr. A 917(2001) 245-250 

An, M., Haig, T., Hatfield, P. 

headspace 

2555 Furfural in 

Diffusive sampling of airborne furfural by SPMEdevice with on-fiber 

derivatization 65µm PDMS/DVB GC-MS 

Air J. Chromatogr., A 1129. #1, 29-33 (2006-09-29) 25°C 

Tsai, S. W.; Kao, K. Y. PFBHA derivative 


Application of headspace-SPME-HPLC for the analysis of the aroma 

Volatile components of treacle and determination of its content headspace HPLC 

from treacle of 5-hydroxymethylfurfural (HMF). 

Food Chemistry 104, #3, 1310-1314 (2007) 

Edris, A. E.; Murkovic, M.; Siegmund, B. 

2428 Fragrance 

Isolation and characterization of the volatile aroma compounds 

from the concrete headspace and the absolute of Jasminum 100µm PDMS GC-MS 

in flowers sambac (L.) Ait. (Oleaceae) flowers grown in Egypt 

Eur. Food Res. Technol. 226, #3, 621-626 (January 2008) 

headspace 





Chizola, Remigus; Edris, Amr E.; Franz, Chlodwig 


125 Fragrance 

IFF Announces New Method for Living Flower Analysis 

Spray Technology & Marketing Oct. 1996, pp 26-30 75µm Carboxen/PDMS GC-MS 

in flowers Anon headspace 

126 Fragrance 

Flavors of Heliotrope Flowers, Analyzed by SPME Method 

Gakkaishi 2: 6 (1995) GC-MS 

in flowers Nippon, Shokuhin Kagaku 

The study of the aroma profile characteristics of durian pulp during 

2365 Aroma compounds storage by the combination sampling method coupled with GC-MS. GC-MS 

in durian pulp Flavour and Fragrance J. 22, #1, 71-77 (2007 ) 

Zhang ZhuoMin; Zeng DanDan; Li GongKe 

headspace 


Analysis of the aroma compunds of the pulp of Borassus 

aethiopum L (Palmaceae) from Cameroon using GC-MS, GC-MS 

in pulp SPME-GC-MS and olfactormetry 

Ernaehung (Vienna) 24(2000) 159-161 

Jirovetz, L., Buchbauer, G., Ngassoum, M. 


Headspace sampling of the volatile fraction of vegetable matrices 

J.Chromatogr. A 1184,#1-2, 220-233 (MAR 14 2008) 

from vegetables Bicchi, C.; Cordero, C.; Liberto, E.; Sgorbini, B.; Rubiolo, P. 

Influence of fiber coating in headspace SPME-GC analysis 

746 Volatiles of aromatic and medicinal plants Carboxen/DVB/PDMS GC-FID 

from plants J.Chromatogr. A (2000) 892, 469-485 1hr, headspace 

Bicchi, C., Drigo, S., Rubiolo, P. 

2828 Organochlorine 

Application of microwave-assisted micellar extraction combined 

with SPME-HPLC with UV detection for the determination of 65µm DVB/PDMS LC-UV 

pesticides in organochlorine pesticides in different mud samples 

mud samples Int. J. Environ. Anal. Chem.88, #3, 185-197 (March 2008) 

Santana-Rodriguez, Jose Juan; Sosa, Zoraida; Vega, Daura 


SPME and SPE comparative study for coupling with microwaveassisted 

micellar extraction in the analysis of organochlorine LC-PAD 

pesticides in pesticides residues in seaweed samples 

seaweed Microchemical Journal 87, #2, 139-146 (DEC 2007) 

Moreno, Daura Vega; Ferrera, Zoraida Sosa; Rodiriguez, Jose 


SPME associated with microwave assisted extraction 

of organochlorine pesticides in medicinal plants PDMS GC-ECD 

medicinal plants Anal. Chim. Acta (2001) 428(1), 111-120 

Ho, W.-H.; Hsieh, S.-J 

90min, 

Evaluating Peats for their capacities to remove 

465 C2-C10 Acid, phenols, odorous compounds from liquid swine manure 85µm Polyacrylate GC-MS 

aldehydes using headspace SPME 20 min @ 72°C 

in swine manure J. Environ. Sci.Health, B34(4), 709-748 (1999) 

Rizzuti, A., Cohen, A., Hunt, P., Vanotti, M. 

headspace, pH 2 

127 Cinnamon 

Classification of the Botanical Origin of Cinnamon by SPME-GC 

Chromatographia 42: 2187 (1996) 

Miller, K,. Poole, C., Pawlowski, T. 

321 Epicuticular 

SPME of Insect Epicuticular Hydrocarbons for GC-MS Analysis 

Rapid Commun. Mass Spectrom. 11 (8): 857-862 (1997) GC-MS 

hydrocarbons 

in insect culture 

Moneti, G., Dani, F., Pieraccini, G., Turillazzi, S. 

Solid- and vapor-phase antimicrobial activities of six essential oils: 

2252 Antimicrobial Susceptibility of selected foodborne bacterial and fungal strains headspace GC/MS 

activitie of J Ag Food Chem, 53, #17, 6939-6946 (2005) 





essential oils Lopez, P.; Sanchez, C.; Batlle, R.; Nerin, C. 

Determination of microbial volatile organic compounds from 

2217 Volatile organics Staphylococcus pasteuri against Tuber borchii using SPME-GC-MS GC-MS 

in bacteria Rapid Communications Mass Spectrometry 19 #22, 3411-3415 (2005) 

Barbieri, E.; Gioacchini, A. M.; Zambonelli, A.; Bertini, L.; Stocchi, V. 

2372 poly(3-hydroxy 

Use of headspace solid-phase microextraction for the quantification 

of poly(3-hydroxybutyrate) in microbial cells headspace GC-FID 

-butyrate) J. Chromatogr., A 1154, #1-2, 34-41 (2007-06-22) 

in microbial cells Monteil-Rivera, F.; Betancourt, A.; van Tra, H.; Yezza, A.; Hawari, J 

811 Volatile hydrocarbon 

Development of a method for the application of SPME 

to monitor biodegradation of volatile hydrocarbons GC-FID 

from bacterial during bacterial growth on crude oil 45min @ 30°C 

growth J Indus Microb & Biotech (2000) 25(3), 155-162 

Van Hamme, J. D.; Ward, O 

headspace 

Solid-phase microextraction of volatile compounds from the chopped leaves of 

three species of Eucalyptus. 


1054 from Eucalyptus. Journal of Agricultural and Food Chemistry (2003) 51 (9), 2679-2686. 

Pawliszyn, Janusz; Caramao, Elina B.; Christensen, Eva; Zanin, Kelen D.; Zini, 

Claudia A. 

Sampling and sample preparation for analysis of aromas and fragrances. 

1082 Aromas and fragrances Trends in Analytical Chemistry (2003) 22 (3), 160-169. 

Augusto, Fabio; Leite e Lopes, Alexandre; Zini, Claudia Alcaraz 

Localization and speciation of selenium and mercury in Brassica 

2169 Selenium, mercury juncea - Implications for Se-Hg antagonism headspace GC-ICP-MS 

in plants J Anal At Spectrom 21, #4, 404-412 (2006) GC-TOFMS 

Caruso, J.; Meija, J.; Mounicou, S.; Shah, M.; Shann, J.; Vonderheide,A. 

Simultaneous monitoring of volatile selenium and sulfur species from Se 

accumulating plants (wild type and genetically modified) by gas chromatography 

mass spectrometry and gas chromatography-inductively coupled plasma mass 

spectrometry using solid-phase microextraction for sample introduction. 

Selenium and sulfur 

1092 from plants. Analytical Chemistry (2002) 74 (22), 5837-5844. 

Meija, J.; Montes-Bayon, M.; Le Duc, D. L.; Terry, N.; Caruso, J. A.* 

GC-ICP MS 

Use of solid-phase micro-extraction as a sampling technique in the 

determination of volatiles emitted by flowers, isolated flower parts and pollen 

1120 Volatiles from flowers Journal of Chromatography A (2003) 1000 (1-2), 229-233. 

Cioni, Pier Luigi; Flamini, Guido; Morelli, Ivano 


Enantiomeric purity of (+/-)-methyl jasmonate in fresh leaf samples 

and commercial fragrances headspace GC/MS. 

from Jasminum J. Sep. Sci.30, #13, 2117-2122 (August 2007) 

leaves Blanch, Gracia P.; Ruiz del Castillo, Maria Luisa 

Composition and antimicrobial activity of Anemopsis 

2220 Volatiles californica leaf oil GC 

from califonica leaf J Ag Food Chem, 53, #22, 8694-8698 (2005) 

Medina, A.; Lucero, M.; Holguin, F.; Estell, R.; Posakony, J.; 

Simon,J.; O'Connell, M 

The composition of dalea formosa oil determined by steam 

2228 Volatile organics distillation and SPME 100um PDMS GC-FID and 

in dalea J. Essent. Oil Res. 17 #6, 645-647 (2005) GC/MS. 

formosa oil Estell, Rick E.; Lucero, Mary E.; Sedillo, Ruth L. 

Identification and quantification of methyl jasmonate in leaf volatiles of 

Arabidopsis thaliana using solid-phase microextraction in combination with gas 

chromatography and mass spectrometry. 





1121 Methyl jasmonate Phytochemical Analysis (2003) 14 (3), 155-159. 

Dubery, Ian A.; Meyer, Riaan; Rautenbach, George F. 

GC-MS 

Identification of sulcatol, a potential pheromone of the ambrosia beetle 

Gnathotrichus materiarius (Col., Scolytidae). 

1139 Sulcatol from beetles Journal of Applied Entomology (2003) 127 (4), 189-194. 

Flechtmann, C. A. H.; Berisford, C. W. 

1165 Mercury and tin 

Elevated lead levels: A possible factor behind the forest die back of Montane 

forests in Sri Lanka? 

Journal De Physique. IV : JP (2003) 107 (II), 1439. 

Dissanayake, C.B.; Ranasinghe, P.N. 

PDMS GC-MIP/AES 

2902 Methanol from 

Determination of methanol in biodiesel by headspace SPME 

Bioresour. Technol. 99, #13, 5901-5905 (September 2008) 75µm Carboxen GC-FID 

1170 

biodiesel Alley, E.; Armbrust, K.; French, W.; Hernandez, R.; Paraschivescu, M. headspace 

Ethanol from wood 

pulp 

Determination of methanol released from wood and mechanical pulp by 

headspace solid-phase microextraction 

J Pulp Pap Sci (2002) 28(6), 199-203 

Eckerman, C.; Holmbom, B.; Pranovich, A.V. 

2377 Chlorophenols in 

Focused microwave-assisted micellar extraction combined with 

SPME-GC-MS to determine chlorophenols in wood samples GC-MS 

wood samples Anal. Chim. Acta 582,#1, 10-18 (2007-01-16) 

Pino, V.; Ayala, J. H.; Gonzalez, V.; Afonso, A. M. 

2504 

Pentachlorophenol 

Removal of 2,4-dichlorophenol and pentachlorophenol from waters by 

sorption using coal fly ash from a Portuguese thermal power plant 

2,4-dichlorophenol J Hazardous Materials 143, #1-2, 535-540 (MAY 8 2007) 

in water Estevinho, B.; Martins, Isabel; Ratola, Nuno; Alves, Arminda; Santos, L. 

GC-ECD 

Development of a SPME method for direct determination of 

2264 Pentachlorophenol pentachlorophenol in paper and board samples: Comparison with PDMS & PA GC-ECD 

in paper samples conventional extraction method 

J. Chromatogr. A, 1095 #1-2, 8-15 (2005) 

Domeno, C.; Munizza, G.; Nerin, C. 

2661 

Pentachlorophenol 

Development of a SPME-GC-MS method for the determination of 

pentachlorophenol in human plasma using experimental design. headspace GC-MS 

in plasma Chemosphere 70, #2, 256-62 (2007 Dec) 

Zhou, Ying; Jiang, Qingwu; Peng, Qian; Xuan, Dongliang; Qu, Weidong acetylation 


The composition of volatiles from tatami mats containing hinoki 

(Chamaecyparis obtusa) wood-wool and its decline over the long term headspace GC 

tatami mats J. Wood Sci. 53, #6, 529-532 (December 2007) 

Hiramatsu, Y.; Imai, Y.; Matsui, N.; Miyazaki, Y.; Ohira, T. 

1171 Volatiles in wood 

On-line wood species sensor 

Process Control News Pulp Paper Industry (2002) 22(1), 10-11 

Fuhr, B.; Henry, D.; Sedgwick, G.; Smith, G.; Woolley, J. 

GC 

Reevaluation of the chemical secretion of the sternal glands of Polistes social 

wasps (Hymenoptera Vespidae). 

1173 Ethology Ecology & Evolution (2003) 15 (1), 73-82. 

Dani, F. R.; Jones, G. R.; Morgan, E. D.; Turillazzi, S. 

1181 

Characterization of Citrus unshiu ( C. unshiu Marcov. forma Miyagawa-wase ) 

blossom aroma by solid-phase microextraction in conjunction with an electronic 

nose. 


Choi, H. S. 

GC-MS 


1183 




VOCs in herbal drug 

preparations 

Chemical composition of some traditional herbal drug preparations: Essential oil 

and aromatic water of costmary (Balsamita suaveolens Pers.). 


Gallori, Sandra; Bilia, Anna Rita; Flamini, Guido; Landini, Andrea; Morelli, 

Ivano; Vincieri, Franco Francesco 

Rapid determination of floral aroma compounds of lilac blossom by 

2920 Floral aroma from fast GC combined with surface acoustic wave sensor headspace GC-MS 

lilac blossoms Journal of Chromatography A (Mar 7 2008) 1183(1-2), 170-178 

Oh, Se Yeon; Du Shin, Hyun; Kim, Sung Jean; Hong, Jongki 

1195 Floral scent 

SPME - A valuable tool for investigation of flower scent 

Journal of Separation Science (2003) 26 (8), 715-721. 

Bartak, Petr; Bednar, Petr; Cap, Lubomir; Ondrakova, Lenka; Stransky, Z. 

Carboxen/PDMS GC-MS 

Sensory and instrumental evaluation of catnip (Nepeta cataria L.) aroma. 

1204 Catnip aroma. Journal of Agricultural and Food Chemistry (2003) 51 (13), 3840-3848. 

Venskutonis, Rimantas P.; Baranauskiene, Renata; Demyttenaere, Jan C. R. 

Analysis of volatile components of Chrysanthemum coronarium L. by gas 

chromatography-mass spectrometry with solid-phase microextraction. 

Alpha pinene, 

1239 ocimene. Fenxi Ceshi Xuebao (2003) 22 (3), 87-89. 

Weng, X. X.; Deng, C. H.; Song, G. X.; Hu, Y. M.; Zheng, X. H. 

GC-MS 

1276 

1318 

Application of headspace solid-phase microextraction and gas chromatography 

to the screening of volatile compounds from some Brazilian aromatic plants. 


Brazilian aromatic 

plants. Chromatographia (2003) 57 (5-6), 351-356. 100 um PDMS GC-MS 

Sartoratto, A.; Augusto, F. * 

Volatile compound analysis of ageing Pinus sylvestris L. (Scots pine) seeds. 


from Scots pine seeds. Flavour and Fragrance Journal (2003) 18 (4), 290-295. GC-MS 

Tammela, P.; Hiltunen, R.; Hopia, A.; Laakso, I.; Nygren, M.; Vuorela, H. 

HS-SPME analysis of volatile organic compounds of coniferous needle litter 

VOC's in coniferous 

1324 needle litter. Atmospheric Environment (2003) 37 (33), 4645-4650. 

Isidorov, V.A.; Rafalowski, K.; Vinogorova, V.T. 

GC-MS 

Optimization of headspace sampling using solid-phase microextraction for 

volatile components in tobacco. 

1327 Volatiles in tobacco Journal of Chromatography A (2002) 942(1-2), 33-39 

Yang, S. S.; Huang, C. B.; Smetena, I. 

1352 

Volatiles in Michelia 

alba 

Rapid determination of volatile constituents of Michelia alba flowers by gas 

chromatography-mass spectrometry with solid-phase microextraction 


Hu, Yaoming; Deng, Chunhui; Hu, Keji; Shang, Chunqing 

100um PDMS, 25 

degrees C, 4 hours, 

headspace 

1379 Biogenic VOC's 

Monitoring biogenic volatile compounds (BVOC) emitted by Eucalyptus 

citriodora using SPME 

Analytical Chemistry (2001) 73(19), 4729-4735. 

Alcaraz Zini, C.; Augusto, F.; Christensen, E.; Smith, B. P.; Caramao, E. B.; 

Pawliszyn, J. * 

PDMS/DVB GC 


GC-MS




1398 

Volatiles from potential hosts of Rhopalicus tutela a bark beetle parasitoid. 

Journal of Chemical Ecology (2001) 27(11), 2219-2231. 

Pettersson, Eva M 

Species specificity of trail pheromones of fungus-growing termites from northern 

Vietnam. 

Carbowax/DVB GC-MS 

1404 

Pheromones in 

termites Insectes Sociaux (2001) 48(3), 245-250. GC-MS 

Bordereau, C.; Bonnard, O.; Peppuy, A.; Robert, A.; Semon, E.; Son, Ngo 

Truong 

Optimization of headspace solid phase microextraction for gas 

chromatography/mass spectrometry analysis of widely different volatility and 

polarity terpenoids in olibanum. 

1455 Terpenoids in olibanum Journal of Chromatograpy A (2003) 1018(1), 73-78 Various fibers compared GC-MS 

1458 

Terpenes in black 

currant 

Hamm, S.; Lesellier, E.; Bleton, J.; Tchapla, A. 

Influence of stage of ripeness on the enantiomeric distribution of chiral terpenes 

in blackcurrant fruits (Ribes nigrum L.). 

Journal of Food Science (2002) 67(9), 3284-3288 

Ruiz del Castillo, M. L.; Dobson, G. 

GC-FID 


Fungal Biotransformation of Monoterpenes Found in Agro-Industrial 

Residues from Orange and Pulp Industries into Aroma headspace GC 

agro-industrial Compounds: Screening Using SPME 

wastes Food Sci. Biotech. 16, #1, 37-42 (2007-02-00) 

Marostica, M. R.,Jr.; Mota, N. O.; Baudet, N.; Pastore, G. M. 

Sampling volatile compounds from natural products w/headspace/SPME 

2511 Aroma compound J. Biochem. Biophys. Meth. 70, #2, 235-242 (2007-03-10) headspace GC 

in natural products 

Stashenko, E. E.; Martinez, J. R. 

2441 Aroma compound 

Development of a headspace-SPME method to monitor changes in 

volatile profile of rose (Rosa hybrida , cv David Austin) petals 60µm PDMS/DVB GC 

in roses during processing headspace 

J. Chromatogr., A 1150, #1-2, 190-197 (2007-05-25) 

Bianchi, G.; Nuzzi, M.; Leva, A. A.; Rizzolo, A. 

30 min @ 60°C 

1466 


roses 

Analysis of rhythmic emission of volatile compounds of rose flowers. 

Molecular Methods of Plant Analysis (2002) 21, 199-221 

Verstappen, F. W. A.; Helsper, J. P. F. G.; Davies, J. A. 

Detection of physiologically active flower volatiles using gas chromatography 

coupled with electroantennography. 

1467 Volatiles in flowers Molecular Methods of Plant Analysis (2002) 21, 173-198 

Schiestl, F. P.; Marion-Poll, F. 

1469 

Fragrance compounds 

from Lavandula 

Comparison of different extraction methods for the analysis of fragrances from 

Lavandula species by gas chromatography-mass spectrometry. 

Journal of Chromatography A (2002) 982(1), 31-47 100um PDMS GC-MS 

Lee, Dong-Sun; Kim, Nam-Sun 

Selenium in plants by mass spectrometric techniques: Developments in bioanalytical 

methods. Plenary Lecture. 

1477 Selenium in plants Journal of Analytical Atomic Spectrometry (2002) 17(9), 1015-1023 GC-ICP-MS 

Caruso, Joseph A.; Grant, Tyre D.; Meija, Juris; Montes-Bayon, Maria 

2654 Selenium in 

Chemosensitization of B-cell lymphomas by methylseleninic acid 

involves nuclear factor-kappa B inhibition and the rapid generation headspace GC 

cytotoxic drugs of other selenium species 





CANCER RES 67, #22, 10984-10992 (15 NOV 2007) 

Juliger, S.; Goenaga-Infante, H.; Lister, T. A.; Fitzgibbon, J.; Joel, S. P. 

Determination of ochratoxin A in human urine by SPME- 

2655 Ochratoxin A HPLC-fluorescence detection. 65µm PDMS-DVB LC-FD 

in human urine J Pharm Biomed Anal 44, #4, 1014-8 (2007 Aug 15) 

Vatinno, R,; Aresta, Antonella; Zambonin, Carlo G; Palmisano, Francesco 

2762 Ochratoxin A 

Determination of Ochratoxin A in green coffee beans by SPME-LC 

with fluorescence detection headspace LC-FD 

green coffee J. Chromatogr., A 1187, #1-2, 145-150 (APR 11 2008) 

beans Aresta, Antonella; Palmisano, F.; Vatinno, Rosa; Zambonin, C. 

Reliability of fibres in SPME for routine analysis of the headspace of 

2382 Volatiles from aromatic and medicinal plants Car/DVB 50/30µm 

medicinal plants J. Chromatogr., A 1152, #1-2, 138-149 (2007-06-08) headspace 

Bicchi, C.; Cordero, C.; Liberto, E.; Sgorbini, B.; Rubiolo, P. 

1508 

Volatiles from 

medicinal plants 

A review of modern sample-preparation techniques for the extraction and 

analysis of medicinal plants. 

Analytical and Bioanalytical Chemistry (2002) 373(1-2), 23-30 

Huie, Carmen W. 

Extraction methods for Capsaicin encountered in aerosol defense sprays; a 

comparative analysis. 

1510 Capsaicin Abstracts of Papers American Chemical Society (2002) 223(1-2), ANYL 76 

Spicer, Oliver; Almirall, Jose R. 

1512 

1513 

Fragrances from 

Laurus nobilis 

Aroma volatiles from 

Eruca stavia 

Differences in the fragrances of pollen and different floral parts of male and 

female flowers of Laurus nobilis. 


Flamini, Guido; Cioni, Pier Luigi; Morelli, Ivano 

Aroma compound analysis of Eruca sativa (Brassicaceae) SPME headspace 

leaf samples using GC, GC-MS, and olfactometry. 

Journal of Agricultural and Food Chemistry (2002) 50(16), 4643-4646 headspace GC-MS 

Jirovetz, Leopold; Buchbauer, Gerhard; Smith, David 

Automation of solid-phase microextraction-gas chromatography-mass 

spectrometry extraction of eucalyptus volatiles. 

1544 Volatiles in Eucalyptus Journal of Chromatographic Science (2002) 40(3),140-146 GC-ITMS 

Zini, Claudia A.; Pawliszyn, Janusz; Lord, Heather; de Assis, Teotonio F.; 

Caramao, Elina B.; Christensen, Eva 

Semiquantitative determination of off-notes in mint oils by solid-phase 

microextraction 

1545 Volatiles in mint oils Journal of Chromatographic Science (2002) 40(3), 133-139 

Coleman, W. M., III; Cole, S. K.; Lawrence, B. M. 

Analysis of the essential oil of the aerial parts of Viola etrusca from Monte 

Labbro (South Tuscany, Italy) and in vivo analysis of flower volatiles using 

SPME 

1549 Volatiles from flowers Flavour and Fragrance Journal (2002) 17(2), 147-149 

1553 

Volatiles in 

sachalinmint 

Flamini, Guido; Cioni, P. L.; Morelli, I. 

Essential oil composition of sachalinmint from Norway detected by solid-phase 

microextraction and gas chromatography-mass spectrometry analysis. 


Rohloff, Jens 

Production of volatile compounds by hairy root cultures of Cichorium intybus L 

under the influence of fungal elicitors and their analysis using solid-phase micro 

extraction gas chromatography-mass spectrometry. 

Volatiles from fungal 

1138 cultures Journal of the Science of Food and Agriculture (2003) 83 (8), 769-774. GC-MS 





Bais, Harsh Pal; Dattatreya, B. S.; Ravishankar, G. A. 


Volatile constituents of benzoin gums: Siam and Sumatra, part 2. 

2208 Volatiles from Study of headspace sampling methods DVB/Car 50/30µm GC-MS 

benzoin gums Flavour and Fragrance Journal 21, #1, 59-67 (2006) 

Castel, C.; Fernandez, X.; Lizzani-Cuvelier, L.; Loiseau, A.; headspace 

Perichet, C.; Delbecque, C.; Arnaudo, J. 


Volatile constituents of benzoin gums: Siam and Sumatra. Part 1. 

Flavour and Fragrance Journal (2003) 18 (4), 328-333. 

Lizzani-Cuvelier, Louisette; Delbecque, Claire; Fernandez, Xavier; Loiseau, 

Carboxen/PDMS, GC-MS 

benzoin gums Andre-Michel; Perichet, Christine carbowax/DVB 


Quantitative analysis of terpenoids in the gas phase using headspace solidphase 

microextraction (HS-SPME). 

Flavour and Fragrance Journal (2001) 16(6), 411-416. 

Zabaras, D.; Wyllie, S. G. 

PDMS 

The use of pine bark as a natural adsorbent for persistent organic pollutants: 

Study of lindane and heptachlor adsorption. 

Lindane and 

1022 heptachlor J Chemical Technology and Biotechnology (2003) 78 (2-3), 347-351. 

Alves, Arminda; Botelho, Cidalia; Ratola, Nuno 

GC-ECD 

1094 

Bioconcentration of organic chemicals: is a solid-phase microextraction fibre a 

good surrogate for biota? 

Environmental Science and Technology (2002) 36 (24), 5399-5404. 

Leslie, H. A.; Ter Laak, T. L.; Busser, F. J. M.; Kraak, M. H. S.; Hermans, J. L. 

M. 

15 um PDMS GC-ECD 

1333 

Classification of Duvernay sourced oils from central and southern Alberta using 

Compound Specific Isotope Correlation (CSIC) 

Bulletin of Canadian Petroleum Geology (2003) 51 (5), 357-368. CF-IRMS 

Fowler, Martin G.; Harris, Scott A.; Whiticar, Michael J. 

1039 Pyrene 

Sorption of pyrene to dissolved humic substances and related model polymers. 

2. Solid-phase microextraction ( SPME ) and fluorescence quenching technique 

(FQT) as analytical methods. 


MacKenzie, K.; Georgi, A.; Kumke, M.; Kopinke, F. -D.* 

PDMS GC-FID 

1198 

Analysis of the volatile constituents of Apium graveolens L. and Oenanthe L. by 

gas chromatography-mass spectrometry, using headspace solid-phase 

microextraction. 

Chromatographia (2003) 57 (11-12), 805-809. 

Deng, C. H.; Song, G. X.; Zheng, X. H.; Hu, Y. M.*; Zhang, X. M. 


1343 

Analysis of the volatile constituents of Schisandra chinensis (Turz.) Bail by gas 

chromatography-mass spectrometry, using headspace solid-phase 


Chromatographia (2003) 58 (5-6), 289-294. PDMS, carbowax/DVB GC-MS 

Deng, C. H.; Song, G. X.; Hu, Y. M.*; Zhang, X. M. 

Diet-mediated inter-colonial aggression in Formosan 

1770 Cuticular subterranean termite Coptotermes formosanus headspace GC-MS 

hydrocarbons J Chemical Ecology, 30, #12, 2559-2574 

from wood Florane, C.; Bland, J.; Husseneder, C; Raina, A. 

Evaluation of the major female Eurytoma amygdali 

1771 Pheromones sex pheromone components, (Z,Z)6,9-tricosadiene and headspace GC 

from wasp (Z,Z)-6,9-pentacosadiene for male attraction in field tests 

J Chemical Ecology, 30, #6, 1245-1255 

Mazomenos, B.; Athanassiou, C; Kavallieratos, N; Milonas, P 

Avian exocrine secretions. I. Chemical characterization 

1772 Volatiles from of the volatile fraction of the uropygial secretion of dimethyl disulfide GC-MS 

secretion the green woodhoopoe, Phoeniculus purpureus derivatization 

J Chemical Ecology, 30, #8, 1603-1611 

Burger, B.; Reiter, B.; Borzyk, O.; Du Plessis, M. 

Volatile constituents of different organs of 





1773 Essential oil Psoralea bituminosa L Headspace GC, GC-MS 

P. bituminosa Flavour Fragrance J., 19,#2, 166-171 

from leaves Bertoli, A; Menichini, F; Morelli, I; Noccioli, C; Pistelli, L 

Volatile constituents of the roots of Echinops kebericho mesfin 

2363 Volatiles from Flavour Fragrance J. 22. #1, 35-38 (2007) Headspace GC-MS 

roots Hymete, A.; Rohloff, J.; Iversen, T. -H.; Kjøsen, H. 

Volatile constituents of different parts (roots, stems 

1774 Volatiles from and leaves) of Smyrnium olusatrum L Headspace GC, GC-MS 

plants Flavour Fragrance J., 19,#6, 522-525 

Bertoli, A.; Fraternale, D.; Giamperi, L..; Morelli, I.; 

Pistelli, L.; Ricci, D. 


Headspace SPME-GC-MS method for the identification of cosmetic 

ingredients causing delamination of packagings 75u Carboxen GC-MS 

cosmetics J. Chromatogr. A, 1101, #1-2, 32-37 (2006) headspace 

Ortiz, Gustavo; Tena, Maria Teresa 40°C 

Quantitative determination of formaldehyde in 

1775 Formaldehyde cosmetics using a combined SPME- 65µm PDMS-DVB GC-MS 

in cosmetics isotope dilution mass spectrometry method. pentafluorophenyl 

J. Chromatogr. A, 1029, #1-2, 217-222 hydrazine derivative 

Rivero, R. T.; Topiwala, V. headspace 

Vapor-phase analysis of isobutyl acetate, isopropyl 

1776 Solvent acetate, n-propyl acetate and their respective headspace GC-MS 

esters alcohols using SPME-GC w/ mass selective detector 

J Chromatography, A, 1066, #1-2, 225-230 

Cobb, G.; Cox, S.; Polydore, C.; Radtke, C. 

Sensory and analytical evaluations of paints with and without texanol 

2387 Volatiles from Environ. Sci. Technol. 42, #1. 243-248 (01 Jan 2008 ) headspace GC-MS 

paint Gallagher, M.; Dalton, P.; Sitvarin, L.; Preti, G. 

Disposable ionic liquid coating for headspace SPME 

1777 Solvents in of benzene, toluene, ethylbenzene, and headspace GC-FID 

paint xylenes in paints followed by GC-FID 

J. Chromatogr. A, 1066, #1-2, 27-32 

Liu, Jing-Fu; Li, Ning; Jiang, Gui-bin; Liu, Jie-min; 

Jonsson, Jan Ake; Wen, Mei-juan 

Comparison of terpene composition in Engelmann spruce 

1778 Terpenes in (Picea engelmannii) using hydrodistillation, SPME and PLE headspace GC 

spruce trees Zeitschrift fuer Naturforschung, 59, #9-10, 641-648 

Mardarowicz, M; Wianowska, D., A.; Sawicki, R. 

Use of headspace SPMEand headspace sorptive 

1779 Fugal volatiles extraction for the detection of the volatile headspace GC-MS 

on Agar metabolites produced by toxigenic Fusarium species. 

J Chromatogr A, 1027, #1-2, 147-154 

Demyttenaere, J; Morina, R; De Kimpe,N; Sandra, P 

Natural variability of the enantiomeric composition 

1780 Terpenes of bioactive chiral terpenes in Mentha piperita headspace GC-MS 

in plant J Chromatogr A, 1054,#1-2, 87-93 

emissions Blanch, G.P.; Herraiz, M.; Ruiz Del Castillo, M.L. 

2391 Terpenes from 

Enantiomeric monoterpene emissions from natural and damaged Scots 

pine in a boreal coniferous forest measured using SPME-GC-MS 65µm PDMS-DVB GC-MS 

Scots pine J. Chromatogr., A 1141 #1, 138-144 (2007-02-02) 

Yassaa, N.; Williams, J. 

1 min air sample 

Analysis of enantiomeric and non-enantiomeric 

1781 Terpenes monoterpenes in plant emissions using portable dynamic 65µm PDMS-DVB GC-MS 

in plant air sampling/SPME and chiral GC-MS direct air sampling 

emissions Atmos. Environ., 39, #27, 4875-4884 

Williams, Jonathan; Yassaa, Noureddine 

The release of terpenes during storage of biomass 

1782 Terpenes Biomass Bioenergy, 28, #1, 29-34 headspace GC-MS 

in biomass Rupar, Katarina; Sanati, Mehri 


Analysis of Platycladus orientalis volatiles and their 

electroantennogram responses with Semanotus headspace in situ GC-MS 





from trees bifasciatus 

Forest Research, 18, #3, 260-266 

Kong X; Zhang Z; Wang H; Yang Jie; Hu Y 

Determination of volatile components of Amomum 

1784 Volatiles of villosum Lour. by GC-MS with head-space SPME headspace GC-MS 

dried fruit Fudan Xuebao Zirankexueban, 43, #4,676-679 

Amomum Song Guo-xin; Deng Chun-hui; Wu Dan; Hu Y 

villosium 

A direct quantitative analysis method for monitoring 

1785 Volatiles biogenic volatile organic compounds released 50/30µm DVB/CAR GC-MS 

from leaves from leaves of Pelargonium hortorum in situ. 20 min extract 

Anal and Bioanal Chemistry, 380, #7-8, 950-957 headspace 

Deng, X.; Peng, J.; Luo, B.; Wei, M.; Hu, W.; Du, J. 

(SPME) with GC/MS and GC/matrix isolation-IR analysis in the 

2334 Volatiles from identification of volatile organic compounds in food products. GC/MS 

food products Abstracts of Papers Am Chem Society (2004) 227 Part1, U99 

Schneider, J.; Reed, Larry; Sytsma, Louis F.; Anderson, Ken B. 

Determination of nonylphenol and octylphenol in paper 

1786 Ocytl-, nonyl- by microwave-assisted extraction coupled to headspace Headspace GC-MS 

phenol in SPME and GC-MS 

paper J Chromatogra, A, 1065, #2, 251-256 

Barcelo, D.; Lacorte, S.; Latorre, A.; Montury, M. 

SPME-based approach to determine free-base nicotine in 

1787 Nicotine in trapped mainstream cigarette smoke total particulate matter. headspace GC-MS 

cigarette J Agr Food Chem, 52, #24, 7240-7245 

smoke Watson, C. H.; Trommel, J. S.; Ashley, D. L. 

Analysis of aroma constituents in tobacco flavour by 

1788 Flavour aroma GC-MS with solid-phase microextraction. 100µm PDMS GC-MS 

in tobacco Fenxi Shiyanshi, 23, #10, 22-25 85µm polyacrylate 

Dong, L.; Zhu, S. K.; Su, X. L.; Wu, C. Y.; headspace 

Xiong, G. X.; Chen, Z. G.; Li, D. 

The moss Physcomitrella patens releases a 

1789 Diterpenes tetracyclic diterpene Headspace GC 

from moss Plant Cell Reports, 22, #10, 780-786 

von Schwartzenberg, K.; Schultze, W.; Kassner, H. 

Identification and synthesis of volatiles released by 

1790 Volatiles from the myxobacterium Chondromyces crocatus headspace GC 

crocatus Tetrahedron, 60, #17, 3863-3872 

Schulz, Stefan; Fuhlendorff, Jens; Reichenbach, H. 

2151 Phenolic & 

Molecular characterisation of birch bark tar by headspace SPME- 

GC-MS: A new way for identifying archaeological glues headspace GC-MS 

sesquiterpenoids J. Chromatogr. A, 1101, #1-2, 245-253 (2006) 

in birch bark tar Regert, A; Alexandre, V.; Thomas, N.; Lattuati-Derieux, A. 

Determination of volatile compounds in Magnolia 

1791 Volatiles in bark by microwave-assisted extraction coupled headspace GC-MS 

magnolia to headspace SPME and GC-MS 

bark Analytical Sciences, 20, #5, 857-859 

Sha, Y. F.; Huang, T. M.; Shen, S.; Duan, G. L.* 

Chemical components of Vetiveria zizanioides volatiles. 

1792 Volatils of Yingyong Shengtai Xuebao, 15, #1, 170-172 headspace GC-MS 

zizanioides Huang Jinghua; Li Huashou; Yang Jun; Chen Yufen; 

Liu Yinghu; Li Ning; Nie Chengrong 

Headspace solid-phase microextraction (HS-SPME): A 

1793 Terpens in microscale sampling technique for determination of mono- headspace GC/MS 

coniferos terpene hydrocarbons in coniferous needles by GC-MS 

needles Anal. Bioanal. Chem., 378, #1, 150-158 

Chvilickova, I.; Kuban, V. 

Comparative study of two chromatographic methods for quantifying 

2673 2,4,6-trichloranisole 2,4,6-trichloranisole in wines headspace ECD 

in wines J. CHROMATOGR. A 1138, #1-2, 18-25 (05 JAN 2007) GC-MS 

Riu, M.; Mestres, M.; Busto, O.; Guasch, J. 





Quantification of chloroanisoles in cork using headspace SPME 


2319 Chloroanisoles gas chromatography with electron capture detection headspace ECD 

in cork stoppers J. Chromatogr. A 1107 #1-2, 240-247 (2006) 

Busto, O.; Guasch, J.; Mestres, M.; Riu, M. 

2155 Chloroanisoles 

Determination of total chloroanisoles in different kinds of cork stoppers 

Anal. Chim. Acta, 563, #1-2, 310-314 (2006) headspace GC-MS 

in cork stoppers Busto, O.; Guasch, J.; Mestres, M.; Riu, M. 

Determination of odour-causing volatile organic compounds 

1794 Volatile odors in cork stoppers by multiple headspace SPME 50/30µm DVB/CAR GC-MS 

from cork J. Chromatogr. A, 1068, #2, 201-208 45min @ 100°C 

Ezquerro, Oscar; Tena, Maria Teresa headspace 

GC-MS following pressurized hot water extraction and SPME 

2414 Volatiles from for quantification of eucalyptol, headspace GC-MS 

Eucalyptol J. Sep. Sci. 30, #1, 86-89 (2007-01) 

Dong, L.; Wang, J. Y.; Deng, C. H.; Shen, X. Z. 

Rapid determination of essential oil in Acorus tatarinowii 

1795 Essential oils Schott. by pressurized hot water extraction followed 10min @ 60°C GC-MS 

from chinese followed by SPME-GC-MS headspace 

medicine J. Chromatogr. A, 1059, #1-2, 149-155 

Deng, Chunhui; Li, Ning; Zhang, Xiangmin 

Identification of volatile organic compounds emitted by 

1796 Volatiles from a naturally aged book using SPME-GC-MS. headspace GC-MS 

aged book J. Chromatogr. A, 1026, #1-2, 9-18 contact sampling 

Lattuati-Derieux, A.; Bonnassies-Termes, S.; Lavedrine, B. 

Identification by GC-MS of the volatile organic compounds 

1797 Volatiles from emitted from the wood-rotting fungi Serpula lacrymans and headspace GC-MS 

wood fungi Coniophora puteana, and from Pinus sylvestris timber 

Mycological Research, 108, #7, 806-814 

Ewen, Richard J.; Jones, Peter R. H.; Ratcliffe, N.; 

Spencer-Phillips, Peter 

Chemical released from host Acacia by feeding 

1798 t-2-hexenal herbivores is detected by symbiotic Acacia-ants. headspace GC 

from Caribbean J of Science, 40, #3, 396-399 

acacia leaves. Wood, William F.; Wood, Brenda 

Aroma evaluation of an aquatic herb, changpo (Acorus 

1799 volatile flavor calamus var. angustatus Bess), by AEDA and SPME headspace GC-MS 

changpo J Agr Food Chem, 52, #26, 8099-8104 

Choi, H. S. 

Characterization of the volatile fraction emitted by phloems of four 

2182 Volatiles from pinus species by SPME-GC-MS headspace GC-MS 

pine tree J. Chromatogr. A, 1105, #1-2,191-198 (2006) 50/30µm PDMS/ 

Branco, M.; Farrall, M.; Gomes Da Silva, M.; Mateus, E.; Paiva, M.R.; Carboxen 

Santos, A.M.;Vasconcelos, T. 

Aroma-active compounds of Pinus densiflora 

1800 Volatiles from (red pine) needles 100µm PDMS GC-MS 

pine needles Flavour Fragrance J., 19, #6, 532-537 75µm Carboxen 

Kim, Kyoung Heon; Kim, Tae Hwan; Lee, Hyong Joo; Yu, E headspace 

Headspace-SPME analysis of the sapwood and heartwood of Picea Abies, 

2622 Hydrocarbons Pinus Sylvestris and Larix Decidua headspace GC-MS 

emissions J. Essent. Oil Res. 19. #2, 125-133 (March/April 2007) 

from wood Holmbom, B.; Pranovich, A.; Reunanen, M.; Wajs, A.; Willfor, S. 

Evaluation of hydrocarbon emissions from heart-And 

1801 Hydrocarbons sapwood of Scots pine using a laboratory-scale wood drie headspace @ 50°, 70°, GC-MS 

emissions Holzforschung, 58, #6, 660-665 and 90°C 

from pine Bengtsson, Peter; Sanati, Mehri 

Representativeness of extracts of offset paper 

1802 Odors from packaging and analysis of the main 100µm PDMS GC-MS 

packaging odor-active compounds 3 min @ 40°C 

J Agr Food Chem, 52, #8, 2326-2334 headspace 

Landy, P.; Nicklaus, S.; Semon, E.; Mielle, P.; Guichard, E. 

Identification of biogenic dimethyl selenodisulfide in the 





2189 Dimethyl headspace gases above genetically modified Escherichia coli headspace GC-MS 

selenodisulfide Analytical Biochemistry 348, #1, 115-122 (2006) 

from Escherichia Swearingen, J.; Frankel, D.; Fuentes, D.; Saavedra, C.;Vasquez, C., 

coli Chasteen, Thomas 

Production of the long-chain alcohols octanol, decanol, and 

2267 Alcohols from dodecanol by Escherichia coli headspace 

Escherichia Current Microbiology 51 #2, 82-86 (2005) 

coli Hamilton-Kemp, T.; Newman, M.; Collins, R.; Elgaali, H. Yu, K; 

Archbold, Douglas 

SPME, GC, and MS coupled w/discriminant factor 

1803 E coli volatiles analysis and multilayer perceptron neural network for headspace @ 37°C GC-MS 

coli from detection of Escherichia coli 

brooth J of Food Protection, 67, #8, 1597-1603 

Siripatrawan, Ubonratana; Linz, John E.; Harte, Bruce R. 

Catnip, Nepeta cataria (Lamiales: Lamiaceae) 

1804 Floral A closer look: Seasonal occurrence of epetalactone headspace GC-MS 

volatiles isomers and comparative repellency of three 

from catnip terpenoids to insects 

Environmental Entomology, 33, #6, 1562-1569 

Schultz, G; Simbro, E; Belden, J; Zhu, J; Coats, Joel 

Optimization of the SPME method in the determination of 

2190 Volatiles from Ixodes ricinus (L.) volatiles 100um PDMS GC-MS 

tick J. Sep. Sci., 29, #2, 236-241 (2006) headspace 

Bouman, Edwin A.P.; Zahradnickova, Helena 15 min 


Practical approaches to plant volatile analysis 

Plant Journal, 45, #4, 540-560 (2006) headspace GC-MS 

plants Tholl, D.; Boland, W.; Hansel, A.; Loreto, F.; Roese, U..;Schnitzler, J. 

Comparison of different extraction methods for the 

1805 Volatiles analysis of volatlle secondary metabolites of headspace GC-MS 

from plants Lippia alba )Mill) N.E. Brown, grown in Colombia, and 

evaluation of its in vitro antioxidant activity. 

J Chromatogr A, 1025, #1, 93-103 

Stashenko, E.; Jaramillo, B.; Martinez, J 

Biotransformation of (R)-(+)-and (S)-(-)-citronellol 

1806 Rose/nerol by Aspergillus sp. and Penicillium sp, and the use headspace GC-MS 

oxides of SPME for screening. steam distillation @ 

J Chromatogr A, 1027,#1-2, 137-146 3.5 pH 

Demyttenaere, J; Vanoverschelde, J; De Kimpe, N 

Headspace-SPME & hydrodistillation of two fragrant Artemisia 

1807 Fragrances Flavour Fragrance J., 20. #4, 395-398 headspace GC, GC-MS 

from Artemicia Baser, K. Husnu Can; Demirci, Betul; Demirci, Fatih 

plants 

Volatiles associated with preferred and non- 

1808 Volatiles from preferred hosts of the Nantucket pine tip moth, direct sampled GC-EAD 

slash/ loblolly Rhyacionia frustrana 

pine J Chemical Ecology, 30, #5, 977-990 

Asaro, C.; Sullivan, B.; Dalusky, M.; Berisford, C. 

Neocembrene A, a major component of the trail-following 

1809 Pheromone pheromone in the genus Prorhinotermes (Insecta, headspace GC-MS 

of canalifrons Isoptera, Rhinotermitidae) 

Chemoecology, 15, #1, 1-6 

Sillam-Dusses, D.; Semon, E.; Moreau, C.; 

Valterova, I.; Sobotnik, J.; Robert, A.;Bordereau, C 

Partial elucidation of Trichogramma putative sex 

1810 Pheromone pheromone at trace levels by SPME-GC-MS studies headspace for GC-MS 

from wasp J. Chromatogr. A, 1067, #1-2, 311-321 20-50hr 

Melo, R; Posthumus, M.; Silva, I.; Van Beek, T 

New type of sesiidae sex pheromone identified 

1811 Sesiidae sex from the hornet moth Sesia apiformis headspace GC-MS 

pheromone J Chemical Ecology, 30, #4, 805-817 2-alkenals derivative 

from hornet Francke, W.; Karalius, V.; Plass, E.; Lehmann, L.; 

moth dos Santos, A.; Buda, V.; Mozuraitis, R. 

Borg-Karlson, A.; 





Flight activity and further evidence for a female- 

1812 Pheromone produced sex pheromone of the apple leaf headspace GC-EAD 

emission midge, Dasineura mali, in Nova Scotia 

from leaf Northeastern Naturalist, 12, #1, 93-102 

midge Heath, J.; Zhang, Aijun; R., Wendell L.; Smith, R. 

Effect of aging on pheromone emission from a 

1813 Pheromone commercial beet armyworm (Lepidoptera : headspace GC-MS 

emission Noctuidae) lure and trap efficiency 

from traps J Economic Entomology, 98, #2, 373-377 

Showler, A..; Salgado, E.; Fraser, I.; Robacker, D. 

Semiochemicals related to the aphid Cinara pilicornis and its host, 

2395 Volatiles released Picea abies: A method to assign nepetalactone diastereomers headspace GC/MS 

from Norway J. CHROMATOGR. A 1180, #1, 165-170 (2 -08 FEB 2008 ) 

spruce Pettersson, M.; Unelius, C. R.; Valterova, I.; Borg-Karlson, A. -K 

Tick repellent substances in the essential oil of Tanacetum vulgare 

2825 Volatiles from Journal of Medical Entomology 45, #1, 88-93 (JAN 2008) headspace GC/MS 

Essential oils of Palsson, K.; Jaenson, Thomas G.; Baeckstrom, P.; Borg-Karlson, A. 

aromatic plant 

Evaluation of extracts and oils of tick-repellent plants from Sweden 

2322 Volatiles from Medical and Veterinary Entomology 19 #4, 345-352 (2005) headspace GC/MS 

leaf extracts Jaenson, T. G. T.; Palsson, K.; Borg-Karlson, A.-K. 

2253 Volatile releases 

Role of (E)-beta-farnesene in systematic aphid prey location by 

Episyrphus balteatus larvae (Diptera : Syrphidae) headspace GC/MS 

from aphids European Journal of Entomology 102 #3, 431-436 (2005) 

and plants Francis, Frederick; Martin, Thibaut; Lognay, Georges; Haubruge, E. 

A cost of alarm pheromone production in cotton 

1814 Pheromone apids, Aphis gossypii headspace GC-MS 

from aphids Naturwissenschaften, 92, #2, 69-72 

Byers, John A. 

Release of sex pheromone and its precursors in the pine sawfly 

2254 Sex pheromone Diprion pini (Hym., Diprionidae) headspace GC/MS 

of pine sawfly Chemoecology 15 #3, 147-151 (2005) 

Anderbrant, O.; Ostrand, F.; Bergstrom,G .; Wassgren, A.; 

Auger-Rozenberg, M.; Geri, C.; Hedenstrom, E.; Hogberg, H.; 

Hertz, Annette; Heitland, Werner 

Acetate esters of saturated and unsaturated alcohols (C12-C20) are 

2279 Acetate esters major components in Dufour glands of Bracon cephi and Bracon headspace GC-MS 

from wheat stem lissogaster (Hymenoptera : Braconidae), parasitoids of the wheat 

sawfly stem sawfly, Cephus cinctus (Hymenoptera : Cephidae) 

Biochemical Systematics and Ecology 33 #8 757-769 (2005) 

Baker, J.; Howard, R.; Morrill, W.; Meers, S.; Weaver, D. 

SPME for the investigation of sex pheromone of 

1815 Pheromone Eucosam notanthes Meyrick headspace GC-MS 

from fruit Talanta, 65, #3, 743-749 5min @ 20°C 

borer Chu, T. Y.; Hung, C. C.; Hsu, C. Y. 

Rapid determination of volatile compounds emitted 

1816 Fragrance from Chimonanthus praecox flowers by headspace headspace GC-MS 

from flowers SPME-GC-MS 

Zeitschrift fuer Naturforschung, 59, #9-10, 636-640 

Deng, Chunhui; Song, Guoxin; Hu, Yaoming 

Single step determination of fragrances in Cucurbita 

1817 Fragrance flowers by coupling headspace SPME low-pressure 65µm PDMS-DVB GC-MS-MS 

from flowers GC-tandem mass spectrometry 5min @ 60°C 

J. Chromatogr. A, 1045, #1-2, 173-179 headspace 

Egea Gonzalez, F.; Garrido Frenich, A.; Guerra Sanz, J.; 

Martinez Vidal, J.L.; Mena Granero, A. 

Headspace-SPME of in vitro shoot-cultures and micropropagated plants 

2776 Volatiles from of Lavandula viridis headspace GC-MS 

shoot-cultures Biologia Plantarum (Prague) 52, #1, 133-136 (MAR 2008) 

Goncalves, S.; Serra, H.; Nogueira, J.; Almeida, R.; 

Custodio, L.; Romano, A. 





Sex and developmental stage of carob flowers 

1818 Fragrance affects composition of volatiles headspace GC-MS 

from Carob J Horticultural Sci & Biotechnology, 79, #5, 689-692 

flower Custodio, L.; Nogueira, J. M. F.; Romano, A. 

Direct extraction of volatiles of rice during cooking using SPME 

2690 Volatiles from Cereal Chemistry 4, #5, 423-427 (2007) 

cooked rice Zeng Zhi; Zhang Han; Chen JieYu; Zhang Tao; Matsunaga, R. 

Determination of flavour profile in Iranian fragrant rice samples 

2476 Volatiles from using cold-fibre SPME-GC-TOF-MS 100um PDMS GC-TOF-MS 

scented rice Flavour and Fragrance J. 22, #5, 377-391 (SEP-OCT 2007) headspace 

Ghiasvand, Ali Reza; Setkova, Lucie; Pawliszyn, Janusz 

Rapid discrimination of scented rice by SPME, mass spectrometry, 

2418 Volatiles from and multivariate analysis used as a mass sensor headspace GC-MS 

scented rice J. Agric. Food Chem. 55, #4, 1077-1083 (2007-02-21) 

Laguerre, M.; Mestres, C.; Davrieux, F.; Ringuet, J.; Boulanger, R. 

SPME-GC and olfactory analysis of the scent and 

1819 Essential oils fixative properties of the essential oil of Rosa headspace GC-FID and GC-MS 

from Chinese damascena L. from China 

rose oil Flavour and Fragrance J, 20, #1, 7-12 

Jirovetz, Leopold; Buchbauer, Gerhard; S, A; 

Balinova, A.; Guangjiun, Z.; Xihan, Ma 

Comparison of odorous volatile compounds from fourteen 

1820 Volatiles from different commercial composts using SPME. headspace GC 

compost Trans. Am. Soc. Agric. Eng., 48, #1, 315-320 

Kim, H.; McConnell, L.L.; Millner, P. 

Why are some floral nectars scented? 

1821 Nectar odors Ecology (Washington D C), 85, #6, 1486-1494 headspace GC-MS 

from flowers Raguso, Robert A. 

Quality assessment of Flos Chrysanthemi Indici from 

1822 Volatiles different growing aras in China by SPME-GC-MS 65µm PDMS-DVB GC-M 

from China J. Chromatogr. A, 1047, #2, 281-287 30min @ 60°C 

medicine Chen, J; Deng, C; Fu, D; Sha, Y; Shen, S Zhang, X headspace 

SPME-GC-MS analysis of volatile compounds in compounded 

1823 Volatiles Chinese medicinal prescription, Xiao-Cheng-Qi-Tang 100µm PDMS GC-MS 

from China Journal of Pharma Biomed Analysis, 36, #2, 381-385 20min @ 90°C 

medicine Sha, Yunfei; Shen, Shun; Duan, Gengli stirring, headspace 

Application of HS-SPME and GC-MS to characterization of 

1824 Volatiles from volatile compounds emitted from osmanthus flowers 65µm CW/DVB GC-MS 

osmanthus Annali di Chimica, 94, #12, 921-927 10 min @ 22°C 

flowers Deng, Chunhui; Song, Guoxin; Hu, Yaoming headspace 

An evaluation of SPME for analysis of odorant 

1825 Odors from emissions from stored biosolids cake 75µm Carboxen GC-MS 

biosolids Water Res., 38, #17, 3800-3808 headspace 

Parker, W.J.; Visan, M. 

Effects of petroleum spray oils on oviposition behaviour and 

1826 Volatiles from larval survival of Helicoverpa armigera Hubner (Lepidoptera headspace GC 

maize plants Noctuidae) and Ostrinia nubilalis Hubner (Lepidoptera:Pyralidae) 

Intl J of Pest Mgmt, 51, #2, 111-119 

Mensah, Robert; Frerot, Brigitte; Al Dabel, Faiza 

Pharmaceuticals 


Application of Head-Space SPME for the Analysis of 

Volatile Metabolites GC-MS 

biological fluids J. Microbiol. Methods 25: 245 (1996) 

Milsson, T., Larsen, T., Montanarella, L., Madsen, J. 

338 Solvents in 

Determination of Residual Solvents in Pharmaceuticals 

with Automated SPME 100µm PDMS GC-FID 

pharmaceutical Chem. N. Z. 61 (4): 10-12 (1997) 15 min 

products Penton, Z. headspace 

149 Components 

Analysis of Components in Crude Drugs by Headspace 

SPME Method 





in drugs Zasshi 16: 251 (1996) 

Yakugaku 


Headspace SPME method optimization for 

residual solvent analysis 65µm DVB/PDMS GC 

pharmaceutical Acta pharm. Hung., 1999, 69(2), 77-84 30 min headspace 

samples Camarasu, C., Mezei, M., Szabo, A 2gm NaCl, 


Headspace SPME method development for the analysis of 

volatile polar residual solvents by GC-MS 

pharmaceutical J. Pharm. & Biomediecal Aanlysis 2000, 23(1) 197-210 

samples Camarasu, C. 

Verapamil drug metabolism studies by automated in-tube solid phase 


1002 Verapamil Jnl of Pharmaceutical and Biomedical Analysis (2002) 30 (2), 307-319. LC-MS 

Walles, M.; Mullett, W. M.; Levsen, K.; Borlak, J.; Wuensch, G.; Pawliszyn, J. 

New trends in sample preparation for clinical and pharmaceutical analysis 

1006 Trends TrAC-Trends in Analytical Chemistry (2003) 22 (4), 232-244. 

Kataoka, Hiroyuki 

1024 clenbuterol 

Solid-phase micro extraction (SPME) and headspace derivatization of 

clenbuterol followed by GC-FID and GC-SIMMS quantification. 

Analytical and Bioanalytical Chemistry (2003) 375 (3), 460-464. 

Wenclawiak, B. W.; Engelmann, M. D.; Hinz, D. 

85 µm polyacrylate GC-FID, GC-SIMMS 

Residual solvent testing: A review of gas-chromatographic and alternative 

techniques. 

1032 Review Pharmaceutical Research (Dordrecht) (2003) 20 (3), 337-344. 

B'Hymer, Clayton 

New designer drug 4'-methyl-alpha-pyrrolidinohexanophenone: Studies on its 

metabolism and toxicological detection in urine using gas chromatographymass 

spectrometry. 

1101 MPHP in urine Journal of Chromatography B (2003) 789 (1), 79-91. GC-MS 

Maurer, Hans H.; Fritschi, Giselher; Peters, Frank T.; Springer, Dietmar 


Use of solid-phase microextraction coupled with gas chromatography for the 

determination of residual solvents in pharmaceutical products 


Dugay, Jose; Legrand, Stephanie; Vial, Jerome 

Various 

1133 

1142 

Residual solvents in 

drug products 

Unknown residual solvents identification in drug products by headspace solid 

phase microextraction gas chromatography-mass spectrometry. 

Chromatographia (2002) 56(supplement), S131-S135 headspace GC-MS 

Camarasu, C. C. 

Determination of volatile residual solvents in traditional Chinese medicines by 

headspace solid-phase microextraction and cryogenic gas chromatography with 

flame ionization detection 

Volatile residual 

solvents in Chinese 

medicines. Journal of AOAC International (2003) 86 (3), 461-466. PDMS/DVB GC-FID 

Jiang, Guibin; Liu, Jiemin; Liu, Jingfu; Liu, Jiyan; Wen, Meijuan; Zhou, Qunfang 

Determination of methylmalonic acid and glutaric acid in urine by 

2608 Methylmalonic & aqueous-phase derivatization followed by headspace SPME-GC-MS 100 µm PDMS GC/MS 

glutaric acid J. Sep. Sci. 30, #2, 266-271 (2007-02) 55°C for 30 min, 

in urine Li, N.; Deng, C. H.; Zhang, X. M. diethyl sulfate 

derivatives 

Development of SPME-GC method to determine 

2324 Methylformamide N-hydroxymethyl-N-methylformamide and N-methylformamide in urine 65µm DVB/PDMS GC-NPD 

in urine J. Chromatogr. B, 828 #1-2, 103-107 (2005) headspace 

Knupp, V.; Alvarez Leite, Edna Maria; de Lourdes Cardeal, Zenilda 80°C for 15 min, 





Determination of clenbuterol in urine using headspace SPME or 

2247 Clenbuterol liquid-liquid-liquid microextraction headspace GC/MS 

in urine Analytica Chimica Acta 552 #1-2, 67-75 (2005) HMDS derivatives 

Melwanki, Mahaveer B.; Hsu, Wei-Hsun; Huang, Shang-Da 

1169 Clenbuterol in urine 

Quick analysis of small beta -agonists in urine by solid-phase microextraction 

with headspace derivatization and gas chromatography-mass spectrometry. 

Fenxi Huaxue (2003) 37 (3), 326-328. 

Liang, Y. L.; Yin, B. Z.; Hu, X. Z.*; Yu, J. X.; Liu, H. W.; Lin, Y. F.; Wu, T. 

Polyacrylate GC-MS 

Simple and rapid analysis of endocrine disruptors in liquid medicines and 

intravenous injection solutions by automated in-tube solid-phase 

microextraction/high performance liquid chromatography. 

Endocrine disruptor 

1279 contaminants. Journal of Pharmaceutical and Biomedical Analysis (2003) 32 (3), 469-478. 

Mitani, K.; Narimatsu, S.; Izushi, F.; Kataoka, H. * 

HPLC 

1308 Drug analysis 

Solid-phase microextraction and liquid chromatography/mass spectrometry in 

drug analysis 

Analytica Chimica Acta (2003) 492 (1-2), 49-67. 

Kumazawa, Takeshi; Lee, Xiao-Pen; Sato, Keizo; Suzuki, Osamu 

LC-MS 

Determination of pharmaceutical process impurities by solid phase 

microextraction gas chromatography 

Pharma process 

1312 impurities Journal of Separation Science (2003) 26 (12-13), 1097-1103. 

Frost, Richard P.; Hussain, Mumtaz S.; Raghani, Anil R. 

Carboxen/PDMS/DVB GC 

In vivo sampling with solid phase microextraction 

2445 Drugs in J. Biochem. Biophys. Meth. 70, #2, 181-193 (2007-03-10) 

biological fluids Musteata, F. M.; Pawliszyn, J. 

Development and evaluation of a solid-phase microextraction probe for in vivo 

pharmacokinetic studies 

1336 Analytical Chemistry (2003) 75 (19), 5103-5115. polypyrrole 

Fahie, Brian; Grant, Russell P.; Incledon, Bev; Lord, Heather L.; Pawliszyn, 

Janusz B.; Walles, Markus 

1361 

Automated sample preparation using in-tube solid-phase microextraction and 

its applications long dash a review. 

Drugs in biological 

fluids Analytical and Bioanalytical Chemistry (2002) 373(1-2), 31-45. 

Kataoka, H. 

LC-MS 

Comparison of SPME and liquid-liquid extraction in 96-well format for 

2753 Drugs in the determination of a drug compound in human plasma by LC-MS LC-MS 

plasma J. PHARM. BIOMED. ANAL. 45, #4, 599-608 (30 NOV 2007) 

Xie, W.; Pawliszyn, J.; Mullett, W. M.; Matuszewski, B. K. 

2562 Asarones 

Development of GC-MS following headspace SPME for fast . 

determination of asarones in plasma headspace GC-MS 

in plasma Rapid Commun. Mass Spectrom.20, #14, 2120-2126 (2006-06-09) 

Deng, C. H.; Lin, S.; Huang, T. M.; Duan, G. L.; Zhang, X. M. 

2905 Nitromethane 

Method for quantifying nitromethane in blood as a potential biomarker 

of halonitromethane exposure headspace GC/MS 

in blood Environ. Sci. Technol. 42, #7, 2522-2527 (Apr 1 2008) 

Alwis, K. ; Blount, Be.; Loose, K; Silva, Lalith K.; Smith, M. 

SPME method for carbon isotopic analysis of volatile carboxylic acids in 

2561 Carboxylic acid human plasma byGC/combustion/isotope ratio mass spectrometry. 75µm Carboxen GC/C/IRMS 

in plasma Rapid Commun. Mass Spectrom. 20, #23, 3573-3578 (2006-11-13) 

Ferchaud-Rocher, V.; Albert, C.; Champ, M.; Krempf, M. 

headspace 

Simultaneous determination of selegiline and desmethylselegiline in 





2707 Selegiline human body fluids by headspace SPME-GC-MS headspace GC/MS 

in human blood J. Chromatogr., B: 844, #2, 283-291 (2006-12-05) 

Kuriki, A.; Kumazawa, T. ; Lee, X. P,; Hasegawa, C.; Kawamura, M.; 

Suzuki, O.; Sato, K. 

2456 Paeonol in plasma 

Fast determination of paeonol in plasma by headspace SPME followed 

by gas chromatography-mass spectrometrY 

Anal. Chim. Acta 585, #1, 76-80 (2007-02-28) 

Dong, L.; Deng, C. H.; Wang, J. Y.; Shen, X. Z. 


2425 Fluoxetine and 

SPME-LC determination of fluoxetine and norfluoxetine in plasma using 

a heated liquid flow through interface 65µm PDMS/DVB LC-MS 

norfluoxetine in J. Chromatogr., B: 847, #2, 217-223 (2007-03-01) 

plasma Fernandes, C.; dos Santos Neto, A.; Rodrigues, J.; Alves, C.; Lancas, F. 

1392 Drugs in plasma 

Application of solid-phase micro-extraction technology to drug screening and 

identification. 

Annals of Clinical Biochemistry (2001) 38(5), 541-547. 

Mosaddegh, M. H.; Richardson, T.; Stoddart, R. W.; McClure, J. 

Polyacrylate, carbowax/D GC-MS 

1470 Amphetamine-like 

drugs 

1497 


pharmaceuticals 

Simultaneous detection of amphetamine-like drugs with headspace solid-phase 

microextraction and gas chromatography-mass spectrometry. 

Journal of Chromatography B (2002) 780(1), 183-192 GC-MS 

Macchia, Teodora; Chiarotti, Marcello; Gentili, Stefano; Marsili, Remo; Torresi, 

Alessio 

High-speed gas chromatographic analysis of solvents in pharmaceuticals using 

solid phase microextraction 

Journal of Pharmaceutical and Biomedical Analysis (2002) 29(3), 507-518 

Raghani, A. R. 


PDMS, 65um PDMS 

DVB 

2769 citalopram, 

Simultaneous determination of citalopram, fluoxetine and their 

main metabolites in human urine samples by SPME-LC HPLC-UV 

fluoxetine in J Pharma and Biomedical Analysis 46(4), 763-770 (MAR 13 2008) 

human urine Unceta, Nora; Gomez-Caballero, Alberto; Sanchez, Alicia; Millan, S.; 

Carmen Sampedro, M.; Aranzazu Goicolea, M.; Salles, J.; Barrio, R. 

Determination of delorazepam in urine by solid-phase microextraction coupled 

to high performance liquid chromatography. 

1514 Delorazepam in urine Journal of Pharmaceutical and Biomedical Analysis (2002) 28(5), 965-972 

Zambonin, Carlo Giorgio; Aresta, Antonella; Monaci, Linda 

50um Carbowax TPR, 

60um PDMS DVB 

HPLC-UV 

Rapid screening of 2-"fluorine-18"-fluoro-2-deoxy-D-glucose infusions for volatile 

organic compound contaminants by solid phase microextraction with gas 

chromatography-selective ion monitoring mass spectrometry (SPME-GC- 

SIMMS). 

1201 Applied Radiation and Isotopes (2003) 58 (2), 193-200. 

Kanu, A. B.; Dixon, M.; Zu, Y. Y.; Bailey, J.; Gillies, J. M.; Zweit, J.; Thomas, C. 

L. P.* 

1280 

Determination of trace retinoic acid by capillary electrophoresis-solid-phase 

microextraction with direct UV detection. 

Journal of Chromatographic Science (2003), 41 (6), 301-304). 

Fang, M.; Xu, G. W. 

CE 

Study of multiple SPME combined off-line w/HPLC 

1827 Pharmaceuticals Application in analysis of pharmaceuticals in urine 100µm PDMS & HPLC 

in urine Anal. Chim. Acta, 516, #1-2, 197-204 85µm polyacrylate 

Aikaterini Lontou, M.; Gondova, T.; Michopoulos, F.; immersed 

Sucha, M.; Theodoridis, G. salt added 

Biological 

2205 Phosphoric acid 

Determination of phosphoric acid triesters in human plasma using 

SPME and GC coupled to inductively coupled plasma MS 65µm DVB/PDMS GC-MS 

triesters in J. Chromatogr. A, 1103, #2, 329-336 (2006) immersion 

human plasma Shah, Monika; Meija, Juris; Cabovska, Baiba; Caruso, Joseph A. 30min @40°C 


GC




deproteinization 

2204 Proteomics 

Sample preparation techniques for mass spectrometry in proteomics 

using recently developed highly selective materials 

Current Proteomics 2 #4, 269-285 (2005) 

Huck, Christian W.; Bakry, Rania; Bonn, Guenther K. 

MS 

Evaluation of SPME for the study of protein binding in human 

638 Anesthetics plasma samples 60µm Carbowax/DVB NPD 

in plasma J. Chromatogr. Sci. (2000), 38(10), 458-464 32°to 40°C 

Abdel-Rehim, M., Calsson, G., Bielenstein, M., Arvidsson, T., pH 6.4-9.4 

Blomberg, L. 

Influence of albumin on sorption kinetics in SPME: Consequences 

2613 Pyrene diffusion for chemical analyses and uptake processes 

serum albumin Anal. Chem. 79,#18, 6941-6948 (Sep 15 2007) 

Hermens, Joop L. M.; Kramer, Nynke I.; Van Eijkeren, Jan C. H. 

Application of SPME in the investigation of protein binding of 

2227 Drugs in pharmaceuticals HPLC 

serum albumin J. Chromatogr. B 830 #2, 238-244 (2006) 

Theodoridis, Georgios 

Measurement of the Free Concentration Using SPME: 

99 Aniline, nitrobenzene, Binding to Protein 85µm polyacrylate GC-MS 

4-n-pentylphenol, J. Anal. Chem. 68: 4463-4467 (1996) 24°C, 9-14 min 

4-chloro-3methylphenol 

Vaes, W., Ramos, E., Verhaar, H., Seinen, W., Hermens, J. stirring 

in bovine serum 

albumin K2PO4 buffered 

Modeling bovine serum albumin binding of flavor compounds (alcohols, 

2843 Flavor compounds aldehydes, esters, and ketones) as a function of molecular properties headspace GC 

bovine serum Journal of Food Science 73, #1, S56-S63 (JAN-FEB 2008) 

Tan, Y.; Siebert, K. J. 

Quantification of solute-solute interactions using negligible-depletion 

2888 Estradiol in SPME: Measuring the affinity of estradiol to bulk organic matter 

organic matter Environ. Sci. Technol. 42, #8, 2886-2892 (Apr 15 2008) 

Escher, Beate I.; Neale, Peta A.; Schafer, Andrea I. 

The binding constant of estradiol to bovine serum albumin. An 

2320 Estradiol from upper-level experiment utilizing tritium-labeled estradiol and headspace GC 

bovine serum liquid scintillation counting 

albumin J Chem Educ 83 #2, 294-295 (2006) 

Adhyaru, Bhavin; Liang, Peihong; Pearson, Wright L.; Williams, K. 

Solid Phase Microextraction of Biopolymers, Exemplified 

140 Protein in with Adsorption of Basic Proteins onto a Fiber Coated 85µm polyacrylate HPLC-UV 

bovine serum albumin with Polyacrylic Acid 5-240 sec 

J. Microcolumn Sep. 8: 1 (1996) 

Liao, J., Zeng, C., Hjerten, S., Pawliszyn, J. 

immersion 

Sorbent preconcentration procedures coupled to capillary 

2899 Review article electrophoresis for environmental and biological applications 

Anal. Chim. Acta 616, #1, 1-18 (May 26 2008) 

Aguilar, Carme; Borrull, Francesc; Calull, Marta; Puig, Patricia 

411 Proteins 

Optimization of SPME-Capillary Zone Electrophoresis-MS for 

High Sensitivity Protein Identification capillary zone 

Electrophoresis (1998), 19(13), 2338-2347 electrophoresis- 

Figeys, D., Ahang, Y., Aebersold, R. MS 

Bio-compatible in-tube SPME capillary for the direct extraction and HPLC 

determination of drugs in human serum. 

988 Drugs in human serum J.Chromatogr. A (2002) 963(1-2), 325-334 HPLC 





Mullett, W.M.; Levsen, K.; Lubda, D.; Pawliszyn, J. 


Rapid diagnosis of ulcerative colitis and Crohns disease by the 

2237 Volatiles from analysis of flatus headspace GC/MS 

stool samples Gastroenterology 126, #4 Suppl 2, A203 (2004) 

Probert, Christopher S. J.; Garner, C. E.; Ratcliffe, Norman 

Rapid diagnosis of GI infection from flatus. 

1020 Gut (2003) 52 (Supplement 1), A93. 

Probert, C. S.; Jones, P.; Ratcliffe, N. 

1036 Semi-volatiles in saliva 

Solid-phase micro-extraction-gas chromatography-mass spectrometry and 

headspace-gas chromatography of tetrahydrocannabinol, amphetamine, 

methamphetamine, cocaine and ethanol in saliva samples 

Journal of Chromatography B: Analytical Technologies in the Biomedical and 

Life Sciences (2003) 789 (1), 73-78. PDMS GC-MS 

Alves Silva, Ovandir; De Moraes Moreau, Regina Lucia; Tawil, Nadia; 

Yonamine, Mauricio 

Single hair analysis of methamphetamine and amphetamine by 

2711 Amphetamines solid phase microextraction coupled with in matrix derivatization 

Journal of Chromatography B: Analytical Technologies in the Biomedical 

GC 

in hair. 

and Life Sciences 842 #2, 106-110. (2006-10-02) 

Nishida, M.; Yashiki, M.; Namera, A.; Kimura, K. N-propoxycarbonyl 

derivatives 

1037 Amphetamines in hair. 

Determination of amphetamines in human urine by headspace solid-phase 

microextraction and gas chromatography 


Life Sciences (2003) 789 (1), 59-63. 100 um PDMS GC-FID 

Christopoulou, Klio; Psaroulis, Dimitrios; Raikos, Nikolaos; Theodoridis, 

Georgios; Tsoukali, Heleni 

Investigation into the production of 2-Pentylfuran by Aspergillus 

2869 2-Pentylfuran fumigatus and other respiratory pathogens in vitro and human headspace GC/MS 

in breath breath samples 

Medical Mycology 46, #3, 209-215 (2008) 

Syhre, Mona; Scotter, Jennifer M.; Chambers, Stephen T. 

Determination of aldehydes in human breath by on-fibre derivatization, 

2743 Aldehydes in solid-phase microextraction and GC-MS 65µm PDMS/DVB GC/MS-SIM 

breath J Chromatogr B 860, #1, 86-91 (2007 Dec 1) headspace 

Svensson, S.; Larstad, M.; Broo, K.; Olin, A. -C. 

PFBHA derivative 

An optimized method for determination of benzene in exhaled 

2785 Benzene in air by GC-MS using SPME as a sampling technique GC/MS 

breath J Chromatogr B, 865, #1-2, 141-146 (Apr 1 2008) 

Amorim, Leiliane C.A.; Cardeal, Zenilda L.; Carneiro, Joana P. 


Breath air analysis and its use as a biomarker in biological monitoring 

of occupational and environmental exposure to chemical agents. air sampling GC 

breath J Chromatogr B, 853, #1-2, 1-9 (2007 Jun 15) 

Amorim, Leiliane Coelho A; de L Cardeal, Zenilda 

Evaluation of the SPME technique for the analysis of human 

2249 Aroma compounds breath during eating PDMS GC/MS 

in human breath Sciences des Aliments 25 #3, 193-206 (2005) headspace 

Pionnier, E.; Semon, E.; Chabanet, C.; Salles, C. 

Application of low-temperature glassy carbon-coated macrofibers for solidphase 

microextraction analysis of simulated breath volatiles 

1038 Volatiles in breath Analytical Chemistry (2003) 75 (7), 1604-1614. PDMS-DVB 

Giardina, Matthew; Olesik, Susan V. 

The frequency of occurrence and discriminatory power of compounds 

2501 VOCs in hand found in human scent across a population determined by SPME-GC/MS headspace GC/MS 

odor samples J. CHROMATOGR. B, 846, #1-2, 86-97 (01 FEB 2007) 

Curran, A. M.; Ramirez, C. F.; Schoon, A. A.; Furton, K. G. 

2250 Volatile organic 

Comparison of the volatile organic compounds present in human 

odor using SPME-GC/MS headspace GC/MS 

in human odor Journal of Chemical Ecology 31 #7, 1607-1619 (2005) 





Curran, Allison M.; Rabin, Scott I.; Prada, Paola A.; Furton, K. 

A respiration-metabolism chamber system and a GC-MS method 

2271 Perfluorobutane for studying exhalation of perfluorobutane in rats after intravenous 75µm Carboxen GC-MS 

from exhaled air injection of the ultrasound contrast agent Sonazoid Headspace 

J Pharma Biomedical Analysis, 39, #3-4, 746-751 (2005) 

Uran, S.; Landmark, K.; Normann, P.; Hals, P.l Toft, K.;Skotland, T. 

Urine from stressed rats increases immobility in receptor rats 

2342 2-heptanone forced to swim: role of 2-heptanone headspace GC-MS 

from rat urine Physiol Behav 91, #1, 166-172 (2007 May 16) 

Gutioerrez-Garcoa, A; Contreras, C.; Mendoza-Loopez, M.; 

Garcoa-Barradas, O.; Cruz-Soanchez, J 

Metasternal gland volatiles and sexual communication in the 

2872 Pheromones triatomine bug, Rhodnius prolixus headspace GC-MS 

from triatomine Journal of Chemical Ecology 34, #4, 450-457 (APR 2008) 

bugs Pontes, Gina B.; Bohman, Bjorn; Unelius, C. Rikard; Lorenzo, Marcelo G. 

Male bugs modulate pheromone emission in response to vibratory signals from 

conspecifics. 

Pheromones from male 

1056 bugs. Journal of Chemical Ecology (2003) 29 (3), 561-574. 

Renou, Michel; Lasnier, Therese; Miklas, Nadege 


New developments and applications of solvent-free sampling and sample 

preparation technologies for the investigation of living systems 

Australian Journal of Chemistry (2003) 56 (2-3), 155-158. 

Pawliszyn, Janusz 

LC-MS 

1076 Organophosphorus 

pesticides in blood 

Simple determination of 22 organophosphorus pesticides in human blood using 

headspace solid-phase microextraction and gas chromatography with mass 

spectrometric detection. 

Journal of Chromatographic Science (2002) 40(1), 29-34 GC-MS 

Musshoff, F.; Junker, H.; Madea, B. 

Determination of phthalic monoesters in aqueous and urine samples by solidphase 

microextraction-diazomethane on-fibre derivatization-gas 

chromatography-mass spectrometry. 

Phthalic monoesters in 

1060 urine. Journal of Separation Science (2003) 26 (1-2), 87-96. PDMS-DVB GC-MS 

Alzaga, R.; Pena, A.; Bayona, J. M.* 25 C, 20 minutes, headspace 

1104 PAHs in urine. 

Determination of polycyclic aromatic hydrocarbons in urine of coke oven workers 

by headspace solid phase microextraction and gas chromatography-mass 

spectrometry. 

Chemico-Biological Interactions (2003) 145 (2), 165-174. 

Rappaport, Stephen M.; Waidyanatha, Suramya; Zheng, Yuxin 

GC-MS 

Rapid absorption of dietary 1,8-cineole results in critical blood 

2326 1,8-cineole concentration of cineole and immediate cessation of eating in the headspace GC/MS 

in blood common brushtail possum (Trichosurus vulpecula) 

J Chemical Ecology 31 #12, 2775-2790 (2005) 

Boyle, Rebecca R.; McLean, Stuart; Brandon, Sue; Wiggins, Natasha 

1158 1,8-cineole in blood 

Application of solid-phase microextraction to the quantitative analysis of 1,8cineole 

in blood and expired air in a Eucalyptus herbivore, the brushtail possum 

( Trichosurus vulpecula ). 

Journal of Chromatography, B: Analytical Technologies in the Biomedical and 

Life Sciences (2002) 780 (2), 397-406. GC 

Boyle, R. R.; McLean, S.; Brandon, S.; Pass, G. J.; Davies, N. W. 

Fatty acid ethyl esters in neonatal hair: A possible biomarker for in utero ethanol 

exposure. 

Fatty acid esters in 

1162 hair. Alcoholism Clinical and Experimental Research (2003) 27 (5 supp), 39A. 

Koren, G.; Klein, J.; Caprara, D. 

Headspace solid-phase microextraction (SPME) and gas chromatography-mass 

spectrometry (GC-MS) for the determination of 5alpha-androst-2-en-17-one and 

-17beta-ol in the female Asian elephant: Application for reproductive monitoring 

and prediction of parturition. 





Journal of Steroid Biochemistry and Molecular Biology (2003) 84 (2-3), 383- 


1163 Phermomens 391. GC-MS 

from female elephant Dehnhard, M.; Eulenberger, K.; Hatt, J.-M.; Ochs, A.; Strauss, G. 

Use of automated solid phase dynamic extraction (SPDE)/GC-MS 

2840 Pheromones and novel macros in the search for African elephant pheromones 

from African Chemical Signals in Vertebrates 11, 25-35 (2008) 

elephant Goodwin, T.; Brown, P.; Eggert, M.; Evola, M.; House, S.; 

Weddell, M.; Chen, C.; Jackson, S.; Aubut, Y.; Eggert, J. 

Schulte, B.; Rasmussen, L.; Morshedi, R.; 

Use of SPME, reverse phase SPE, and GC-MS in a search for African 

2259 Pheromones elephant urinary pheromones GC/MS 

from African Abstracts of Papers Am Chem Society 229 #1, U395 (2005) 

elephant Brown, P.; Eggert,M.; Evola,M.; Goodwin,T.; Rasmussen,L.,,Schulte,B. 

1205 Busulphan in plasma 

On-line derivatization utilizing solid-phase microextraction (SPME) for 

determination of busulphan in plasma using gas chromatography-mass 

spectrometry (GC-MS). 

Therapeutic Drug Monitoring (2003) 25 (3), 400-406. 

Abdel-Rehim, Mohamed; Blomberg, Lars; Hassan, Moustapha; Hassan, 

Zuzana 

Carbowax/DVB GC 

1207 

Midazolam in human 

plasma 

Determination of midazolam in human plasma by solid-phase microextraction 

and gas chromatography/mass spectrometry. 

Rapid Communications in Mass Spectrometry (2001) 15(24), 2497-2501 85um Polyacrylate GC-MS 

Davide Ferrara, Santo; Frison, Giampietro; Maietti, Sergio; Tedeschi, Luciano 

Use of SPME and GC-MS for chemical analysis of urine from African elephants 

in musth. 

1261 Elephant urine Abstracts of Papers American Chemical Society (2003) 225 (1-2), CHED 614. 

Hicks, Adam R.; Goodwin, Thomas E.; Dill, Whitney M.; Davis, Ben L.; Alberts, 

Susan C.; Hollister-Smith, Julie 

Monitoring potential semiochemicals in individual mouse urine samples 

2255 Sex pheromone Chemoecology 15 #3, 139-146 (2005) headspace GC/MS 

mouse urine Kayali-Sayadi, M. N.; Polo-Diez, L. M.; Salazar, I. 

Chemical analysis of preovulatory female African elephant urine: A search for 

putative pheromones. 

1262 Pheromones in urine. Abstracts of Papers American Chemical Society (2003) 225 (1-2), CHED 409. 

Hicks, Adam R.; Goodwin, Thomas E.; Dill, Whitney M.; Davis, Ben L.; Loizi, 

Helen; Rasmussen, L. E. L.; Schulte, Bruce A. 

Analysis of odours in human armpit by GC-MS with headspace solid-phase 


Odours in human 

1301 armpit. Fenxi Ceshi Xuebao (2003) 22 (4), 21-24. 

Wu, D. H.; Xu, H. K.; Wang, Z. P.; Zhang, L.; Wang, X. L.* 

70 um DVB/carbowax GC-MS 

1310 

Amitraz in canine 

plasma. 

Determination of amitraz in canine plasma by solid-phase microextraction-gas 

chromatography with thermionic specific detection 


Life Sciences (2003) 794 (2), 337-342. PDMS GC-TSD 

Carvalho, D.; Farias, A.; Lancas, F.M.; Queiroz, M.E.C.; Valadao, C.A.A. 

Application of solid-phase microextraction and gas chromatography-mass 

spectrometry to the determination of volatile organic compounds in end-exhaled 

breath samples. 

VOC's in exhaled 

1344 breath Journal of Chromatography, A (2003) 1011 (1-2), 125-134. 

Prado, C.; Marin, P.; Periago, J. F. 

GC-MS 


Mating disruption of codling moth Cydia pomonella with high densities 

of Ecodian sex pheromone dispensers field sampling 

from moths Journal of Applied Entomology 131, #5, 311-318 (JUN 2007) 





Angeli, G.; Anfora, G.; Baldessari, M.; Germinara, G. S.; Rama, F.; 

De Cristofaro, A.; Ioriatti, C 


Investigation by solid-phase microextraction and gas chromatography/mass 

spectrometry of trail pheromones in ants. 

1346 Pheromones in ants. Rapid Communications in Mass Spectrometry (2003) 17 (18), 2071-2074. GC-MS 

di Tullio, A.; de Angelis, F. *; Reale, S.; Grasso, D. A.; Visicchio, R.; Castracani, 

C.; , A.; le Moli, F. 

1359 Volatile aldehydes 

SPME determination of volatile aldehydes for evaluation of in-vitro antioxidant 

activity. 

Analytical and Bioanalytical Chemistry (2002) 373(1-2), 70-74. 

Stashenko, E. E.; Puertas, M. A.; Martinez, J. R. 

GC-MS 

1360 VOCs in body fluids 

Cryogenic oven-trapping gas chromatography for analysis of volatile organic 

compounds in body fluids. 


Watanabe-Suzuki, K.; Ishii, A.; Suzuki, O. 

GC-MS 

1365 

Solid-phase microextraction for the detection of termite cuticular hydrocarbons. 

Hydrocarbons in 

cuticles Journal of Chromatography, A (2001) 932(1-2), 119-127. GC-MS 

Bland, J. M.; Osbrink, W. L. A.; Cornelius, M. L.; Lax, A. R.; Vigo, C. B. 

Solid-phase microextraction and GC-MS analysis of p, p' -DDE in biological 

samples. 

p,p'-DDE in biological 

1375 samples Journal of Chromatography, B: Biomedical Applications (2001) 761(1), 93-98. PDMS 

Kusakabe, T.; Saito, T. *; Takeichi, S. 

GC-MS 

Detection of perfluorocarbons in blood by headspace solid-phase 

microextraction combined with gas chromatography-mass spectrometry. 

Perfluorocarbons in 

1380 blood. Biomedical Chromatography (2001) 15(7), 443-451. 

Mathurin, J. -C.; de Ceaurriz, J.; Audran, M.; Krafft, M. -P. 

GC-MS 

Determination of ropivacaine and its metabolites in human plasma using solid 

phase microextraction and GC-NPD/GC-MS. 

1396 Ropivacaine in plasma Journal of Microcolumn Separations (2001) 13(8), 313-321. Various Gc-MS 

Abdel-Rehim, M.; Andersson, M.; Portelius, E.; Norsten-Hoog, C.; Blomberg, L. 

G. 

Effect of thickeners on aroma compound behavior in a model dairy gel 

2729 Volatiles from J Agri Food Chem 55, #12, 4835-4841 (JUN 13 2007) headspace GC-MS 

dairy gel Lubbers, S; Decourcelle, N.; Martinez, D.; Guichard, E.; Tromelin, A. 


Study on the Influence of Pasture on Volatile Fraction of Ewes' Dairy 

Products by SPME-GC-MS headspace GC-MS 

milk, cheese J. Dairy Sci. 90, # 2, 556-569 (2007-02-00) 

Povolo, M.; Contarini, G.; Mele, M.; Secchiari, P. 

SPME-GC-MS analysis of dairy product volatiles for the 

2883 Volatiles from determination of shelf-life headspace GC-MS 

milk Int. Dairy J. 18, #8, 819-825 (August 2008) 

Condurso, C.; Conte, F.; Romeo, V.; Verzera, A.; Ziino, M. 

Characterization of volatile compounds in ultra-high- 

2882 Volatiles from pressure homogenized milk headspace GC-MS 

milk Int. Dairy J. 18, #8, 828-834 (August 2008) 

Ferragut, V.; Guamis, B.; Jaramillo, D.P.; Pereda, J.; 

Quevedo, J.M.; Trujillo, A.J. 


Identification of volatile compounds in soymilk using SPME-GC 

Food Chem. 99, #4, 759-766 (2006-07-07) 75µm Carboxen. GC 

soymilk Achouri, A.; Boye, J. I.; Zamani, Y. 

Selected odor compounds in cooked soymilk as affected by 

20 min @ 40°C 

headspace 

2490 Volatiles from soybean materials and direct steam injection headspace GC-MS 





soymilk J of Food Science 72, #7, S481-S486 (SEP 2007) 

Yuan, S. H.; Chang, S. K. C. 

Quantification of naltrexone and 6,beta-naltrexol in plasma and milk using gas 

chromatography-mass spectrometry. Application to studies in the lactating 

sheep. 

Naltrexone, 6,beta- 

1413 naltrexol Journal of Chromatography B (2001) 761(1), 85-92. 

Ilett, Kenneth F.; Bencini, Roberta; Chan, Chooi Fen; Chiswell, Gregory M.; 

GC-MS 

in milk 

Dusci, Leon J.; Hackett, L. Peter 

Monitoring and fast detection of mycotoxin-producing fungi based on 

headspace solid-phase microextraction and headspace sorptive extraction of 

the volatile metabolites. 

1225 Journal of Chromatography, A (2003) 985 (1-2), 127-135. GC-MS 

Demyttenaere, J. C. R.; Morina, R. M.; Sandra, P. 

1159 Phthalates from toys 

Determination of bis(2-ethylhexyl) phthalate of plastic toys leached in stimulant 

saliva by gas chromatography with solid-phase microextraction 


Yang, Z. J.; Zhang, W. Y.; Pan, K. Y.; Yu, J. X.; Wu, C. Y.; Wang, C. Y. 

PDMS-fullerene GC 

1210 

Volatile fatty acids in 

rumen. 

Characterizing volatile fatty acids and other gases in a rumen closed in vitro 

fermentation system using solid phase microextraction 

Transactions of the American Society of Agricultural Engineers (2003) 46 (2), 

585-588. 

Chirase, Norbert K.; Koziel, Jacek A.; Spinhirne, Jarett P. 

DVB/Carboxen/PDMS GC-MS 

2798 Crude oil 

A comparison of results obtained using liquid injection and 

headspace SPME for crude oil analysis by GC-MS 

J of Chrom Sci. 46, #4, 332-338 (APR 2008) 

D'Auria, Maurizio; Racioppi, Rocco; Velluzzi, Vincenzina 


Volatile hydrocarbon biodegradation by a mixed-bacterial culture during growth 

on crude oil. 

1412 Volatile hydrocarbons Journal of Industrial Microbiology & Biotechnology (2001) 26(6), 356-362. 

Van Hamme, J. D.; Ward, O. P 

1311 

Production of flavoured volatile organic compounds (VOCs) by Candida 

oleophila GK10: Optimisation using factorial design and response surface 

analysis 

Enzyme and Microbial Technology (2003) 33 (5), 668-675. 

Buzzini, Pietro; Davoli, Paolo; Martini, Alessandro; Pagnoni, Ugo Maria 

GC-MS 

2791 Bromocyclen 

Enantioselective determination of the organochlorine pesticide 

bromocyclen in spiked fish tissue using SPME-GC-ECD and ICP-MS 

GC-ECD 

in fish tissue Talanta 75, #3, 710-716 (May 15 2008) ICP-MS 


pesticides in fish 

1456 

1468 

Pheremones in mouse 

urine 

Sufentanil in human 

plasma 

Blanco-Gonzalez, E.; Fidalgo-Used, N.; Montes-Bayon, M.; Sanz-Medel, A 

Solid-phase microextraction as a clean-up and preconcentration procedure for 

organochlorine pesticides determination in fish tissue by gas chromatography 

with electron capture detection 

Journal of Chromatography A (2003) 1017(1-2), 35-44 GC-ECD 

Blanco-Gonzalez, Elisa; Centineo, Giuseppe; Fidalgo-Used, Natalia; Sanz- 

Medel, Alfredo 

Identification of pheromones in mouse urine by head-space solid phase 

microextraction followed by gas chromatography-mass spectrometry. 

Journal of Chromatography B (2003) 796(1), 55-62 85um Carboxen PDMS GC-MS 

Kayali-Sayadi, M. N.; Bautista, Jose M.; Polo-Diez, L. M.; Salazar, Ignacio 

Solid-phase microextraction of human plasma samples for determination of 

sufentanil by gas chromatography-mass spectrometry. 

Therapeutic Drug Monitoring (2002) 24(6), 768-774 


65um PDMS DVB, 

10mins, immersion 

GC-MS

1485 

1487 

1503 

1506 




Boulieu, Roselyne; Bolon, Magali; Dufresne, Christelle; Paradis, Chantal 


Volatiles in live 

biological samples 

Pheremones from 

Lepidoptera 

Organic compounds in 

elephant urine 

C9-C20 hydrocarbons 

in shellfish 

Applications of solid-phase microextraction to chemical analysis of live biologica 

samples. 

Trends in Analytical Chemistry (2002) 21(6-7), 428-438 

Augusto, Fabio; Valente, Antonio Luiz Pires 

Lepidoptera (Sesamia nonagrioides (Lefebvre) (Lepidoptera Noctuidae)) by 

solid-phase microextraction 

Redia (2001) 84, 7-18 

Rotundo, Giuseppe; Germinara, Giacinto Salvatore; De Cristofaro, Antonio 

Implementation of SPME and GC-MS to identify organic compounds in African 

elephant urine. 

Abstracts of Papers American Chemical Society (2002) 223(1-2), CHED 234 

dwin, Thomas E.; Dowdy, Nichole C.; Rasmussen, L. E. L. 

Determination of petroleum contamination in shellfish using solid phase microextraction 

with gas chromatography-mass spectrometry. 

100µm PDMS, 20mins, 

120 degrees C, 

headspace 

GC-MS 

Analytical and Bioanalytical Chemistry (2002) 373(3), 147-152 100um PDMS GC-MS 

Stack, Mary A.; James, Kevin J.; O'Connell, Sharon 

Systemic availability and pharmacokinetics of thymol in humans. 

1519 Thymol in humans Journal of Clinical Pharmacology (2002) 42(7) 731-737 LC-MS-MS 

Veit, Markus; Abel, Gudrun; Brinkhaus, Benno; Derendorf, Hartmut; Graefe, 

Eva-Ulrike; Kohlert, Claudia; Maerz, Reinhard W.; Schindler, Gernot 


Quantification of 31 volatile organic compounds in whole 

blood using SPME-GC-MS headspace GC-MS 

in blood J. Chromatogr. B Anal. 832, #2, 292-301 (2006) 

Ashley, D.; Blount, B.; Cardinali, F.; Chambers, D.;Kobelski, R.; 

McElprang, David O.; Morrow, John C. 

Optimization of solid-phase microextraction conditions for gas chromatographic 

determination of ethanol and other volatile compounds in blood. 

1529 Ethanol in blood Journal of Chromatography B (2002) 773(1), 75-82 

Zuba, Dariusz; Parczewski, Andrzej; Reichenbacher, Manfred 

65um Carbowax DVB, 

60 degrees C, 10mins, 

stirring, NaCl addtion, 

headspace 

GC-FID 

2361 Hydroxychloro- 

Stereoselective determination of hydroxychloro-quine and its major . 

metabolites in human urine by SPMEand HPLC 60µm PDMS-DVB HPLC 

quine metabolites J. Sep Sci 3, #15, 2351-2359 (Oct-2007) 40 min at 25°C 

in human urine Moraes del Oliveira, A/; Sueli Bonato, P. 

Determination of naproxen in human urine by SPME coupled LC 

pH 11 

10% NaCl 

2272 Naproxen J Pharma Biomedical Analysis, 39, #3-4, 643-647 (2005) 50µm CW/TPR LC 

in human urine Aresta, Antonella; Palmisano, Francesco; Zambonin, Carlo G. 

1532 

Quantitation of 2-chlorovinylarsonous acid in human urine by automated solidphase 

microextraction-gas chromatography-mass spectrometry. 

2-chlorovinylarsonous 

acid in human urine 

Journal of Chromatography B (2002) 772(1), 147-153 

Calafat, Antonia M.; Ashley, David L.; Wooten, Joe V. 

GC-MS 

1533 

Fluoroacetic acid in 

biological samples 

Headspace solid-phase microextraction with 1-pyrenyldiazomethane on-fibre 

derivatization for analysis of fluoroacetic acid in biological samples. 

Journal of Chromatography B (2002) 772(1), 45-51 


85um Carboxen PDMS 

Stableflex, on-fiber 

derivatization with 

1-pyrenyldiazomethane

1540 




Pragst, Fritz; Huebner, Sandra; Mills, Graham; Sporkert, Frank 


carbamazepine, 

carbamazepine 

epoxide, phenytoin, 

phenobarbital, and 

primidone in human 

plasma 

Determination of lamotrigine simultaneously with carbamazepine, 

carbamazepine epoxide, phenytoin, phenobarbital, and primidone in human 

plasma by SPME-GC-TSD. 


Lancas, F. M.; Carvalho, D.; Queiroz, M. E. C.; Silva, S. M. 

1427 Microcystins 

Determination of microcystins in cyanobacterial blooms by solid-phase 

microextraction : High-performance liquid chromatography. 

Environmental Toxicology and Chemistry (2001) 20(8), 1648-1655. HPLC 

Lam, Michael Hon-wah; Lam, Paul K. S.; Poon, Ka-Fai; Wong, Bryan S. F. 

New trends in hair analysis and scientific demands on validation 

2597 Review of Trends and technical notes 

forensic analysis Forensic Sci Intl 165, #2-3, 204-215 (JAN 17 2007) 

Musshoff, Frank; Madea, Burkhard 

Simple and sensitive determination of tetrahydrocannabinol, cannabidiol 

2516 Cannabinols and cannabinol in hair by combined silylation, headspace SPME-GC-MS Headspace GC-MS 

in hair J. CHROMATOGR. B 846, #1-2, 78-85 (01 FEB 2007) trifluoroacetamide 

Nadulski, T.; Pragst, F derivative 

Rapid screening procedure based on headspace 

1828 Drugs in SPME-GC-MS for the detection of many Headspace, GC-MS 

hair recreational drugs in hair. 5min @ 90°C 

J. Chromatogr. B, 801, #2, 289-296 

Gentili, S.; Cornetta, M.; Macchia, T. * 

Determination of methyl and ethyl esters of methanesulfonic, 

2273 Sulfonic acids benzenesulfonic and p-toluenesulfonic acids in active pharmaceutical GC-MS 

esters in ingredients by solid-phase microextraction 

pharmaceutical J Pharma Biomedical Analysis, 39, #3-4, 477-485 (2005) 

ingredients Colon, Ivelisse; Richoll, Stephen M. 

Optimisation of a SPME method for the determination of parabens in 

2709 Parabens in water samples at the low ng per litre level 85µm polyacrylate GC-MS/MS 

water J. Chromatogr. A, 1124, #1-2, 3-10 (2006-08-18) immersed 

Canosa, P.; Rodriguez, I. ; Rubi, E.; Bollain, M. H.; Cela, R. TBMS derivative 

sat. salt 

Determination of parabens in pharmaceutical formulations by 

1829 Parabens in SPME ion-mobility spectrometry GC-IMS 

pharmaceutics Anal. Chem., 77, #18, 5938-5946 

Lokhnauth, John; Snow, Nicholas 

Simultaneous derivatization and extraction of amphetamine-like 

1830 Amphetamine drugs in urine with headspace SPME followed by GC-MS 100µm PDMS GC-MS 

drugs in Anal. Chim. Acta, 539, #1-2, 49-54 30min @ 90°C 

urine Chia, Kan-Jung; Huang, Shang-Da HFBA derivative 

headspace 

Poly(methacrylic acid-ethylene glycol dimethacrylate) 

1831 Amphetamine monolith in-tube SPME coupled to HPLC and analysis of polycrylate coated HPLC-UV 

drugs in amphetamines in urine samples capillary tube 

urine J. Chromatogr. A, 1074, #1-2, 9-16 

Da, Shi-Lu; Fan, Yi; Feng, Yu-Qi; Zhang, J; Zhang, M 

Application of SPME combined with derivatization to 

1832 Amphetamine the determination of amphetamines by liquid chromatog 50µm CW-TPR HPLC-UV 

drugs in Analytical Biochemistry, 333, #2, 328-335 FMOC derivative 

urine Chafer-Pericas, C.; Campins-Falco, P.; Herraez-Hernandez, R. 

1833 Amphetamine 

Enantiomeric determination of amphetamines: Exploring 

A novel one-step SPME-based approach 100µm PDMS GC-SIM-MS 

drugs in J. Chromatogr. B, 825, #1, 79-87 10min @ 70°C 

urine Wang, Sheng-Meng 

SPME with LC-electrospray ionization-tandem MS 

prolyl chloride 

derivative 

1834 Amphetamine for analysis of amphetamine and methamphetamine in serum LC-ESI-MS/MS 





in serum Anal. Chim. Acta, 538, #1-2, 49-56 

Chou, Chi-Chi; Lee, Maw-Rong 

Comparison and classification of methamphetamine seized in Japan 

2800 Methyl and Thailand using GC with liquid-liquid extraction and SPME GC-FID 

amphetamine Forensic Science International 175, #2-3, 85-92 (MAR 5 2008) 

Kuwayama, K.; Inoue, H.; Phorachata, J.; Kongpatnitiroj, K.; 

Puthaviriyakorn, V.; Tsujikawa, K.; Miyaguchi, H.; Kanamori, T.; 

Iwata, Yuko T.;Kamo, Naoki; Kishi, Tohru 

Excretion of unchanged volatile organic compounds (toluene, 

2836 Volatile organics ethylbenzene, xylene and mesitylene) in urine as result of headspace GC 

in human urine experimental human volunteer exposure 

Intl Archives of Occupational Environ. Health 81, #4, 443-449 (2008) 

Janasik, Beata; Jakubowski, Marek; Jalowiecki, Piotr 

Quantitative analysis of benzene, toluene, 

1835 BTX solvents and xylenes in urine by headspace SPME headspace GC-MS 

in urine J Chromatogr A, 1027, #1-2, 37-40 

Alkalde, T; Peralba, M; Zini, C; Caramao, E. 

SPME w/ on-fiber derivatization for the determination of 

1836 PCB metabolite hydroxy-polychlorinated biphenyl compounds in urine 65µm PDMS-DVB GC/MS 

in urine Anal. Chim. Acta, 539, #1-2 55-60 60min @ 90°C 

Hong, Jee Eun; Lee, Won; Park, Song-Ja; Pyo, Heesoo BSTFA derivative 

headspace 

Single drop microextraction or SPME-GC-MS 

1837 Iodine in for the determination of iodine in pharmaceuticals, iodate derivatives GC 

various iodized salt, mil powder and vegetables 

matrices involving conversion into 4-iodo-N,N-dimethylaniline 

J Chromatogr A, 1023, #1, 33-39 

Das, P; Gupta, M; Jain, A; Verma, K. 

Determination of quinalphos in blood and urine by direct SPME 

2315 Quinalphos in combined with GC-MS 100µm PDMS GC/MS 

blood J. Chromatogr. B 832 #1, 162-168 (2006) direct 

Barroso, M.; Cruz, A.; Gallardo, E.; Lopez-Rivadulla, M.; 

Margalho, C.; Vieira, D.N 

Investigations on the medico-legal relevance of spirits containing 

2290 Thujone thujone with special regard to toxicological-analytical aspects headspace GC/MS 

in blood Blutalkohol 42 #4, 263-271 (2005) (German) 

Kroner, L.; Padosch, S.; Lachenmeier, D.; Madea, B. 

Monitoring of drugs and metabolites in whole blood 

1838 Diazipenes in by restricted-access SPME coupled to LC-MS restricted access LC-MS 

biological fluid J Chromatogr A, 1025, #1, 85-92 coated fibers 

Walles, M.; Mullett, W. M.; Pawliszyn, J. headspace 

An accurate and sensitive method for determination 

1839 Methyl methylmercury in biological specimens 100µm PDMS ICP-MS 

mercury from using GC-ICP-MS with solid phase microextraction methyl, ethyl, phenyl 

biological J Anal At Spectrom, 19, #12, 1546-1551 derivatives 

specimens Christopher, S.J.; Davis, W. Clay; Day, Rusty D.; microwave extraction 

Long, S.E.; Schantz, Michele M.; Vander Pol, Stacy S. 

Sampling and analysis of volatile organic compounds 

1840 Volatiles in in bovine breath by SPME-GC-MS 50/30µm DVB/CAR GC-MS 

bovine breath J Chromatogr A, 1025, #1, 63-69 15min @ 22°C 

Spinhirne, J.; Koziel, J.; Chirase, N. headspace 

High-throughput analysis of phthalate esters in 

1841 Phlated esters human serum by direct immersion SPME followed 85µm polyacrylate GC-MS 

in serum by isotope dilution-fast GC/MS direct immersion 

Anal. Bioanal. Chem., 380,#2, 275-283 

Colon, Ivelisse; Dimandja, Jean-Marie D. 

Development of pressurized hot water extraction 

1842 Ligustilides followed by headspace SPME-GC-MS determination headspace GC-MS 

in Chinese ligustilides in Ligusticum chuanxiong and Angelica sinensis 

medicines J. Sep. Sci., 28, #11, 1237-1243 

Deng, Chunhui; Ji, Jie; Wang, Xiaochuan; Zhang, X 

1843 Benzene 

Urinary benzene determination by SPME/GC-MS: 

A study of variables by fractional factoria 1 min @ 15°C GC-MS 

from urine design and response surface methodology headspace 





J. Chromatogr. B, 804, #2, 255-261 

Garrido, J.; Periago, J.F.; Prado, C. 

Rapid measurement of C13-enrichment of acetic, propionic 

1844 Faty Acids in and butyric acids in plasma with SPME coupled to GC-MS 75µm Carboxen GC-MS 

plasma Anal. Chim. Acta, 512, #2, 305-310 5min extract 

Champ, M.; Delepee, R.; Dumon, H.; LeBizec, B.; headspace 

Martin, L.; Maume, D.; Moreau, N.; Nguyen,P 

cDNA isolation and functional expression of myrcene 

1845 Monoterpenes synthase from Perilla frutescens GC 

from Perilla Biological & Pharmaceutical Bulletin, 27, #12, 1979-1985 

frutescens Hosoi, Madoka; Ito, Michiho; Yagura, Toru; 

Adams, Robert Phillip; Honda, Gisho 

Determination of acetone in seawater using derivatization SPME 

2735 Acetone in Anal. Bioanal. Chem., 388, #5-6, 1272-1282 (2007-07) headspace GC-MS 

seawater Hudson, E. D.; Okuda, K.; Ariya, P. A. 


Rapid determination of acetone in human plasma 

1846 Acetone in by GC-MS and SPME with on-fiber derivatization 65µm PDMS-DVB GC-MS 

plasma J. Chromatogr. B, 805, #2, 235-240 PFBHA derivative 

Deng, Chunhui; Zhang, Jie; Zhang, Wei; Zhang, Xiangmin 

Rapid determination of amino acids in neonatal blood 

1847 Amino acids samples based on derivatization with isobutyl headspace GC-MS 

in blood chloroformated followed by SPME-GC-MS chloroformate 

Rapid Communications in Mass Spec, 18, #21, 2558-2564 derivative 

Deng, C. H.; Li, N.; Zhang, X. M.* 

Quantifying trimethylamine and trimethylamine- N -oxide 

1848 Trimethylamine in human plasma: interference from endogenous quaternary GC 

in plasma endogenous quaternary ammonium compounds. 

Analytical Biochemistry, 334, #2, 403-405 

Bain, M. A.; Faull, R.; Fornasini, G.; Milne, R. W.; 

Schumann, R.; Evans, A. M. 

Fast assay of angiotensin 1 from whole blood by 

1849 Anigotensin cation-exchange restricted-access SPME alkyl diol silica coating HPLC 

from blood Anal. Chim. Acta, 537, #1-2, 231-237 immersed sampling LC-MS 

Musteata, F.; Pawliszyn, Janusz; Walles, M. 

Comparison of the concentration of fatty acid ethyl esters in hair 

2287 Fatty acid and phosphatidyl ethanol in blood of alcoholics with other Headspace GC 

ethyl esters biological state markers and self reported ethanol intake Ethyl ester 

in hair Alcoholism Clinical and Experimental Res 28 #5, 158A (2004) derivatives 

Wurst, F.; Alling, C.; Aradottir, S; Alexson, S; Wolfersdorf, M.; 

Jachau, K.; Huber, P.; Auwaerter, V.; Allen, J.; Pragst, F. 

Concentration of fatty acid ethyl esters in hair of 

1850 Fatty acid alcoholics: Comparison to other biologica Headspace GC-MS 

ethyl esters state markers and self reported-ethanol intake. Ethyl ester derivatives 

in hair Alcohol and Alcoholism, 39, #1, 33-38 

Wurst, F.; Alexson, S.; Wolfersdorf, M.; Bechtel, G; 

Forster, S.' Alling.C.; Aradottir, S.; Jachau, K.; Huber, P.; 

Allen, J.; Auwaerter, V.; Pragst, F. 

Comparison of ethyl glucuronide and fatty acid ethyl ester 

1851 Fatty acid concentrations in hair of alcoholics, social drinkers, Headspace GC-MS/NCI 

ethyl esters and teetotallers Ethyl ester derivatives 

in hair Forensic Science Intl,145, #2-3, 167-173 

Yegles, M.; Labarthe, A.; Auwarter, V.; Hartwig, S.; Vater, H.; 

Wennig, R.; Pragst, F. 

SPME with on-fiber derivatization for the analysis 

1852 Anti- of anti-inflammatory drugs in water samples. 85µm polyacrylate GC-MS 

inflamatory J Chromatogr A, 1024, #1-2, 1-8 MTBSTFA derivative 

drugs in Rodriguez, I.; Carpinteiro, J.; Quintana, J. B.; . Headspace 

water Carro, A. M.; Lorenzo, R. A.; Cela, R 

Application of SPME-GC-MS in analysis of poison 

1853 Fluoroacet- Zhipu Xuebao, 25, Suppl, 151-152 LC-MS 

amide in body Cai, X. L.; Wu, G. P. 

fluids 

Fast detection of fluoroacetamide in body fluid 





1854 Fluoroacet- using GC-MS after SPME. 100µm PDMS GC-MS 

amide in body J Chromatogr, B:802, #2, 239-245 25min @ 70°C 

fluids Cai, X.; Zhang, D.; Ju, H. X.; Wu, G.; Liu, X. immersed 

Sensitive methods for trace level analysis of 

1855 Trichloro- trichloroethylene (TCE) in rat blood and tissues. headspace @ 55°C GC-MS 

ethylene in Proc. 50th ASMS Conf. Mass Spectrom. Allied Top. 

blood/tissues 2002, p629-630 

Bartlett, Michael G.; Brown, Stacy D.; Bruckner, James V.; 

Dixon, Amy M.; Muralidhara, S. 

Photocatalytic oxidation of aqueous trichloroethylene using dye 

2916 Trichloro- sensitized buoyant photocatalyst monitored via micro-headspace 100µm PDMS GC/ECD 

ethylene in SPME-GC-ECD and MS headspace 

water Microchemical Journal 88, #1, 38-44 (FEB 2008) 

Alexander, Matt V.; Rosentreter, Jeffrey J. 

Trace level determination of trichloroethylene in biological samples 

2794 Trichloro- by headspace SPME-GC/negative chemical ionization MS 100µm PDMS GC-MS 

ethylene in Rapid Communications in Mass Spectrometry 22, #6 797-806 (2008) headspace 

biological samples Liu, Yongzhen; Muralidhara, S.; Bruckner, James V.; Bartlett, M. 

Determination of trichloroethylene in biological samples by headspace 

2770 Trichloro- SPME-GC-MS 100µm PDMS GC-MS 

ethylene in J Chromatogr, B: 863, #1, 26-35 (2008) headspace 

biological samples Liu, Yongzhen; Muralidhara, S.; Bruckner, James V.; Bartlett, M. 

A study of the performance characteristics of immunoaffinity SPME 

2457 Benzodiaze- probes for extraction of a range of benzodiazepines. 

pines in J. Pharm. Biomed. Anal. 44, #2, 506-519 (2007-06-28) 

blood Lord, H. L.; Rajabi, M.; Safari, S.; Pawliszyn, J. 

Analysis of benzodiazepines from whole blood 

1856 Benzodiaze- by SPME coupled to LC-MS-MS 50µm CW-TPR LC-MS-MS 

pines in Proc. 50th ASMS Conf. Mass Spectrom. Allied Top. 

whole blood 2002, p513-514 

Grant, R; Incledon, B; Lord, H; Pawliszyn, Janusz 

Application of the standard addition approach for the 

1857 Benzene in quantification of urinary benzene headsapce GC-MS 

urine J. Chromatogr. B, 818, #2, 293-299 

Acampora, A.; Basilicata, P.; Miraglia, N; 

Pieri, M.; Sannolo, N.; Soleo, L. 

Determination of urinary ortho- and meta-cresol in 

1858 Cresols in humans by headspace SPME-GC-MS 100µm PDMS GC-MS 

urine J. Chromatogr. B, 817, #2, 309-317 headsapce 

Campo, L.; Foa, V.; Fustinoni, S.; Mercadante, R.; 

Scibetta, L.; Valla, C. 

SPME and chiral HPLC analysis of ibuprofen in urine 

1859 Ibuprofen J. Chromatogr.B, 818, #2, 285-291 65µm PDMS- DVB HPLC-UV 

in urine Bonato, P.; Cesarino, E.; De Oliveira, A. immersion sampling 

Stereoselective determination of the major ibuprofen 

1860 Ibuprofen metabolites in human usrine by off-linecoupling SPME-HPLC 50µm CW-TPR HPLC 

metabolites Anal. Chim. Acta, 538, #1, 25-34 immersion sampling 

in urine De Oliveira, A;, DeSantana, Fo; Bonato, P 

Simultaneous determination of barbiturates in human 

1861 Barbiturates biological fluids by direct immersion SPME and GC-MS immersion sampling GC-MS 

in blood/urine J. Chromatogr. B, 806, #1, 65-73 salt added 

Arinobu, T.; Hattori, H.; Ishii, A.; Iwai, M.; Suzuki, O.; 

Kumazawa, T., Noguchi, H., Noguchi, H.; Seno, H. 

Monitoring of urinary acrolein concentration in 

1862 Acrolein in patients receiving cyclophosphamide and ifosphamide headsapce GC-MS 

urine J. Chromatogr. B, 806, #1, 59-63 

Namera, A.; Sakura, N.; Takamoto, S.; Yashiki, M. 

Headspace SPME and capillary GC-MS determination 

1863 Rivastigmine of rivastigmine in canine plasma samples 65µm PDMS/DVB GC-MS 

in plasma J. Chromatogr. B, 806, #2, 271-276 30min @ 100°C 

Deng, Chunhui; Duan, Gengli; Huang, Taomin; Liu, Zhen; headspace 

Sha, Yunfei; Yang, Bei NaOH/NaCO 3 buffer 





Determination of the immunosuppressant mycophenolic 

1864 Mycophnolic acid in human seum by SPME coupled to LC 50µm CW-TPR HPLC-UV 

acid in serum J. Chromatogr. B, 806, #2, 89-93 headspace 

Aresta, A; Palmisano, F; Zambonin, C 

Fuzzy rule-building expert system classification of fuel using 

2660 Neat Fuels SPME in two-way GC differential mobility spectrometric data headspace GC-DMS 

Anal. Chem. 79, #4, 1485-1491 (Feb 15 2007) 

Bunker, C.; Harrington, Peter B.; Karnes, John J.; Rearden, P. 

Determination of JP-8 components in soils using SPME-GC-MS 

2910 JP-8 fuel from Fuel 87, #10-11, 2334-2338 (August 2008) headspace GC-MS 

soil Brown, Stacy; Caldwell, Thomas; Rickrode, Mark 

A PBPK modeling assessment of the competitive metabolic interactions 

2379 JP-8 fuel from of JP-8 vapor with two constituents, m-xylene and ethylbenzene headspace GC-MS 

rat tissue INHAL. TOXICOL. 19, #3, 265-273 ( MAR 2007) 

Campbell, Jr J. L.; Fisher, J. W. 

Dose related absorption of JP-8 jet fuel 

1865 JP-8 fuel on hydrocarbons through porcine skin w/ quantitative GC-FID 

porcine skin structure permeability relationship analysis 

Toxic Mechanisms & Methods 14, #3, 159-166 

Muhammad, F.; Baynes, R.; Monteiro-Riviere, N.; 

Xia, X.; Riviere, J. 

GC-MS analysis of volatile compounds from 

1866 Volatiles in Houttuynia cor-data Thunb after extraction by SPME, 100µm PDMS GC-MS 

Houttuynia flash evaporation and steam distillation headspace 

cordata thunb Analytica Chimica Acta, 531, #1,07-104 

Liang, M; Qi, M; Zhang, C; Zhou, S; Fu, R; Huang, J 

Rapid screening of selective serotonin re-uptake 

1867 Serotonin inhibitors in urine samples using SPME-GC-MS 65µm PDMS-DVB GC-MS 

in urine Anal. Bioanal. Chem., 382, #6, 1351-1359 in-situ derivatization 

Cela, R.; Garcia-Jares, Carmen; Lamas, J.; 30min analysis 

Llompart, M.; Salgado-Petinal, C. 

Determination of dichloromethane, trichloroethylene and 

1868 Chlorinated perchloroethylene in urine samples by HD-SPME-GC-MS 75µm Carboxen GC-MS 

hydrocarbons J. Chromatogr. B, 820, #1, 95-102 22°C, saturated salt 

in urine Andreoli, R; Franchini, I; Manini, P; Mutti, A; Poli, D headspace 

agitated 

SPME-GC analysis of organophosphorus pesticides 

1869 Organo- in biological samples headspace GC-NPD 

phosphorus J. Chromatogr. B,822, #1-2, 194-200 

pesticides in Grigoratou, I; Raikos, N; Theodoridis, G; Tsoukali, H 

blood, urine 

Rapid determination of tramadol in human plasma by 

1870 Tramadol headspace SPME and capillary GC-MS 65µm PDMS-DVB GC/MS 

in plasma J Pharma and Biomed Analysis, 37, #1, 143-147 30min @ 100°C 

Sha, Y. F.; Shen, S.; Duan, G. L. 0.1 M NaOH 

headspace 

Lung cancer diagnosis method by detecting metabolic gases 

2779 Lung Cancer of lung cells headspace GC 

Biomakers Zhejiang Daxue Xuebao 42, #2, 294-298+348 (Feb 2008) 

in breath Cao, Ming-Fu; Chen, Xing; Hao, Yan; Wang, Ping; Wang, Yong-Qing; 

Wang, Yue; Xu, Feng-Juan; Zhang, Wei-Min 

Identification of volatile organic compounds secreted from cancer 

2911 Volatile organics tissues and bacterial cultures headspace GC/MS 

from stomach J. Chromatogr. B, 868, #1-2, 88-94 (Jun 1 2008) 

tissue Buszewski, B.; Jackowski, M.; Klodzinska, E.; Ligor, T.; Szeliga, J. 

Ulanowska, A. 

Investigation of volatile biomarkers in liver cancer blood using 

2881 Cancer SPME-GC-MS headspace GC/MS 

Biomakers Rapid Comm Mass Spectrometry 22, #8, 1181-1186 (APR 2008) 

in liver cancer Xue, Ruyi; Dong, Ling; Zhang, Si; Deng, Chunhui; Liu, Taotao; 

Wang, Jiyao; Shen, Xizhong 

2350 Cancer 

A study of the volatile organic compounds exhaled by lung cancer 

cells in vitro for breath diagnosis headspace GC 

Biomakers Cancer 110, #4, 835-44 (2007 Aug 15) 

in breath Chen, X.; Xu, F.; Wang, Y.; Pan, Y.; Lu, D.; Wang, P.; Ying, K.; 





Chen, E.; Zhang, W 

Investigation of volatile biomarkers in lung cancer 

1871 Cancer blood using SPME and capillary GC-MS headspace GC/MS 

Biomakers J. Chromatogr. B, 808, #2, 269-277 

in blood Deng, Chunhui; Li, Ning; Zhang, Xiangmin 

A study of an electronic nose for detection of lung 

1872 Cancer cancer based on a virtual SAW gas sensorsarray headspace GC/MS 

Biomakers and imaging recognition method 

in blood Meas. Sci. Technol., 16, #8, 1535-1546 

Cao, M.; Chen, X.; Hu, W.; Li, Yi.; 

Pan, H.; Wang, P.; Ying, K. 

2146 Dinitrotoluenes 

Solid phase microextraction of aminodinitrotoluenes in tissue 

Chemosphere, 63. #1, 58-63 (Feb 2008) 85µm Polyacrylate GC 

in tissue Bowen, Alethea T.; Conder, Jason M.; La Point, Thomas W. immersed 

agitated 

In situ derivatization/SPME-GC negative CI-MS for the determination 

2883 Trichloro- of trichloroethylene metabolites in rat blood headspace GC/CI-MS 

ethylene in Rapid Communications in Mass Spectrometry 22, #7, 1021-1031 (2008) ethyl esters 

rat blood Liu, Y.; Muraildhara, Srinivasa; Bruckner, James V.; Bartlett, M. 

Optimization of SPME for analysis of trichloroethylene in rat 

1873 Trichloro- blood and tissues by SPME-GC/MS headspace GC/MS 

ethylene in Instrum Sci Technol, 33, #2, 175-186 5 min 

rat blood Bartlett, M.; Brown, S.; Bruckner, J.; Dixon, A.; 

Muralidhara, S. 

Rapid measurement of 13 C-enrichment of acetic, 

1874 Fatty propionic, and butyric acids in plasma w/ SPME 75µm Carboxen GC-MS 

acids in coupled to GC-MS 5 min extract 

plasma Analytica Chimica Acta, 512, #2, 305-310 

Moreau, N. M.; Delepee, R.; Maume, D.; le Bizec, B.; 

Nguyen, P..; Champ, M..; Martin, L..;Dumon, H. 

Toward more useful in vitro toxicity data with measured 

1875 Animal testing free concentrations in-vitro sampling GC 

Environ. Sci. Technol., 38. #23, 6263-6270 

Busser, F; Heringa, M.; Hermens, J.; Schreurs, R.; 

Van Der Burg, Bart; Van Der Saag, Paul T. 

Development of microwave-assisted extraction followed by headspace 

2574 Camphor and SPME-GC-MS for quantification of camphor and borneol in 65µm PDMS-DVB GC-MS 

borneol in Flos Chrysanthemi Indici. 20min @ 40°C 

chinese Anal. Chim. Acta: 575, #1, 120-125 (2006-08-04) headspace 

medicines Deng, C. H.; Mao, Y.; Yao, N.; Zhang, X. M. 

SPME followed by GC-MS analysis of the volatile 

1876 Volatiles in components of Flos Chrysanthemi indici in headspace GC-MS 

chinese different growing areas. 

medicines Chromatographia, 59, #11-12, 763-767 

Wu, Q.; Deng, C. H.; Shen, S.; Song, G. X.; Hu, Y. 

M.; Fu, D. X.; Chen, J. K.; Zhang, X. M.* 

Application of SPME to in vitro skin permeation experiments 

1877 Diethyl example using diethyl phthalate GC 

phthalate Toxicology In Vitro, 19, #2, 253-259 

on skin Frasch, H. Fred; Barbero, Ana M. 

Identification of biogenic organotellurides in Escherichia 

1878 Volatiles from coli K 12 headspace gases using SPME-GC 75µm Carboxen GC-MS 

cell culture Analytical Biochemistry, 331. #1, 106-114 headspace 

Swearingen, J.; Araya, M.; Plishker, M.; Saavedra, C.; 

Vasquez, C.Chasteen, T. 

The effect of oligofructose on urea metabolism and 

1879 Faecal Odor faecal odour components in cats headspace GC 

from cats J Animal Physiology and Animal Nutr, 89, #3-6, 208-214 

Hesta, M.; Hoornaert, E.; Verlinden, A.; Janssens, G. P. J. 

Application of SPME to determination of strychnine in blood 

1880 Strychnine J Chromatogra B, 816, #1-2, 29-34 65µm CW-DVB GC/EI-MS 

in blood Barroso, M.; Gallardo, E.; Margalho, C; Avila, S; 20min extraction 





Marques, E; Vieira, D. N.; Lopez-Rivadulla, M. immersion sampling 

Development of headspace SPME w/ on-fiber derivatization 

1881 Hexanal, for determination of hexanal and heptanal in human blood 65µm PDMS-DVB GC-MS 

heptanal J Chromatogr, B: 813, #1-2, 47-52 8min @ 60°C 

in blood Deng, C. H.; Li, N.; Zhang, X. M.* PFBHA derivatives 

headspace 

Determination of low level methyl tert-butyl ether, ethyl tert-butyl ether 

2585 TAMEM, MTBE, and methyl tert-amyl ether in human urine by HS-SPME GC-MS headspace GC-MS 

ETBE and ANAL. CHIM. ACTA: 581,#1, 53-62 (02 JAN 2007) 65µm PDMS-DVB 

in urine Scibetta, L.; Campo, L.; Mercadante, R.; Foa&grave;, V.; Fustinoni, S. 

Identification and elimination of polysiloxane curing agent 

1882 Methyl tert- interference encountered in the quantification of low- headspace GC-MS 

butyl ether picogram per milliliter methyl tert-butyl ether in blood by 

in blood SPME headspace analysis 

Anal. Chem, 77,#9, 2912-29-19. 

Blount, Benjamin C.; Chambers, David M.; Hughes, T.; 

Mauldin, J.; McElprang, David 

SPME coupled w/ ion mobility spectrometry for the 

1883 Ephedrine analysis of ephedrine in urine immersion sampling IMS 

in urine J. Sep. Sci.28. #7,612-618 

Lokhnauth, John K.; Snow, Nicholas H. 

Determination of ethanol in human blood and urine by 

1884 Ehtanol in automated headspace SPME and capillary GC headspace GC 

biological Anal. Chim. Acta, 522, #2, 163-168 

fluids De Martinis, B.; Martins R., Maria A.; Santos M., Carmen C. 

A simple, rapid and sensitive method for determination 

1885 Aldehydes in aldehydes in human blood by GC-MS and SPME PFBHA derivative GC-MS 

blood with on-fibre derivatization. headspace 

Rapid Communications in Mass Spect, 18, #15, 1715-1720 

Deng, C. H.; Zhang, X. M.* 

Identification of components responsible for the odor of cigar 

2164 Odorous smoker's breath headspace GC-MS 

compounds in J Ag Food Chem, 54, #2, 497-501 (2006) 

SPME for analysis of alkanes and aromatic hydrocarbons in 

2218 Hydrocarbons in human breath GC 

breath J. Chromatogr. B, 826, #1-2,69-74 (2005) 

Yu, Hao; Xu, Liang; Wang, Ping 

Determination of acetone in human breath by GC-MS 

1886 Acetone in and SPME with on-fiber derivatization 65µm PDMS-DVB GC-MS 

human breath J. Chromatogr. B , 810, #2, 269-275 PFBHA derivative 

& plasms Deng, Ci; Yu, X; Zhang, J; Zhang, W Zhang, X 4 min extract 

agitated 

Impact of inspired substance concentrations on the results 

1887 Breath marker of breath analysis in mechanically ventilated patients headspace GC-MS 

in blood & Biomarkers, 10, #2-3, 138-152 

breath Schubert, J.; Miekisch, W.; Birken, T.; Geiger, K.; 

Noelge-Schomburg, G 

Capillary LC determination of cellular flavins 

1888 Flavins J. Chromatogr. A, 1053, #1-2, 71-78 in-tube silica-ODS LC-MS 

Jia, Li; Tanaka, Nobuo; Terabe, Shigeru 

Study of ligand-receptor binding using SPME: Investigation 

1889 Protein of receptor, free, and total ligand concentrations restricted access LC-MS 

binders J of Proteome Res, 4, #3, 789-800 molecularly imprinted 

Musteata, Florin Marcel; Pawliszyn, Janusz immobilized antibodies 

Determination of sterols in biological samples by SPME 

1890 Sterols in with on-fiber derivatization and GC/FID BSTFA derivative GC-FID 

serum Anal. Bioanal. Chem., 381, #8, 1576-1583 headspace 

samples Domeno, Celia; Nerin, Cristina; Ruiz, Barbara 

Poly (methacrylic acid-ethylene glycol dimethacrylate) 

1891 Basic drugs monlithic capillary for intube SPME coupled to HPLC and its polymethacrylate HPLC-UV 

in serum application to determination of basic drugs in human serum coated tube 

Anal. Chim. Acta, 523, #2. 251-258 

Da, Shi-Lu; Fan, Yi; Feng, Yu-Qi; Shi, Zhi-Guo 





Analysis of Rhioxma Curcumae Aeruginosae volatiles by 

1892 Volatiles from SPME w/GC-MS headspace GC-MS 

Chinese Zeitschrift fuer Naturforschung Section C J of Biosciences 

medicine 59, #7-8, 533-537 

Sha, Yuri F.; Shen, Shun; Duan, Geng L. 

Comparison between dynamic headspace and headspace SPME for 

2754 BTEX in gas chromatography of BTEX in urine headspace GC-PID 

urine ARH. HIG. RADA TOKSIKOL. 58, #4, 421-427 (01 DEC 2007) 

Karaconji, I. B.; Skender, L. 

Analytical method for evaluation of exposure to benzene, 

1893 BTEX in toluene, xylene in blood by GC preceded by SPME headspace GC 

blood J Chromatogr B, 809, #1, 183-187 

Alegretti, Ana Paula; Thiesen, Flavia V.; Maciel, Gisele 

Chronic toxicity and body residues of the nonpolar narcotic 

1894 1,2,3,4- 1,2,3,4-tetrachlorobenzene in Chironomus riparius headspace GC 

tetrachloro- Env Toxicology and Chem, 23, #8, 2022-2028 

bezene in Leslie, Heather A.; Kraak, Michiel; Hermens, Joop L. 

body residue 

Application of SPME to the determination of alkylphenols and 

2889 Bisphenol A bisphenol A in cyanobacteria culture media 65µm CW-DVB GC-FID 

cyanobacteria Anal. Bioanal. Chem. 391, #1, 425-432 (May 2008) headspace 

culture media Baptista, M.; Basto, M.; Carvalho, P.; Stoichev, T,; Vasconcelos, M. sat. salt 

Baseline toxicity of a chlorobenzene mixture and total body 

1895 Chlorobenzene residues measured and estimated with SPME headspace GC 

in body Env Toxicology and Chemistry, 23, #8, 2017-2021 

residue Leslie, Heather A.; Hermens, Joop L. M.; Kraak, Michiel H. S. 

Use of SPME followed by on-column silylation for determining 

1896 Chlorinated chlorinated bisphenol A in human plasma by GC-MS 85µm polyacrylate GC-MS-SIM 

bisphenol A J Chromatogra, B, 817, #2, 167-172 BSTFA derivative 

in plasma Del Olmo, M.; Gonzalez-Casado, A.; Suarez, B.; Taoufiki, J. 

Vilchez, J.L.; Zafra, A. 

Toxicology 

Application of solid-phase microextraction in analytical toxicology 

2633 Review Trends Anal. Bioanal. Chem. 388, #7, 1393-1414 (August 2007) 

Pragst, Fritz 

639 Drugs 

Microextraction of drugs 

J. Chromatogr.,A, 922(2000) 17-63 

Lord, H., Pawliszyn, J. 

review article 

912 Drugs 

High-temperature SPME procedure for the detection of 

drugs by GC-MS 85µm polyacrylate GC-MS 

J. Chromatogr. B (2000) 745(2), 399-411 10min @200°C 

Staerk, U., Külpmann, W. headspace 

acetic anhydride-pyridine 

640 Drugs 

Solid phase microextraction in biomedical analysis 

J. Chromatogr.,A, 902(2000) 167-194 review article 

in body fluids S. Ulrich 

641 Volatile, 

Headspace SPME procedures for gas chromatographic 

analysis of biological fluids and materials. review article GC 

semivolatiles J. Chromatogr.,A, 902(2000) 267-287 

in biological fluids Mills, G., Walker, V. 

847 Volatile, 

Headspace SPME profiles of volatile compounds in urine: 

Application to metabolic investigations 75µm Carboxen/PDMS GC-MS 

in urine J. Chromatogr.,B 753(2001) 259-268 

Mills, G., Walker, V. 

Accessing the aquatic toxicity of complex hydrocarbons 

headspace 

pH 9 

642 Hydrocarbon mixture mixtures using SPME 





in water Toxicol. Lett. 2000, 112-1113, 273-282 

Parkerton, T, Sone, M., Letiski, D. 

643 Methadone 

SPME in the determination of methadone in human 

saliva by GC-MS 100µm PDMS 

in saliva J. Anal Toxicol (2000), 24(2), 93-96 

Dos Santos Lucas, A., Bermejo, A., 

Fernandez, P., Tabernero, M 

30 min 

29 Methadone 

Gas Chromatographic Analysis of Methadone in Urine Samples 

after Solid Phase Microextraction 100µm PDMS GC-MS 

in urine J. Microcolumn Sep. 6: 577-581 (1994) 15 min 

Chiarotti, M., Marsili, R. 

Use of SPME for the determination of methadone and 

immersion 

pH 7.7 

644 Methadone, EDDP EDDP in human hair by GC-MS 100µm PDMS GC-MS 

in human hair Forensic Sci. Int (2000) 107(1-3), 225-232 

Luca, A., Bermejo, A., Tabernero, M., Fernadez, P., 

Strano-Rossi, S. 

30 min, immersed 

563 Methadone, EDDP 

Use of SPME for the determination of Methadone and 

its main metabolite, EDDP, in plasma by GC-MS 100µm PDMS GC-MS 

in plasma J. Anal. Toxicol. 24, 66-69 (2000) 30 min immersion 

Bermejo, A., Seara, R., dos Santos Lucas, A., 

Tabernero, M., Fernandez, P., Marsili, R. 

1:4 delution @ pH 9 

474 Anorectics 

SPME and GC analysis of anorectic compounds in 

human urine GC-MS 

in urine J.Microcolumn Sep. 1997, ((4), 249-252 

Chiarotti, M. Strano-Rossi, S., Marsili, R. 

Analysis of tetramethylene disulfotetramine in foods using SPME 

2891 Tetramethylene gas chromatography-mass spectrometry 70 μm CW/DVB GC/MS 

disulfotetramine J. Chromatogr. A 1192, #1, 36-40 (May 23 2008) headspace 

in foods De Jager, Lowri S.; Diachenko, Gregory W.; Perfetti, Gracia A. 

Determination of tetramethylenedisulfotetramine in human urine with 

2715 Tetramine GC-flame thermionic detection coupling with direct immersed SPME 85µm polyacrylate GC-FPD 

in human urine Forensic Sci. Int. 159, #2-3, 168-174 (2006-06-02) 

Zeng, D.; Chen, B. ; Yao, S. Z.; Ying, J. Y. 

immersed 

Rapid detection of tetramethylenedisulfotertramine 

645 Tetramine in human blood by SPME-GC 100µm PDMS GC-FPD 

in blood Anal. Chim. Acta (2000), 404(2), 329-334 

Luan, T., Li, G., Zhao, M., Zhang, Z. 

SPME-GC-MS method for the determination of 

930 Anesthetics inhalation anesthetics in urine 50:30µm DVB/Carboxen/ GC-MS 

in urine J. Chromatogr. B (1999), 732(1) 115-125 PDMS 

Poli, D., Bergamaschi, E., Maini, P., Andreoli, R., Mutti, A. 

Detection of Ten Local Anesthetics in Human Blood Using 

20min headspace 

10% NaCl 

65 Anesthetics Solid Phase Microextraction and Gas Chromatography 100µm PDMS GC-FID 

in human blood Jpn. J. Forensic Toxicol. 13 (2): 182-188 (1995) 100°C, 40 min 

Kumazawa, T., Lee, X., Sato, K., Seno, H., Ishii, A., Suzuki, D. 

Extraction of Local Anesthetics from Human Blood 

headspace 

perchloric acid added 

144 Anesthetics by Direct Immersion-SPME 100µm PDMS GC-FID 

in blood Chromatographia 43: 59-62 (1996) 40 min 

Kumazawa, T., Sato, K., Seno, H., Ishii, A., Suzuki, O. immersion 

342 Anesthetics 

Simple Analysis of Local Anesthetics in Human Blood Using 

Headspace SPME and GC-MS-Electron Impact Ionization 100µm PDMS GC-MS 

in human blood Selected Ion Monitoring 120°C, 45 min 

J. Chromatog. B, 709 (1998), 225-232 headspace 

Watanabe, T., Namera, A., Yaskiki, M., Iwasaki, Y., Kojima, T. NaOH added 





475 Nereistoxin in 

Simple and Sensitive Analysis of Nereistoxin and its 

Metabolites in Human Serum using Headspace 65µm DVB/PDMS GC-MS 

human serum SPME-GC-MS 30 min @ 70°C 

J. Chromatographic Science 37(3):77-82(1999) NaCl added, 

Namera,A., Watabe,T., Yashiki,Y., Kojima,T., Urabe,T. headspace 

419 Lidocaine 

Direct SPME Combined with Gas and Liquid Chromatography 

for the Determination of Lidocaine in Human Urine GC, HPLC 

in urine Chromatographia (1998), 47(11/12), 678-684 

Koster, E., Hofman, N., DeJong, G . 

646 Lidocaine 

Determination of lidocaine in plasma by direct SPME 

combined with GC 65µm PDMS/DVB GC 

in plasma J. Chromatogr., B. Biomed Sci. Appl (2000), 739(1), 175-182 10 min 

Koster, E., Wemes, C., Morsink, J., deJong, G. 

Evaluation of SPME in combination with GC as a tool 

immersed 

salt added 

647 Lidocaine for quantitative bioanalysis Carbowax-DVB GC-NPD 

in plasma J. Microcolumn Sep. 2000, 12(5), 308-315 

Abdel-Rehim, M., Bielenstein, M, Arvidsson, T. pH 9 


Determination of Persistent Organochlorine Compounds in 

Blood by SPME Extraction and GC-ECD GC-ECD 

compounds Fresenius' J. Anal. Chem. (1998), 361(2), 192-196 

in blood Roehrig, L., Puettmann, M., Meisch, H. 

141 Chloroethers 

Determination of Chloroethenes in Environmental Biological 

Samples Using GC Coupled with SPME 

in biological samples Chromatographia 42(5/6): 313-17 (1996) 

Xu, N., Vandegrift, S., Sewe, G. 

67 Solvent thinners 

Simple Analysis of 5 Thinner Components in Human-Body 

Fluids by Headspace SPME 100µm PDMS GC-FID 

in urine, blood J. Legal Medicine 107: 310-313 (1995) 

Lee, X., Kumazawa, T., Sato, K. 

Improved extraction of thinner components from human 

80°C, 5 min 

headspace 

877 Solvent thinners body fluids by headspace SPME with a Carboxen/PDMS 65µm Carboxen/PDMS 

in urine, blood coated fiber 

Leg. Med. 1(1999) 231-237 

Lee, X., Kumazawa, T., Kondo, K., Furuta, S., Sato, K. 


Determination of volatile organic compounds in blood 

by headspace SPME-GC 100µm PDMS GC-FID 

in blood Weosjemg Uamkoi 2000, 29(1), 37-39 

Hao, S., Kang, J., Zhou, S, Cui, J., Qi, Q., Han, K. 

10 min 


The use of SPME in conjunction with benchtop quadropole MS 

for the analysis of volatile organic compounds in human 100µm PDMS GC-MS 

in blood blood at low ppt. Levels 


Cardinali, F., Ashley, D., Wooten, J., McCraw, J., Lemire, S. 


795 Benzene 

Urinary benzene as a biomarker of exposure among 

occupationally exposed and unexposed subjects. GC-MS 

in urine Carcinogenesis (Oxford) (2001) 22(2), 279-286 

Rappaport, S; Bechtold, W; Dosemeci, M; Fustinoni, S 

Guilan, Li; Hayes, R 


Determination of organochlorine pesticides and PCBs in human 

serum using headspace SPME-GC-ECD 100µm PDMS GC-ECD 

pesticides, PCBs J. Chromatogr., B: 846, #1, 298-305 (2007-02-01) 50min @ 85°C 

in human serum Lopez, R.; Goni, F.; Etxandia, A.; Millan, E. headspace 





Determination of PAHs in human blood seum by proteolytic 


914 PAHs digestion-direct immersion SPME 

in blood serum Analytica Chimica Acta (1999) 396(2-3) 303-308 

Poon, K., Lam, P., Lam, M. 

887 PAHs 

Quantification of the PAH (Polycyclic Aromatic hydrocarbons) 

metabolites as a biomarker for PAH exposure. 

Abstracts of Papers ACS (2001) 221(1-2) ANYL117 

Walcott, C; Smith, C; Patterson, D; Maggio, V; 

Huang, W; Grainger, J 

Analysis of Inflammable Substances in Blood Using 

146 HydrocarbonsC9-C20 Head Space-SPME and Chemical Ionization and 100µm PDMS GC-MS 

blood Chemical Ionization Selected Ion Monitoring 10min.@90C 

in blood Jpn. J. Forensic Toxicol. 13 (2): 189-194 (1995) 

Iwasaki, Y., Yahiki, M., Nagsawa, N., Kojima, T., Miyazaki, T. 

Analysis Method of Flammables in Blood by 

NaOH added 

headspace 

476 Flammables using headspace- SPME and Chemical 100µm PDMS GC-MS 

blood, urine ionized MS Detection 10 min @ 90°C 

Jpn. J. Legal. Med (49 Append): 80(1995) 

Iwasaki,Y., Yashiki,M., Nagasawa,N., 

Miyazaki,T., Kojima,T 

headspace 

195 Cresol, phenols 

Detection of Cresol Isomers and Phenol in Human Whole Blood 

by Headspace SPME and Capillary GC 85µm polyacrylate GC-FID 

in human blood Jpn. J. Forensic Toxicol. 15 (1): 21-28 (1996) 30 min @ 100°C 

Lee, X., Kumazawa, T., Furuta, S., Kurosawa, T., Akiya, K., NaCl added 

Skiya, I., Sato, K. headspace 

420 Chlorophenols 

Application of SPME and GC-MS for the Determination 

of Chlorophenols in Urine 85um polyacrylate GC-MS 

in urine J. Chromatogr. B: Biomed. Sci. Appl. (1998), 707(1+2), 91-97 50 min, immersed 

Lee, M., Yeh, Y., Hsiang, W., Chen, C. pH 1 

583 4-Chlorophenol 

Total 4-chlorophenol determination in urine samples of 

subjects exposed to chlorobenzene, using SPME and GC-MS. 85µm polyacrylate GC-MS 

in urine J-High-Resolut-Chromatogr. Jul 1999; 22(7): 427-428 30 min 

Guidotti,-M; Ravaioli,-G; Vitali,-M salt added 

2530 O-cresol, toluene 

Comparison between urinary o-cresol and toluene as biomarkers 

of toluene exposure headspace GC-MS 

in urine J. Occup. Environ. Hyg. (USA) 4, #1, 1-9 (Jan. 2007) 

Fustinoni, S.; Mercadante, R.; Campo, L.; Scibetta, L.; Valla, C.; 

Consonni, D.; Foa, V. 

Immersed SPME to measure chemical activity of lipophilic 

2788 PCBs in organic contaminants in fatty tissue samples 

biological tissue Chemosphere 71, #8, 1502-1510 (April 2008) 

Mayer, P.; McLachlan, M..; Ossiander, Lia; Reichenberg, F. 

Sample pretreatment method for the determination of PCBs in bird livers 

2712 PCBs in using ultrasonic extraction followed by headspace SPME-GC-MS headspace GC-MS 

bird liver J. Chromatogr. A 1124, #1-2, 97-105 (2006-08-18) 

Lambropoulou, D. A.; Konstantinou, I. K.; Albanis, T. A. 

477 PCBs in 

Determination of PCBs in human blood serum by SPME 

Cheosphere, 1999, 39(6), 905-912 GC-ECD 

human serum Poon, K., Lam, P., Lam, M. 

68 Valproic acid 

Solid Phase Microextraction for the Determination of the 

Free Concentration of Valproic Acid in Human Plasma 100µm PDMS GC-FID 

in human plasma by Capillary GC 3 min 

J. Chromatogr. B 673: 299-305 (1995) immersion 





Krogh, M., Johansen, K., Gonnesen, F., Rasmussen, K. pH 2 

69 Nicotine, cotinine 

Rapid Analysis of Nicotine and Cotinine in Urine 

Using Head Space Solid Phase Microextraction 100µm PDMS GC-MS 

in urine and Selected Ion Monitoring 80°C, 5 min 

Jpn. J. Forensic Toxicol. 13 (1): 17-24 (1995) 

Yashiki, N., Magasawa, T., Kojima, T., Miyazaki, T., Iwasaki, Y. 

headspace 

478 Cartap 

Simple Analysis of Cartap and Its Metabolites Using Solid 

Phase Microextraction and GC/MS 65µm DVB/PDMS GC-MS 

in human serum Jpn. J. Forensic Toxicol. 16(2):142-143(1998) 30 min @ 70°C 

Namera,A., Watanabe,T., Yashiki,M., Iwasaki,Y., Kojima,T. immersed, NaOH added 

479 Nicotine, cotinine 

Analysis of Nicotine and Cotinine in biological fluid 

sample by SPME 100µm PDMS GC-MS 

in urine Jpn. J. Legal. Med (49 Append): 80(1995) 80°C, 5 min 

Iwasaki,Y., Yashiki,M., Nagasawa,N., Miyazaki,T., Kojima,T. headspace 

480 Stimulants 

Analysis of Stimulants and Narcotics 

Bunseki 10:816-822(1995) 100µm PDMS GC-NPD 

in blood & urine Yashiki,M., Kojima,T. 20 min @100°C 

3pH, (NH4)2SO4,NaCl 

headspace 

918 Stimulants 

Determination of stimulants in human urine and hair samples 

by polypyrrole coated capillary in-tube SPME coupled w/ LC-MS polypyrrole capillary LC-MS 

urine, hair samples Talanta 2001, 54(4) 655-672 

Wu, J., Lord, H., Pawliszyn, J. 

650 Fenfluramine, 

Simple and simultaneous analysis of fenfluramine, 

amphetamine, and methamphetamine in whole GC-MS 

amphetamine, blood by GC-MS after headspace SPME and derivatization 15 min, headspace 

methamphetamine Forensic Sci. Int. 2000, 109(3), 215-223 

in blood Namera, A., Yahiki, M., Liu, M., Okajima, K., Hara, K., 

Imamura, T., Kojima, T. 

808 Amphetamine, 

Highly sensitive analysis of methamphetamine and 

amphetamine in human whole blood using headspace GC-MS GC-MS 

methamphetamine Forensic Sci. Int. 2000, 116(1), 15-22 30 min @ 90°C EI-SIM 

in blood Namera, A., Kojima, T, Okajima, K., Tskue, I., Yashiki, M. headspace 

842 4-(4-methoxybenzyl) 

Synthesis of 4-methyl-5-arylpyrimidines and 

4-arylpyrimidines: route specific markers for the Leuckardt GC-MS 

pyrimidine preparation of amphetamine, 4-methoxyamphetamine and 

in tablets 4-methylthioamphetamine. 

Forensic Sci Intl (2001) 115(1-2) 53-67 

Kirkbride, K.; Ward, A; Jenkins, N..; Klass, G.; Coumbaros, J. 

headspace 

866 Impurities 

Application of solid-phase microextraction to the profiling of 

an illicit drug: Manufacturing impurities in illicit 

from drug 4-methoxyamphetamine 

J.Forensic Sciences (1999 )44(6), 1237-1242 

Kirkbride, K. Paul; Coumbaros, John C.; Klass, Gunter 


Use of volatile organic components in scat to identify Canid species 

Journal of Wildlife Management 72, #3, 792-797 (APR 2008) headspace GC-FID 

Canid species Burnham, Eric; Bender, Louis C.; Eiceman, G.; Pierce, K.; Prasad, S. 

481 Amphetamines, 

SPME/Capillary GC for the profiling of confiscated 

ecstasy and amphetamine 65µm DVB/PDMS GC-NPD 

ecstasy in Chromatographia, (1999) 50 (3/4), 247-252 headspace/immersed 

powder & tablets Kongshaug, K., Pedersen-Bjergard, S., Krogh,M., 0.1M acetate buffer 

Rasmussen, K pH 5 





Automated determination of ecstasy and amphetamines 


482 Ecstasy and in urine by SPME and capillary GC after 100µm PDMS GC-NPD 

amphetamines polylchloroformate derivatization. 16 min, immersed or MS 

in urine J. Pharm. Bomed. Anal. (1999), 19(3+4), 463-475 

Ugland, H., Kogh, M., Rasmussen, K. 

pH10 

927 Amphetamine, 

Determination of amphetamine, methamphetamine and 

dimethamphetamine in human urine by SPME-GC-MS 100µm PDMS GC-MS 

methamphetamine J. chromatogr. B (1998), 716(1-2) 359-365 30 min, immersed 

pH 12.4 KOH, NaCl 

dimethamphetamine Myung, S., Min, H., Kim, S., Kim, M., Cho, J., Kim, T. 

added 

in urine 

Rapid analysis of amphetamine, methamphetamine, 

stirred 

562 Amphetamines MDA, and MDMA in urine using SPME, direct On-Fiber 100µm PDMS GC-MS 

in urine derivatization, and analysis by GC-MS 10 min @ 100°C 

J. Anal. Toxicol. 24, 11-16 (2000) headspace, 2N NaOH 

Jurado, C., Gimenez, M., Soriano, T., 20 min @ 60°C on fiber 

Menedez, M., Repetto, M. trifluoroacetic anhydride 

483 Amphetamines 

Rapid Analysis Amphetamines in Blood Using SPME 

20th Japan Biomedical Mass Spectrometry:127-130(1995) 100µm PDMS GC-MS 

in urine & blood Yashiki,M., Kojima,T. 5 min @ 80°C 

immersed, NaOH added 


Detection of Amphetamines and Inflammable Compounds in 

Biological Materials Using GC/MS and SPME 100µm PDMS GC-MS 

in urine & blood Jpn. J. Forensic Toxicol. 12(2):120-121(1994) 5 min @ 80°C 

Yashiki, M., Kojima,T., Miyazaki,T. immersed, NaOH added 


Quantitative and Qualitative Analysis of MDMA, MDEA, MA, 

and Amphetamine in Urine by Headspace/SPME and GC/MS 100µm PDMS GC-MS 

in urine Forensic Sci. Intl. 83 (3): 161-166 (1996) 5 min @ 90°C 

Centini, F., Masti, A., Comparini, I. headspace 


Detection of Amphetamines in Urine Using Head Space 

SPME and Chemical Ionization Selected Ion Monitoring 100µm PDMS GC-FID 

in urine Forensic Sci Intl., 76(2), 169-177 (1995) 5 min 

Yashiki, M., Kojima, T., Miyazaki, T., 80°C 

Nagasawa, N., Iwasaki, Y., Hara, K. stirring 

Rapid Analysis of Amphetamines in Blood Using Headspace 

173 Amphetamines SPME and Selected-Ion Monitoring 100µm PDMS GC-SIM-MS 

in blood Forensic Sci. Intl. 78 (2): 95-102 (1996) 5 min @ 80°C 

Nagasawa, N., Yashiki, M., Iwasaki, Y., Hara, K., Kojima, T. 

Method Optimization for the Analysis of Amphetamines in 

heptafluorobutyr- amide 

derivative 

327 Amphetamines Urine by SPME 100µm PDMS GC-FID 

in urine Anal. Chem. 69 (19): 3899-3906 (1997) 15-60 min 


Simple Clean-up of Methamphetamine and Amphetamine in 

headspace 

stirring 

192 Amphetamines Human Urine by Direct-Immersion SPME 100µm PDMS GC-NPD 

in urine Jpn. J. Forensic Toxicol. 14 (3): 228-232 (1996) 30 min @ 65°C 

Ishii, A., Seno, H., Kumazawa, T., Suzuki, O., Na2CO3 added 

Nishikawa, M., Watanabe, K., Hattori, H. immersed 


Application of SPME Technique for the Detection of Urinar 

Methamphetamine and Amphetamine by GC GC 

in urine J. Can. Soc. Forensic Sci. 29(2): 43-48, (1996) 

Ameno, K., Fuke, C., Ameno, S., Kinoshita, H., Ijirei, I. 

2744 Impurities in 

Identification of impurities and the statistical classification of 

methamphetamine using headspace SPME-GC-MS Car/DVB 30/50µm GC-MS 

metamphetamine Forensic Sci. Int. 160, #1, 44-52 (2006-06-27) 30 min @ 85°C 

Kuwayama, K.; Tsujikawa, K.; Miyaguchi, H.; Kanamori, T.; Iwata, Y.; 

Inoue, H.; Saitoh, S.; Kishi, T. 

headspace 





421 Amphetamines, 

Determination of Amphetamine and Methamphetamine in Human Hair 

by Headspace SPME and GC-NPD 100µm PDMS GC-NPD 

methamphetamine J. Chromatogr. B: Biomed. Sci. Appl. (1998), 707(1+2) 99-104 15 min @45°C 

in hair Koide, I., Noguchi, O., Okada, K., Yokoyama, A., Oda, H., 

Yamamoto, S., Kataoka, H. 

immersed, NaOH added 

194 Methamphetamine, 

Rapid Analysis of Methamphetamine and Cocaine in the 

Urine of Drug Abusers with SPME 100µm PDMS GC-FTD 

cocaine Chromatography 18 (3): 185-188 (1996) 15 min 

in urine Makino, Y., Takgi, T., Ohta, S., Hirobe, M. 

Screening Procedure for 21 Amphetamine-Related 

immersion 

pH 10.5 

198 Amphetamines Compounds in Urine Using SPME and 100µm PDMS GC-MS 

in urine Gas Chromatography-Mass Spectrometry 80°C, 10 min 

J. Chromatogr. Sci. 36: 1-7 (1998) headspace 

Battu, C., Marquet, P., Fauconnet, A., Lacassie, E., 

Lachatre, G. 

salt added 

Automated drug analysis by in-tube SPME-LC-MS 

566 Amphetamines in Chromatography. Jun 1999; 20(2): 142-145 60cm x 0.25mm ID tube LC-MS 

urine Kataoka,-H; Lord,-HL; Pawliszyn,-J Omegawax 250 electrospray 

Simple and rapid determination of amphetamine, 

651 Amphetamines methamphetamine and their methylenedioxyl derivatives in In-tube Omegawax 250 

60cmx0.25mmi.d.x0.25µ 

LC-MS 

in urine urine by automated in-tube SPME coupled with LC-electrospray 

ionization mass spectrometry 

J. Anal. Toxicol (2000), 24(4), 257-265 

Kataoka,-H; Lord,-HL; Pawliszyn,-J 

m electrospray 


Determination of amphetamine and methamphetamine 

in serum via headspace derivatization SPME-GC-MS PDMS GC-MS 

methamphetamine J. Chromatogr. A, 896, (2000) 265-273 40 min, headspace 

in serum Lee, M., Song, Y., Hwang, B., Chou, C. pH 9.5 

heptafluorobutyric 

anhydride ethyl acetate 


On-fiber derivatization for direct immersion SPME part I: 

acylation of amphetamine with pentafluorobenzoyl chloride 

J. Sep. Sci. (2001) 24(2), 116-122 

Koster, E; Bruins, C.; Wemes, C; De Jong, G. 

Determination of automated In-tube SPME-LC-MS 

765 Beta blockers for drug analysis In-tube Omegawax 250 LC-MS 

in urine, serum J.MIcroSeparation,(2000-9), 12(9), 493-500 

Kataoka,-H; Lord,-HL; Pawliszyn,-J 

electrospray 

794 Beta blockers 

Determination of beta-blockers by HPLC w/SPME 

from urine and plasma samples 85µm polyacrylate HPLC 

in urine, serum Analytical Letters (2001) 34(1), 91-101 

Tanabe, S; Shimokawa, K; Matsuda, Y.,Katayama, M; 

Daimon, H,Hara. I; Kaneko, S; Sato, T. 

Comparison of New Solid Phase Extraction Methods for 

71 

Amphetamines, 

alcohols Chromatographic Identification of Drugs in Clinical 100µm PDMS, GC-FID 

in urine, serum Toxicology Analysis 85µm polyacrylate 

Degel, F., Weidemann, G. 

Some Problems of Detecting Amphetamines in Biological 

60°C, 15 min 

headspace 

485 Amphetamines in Materials by using Triage 100µm PDMS GC-MS 

biological fluids Pract. Forens. Med. 40:99-102 (1997) 5 min @ 80°C 

Watanabe,T., Namera,A., Yashiki,M., Iwasaki,Y., Kojima,T. CaCO3 added 

headspace 





Analysis of Drugs and Poisons in Legal Medicine 


234 Drug Summary J. Mass Spectrom. Soc. Jpn. 44: 321-333 (1996) Various fibers & 

Suzuki, O., Seno, H., Ishii, A. conditions 

79 Drugs of abuse 

Determination of Drugs of Abuse Using SPME (German) 

Labor-Med. 18 (2): 112-118 (1995) 100µm PDMS, GC-MS 

in urine Singer, K., Wenz, B., Seefeld, V., Speer, U. 85µm polyacrylate 

40°C, 20 min 


2541 Cocaine in 

Determination of cocaine and cocaethylene in plasma by SPME-GC-MS 

J. Chromatogr., B: 845, #1, 90-94 (2007-01-01) headspace GC-MS 

plasma Alvarez, I.; Bermejo, A. M.; Tabernero, M. J.; Fernandez, P.; Lopez, P 

2534 Cocaine 

Evidence on unusual way of cocaine smuggling: Cocaine-polymethyl 

methacrylate (PMMA) solid solution-study of clandestine laboratory 

samples GC-MS 

in polymethyl FORENSIC SCI. INT. 169, #2-3, 210-219 (04 JUL 2007) 

methacrylate Gostic, T.; Klemenc, S. 

81 Cocaine 

Detection of Cocaine in Human Urine by SPME and Capillary 

GC with Nitrogen-Phosphorus Detection 100µm PDMS GC-FPD 

in urine Jpn. J. Forensic Toxicol. 13 (3): 207-210 (1995) 30 min 

Kumazawa, T., Watanabe, K., Sato, K., Seno, H., immersion, stirring 

Ishii, A., Suzuki, O. NaF added 

Focused microwave-assisted extraction combined with SPME- 

2210 Cocaine from GC-MS for the selective analysis of cocaine from coca leaves 100µm PDMS GC-MS 

coca leaves J. Chromatogr. A, 1112, #1-2,127-132 (2006) immersion 

Bicchi, C.; Bieri, Stefan; Christen, P.; Ilias, Yara; Veuthey, J. 

SPME/GC-MS characterization of volatiles associated 

653 Volatiles with cocaine and heroin 

30/50Carboxen/DVB/PD 

MS GC-MSD 

from cocaine, heroin Am. Lab, Sept. 2000, 32-34 85µm polyacrylate 

Vu, D., Nicholas, P. Erikson, C. 

Field and Laboratory comparison of the sensitivity and 

90 min 

headspace 

486 Methyl Benzoate reliability of cocaine detection on currency using GC-MS-MS 

on currency chemical sensors, humans, K-Os and SPME/GC/MS 

Proceeding SPIE-Int. Soc. Opt. Eng, 3576:41-46 (1999) 

Furton, K., Hsu, Y., Luo, T., Norelus, A., Rose, S. 

907 Daidzein, isoflavon 

Detection of the isoflavone aglycones genistein and daidzein 

in urine using SPME-HPLC-electrospray MS LC-MS 

aglycones genistein J. Chromatogr. B (2001), 759(1) 33-41 

in urine Satterfield, M., Black, D., Brodbelt, J. 

164 Barbiturates 

Determination of Barbiturates by SPME and Ion Trap GC-MS 

J. Chromatogr. A 777: 275-282 (1997) 65µm Carbowax/DVB GC-MS 

in water Hall, B., Brodbelt, J. 

Aqueous phase hexyl chloroformate derivatization and SPME 

20 min 


572 Benzoylecgonine determination of benzoylecgonine in urine by GC- 100µm PDMS GC-EMIS 

in urine Quadrapole ion trap mass spectrometry 10 mi. @ 55°C 

J-Forensic-Sci. May 1999; 44(3): 527-534 hexyl chloroformate 

Hall,-BJ; Parikh,-AR; Brodbelt,-JS derivative 

224 Barbiturates 

Determination of Barbiturates by SPME and Capillary 

Electrophoresis polyvinyl coated electrophoresis 

in urine and serum Anal. Chem. 69: 1217-1222 (1997) metal rod 230nm 

Li, S., Weber, S. 5, 10, 30 min 

80 Meperidine 

Detection of Meperidine (Pethidine) in Human Blood and Urine 

Artificial receptor-facilitated SPME of barbiturates. 100µm PDMS GC-FID 

596 Barbiturates Anal-Chem. 1 Jun 1999; 71(11): 2146-2151 PVC/steel rod CE 

in urine/serum Li,-S; Sun,-LF; Chung,-Y; Weber,-SG 5 min 

immersed 





Detection of Meperidine (Pheonthiazin) in human blood and 


654 Meperidine urine by Headspace SPME and Gas Chromatography 100°C, 30 min GC 

in urine and blood Jpn. J. Forensic Toxicol. 13 (3): 211-215 (1995) headspace 

Seno, H., Kumazawa, T., Ishii, A., Nishikawa, M., 

Hattori, H., Suzuki, O. 

salt & NaOH added 

196 Phencyclidine in 

Simple Extraction of Phencyclidine from Human Body Fluids 

by Headspace SPME 100µm PDMS GC-surface 

blood and urine Chromatographia 43 (5-6): 331-333 (1996) 90°C, 30 min ionization 

Ishii, A., Kumazawa, T., Watanabe, K., Hattori, H., Suzuki, O. headspace detector 

487 Diphenylmethane 

Simple Analysis of Diphenylmethane Antihistaminics 

and their Analogous in bodily Fluids by headspace 100µm PDMS GC-FID 

blood and urine SPME capillary gas chromatography 10 min @ 98°C 

J. Chromatogr. Sci. 35:275-279(1997) 

Nishikawa,M., Seno,H., Ishii,A. Suzuki,O., 

Kumazawa,T., Watanabe,K., Hattori,H. 

10N NaOH 

Shaken not stirred: an analytical assay for antioxidant activity in 

2260 Antioxidant in martinis using quenched luminol chemiluminescence GC/MS 

martinis and SPME-GC-MS 

Abstracts of Papers Am Chem Society 229, #1, U394 (2005) 

McCrum, Erin C.; Shear, Ruth I. 

Comparison of different SPME fibers for the GC-MS analysis of 

2261 Organics in trace organics in a biological matrix (urine). GC/MS 

urine Abstracts of Papers Am Chem Society 229 #1, U353 (2005) 

Eggert,M.; Brown,P.; Evola,M.; Goodwin,T.; Rasmussen,L.;Schulte, B. 

179 Ethanol 

Blood Alcohol Determination with Automated SPME: 

A Comparison with Static Headspace Sampling 65µm Carbowax/DVB GC-FID 

in blood J. Can. Soc. Forens. Sci. 30(1): 7-12 (1997) 3 min 

Penton, Z. 

Detection of Ethanol in Human Body Fluids by Headspace 

headspace 

salt & NaF added 

191 Ethanol in SPME/Capillary GC 65µm Carbowax/DVB GC-MS 

blood, urine Chromatographia 43 (7-8): 393-397 (1996) 70°C, 10 min 

Kumazawa, T., Seno, H., Lee, X., Ishii, A., 

Suzuki, O., Sato, K. 

headspace, (NH4)2SO4 

418 Ethanol in 

Improved Extraction of Ethanol from Human Body Fluids 

by Headspace SPME with a Carboxen/PDMS Fiber Carboxen/PDMS 

blood, urine Chromatographia (1998), 47(9/10), 593-595 

Lee, Z., Kumazawa, T., Sato, K., Seno, H., Ishii, A., 

Suzuki, O. 

206 Antihistamine drugs 

Simple Analysis of Diphenylmethane Antihistamines 

and Their Analogue in Bodily Fluids by Headspace 100µm PDMS GC-FID 

in blood, urine SPME-Capillary Gas Chromatography 90°C, 10 min 

J. Chromatogr. Sci. 35 (6): 275-279 

Nishikawa, M., Seno, H., Ishii, A., Suzuki, O., 

Kumazawa, T., Watanabe, K., Hattori, H. 

headspace 

Determination of sulfonamide antibiotics in wastewater: A comparison 

2719 Sulfonamide of solid phase microextraction and solid phase extraction methods 65µm CW/DVB GC 

antibiotics J. Chromatogr., A 1131, #1-2, 1-10 (2006-10-27) 20 MIN 

in wastewater Balakrishnan, V. K.; Terry, K. A.; Toito, J. 4.5pH, sat. salt 

2648 Antibiotics in 

Determination of antibiotic drug concentrations in circulating human 

blood by means of solid phase micro-extraction LC-MS 

plasma Clinica Chimica Acta 386, #1-2, 57-62 (NOV-DEC 2007) 

Schubert, J.; Miekisch, W.; Fuchs, P.; Scherzer, N.; Lord, H.; 

Pawliszyn, J.; Mundkowski, R. 

2734 Nontricyclic 

Simultaneous determination of nontricyclic antidepressants in human 

plasma by (SPME-LC). LC-MS 





antidepressants J. Anal. Toxicol. 31, #6, 313-320 (Jul-Aug 2007) 

in plasma Silva, B. J. G.; Queiroz, R. H. C.; Queiroz, M. E. C. 

2507 Tricyclic 

Analysis of tricyclic antidepressant drugs in plasma by means of 

SPME-liquid chromatography-mass spectrometry 65µm PDMS/DVB LC-MS 

antidepressants J Mass Spectrometry 42, #10, 1342-1347 (OCT 2007) 30min @ 30°C 

in plasma Alves, C.; Santos-Neto, A.; Fernandes, C.; Rodrigues, J.; Lancas, F. direct extraction 

64 Tricyclic 

Simple Extraction of Tricyclic Antidepressants in Human Urine 

by Headspace SPME 100µm PDMS GC-FID 

antidepressants Jpn. J. Forensic Toxicol. 13 (1): 25-30 (1995) 100°C, 15 min 

in urine Kumazawa, T., Lee, X., Tsai, M., Seno, H., Ishii, A., Sato, K. 

Detection of Tricyclic Antidepressants in Whole Blood by 

headspace 

stirring 

95 Tricyclic Headspace SPME-Capillary GC 100µm PDMS GC-FID 

antidepressants J. Chrom. Sci. 35: 302-308 (1997) 100°C, 60 min 

in blood Lee, X., Kumazawa, T., Sato, K. 

Analysis of Tricyclic Antidepressant and that application 

headspace 

NaOH added 

488 Tricyclic for fatal intoxication by Headspace SPME 100µm PDMS GC-MS 

antidepressants Jpn. J. Legal. Med. 52:69(1998) 45 min @ 120°C 

in urine, blood Watanabe,T., Namera,A., Yashiki,M., Iwasaki,Y., Kojima,T. headspace, NaOH 

352 Tetracyclic 

Simple Analysis of Tetracyclic Antidepressants in Blood 

Using Headspace SPME and GC-MS 100µm PDMS GC-MS 

antidepressants J. Anal. Toxicology, Vol. 22 (5), 1998, 396-400 120°C, 45 min 

in blood Namera, A., Watanabe, T., Yahiki, M., Iwasaki, Y., Kojima, T. 

Direct coupling of microcolumn liquid chromatography 

headspace 

NaOH added 

655 Antidepressant with in-tube SPME for the analysis of antidepressant drugs In-tube HPLC 

in urine Analyst (Cambridge UK) 2000, 125(5), 807-809 

Saito, Y., Kawazoe, M, Jinno, K., Nayhashida, M. 

227 Diazepam 

Solvent-Modified Solid-Phase Microextraction for the 

Determination of Diazepam in Human Plasma Samples 85µm polyacrylate GC-FID or FPD 

in serum by Capillary Gas Chromatography 4 min 

J. Chromatogr. B 689: 357-364 (1997) immersion 

Krough, M., Grefslie, H., Rasmussen, K. pH 5.5 

1-octanol added 

656 Amitriptyline 

SPME coupled with microcolumn LC for the analysis of 

amitriptyline in human urine HPLC 

in human urine Chromatographia, (2000 Sept.) 52(5-6) 309-313 

Jinno, K., Kawazoe, M., Hayashida, M. 

371 Benzophenone-3 

Determination Benzophenone-3 and Metabolites in Water and 

Human Urine by SPME and Quadrupole Ion Trap GC-MS 65µm Carbowax/DVB GC-MS 

in water and urine Anal. Chimica Acta 371 (1998) 195-203 45 min 

Felix, T., Hall, B., Brodbelt, J. immersion 

871 Benzoylecgonine 

Aqueous phase hexylchloroformate derivatization and SPME 

Determination of benzoylecgonine in urine by GC 100µm PDMS GC-MS 

in urine quadrupole ion trap mass spectrometry. 

J Forensic Sci (1999) 44(3) 527-534 

Brodbelt, Jennifer S.; Hall, Brad J.; Parikh, Aashish R. 

Solid Phase Microextraction with Capillary GLC and NDPD for 

hexyl chloroformate 

derivative 

168 Antidepressants the Assay of Antidepressant Drugs in Human Plasma 100µm PDMS GC-NDPD 

in blood J. Chromatogr. B 696: 217-234 (1997) 60 min 

Ulrich, S., Martens, J. immersion 

657 Phenothiazines 

Determination of Phenothiazines in human body fluids by 

SPME and LC-tandem mass spectrometry 85µm Polyacrylate LC-MS 

urine, blood J.Mass Spec. (2000-9) 35(9) 1091-1099 60 min @ 40°C 

Seno, H., Kumazawa, T., Ishii, A., Hattori, H., pH 8 





Nishikawa, M., Watanabe, K., Suzuki, O. stirring 

142 Phenothiazines 

Detection of Some Phenothiazines by Headspace SPME 

and GC 100µm PDMS GC-FID 

urine, blood Jpn. J. Forensic Toxicol. 14: 30 (1996) 40 min @ 140°C 

Kumazawa, T., Seno, H.,, Ishii, A., Hattori, H., Sato, K., headspace 

Watanabe, K., Suzuki, O. NaCl added 

947 Propranolol 

In-Tube Molecularly Imprinted Polymer SPME for the selective 

Determination of Propranolol 

Anal. Chem (2001) 73(11) 2383-2389 

Mullett, Wayne M.; Martin, Paul; Pawliszyn, Janusz 

Quantification of plasma and urinary levels of furan in healthy individuals 

2480 Furan FASEB Journal. 21, #6, A1066 (APR 2007) GC-MS 

in plasma, urine Jun, Hee-Jin; Chung, Mi Ja; Park, Young-Sik; Lee, Kwang-Geun; Lee, S. 

Application of (SPME) technique for the detection of 

946 Carbofuran carbofuran in serum 

in seum J. Can. Soc. Forensic Sci(2001) 34(1), 23-26 

Ameno, K.; Lee, S-K.; Ameno, S.; Kinoshita, H.; Kubota, T.; 

Zhang, X.; Ijiri, 

908 Dinitroaniline 

Headspace SPME and GC determination of dinitroaniline 

herbiciede s in human blood, urine and environmental water 100µm PDMS GC-ECD 

in blood, urine J. Chromatogr. B. (1998), 714(2), 205-213 30 min @ 70°C 

and water Guan, F., Watanabe, K., Ishii, A., Seno, H., Kumazawa, T., headspace 

Hattori, H., Suzuki, O. NaSO4 


Reliable identification of pesticides using linear retention indices 

as an active tool in GC-MS analysis 

J. Chromatogr. A.1186 (1-2), 430-433 (Apr 4 2008) 

Casilli, A.; Dugo, G.; Dugo, Paola; Mondello, L.; Salvatore, Angelo; 

Tranchida, Peter Quinto 

GC-MS 


Evaluation of the pesticide contamination of groundwater sampledl 

over two years from a vulnerable zone in Portuga GC-ECD 

ground water J Agri Food Chem 55, #15, 6227-6235 (2007) 

Goncalves, C. M.; Silva, J. C. G. E. da; Alpendurada, M. F 

GC-MS 

2412 Phenylurea and 

Analysis of phenylurea and propanil herbicides by SPME-LC 

combined with post-column photochemically induced 60µm PDMS/DVB HPLC-PIF-FD 

propanil herbicides fluorimetry derivatization and fluorescence detection fluorimetry 

in ground water Anal. Chim. Acta 593, #2, 157-163 (2007-06-19) 

Mughari, A. R.; Parrilla Vazquez, P. ; Martinez Galera, M. 

derivatization 

183 Herbicides 

SPME and GC-ECD Determination of Dinitroaniline Herbicides in 

Surface Water and Biological Fluids 100µm PDMS GC-ECD 

in water and Jpn. J. Forensic Toxicol. 15 (2): 151-153 (1997) 30 min @ 70°C water 

biological fluids Prosen, F., Watanabe, K., Ishii, A., Seno, H., Suzuki, O. 

Gas chromatographic determination of organochlorine and 

@ 90°C blood 

Na2SO4, headspace 

860 Organochlorine & organophosphorus pesticides in human fluids using SPME GC/ECD/FPD 

organophosphorus Analytica Chimica Acta (2001) 433(2) 217-226 

pesticides in 

biological fluids 

Hernandez, F.; Beltran, J.; Egea, S.; Lopez, F. J.; Pitarch, E. 

Detection of Organophosphate Pesticides in Human Body 

66 Organophosphate Fluids by Headspace SPME and Capillary GC with 100µm PDMS GC-NPD 

pesticides Nitrogen-Phosphorus Detection 100°C, 20 min 

in urine, blood Chromatogrphia 42(3/4): 135-140 (1996) 

Lee, X., Kumazawa, T., Taguchi, T., Sato, K., Suzuki, O. 

pH 3 with HCl 


Optimisation of SPME conditions for headspace analysis 

of organophophorus pesticides in whole blood 

pesticides in Z Zagadnien Nauk Sadowych, 42(2000) 47-59 

whole blood Asri, K., Anderson, R. 





2777 Malathion bait 

Malathion bait consumption and mortality of Anastrepha suspensa 

(Diptera : Tephritidae) 

Annals of the Entomological Society of America 101, #2, 418-429 

Nigg, H.; Schumann, R.; Rouseff, R.; Smoot, John M.; Fraser, 


103 Malathion 

Rapid Analysis of Malathion in Blood Using Head Space 

Solid Phase Microextraction and Selected Ion Monitoring 100µm PDMS GC-MS 

in blood Forensic Sci. Int. 88: 125-131 (1997) 90°C, 5 min 

Namer, A., Yashiki, M., Nagasawa, N., Iwasaki, Y., 

Kojima, T. 

headspace 

489 Parathion 

Rapid analysis of parathion in biological samples using 

headspace SPME and GC-MS GC-MS 

in blood Clin. Chem. Lab. Med. 1999, 37(6), 639-642 

Musshoff, F., Junker, H., Madea, B 

headspace 

136 Carbamate in 

Determination of Some Carbamate Pesticides in Human Body 

Fluids by Headspace SPME/GC 100µm PDMS GC-NPD 

urine, serum Jpn. J. Forensic Toxicol. 14 (3): 199-203 (1996) 70°C, salt 

Seno, H., Kumazawa, T., Ishii, A., Nishif, M. headspace 

797 Amino pesticides 

Separation methods for amino group-possessing pesticides 

in biological samples. 100µm PDMS GC-FID, NPD 

in biological samples J Chromatogr B (2000) 747(1&2), 241-254 30min @ 95°C, salt 

Kumazawa, T; Suzuki, O. headspace 

490 Arylamide Herbicides 

Simple Analysis of Arylamide Herbicides in Serum using 

Headspace SPME and GC-MS 100µm PDMS GC-MS 

in Serum 6th Indo Pacific Congress on Legal Medicine and 45 min @ 90°C 

Forensic Science. 770-773(1998) 

Namera,A., Watanabe,T., Yashiki,M., Iwasaki,Y., Kojima,T. 

headspace, NaCl 

107 Diazepams in 

Solid-Phase Microextraction/Liquid Chromatography (SPME/LC) 

for Drug Analysis in Biological Fluids 85µm polyacrylate HPLC-UV, 

biological fluids Chromatography (1997), 18(4), 244-245, 

Jinno, K 

30°C, 3 hr 200nm 

658 Drugs 

SPME of drugs from biological matrices 

J. Chromatogr. A 885(2000) 445-455 review article 

in biological fluids Snow, N. 

234 Drugs in 

Analysis of Drugs and Poisons in Legal Medicine 

J. Mass Spectrom. Soc. Jpn. 44: 321-333 (1996) 100µm PDMS & GC-MS 

biological fluids Suzuki, O., Seno, H., Ishii, A. 

Confirmation of Volatiles by SPME and GC-MS in the 

85µm polyacrylate 

headspace 

NaCl, Na2SO4, 

108 Volatiles Investigation of Two Traffic Fatalities 85µm polyacrylate GC-MS 

in urine J. Anal. Toxicol. 1997, 21(4), 286-290 60°C, 10 min 

Brewer, W., Galipo, R., Morgan, S., Habben, K. headspace 

564 Tetarchoroethylene 

Tetrachloroethylene and trichloroethylene fatality: 

case report and simple headspace SPME-capillary 100µm PDMS GC-ECD 

trichloroethylene in GC determination in Tissues 1 min headspace 

tissue, urine, serum J. Anal.Toxicol, 24 (1), 22-26, (2000) 

Dehon, B., Humbert, L., Devisme, L., Stievenart, M., Mathieu, D. 

Houdret, N., Lhermitte, M. 

60°C 

2783 steroidal 

SPME followed by on-fiber derivatization of solasodine and 

solanidine aglycones of steroidal glycoalkaloids 60µm CW/DVB GC/MS 

glycoalkaloids J. Liq. Chromatogr.Relat. Technol. 31, #8, 1132-1146 (Jan 2008) immersion 

Eanes, Ritchie C.; Tek, Neslihan TMSI derivative 

2239 Steroid 

SPME with on-fiber silylation for simultaneous determinations 

endocrine disrupting chemicals and steroid hormones by GC-MS 85µm polyacrylate GC/MS 





hormones in J. Chromatogr. A, 1104, #1-2, 23-32 (2006) immersion 

biological Lan, Chongyu; Luan, Tiangang; Yang, Lihua derivatization 

samples 

113 Estrogen, steroids in 

Analysis of Steroids from Human Serum by SPME with 

Headspace Derivatization & GC 85µm polyacrylate GC-MS 

water/biological fluids J. High Res. Chromatogr. 20: 171-173 (1997) 30 min 

Okeyo, P., Rentz, S., Snow, N. 

Analysis of Estrogens and Anabolic Steroids by SPME with 


BSTFA derivative 

373 Estrogen, steroids in On-Fiber Derivatization and GC-MS 85µm polyacrylate GC-MS 

water/biological fluids J. Microcolumn Separations, 10(7) 551-556 (1998) 30 min 

Okeyo, P., Snow, N. 

On-Fiber Derivatization for Analysis of Steroids by SPME-GC-MS 



404 Estrogen, steroids in Book chapter 60µm Carbowax/DVB GC-MS 

water/biological fluids Snow, N. 60°C, 30 min 

immersion 

stirring 


200 Ethanol, acetone, 

Solid Phase Microextraction for the Analysis of Human Breath 

Anal. Chem. 69 (4): 587-596 (1997) 100µm PDMS GC-MS 

isoprene in Grote, C., Pawliszyn, J. 10-60 sec 

human breath 

Determination of isoprene in human expired breath using 

headspace 

659 Isoprene SPME with GC-MS Carboxen/PDMS GC-MS 

in human breath J. Chromatogr, B. Biomed Appl. 739(1), 183-190 10 min @ 40°C from 

Hyspler, R, Crhova, S. Gasparic, J., Cizkova, M., 

Balasova, V., Zadak, Z. 

tedlar bag sample 

322 Chloroethenes 

Determination of Chloroethenes in Environmental Biological 

Samples Using GC Coupled with SPME 

in biological fluids Chromatographia 42 (5/6): 313-317 (1996) 

Xu, N., Vadegrifts, S., Sewell 

660 Halothane 

Rapid analysis of halothane in biological samples 

using headspace SPME and GC-MS - GC-MS 

in biological samples a case of double homicide 

J. Anal. Toxicol. (2000), 24(5), 372-376 

Musshoff, G., Junker, H., Madea, B. 

867 4-Heptanone 

Urine 4-heptanone: A beta-oxidation product of 

2-ethylhexanoic acid from plasticisers GC-MS 

in urine Clinica Chimica Acta (2001) 306(1-2) 51-61 

Walker, Valerie; Mills, Graham A 

491 Clozapine in 

SPME for the assay of clozapine in human plasma 

Fresenius' J. Anal. Chem, 1999, 364(7), 654-655 100µm PDMS 

human plasma Kruggel, S., Ulrich, S. 

SPME for the assay of levomepromazine in human plasma 

30 min 

pH adj. NaOH 

843 Levomepromazine Therapeutic Drug Monitoring (2000) 22(6), 723-728 100µm PDMS GC-NPD 

in human plasma Kruggel, S., Ulrich, S. 

Determination of homocysteine and its related compounds 

30 min @30°c 

chloramitriptyline added 

0. 1 M -NaOH 

575 Homocysteine in by SPME-gas chromatography-mass spectrometry. 85µm polyacrylate GC-MS 

plasma/water J-Chromatogr,-B:-Biomed-Appl. 30 Apr 1999; 727(1-2): 1-8 30 min immersed 

Myung,-S-W; Kim,-M-S; Min,-H-K; Yoo,-E-A; Kim,-K-R pH 3 

906 Ranitidine 

Automated in-tube SPME-LC-electrospray ionization mass 

spectrometry for the determination of ranitidine. 

J. Chromatogr.B (1999), 731(2), 353-359 

Kataoka, H., Lord, H., Pawliszyn, J. 

LC-MS 





Determination of gamma-hydroxybutyrate in water and 

949 g-Hydroxybutyrate human urine by SPME-GC/quadrupole iontrap MS GC-MS 

in human urine J. Forensic Sci (2001), 46(3), 688-693 

and water Blair, S.; Song, M.; Hall, B.; Brodbelt, J. 

869 g-Hydroxybutyrate 

Simple extraction of gamma-hydroxybutyrate in human whole 

blood by headspace solid-phase microextraction 

in human whole Jpn. J. Forensic Toxicol (2001) 19(1) 38-45 

blood Kurihara, R; Ishii, A; Watanabe-Suzuki, K; Kumazawa, T; 

Seno, H; Suzuki, O; Katsumata, Y 

Determination of gamma-Hydroxybutyric Acid (GHB) in 

405 g-Hydroxybutyric Plasma and Urine by Headspace SPME and GC-Positive 50µm Carbowax/TPR100 GC-PICI-MS 

acid in Ion Chemical Ionization MS 70°C, 15 min 

plasma, urine Rapid Commun. Mass Spec(2000) 14(24), 2401-2407 headspace 

Frison, G; Tedeschi, L; Maietti, S; Ferrara, Santo D pH 6-7 

323 1-Phenylethylamine 

Simple Extraction of 1-Phenylethylamine in Human Urine 

by Headspace SPME 65µm PDMS/DVB GC-NPD 

in urine Jpn. J. Forensic Toxicol. 15(3): 189-193 (1997) 30 min @ 90°C 

Ishii, A., Seno, H., Prosen, F., Watanabee, K., 10M NaOH, K2CO3 

Kumanzawa, T., Hattori, H., Suzuki, O. headspace 

324 Benzodiazepines 

Detection of Benzodiazepines in Human Urine by 

Direct Immersion SPME-GC 65µm PDMS/DVB GC-FID 

in urine Jpn. J. Forensic Toxicol. 15 (1): 16-20 (1997) 

Seno, H., Kumazawa, T., Ishii, A., 

30 min 

Watanbe, K., Hattori, H., Suzuki, O. immersion 

325 Benzodiazepines 

Determination of Five Benzodiazepines in Aqueous 

Solution and Biological Fluids, Using SPME with 65µm Carbowax/DVB GC-FID, 

in water & urine Carbowax/DVB Fiber Coating 45°C, 60 min GC-MS 

J. Microcolumn Sep. 10 (2): 193-201 (1998) stirring 

Luo, Y., Pan, L., Pawliszyn, J. pH 7, salt added 

351 Benzophenones 

SPME and GC-ECD of Benzophenones for Detection of 

Benzodiazepines in Urine 100µm PDMS GC-ECD 

in urine J. Anal. Toxicology, Vol. 23, Jan/Feb 1999 , 54-61 30 min 

Prosen, F., Seno, H., Ishii, A., Watanabe, K., immersion, stirring 

Kumazawa, T., Hattori, H., Suzuki, O. 

SPME-Microcolumn LC for the Analysis of Benzodiazepines 

pH 9.4 

KOH added 

357 Benzodiazepines in Human Urine Carbowax/TPR100 HPLC-UV 

in urine Analusis (1998), 26(5), M27-M30 60 min 220nm 

Jinno, K., Taniguchi, M., Hayashida, M. immersion 

Automated in-tube solid-phase microextraction coupled 

779 Benzodiazepines with LC-electrospray ionization MS for the Supelco-Q capillary LC-ESI-MS 

in urine & serum determination of selected benzodiazepines 60cmx0.25mm I.d. 

J. Anal. Toxicology, (2000) Vol. 24(8),718-725 

Yuan, H. ; Mester, Z.; Lord, H.; Pawliszyn, J. 

SPME for Sample Preparation During Drug Metabolism Studies 

326 Pharmazie 53 (3): 172-177 (1998) 

Kroll, C., Borchert, H. 

2739 Cyanide 

An improved method for cyanide determination in blood using 

SPMEand gas chromatography/mass spectrometry 75µm Carboxen GC-MS-SIM 

in blood Rapid Commun. Mass Spectrom. 20, #19, 2932-2938 (2006-09-12) 

Frison, G.; Zancanaro, F.; Favretto, D.; Ferrara, S. D. 

headspace 

328 Cyanide 

Analysis of Cyanide in Blood by Headspace SPME and 

Capillary GC Carbowax/DVB GC-NPD 

in blood Chromatographia 47 (3/4): 209-214 (1998) 50°C, 45 min 

Takekawa, K., Oya, M., Kido, A., Suzuki, O. headspace 

Na2SO4 added 





Determination of Lead in Blood and Urine by SPME-GC 


492 Lead in Anal. Chem. 1999, 71(15), 2998-3002 

whole blood & Urine Yu, X., Yuan, H., Gorecki, T., Pawliszyn, J. 

Speciation of Alkyllead and Inorganic lead by derivatization 

headspace 

sodium tetraethyl 

borate derivative 

747 Lead in with deuterium-labeled sodium tetraethylborate and 100µm PDMS GC-MS 

whole blood & Urine SPME GC-MS 10 min, headspace 

Anal. Chem. 2000, 72,1788-1792 sodium tetraethyl 

Yu, X, Pawliszyn, J. borate derivative 


Production of artifact methylmercury during the analysis of 

certified reference sediments: Use of ionic exchange in the either ethylated GC-MIP-AED 

in sediment sample treatment step to minimise the problem 

Anal. Chim. Acta 582, #1, 109-115 (Jan 16 2007) 

de Diego, Alberto; Delgado, Alejandra; Madariaga, Juan Manuel; 

Prieto, Ailette; Zuloaga, Olatz 

derivatives GC-MS 

Optimisation of the headspace-SPME for organomercury and 

2914 Methylmercury organotin compound determination in sediment and biota 30µm PDMS GC-MS 

in sediment J Separation Science 31, #4, 768-774 (MAR 2008) headspace 

Delgado, A.; Usobiaga, A.; Prieto, A.; Zuloaga, O.; de Diego, A.; NaBEt4 derivative 

Madariaga, Juan 3-24 min @ 20-90 °C 


Determination of Methylmercury in Biological Samples and 

Sediments by Capillary GC Coupled with Atomic Adsorption 5cm fused silica fiber GC-AA 

in biological fluids after hydride derivatization and SPME 90 min 

or sediment J. Anal. At. Spectrom. (1998), 13(10), 1141-1144 headspace 

He, B., Jiang, G., Ni, Z. KBH4 derivative 

493 Alkalated Hg, Pb, Sn 

Simultaneous determination of Hg(III) and alkylated Hg, Pb, 

and Sn species in human body fluids using SPME-GC-MS-MS 100µm PDMS GC-MS-MS 

in urine Fresenius' J.. Anal. Chem. (1999), 363(5-6), 466-468 10 min 

Dunemann, L., Hajimiragha, H., Begerow, J. 

Coupling of SPME and GC-AED for the determination of 

NaBEt4 derivatives 

pH 5.3 

661 Organometallic organometallic compounds 

Mikrochim Acta, (2000) 135 (No.1&2) 91-95 

Mothes, S, Wennrich, R. 

GC-AED 

329 Methanol 

Simple Extraction of Methanol in Human Whole Blood by 

Headspace SPME Carboxen/PDMS GC-FID 

in blood Jpn. J. Forensic Toxicol. 16 (1): 64-68 (1998) 60°C, 10 min 

Lee, X., Kumazawa, T., Jurosawa, T., headspace 

Akiya, K., Akiya, Y., Fruta, S., Sato, K. stirring 

330 Aromatic amines in 

Solid Phase Microextraction of Monocyclic Aromatic Amines 

from Biological Fluid 65µm PDMS/DVB GC-FID 

urine, blood, milk Anal. Chem. 70 (9): 1986-1992 (1998) 45°C, 15 min 

DeBruin, L., Josephy, P., Pawliszyn, J. 

Quantitative determination of trimethylamine in urine by 

headspace, salt added 

KOH added, pH >13 

65µm Carboxen/PDMS, 

494 Trimethylamineuria SPME-GC-MS 

100µm PDMS GC-MS 

in urine J. Chromatogr. B: Biomed Sci. Appl., 1999, 723(1+2), 281-285 15 min @ 59°C 

Mills, G., Walke, V., Mughal, H. 

Determination of acrolein by headspace SPME-GC-MS 

headspace 

stirred 

950 Acrolein J. Chromatogr., B: Biomed (2001), 758(1), 123-128 

in bioligical fluids Takamoto, S.; Sakura, N.; Yashiki, M.; Kojima, T. 

331 PAHs 

Fast Screening Method for the Profile Analysis of Polycyclic 

Aromatic Hydrocarbon Metabolites in Urine, Using 85µm polyacrylate GC-MS 

in urine Derivatization-SPME 35°C, 45 min 

J. Chromatogr. G: Biomed. Sci. Appl. 705 (1): 132-138 (1998) stirring 

Gmeiner, G., Krassnig, C., Schmid, E., Tausch, H. BSTFA derivative 





SPME and GC-MS for determination of monoaromatic 


495 BTEX in hydrocarbons in blood and urine. Application to people 75µm Carboxen/PDMS GC-MS 

in urine & blood exposed to air pollutants 

Chromatographia, 1999, 50(3/4), 167-172 

Andreoli, R., Manini, P. Bergamaschi, E., Brustolin, A., Mutti. A. headspace 

591 BTEX in 

Headspace solid-phase micro-extraction for the 

determination of BTEX in urine. 100µm PDMS GC-EMIS 

urine J-Chromatogr,-B:-Biomed-Appl. 19 Feb 1999; 723(1-2): 105-115 15 min @ 30°C 

Fustinoni,-S; Giampiccolo,-R; Pulvirenti,-S; Buratti,-M; Colombi,-A headspace 

662 Toluene 

The comparison of toluene determination between 

headspace SPME and Headspace methods in glue 100µm PDMS 

in blood sniffer's blood and urine samples 

J. Forensic Sci. (2000), 45(3), 702-707 

Kim, N., Park, S. 

496 Toluene, xylene 

Method for analyzing urinary toluene and xylene by SPME 

and its application to workers using organic solvents 100µm PDMS GC-FID 

in urine Bull. Environ, Contam. Toxicol. (1999), 62(2), 109-116 5 min, 

Asakawa, F., Jitsunari, F., Choi, J., Suna, S., Takeda, N., 

Kitamado, T. 

NaCl, stirring 

497 Toluene, benzene 

Biomonitoring of benzene and toluene in human blood by 

headspace SPME 65µm Carboxen/PDMS GC-MS 

in human blood Fresenius' J. Anal. Chem. (1999), 363(1)m 88-91 30 min @ 20°C 

Schimmiing, E., Levsen, K., Koehme, C., Schuermann, W. headspace 

332 Erythromycin 

A Study of Erythromycin A Decomposition Products in 

Aqueous Solution by SPME-LC-MS 65µm PDMS/DVB LC-MS 

in water Rapid Commun. Mass Spectrom. 10 (2): 225-234 (1998) 15 min 

Volmer, D., Hui, J. 

Rapid Determination of Corticosteroids in Urine by Combined 

immersed 

50% MeOH extr. 

333 Corticosteroids SPME-LC-MS LC-MS 

in urine Rapid Commun. Mass Spectrom. 11 (17): 1926-1934 (1997) 

Volmer, D., Hui, J. 

Polypyrrole coated capillary in-tube SPME coupled 

663 Beta blockers with HPLC electrospray ionization MS for the Polypyrrole capillary LC-ESI-MS 

in urine, serum determination of beta blockers in urine and serum samples 

J. Microcolumn Sep. (2000) 12(4), 255-266 

Wu, J., Lord, H., Pawliszyn, J., Kataoka, H. 

334 Flavor compounds 

Evaluation of SPME for Analysis of Volatile Metabolites 

Produced by Staphylococci 100µm PDMS, GC-FID 

in staphylococci J. Agric. Food Chem. 46 (1): 228-234 (1998) 85µm polyacrylate 

Vergnaise, L., Masson, F., Montel, M., Berdague, J., Talon, R. 

Evaluation and identification of potential organic nematicidal 

headspace 


pH 3 for esters 

2576 Volatiles from volatiles from soil bacteria headspace GC-MS 

soil bacteria Soil Biology & Biochem 39, #10, 2567-2575 (OCT 2007) 

Gu, Ying-Qi; Mo, Ming-He; Zhou, Jun-Pei; Zou, Chang-Song; Zhang, K. 

Application of SPME to measure volatile metabolites 

498 Aldehydes, esters produced by Staphylococcus carnosus and 

100µm PDMS, 

85µm polyacrylate GC-FID 

from bacteria Staphylococcus xylosus 15 min, stirring 

Book- Applied SPME, 1999, 364-371 Royal Society of esters @ 80°C, 

Chemistry, Cambridge, UK Coden: 67TUA8 aldehydes @ 25°C 

Talon, R, Montel, M. headspace 


Application of Head-Space SPME for the Analysis of Volatile 

Metabolites Emitted by Penicillium Species 100µm PDMS, GC-MS 

in penicillium fungi J. Microbiological Methods, 25 (1996) 245-255 85µm polyacrylate 

Nilsson, T., Larsen, T., Montanarrella, L., Madsen, J. 25°C, 30 min (PDMS), 

50 min (PA) 





Biotransformation of (R)-(+)- and (S)-(-)-limonene by 


895 Volatile metabolites fungi and the use of SPME for screening. 

from limonen Phytochemistry (Oxford) (2001) 57(2) 199-208 

Demyttenaere, J.; De Kimpe, N; Van Belleghem, K 

2730 Volatile 

Fungal biotransformation of monoterpenes found in 

agro-industrial residues from orange and pulp industries into : headspace GC 

metabolites from aroma compounds screening using SPME 

monoterpenes Food Sci Biotech 16, #1, 37-42 (2007) 

Marostica, M. R., Jr.; Onoyama Mota, N.; Baudet, N.; Pastore, G. M. 


Biotransformation of geraniol, nerol and citral by sporulated 

surface cultures of Aspergillus niger and Penicillium sp. 

in penicillium fungi Phytochemistry (2000) 55(4), 363-373 

Demyttenaere, J.,del Carmen Herrera, M.; De Kimpe, N 


Use of Digital Aroma Technology and SPME GC-MS to Compare 

Volatile Compounds produced by Bacteria Isolated from 100µm PDMS GC-MS 

bacteria on poultry Processed Poultry 37°C, 30 min 

J. Sci Food Agric. 1998, 78, 343-348 

Arnold, J., Senter, S. 

headspace 


Evaluation of SPME for the Isotopic Analysis of volatile 

compounds produced during fermentation by lactic 70µm Carboxen/PDMS GC-C-IRMS 

lactic acid bacteria acid bacteria 10 min 

J. Agric Food Chem. 2000, 48, 2222-2227 headspace 

Goupry, S., Rochut, N., Robins, R., Gentil, E. salt added 

570 Fatty acid esters 

Headspace SPME with l-pyrenyldiazomethane in-fiber 

derivatization for analysis of fecal short-chain fatty acids 85µm polyacrylate GC-EMIS 

in faeses J-Chromatogr,-B:-Biomed-Appl. 25 Jun 1999; 730(1): 113-122 15 min 

Mills,-GA; Walker,-V; Mughal,-H 

Determination of Cannabinoids in Water and Human Saliva by 

1-pyrenyldiazomethane 

derivative 

335 Cannabinoids SPME and Quadrupole Ion Trap GC-MS 30µm PDMS GC-MS 

in water/saliva Anal. Chem. 70 (9): 1788-1796 (1998) 10 min 

Hall, B., Satterfield-Doeerr, M., Parikh, A., Brodbelt, J. immersion 

665 Dibenzylamine 

Direct comparison of SPE and SPME for the GC 

determination of dibenzylamine in artificial saliva 85µm polyacrylate GC-MS 

in saliva leachates from baby bottle teats 

Anal Chim Acta 2000, 414(1-2), 133-140 

Niessner, G., Klampfl, C. 

pH 10 

Extraction and analysis of different Cannabis samples by 

2185 Cannabinoids headspace SPME combined with GC-MS headspace GC-MS 

from Cannabis J SepSci. 28, #17, 2293-2300 (2005) 

samples Ilias, Y.; Rudaz, S.; Mathieu, P.; Christen, P.; Veuthey, Jean 

340 Cannabinoids 

Solid-Phase Microextraction for Cannabinoids Analysis in Hair 

and Its Possible Application to Other Drugs 30µm PDMS GC-MS 

in hair J. Anal. Toxicology, Vol. 23, Jan./Feb. 1999 15 min, immersion 

Strano-Rossi, S., Chiarotti, M. 

Use of headspace SPME in hair analysis for 

hair digested with 

1N NaOH 

666 Lipophilic drugs organic compounds 

in hair Forensic Sci. Int. (2000), 107(1-3), 129-148 headspace 

Sporkiert, F., Pragst, F. hair digested with 

4% NaOH 

941 Lipophilic drugs 

Analysis of hair by headspace SPME and GC-MS. 

Chromatogr Separation Tech (2001), 17(2), 4-8 headspace 

in hair Pragst, F 

SPME in Forensic Toxicology 

hair digested with 

4% NaOH 

336 Review of use Jpn. J. Forensic Toxicol. 16 (1): 1-15 (1998) various fibers 





Namera, A., Yashiki, M., Kojima, T., Fukunaga, N. and conditions 

337 Acylcarnitines 

Determination of Urinary Acylcarnitines by ESI-MS Coupled 

with SPME ESI-MS 

in urine J. Mass Spectrom. 32 (11): 1195-1204 (1997) 

Mioder, M., Loster, H., Hraschuh, R., Popp, R. 

499 Methylxanthines 

Extraction of methylxanthines from human body fluids 

by SPME 65µm Carbowax/DVB GC-NPD 

in blood/urine Anal. Chim. Acta., 1999, 387(1), 53-60 1 hr @ 40°C 

Kumazawa, T., Seno, H., Lee, X., Ishii, A. 1ml of 1M HCl04 

414 Organic acid esters 

Urinary Organic Acid Screening by SPME of the Methyl Esters 

J. Chromatogr. B: Biomed Sci. Appl. (1998), 713(2), 427-432 85µm polyacrylate GC-FID, -MS 

in urine Liebich, H., Gesele, E., Woll, J. 

Validation of negligible depletion SPME as a tool to 

20 min 

immersion w/stirring 

trimethyloxonium 

tetrafluoroborate 

667 Semivolatile determine tissue/blood partition coefficient for semivolatiles 

in tissue/blood and nonvolatile organic chemicals 

Toxicol. Appl. Pharmacol. (2000), 166(2), 138-144 

Garicano, E., Vaes, W., Hermens, J. 

415 

New Mass Spectrometric Methods for the Fast Analysis 

of Biomedical-Relevant Substances 

CLB Chem. Labor Biotech. (1998), 49(11), 414-420 

Volmer, D. 

GC-MS 

417 Verpamil & 

SPME-HPLC Determination of Verpamil and Norverpamil 

Enantiomers in Urine HPLC 

norverapamil J. Mass Spectrom. (1997), 32(11), 1195-1204 

in urine Asafu-Adjaye, E., Shiu, G. 

971 Pesticides in water 

Pesticide toxicity assessment using an electrochemical biosensor. 

Analytical and Bioananalytical Chemistry (2002) 373(8), 696-703 

Farre, M.; Goncalves, C.; Lacorte, S.; Barcelo, D.; Alpendurada, M.F. 

GC-MS 

Absorption through porcine skin exposed to various doses of jet fuel marker 

components determined with GC-FID using head space SPME fiber. 

1034 Jet fuel in porcine skin. Toxicological Sciences (2003) 72 (S-1), 383. 

1050 PAH 

Xia, X. R.; Riviere, J. E.; Muhammad, F.; Monteiro-Riviere, N. A.; Baynes, R. E. 

Determination of selected monohydroxy metabolites of 2-, 3- and 4-ring 

polycyclic aromatic hydrocarbons in urine by solid-phase microextraction and 

isotope dilution gas chromatography-mass spectrometry. 

Journal of Chromatography, B: Analytical Technologies in the Biomedical and 

Life Sciences (2002) 778 (1-2), 157-164. GC-MS 

Smith, C. J.; Walcott, C. J.; Huang, W. L.; Maggio, V.; Grainger, J.; Patterson, 

D. G., Jr. 

1294 

Biomimetic solid-phase microextraction to predict body residues and toxicity of 

chemicals that act by narcosis. 

Environmental Toxicology and Chemistry (2002) 21(2), 229-234 

Leslie, Heather A.; Busser, Frans J. M.; Hermens, Joop L. M.; Kraak, Michiel H. 

S.; Oosthoek, Annelies J. P. 

GC-MS 

1349 

Fatty acid ethyl esters in hair as markers of alcohol consumption. Segmental 

hair analysis of alcoholics, social drinkers, and teetotalers. 

Fatty acid ethyl esters 

in hair Clinical Chemistry (2001) 47(12), 2114-2123. 

Auwaerter, V.; Sporkert, F.; Hartwig, S.; Pragst, F. *; Vater, H.; Diefenbacher, 

A. 

GC-MS 


1381 




Sample preparation with fibre-in-tube solid-phase microextraction for capillary 

electrophoretic separation of tricyclic antidepressant drugs in human urine. 

Tricyclic 

antidepressants in 

urine. Electrophoresis (2001) 22(17), 3785-3790. 

Jinno, K.; Kawazoe, M.; Saito, Y.; Takeichi, T.; Hayashida, M. 

Analysis of fatty acid ethyl esters in hair as possible markers of chronically 

elevated alcohol consumption by headspace solid-phase microextraction (HS 

SPME ) and gas chromatography-mass spectrometry (GC-MS). 

Fatty acid ethyl esters 

1391 in hair. Forensic Science International (2001) 121(1-2), 76-88. 

Pragst, F.; Auwaerter, V.; Sporkert, F.; Spiegel, K. 


Pollution prevention screening of simulated Hanford waste for polychlorinated 

biphenyls by solid phase microextraction/GC-ECD. 

1417 Abstracts of Papers American Chemical Society (2001) 222(1-2), ANYL118. 

Okemgbo, Asopuru A.; Metcalf, Steven G. 

1438 

Methylene chloride in 

urine 

Monitoring of occupational exposure to methylene chloride: Sampling protocol 

and stability of urine samples. 

Journal of Toxicology Clinical Toxicology (2003) 41(5), 735-735 

Tabak, A.; Scherb, I.; Hoffer, E.; Bentur, Y.; Weiner, A. 

2755 Fentanyl in 

Determination of fentanyl in human plasma by head-space SPME-GC-MS 

J. PHARM. BIOMED. ANAL. 43, #5, 1763-1768 (11 APR 2007) headspace GC-MS 

human plasma Bagheri, H.; Es-haghi, A.; Khalilian, F.; Rouini, M. -R. 

1489 

1501 

Fentanyl and 

midazolam in plasma 

Simultaneous determination of fentanyl and midazolam in plasma using direct 

solid-phase microextraction before gas chromatography-mass spectrometry 

analysis. 

Analytical Letters (2002) 35(9), 1575-1590 65um PDMS/DVB 

Dufresne, C.; Bureau, J.; Favetta, P.; Gonin, R.; Guitton, J. 

Fully automated determination of amphetamines and synthetic designer drugs 

in hair samples using headspace solid-phase microextraction and gas 


Amphetamines and 

designer drugs in hair 


Musshoff, Frank; Junker, Heike P.; Kroener, Lars; Lachenmeier, Dirk W.; 

Madea, Burkhard 

GC-MS 

2351 GHV, MAMP, 

A validated SPME-GC-MS method for simultaneous 

quantification of club drugs in human urine. 100µm PDMS GC-MS 

KET, MDMA Forensic Sci Int 71, #2-3, 142-50 (2007 Sep 13) 20 min @ 90°C 

in urine Brown, Stacy D; Rhodes, Daniel J; Pritchard, Boyd J hexylchloroformate/ 

pyridine derivative 

Detection and identification of illicit drugs including GHB, Rohypnol, Ketamine, 

and Psilocybin by refocused Solid Phase Microextraction High Performance 

Liquid Chromatography Mass Spectrometry, (SPME/HPLC/MS). 

1511 Drugs of abuse Abstracts of Papers American Chemical Society (2002) 223(1-2), ANYL 54 HPLC-MS 

1021 

Sabucedo, Alberto; Furton, Kenneth G.; Benson, Andrew; Almirall, Jose 

A fatal human intoxication with the herbicide allyl alcohol (2-propen-1-ol). 

allyl alcohol (2-propen- 

Journal of Analytical Toxicology (2002) 26(1), 55-57 

1-ol) 

Toennes, S. W.; Schmidt, K.; Fandino, A. S.; Kauert, G. F. 

GC-MS 


1530 





cocaine 

Forensics 

Gas chromatographic-mass spectrometric analysis of residual solvent trapped 

into illicit cocaine exhibits using head-space solid-phase microextraction 

Journal of Chromatography B (2002) 772(2), 249-256 headspace GC-MS 

Chiarotti, Marcello; Marsili, Remo; Moreda-Pineiro, Antonio 

748 Review 

The use of SPME-GC in forensic analysis 


Furton, K., Wang, J., Hsu, Y. Walton, J, Almirall, J. 

500 Gasoline 

The detection and analysis of ignitable liquid residues 

extracted from human skin using SPME-GC 100µm PDMS GC-FID 

on skin Almirall, J., Wang, J., Lothridge, K, Furton, K. 

Characterization of SPME-GC for the analysis of gasoline tracers 

15 min 

headspace 

2733 Gasoline volatiles in different microenvironments. 75µm Carboxen GC-FPD 

in varied matries J Air Waste Manag Assoc 57, #3, 355-65 (2007 Mar) 10min 

Ceballos, Diana; Zielinska, Barbara; Fujita, Eric; Sagebiel, John air samples 

SPME samping of fire debris resideus in the presence of 

2385 Fire debris radionuclide surrogate metals headspace GC-MS 

from surrogate Journal of Chromatography A 2007-03-23 22°C 

metals Duff, M., Crump, S., Keisha M. 

2630 Ignitable liquids 

Forensic application of GC-differential mobility spectrometry with 

two-way classification of ignitable liquids from fire debris headspace GC-MS 

in fire debris Anal. Chem. 79, #17, 6752-6759 (Sep 1 2007) 

Harrington, Peter B.; Lu, Yao 

85 Accelerants 

A Simple, Inexpensive, Rapid, Sensitive and Solventless 

Technique for the Analysis of Accelerants in Fire 100µm PDMS GC-FID 

in fire debris Debris Based on SPME 40°C, 20 min 

J. High Res. Chromatogr. 18: 625-629 (1995) 

Furton, K., Bruna, J., Almirall, J. 

headspace 

105 Gasoline, kerosene 

Forensic Application of the SPME Method to the Analysis 

of Gasoline and Kerosene 100µm PDMS GC-NPD 

in fire debris Kaneko, T., Nakada, M. 22°C for 1 hr, or 

80°C for 5 min 

headspace 

Multivariate pattern recognition of petroleum-based accelerants by 

2430 Accelerants SPME-GC with flame ionization detection. headspace GC-FID 

Identification Anal. Chim. Acta 589, #2, 247-254 (2007-04-25) 

Bodle, E. S.; Hardy, J. K. 


Novel Method for Analysis of Gasoline from Fire Debris Using 

Headspace Solid Phase Microextraction 100µm PDMS GC-FID 

in fire debris J. Forensic Sci. 41: 12-22 (1996) 

Furton, K., Almirall, J., Bruna, J. 

40°C, 20 min 

The Recovery of Accelerants in Aqueous Samples from Fire 

115 Accelerants Debris Using SPME 100µm PDMS GC-FID 

in liquid residue Science & Justice 36 (4): 283-287 (1996) 20 min @ 40°C 

Almirall, J., Furton, K., Bruna, J. 


Determination of Liquid Accelerants in Arson Suspected Fire 

Debris Using Headspace SPME 100µm PDMS GC-FID 

in fire debris Anal. Commun. 33: 129 (1996) 

Steffen, A., Pawliszyn, J. 

A comprehensive sample preparation scheme for a 

15 min @ 70°C 

headspace 

594 Accelerants accelerants in suspect arson cases. GC, GC-MS 

in fire debris J-Forensic-Sci. May 1999; 44(3): 504-515 

Ren,-QL; Bertsch,-W 

Immersion mode SPME ECD/GC and TEEM-GC/MS for analysis of 





2269 TNT in sand explosives buried in sand Immersion GC-ECD 

Proc SPIE Int Soc Opt Eng (2005) 5794 #II, 1272-1280 GC/MS 

Baez, B.; Briano, J.; Castro, M..; Correa, S.; De Echevarria, M. 

Hernandez-Rivera, S. 

2270 TNT in sand 

Transport of explosives II: Use of Headspace-SPME/GC-ECD and 

TEEM GC/MS for detection of TNT vapors from sand buried samples Headspace GC-ECD 

Proc SPIE Int Soc Opt Eng (2005) 5794 #II, 1263-1271 

Baez, B.; Briano, J.; Castro, M..; Correa, S.; De Echevarria, M. 

Hernandez-Rivera, S. 

GC/MS 

SPME sampling of high explosive resideus in the presence 

2383 Explosive residue of radionuclides and radioneclide surrogate metals 

J Radioanalytical and Nuclear Chemistry -2007-04-13 

Duff, M., Crump, S., Robert, R., Beals, D. 

Bioconcentration factor hydrophobicity cutoff: An artificial 

2675 PAHs in phenomenon reconstructed 

aquatic worm ENVIRON. SCI. TECHNOL. 41, #21, 7363-7369 (01 NOV 2007) 

Jonker, M. T. O.; Van, Der Heijden S. A. 

668 TNT, 2,4-DNT, RDX 

Development of field screening methods for TNT, 2,4-DNT, 

and RDX in soil. 

in soil Talanta, 39: 419-28 (1992) 

T Jenkens, et al 

812 RDX, HMX 

Detection of the cyclic nitramine explosives hexahydro 

1,3,5-trinitro-1,3,5-triazine (RDX) and octahydro-1,3,5,7- 65µm PDMS/DVB GC-MS 

in soil tetranitro-1,3,5,7-tetrazine (HMX) and their degradation 20MIN @55°c LC-MS 

products in soil environments 

J Chromatog A (2001) 909(1), 53-60 

Hawari, J; Beaudet, S; Groom, C.; Halasz, A; Paquet, L 


344 explosives 

Trace Analysis of explosives in Seawater Using SPME and 

GC-Ion Trap Mass Spectrometry 65µm Carbowax/DVB GC-MS 

in salt water Anal. Chem., Vol. 70, No. 14, July 15, 1998, pg. 3015-3020 60 min 

Barshick, S., Griest, W. immersion 

stirring 

Solid-phase microextraction coupled to GCfor the determination 

2394 2,3-dimethyl-2,3- of 2,3-dimethyl-2,3-dinitrobutane as a marking agent for explosives headspace GC 

dinitrobutane Talanta 72, #4, 1581-1585 (2007-06-15) 30 sec @ 22°C 

from ammonium 

nitrate 

Li, X. J.; Zeng, Z. R.; Zeng, Y. 

Application of a SPME-IMS detection system for explosives detection 

2284 Explosives Proc SPIE Int Soc Opt Eng Vol 5778 #2, 667-672 (2005) headspace GC/IMS 

in open areas. Almirall, Jose R.; Furton, Kenneth G.; Perr, Jeannette M. 

Discrimination of smokeless powders by headspace SPME-GC-MS 

2285 Odors from and SPME-GC-ECD, and the potential implications upon training headspace GC-MS 

smokeless canine detection of explosives GC-ECD 

powders Proc SPIE Int Soc Opt Eng Vol 5778 #2, 638-643 (2005) 

Almirall, Jose R.; Furton, Kenneth G.; Harper, Ross J. 

2370 Explosives 

SPME-HPLC: A new approach to the analysis of explosives 

J. HAZARD. MATER. 14, # 3, 691-697 (2007) 

Gaurav; Kaur, V.; Kumar, A.; Malik, A. K.; Rai, P. K. 

65µm CW/DVB HPLC 


Application of SPME to the recovery of explosives and 

ignitable liquid residues from forensic specimens 65µm Carbowax/DVB GC-ECD 

from solids, water J. Chromatogr A, 885(2000) 419-432 25 min, 25% NaCl HPLC 

Furton, K., Almirall, J., Bi, M., Wang, J., Wu, L. immersion 

stirring 

592 explosives 

An improved interface for coupling SPME to HPLC 

applied to the analysis of explosives 50µm Carbowax/TPR HPLC-UV 





in water J-High-Resolut-Chromatogr. May 1999; 22(5): 279-282 

Wu,-L; Almirall,-JR; Furton,-KG 

254nm 


Optimization of SPME for the recovery of explosives from 

aqueous and post-explosion debris followed by gas and 65µm Carbowax/DVB GC-ECD 

from solids, water liquid chromatographic analysis 50µm Carbowax/TPR HPLC 

J. Forensic Sci. 45: 845-852 (2000) 30 min, 25% NaCl 

Furton, K., Wu, L., Almirall, J. immersion 

stirring 


Analysis of volatile components of drugs and explosives by SPMEion 

mobility spectrometry headspace GC-IMS 

explosives and Journal of Separation Science 31, #2, 402-412 (FEB 2008) 

drugs Lai, Hanh; Guerra, Patricia; Joshi, Monica; Almirall, Jose R. 

2766 VOCs from 

First results on headspace-SPME-GC-MS of volatile organic 

compounds emitted by wax objects in museums headspace GC-MS 

wax objects J. Chromatogr A, 1187, 239-249 (Apr 11 2008) 

Langlois, J.; Lattuati-Derieux, A.; Regert, M.; Thao, S. 

985 

Acetic acid and formic acid concentrations in the museum environment 

measured by SPME-GC/MS 

Acetic and formic acid 

in museum 

environment Atmospheric Environment (2002) 36 (24), 3909-3916 

Ryhl-Svendsen, M.; Glastrup, J. 


986 Explosives in soil 

Detection of explosives and their degradation products in soil environments. 

J.Chromatogr. A (2002) 963(1-2), 411-418 

Halasz, A.; Groom, C.; Zhou, E.; Paquet, L.; Beaulieu, C.; Deschamps, S.; 

Thiboutot, S.; Ampleman, G.; Dubois, C.; Hawari, J. 

GC-MS 

989 

990 

991 

Determination of methylmercury in human hair by ethylation followed by 

headspace SPME/GC 

Methylmercury in 

human hair J.Chromatogr. A (2002) 963(1-2), 345-351 

Diez, S.; Bayona, J.M. 

GC-CVAFS 

Methylmercury determination in biological samples by derivatization, SPME and 

GC. 

Methylmercury in 

biologicals J.Chromatogr. A (2002) 963(1-2), 313-323 

Rodil, R.; Carro, A.M.; Lorenzo, R. A.; Abuin, M.; Cela, R. 

PDMS GC-MS 

Automated headspace SPME and capillary GC analysis of ethanol in postmortem 

species. 

Ethanol in post-mortem 

samples. Forensic Science International (2002) 128(3), 115-119. 

de Martinis, B.S.; Santos Martin, C.C. 

Polyacrylate GC 

1003 L-methadone 

Fatal mixed intoxication caused by L-methadone and chloral hydrate. 

Archiv fuer Kriminologie (2003) 211 (3-4), 90-97. 

Weinmann, Wolfgang; Goerke, Rolf; Perdekamp, Markus Grosse; Thurau, 

Kirsten; Vogt, Susanne 

GC-MS 

2756 Semivolatile 

Determination of semi-volatile priority pollutants in landfill leachates 

and sediments using microwave-assisted headspace SPME headspace GC-MS 

pollutants in Analytical and Bioanalytical Chemistry 386, #2, 324-331 (2006-09-15) 

sediment Herbert, P.; Silva, A.; Joao, M.; Santos, L.; Alves, A. 

2624 Hydrophobic 

Desorption of hydrophobic compounds from laboratory-spiked 

Sediments measured by tenax absorbent and matrix SPME GC 

compounds from Env Sci & Tech 41, #16, 5672-5678 (AUG 15 2007) 

sediment You, Jing; Pehkonen, Sari; Landrum, Peter F.; Lydy, Michael J. 

Nonlinear sorption of three alcohol ethoxylates to marine sediment: 





2595 Alcohol ethoxylates A combined Langmuir and linear sorption process? 85µm Polyacrylate GC-MS 

in marine ENVIRON. SCI. TECHNOL.41, #9, 3192-3198 (01 MAY 2007) 

sediment Droge, S. T. J.; Hermens, J. L. M. 

1013 TNT in sediment 

Nondestructive, minimal-disturbance, direct-burial solid-phase microextraction 

fiber technique for measuring TNT in sediment 


Conder, Jason M.; La Point, Thomas W.; Lotufo, Guilherme R.; Steevens, 

Jeffery A. 

Polyacrylate 

Aplication of tandem mass spectrometry combined with gas chromatography 

and headspace solid-phase dynamic extraction for the determination of drugs of 

abuse in hair samples. 

Drugs of abuse in hair 

1025 samples. Rapid Communications in Mass Spectrometry (2003) 17 (5), 472-478. 

Lachenmeier, Dirk W.; Kroener, Lars; Madea, Burkhard; Musshoff, Frank 

PDMS GC-MS-MS 

1031 

Fatty acid ethyl esters in scalp, pubic, axillary, beard and body hair as markers 

for alcohol misuse. 

Fatty acid esters in 

hair. Alcohol and Alcoholism (2003) 38 (2), 163-168. 

Pragst, Fritz; Auwaerter, Volker; Hartwig, Sven 

1033 

Investigation by solid-phase microextraction and gas chromatography/mass 

spectrometry of secondary metabolites in lichens deposited on stone 

monuments. 

Rapid Communications in Mass Spectrometry (2003) 17 (6), 526-531. 

Di Tullio, Alessandra; De Angelis, Francesco; Ceci, Roberta; Quaresima, 

Raimondo; Reale, Samantha 

GC-MS 

ASTM standards for fire debris analysis: A review. 

1079 Review article Forensic Science International (2003) 132 (1), 63-67. 

Stauffer, Eric; Lentini, John J. 

1135 Cannabinoids in hair. 

Fully automated determination of cannabinoids in hair samples using 

headspace solid-phase microextraction and gas chromatography-mass 

spectrometry. 

Journal of Analytical Toxicology (2002) 26 (8), 554-560. 

Musshoff, F.; Junker, H. P.; Lachenmeier, D. W.; Kroener, L.; Madea, B. 

GC-MS 

Application of tandem mass spectrometry combined with gas chromatography 

and headspace solid-phase dynamic extraction for the determination of drugs of 

abuse in hair samples. 

1242 Drugs of abuse in hair. Rapid Communications in Mass Spectrometry (2003) 17 (5), 472-478. GC-TMS 

Lachenmeier, D. W.; Kroener, L.; Musshoff, F.; Madea, B. 

Development of a GC/MS method for detection of gamma-hydroxybutyric acid 

(GHB) and its precursors. 

Gamma-hydroxybutyric 

1273 acid Abstracts of Papers American Chem Society (2003) 225 (1-2), CHED 209. 

Helwig, Katie; Dema, Anne C.; Wetmore, Lori A. 

GC-MS 

Detection of thiopental and pentobarbital in head and pubic hair in a case of 

drug-facilitated sexual assault. 

Thiopental and 

1286 pentobarbital in hair. Forensic Science International (2003) 133 (1-2), 171-174. 

Ferrara, Santo Davide; Favretto, Donata; Frison, Giampietro; Tedeschi, Luciano 

GC-MS-MS 

Headspace SPME of cannabinoids in human head hair samples. 

2696 Cannabinoids J. Sep. Sci. 30, #1, 128-134 (2007-01) headspace GC-MS 

in hair. Rodrigues de Oliveira, C. D.; Yonamine, M.; de Moraes Moreau, R. L. 

1287 Cannabinoids in hair. 

Automated headspace solid-phase dynamic extraction for the determination of 

cannabinoids in hair samples. 

Forensic Science International (2003) 133 (1-2), 32-38. GC-MS 

Musshoff, Frank; Kroener, Lars; Lachenmeier, Dirk W.; Madea, Burkhard 





Simultaneous detection of some drugs of abuse in saliva samples by SPME 

technique. 

Drugs of abuse in 

1293 saliva Forensic Science International (2003) 134 (1), 40-45. 

Fucci, Nadia; Chiarotti, Marcello; De Giovanni, Nadia 

GC/MS 

SPME on-fiber derivatization of gamma-hydroxybutyric acid (GHB) in forensic 

analysis. 

1509 Gamma-hydroxybutyric 

Abstracts of Papers American Chem Society (2002) 223(1-2), ANYL 134 

acid (GHB) 

Meyers, Jodi E.; Almirall, Jose R.; Galiana, Gigi 

SPME/GC-MS characterization of volatiles associated with methamphetamine: 

Toward the development of a pseudomethamphetamine training material. 

1548 Methamphetamine Journal of Forensic Sciences (2002) 46(5), 1014-1024 

Vu, Doan-Trang T. 

GC-MS 

1550 

Determination of gamma-hydroxybutyrate in water and human urine by solid 

phase microextraction-gas chromatography/quadrupole ion trap spectrometry. 

Gammahydroxybutyrate 

(GHB) Journal of Forensic Sciences (2002) 46(3), 688-693 

in human urine 


Brodbelt, Jennifer; Blair, Sheryl; Hall, Brad; Song, Meansup 

Identification of canis familiaris active odor signature chemicals in controlled 

substances and high explosives. 

1235 Odor chemicals Abstracts of Papers American Chemical Society (2003) 225 (1-2), PRES 25. 

from explosives Lopez, Claudia; Furton, Kenneth G.; Harper, Ross; Hsu, Ya-Li; Walton, John 

1328 Odor chemicals 

Laboratory and field experiments used to identify Canis lupus var. familiaris 

active odour signature chemicals from drugs, explosives, and humans. 

Analytical and Bioanalytical Chemistry (2003) 376 (8), 1212-1224. 

Lorenzo, N.; Wan, T. L.; Harper, R. J.; Hsu, Y. L.; Chow, M.; Rose, S.; Furton, 

CW/DVB and PDMS GC-ECD & GC-MS 

from explosives K. G.* 

Chemical signatures of TNT-filled land mines. 

TNT isomers from land 

1556 mines Talanta 54(3), 2001, 501-514. 

Jenkins, T; Leggett, D; Miyares, P.; Walsh, M.; Ranney, T.; Cragin, J.H.; 

George, V. 

Headspace 

The scientific foundation and efficacy of the use of canines as chemical 

detectors for explosives. 

Odor chemicals from 

1557 explosives. Talanta 54(3), 2001, 487-500. 

Furton, K.G.; Myers, L.J. 

2683 Leachable 

Assessing the aquatic hazard of commercial hydrocarbon resins 

ECOTOXICOL. ENVIRON. SAF. 66, #2, 159-168 (2007) GC 

organics from Woods, R. W.; Letinski, D. J.; Febbo, E. J.; Dzamba, C. L.; . 

hydrocarbon resins Connelly, M. J.; Parkerton, T. F 

Headspace SPME for screening for the presence of 

1897 Terpenes in resins in Egyptian archaeological samples. headspace GC 

resins J Separation Sci, 27, #3, 235-243 

Hamm, Sandrine; Bleton, Jean; Tchapla, Alain 

Improvements in the methylmercury extraction from 

1898 Methyl human hair by headspace SPME followed by GC- headspace GC-cold vapour 

mercury from cold-vapour atomic flourescence spectrometry ethyl derivative atomic spectrometry 

human hair J Chromatogr A, 1025, #1, 71-75 

Montuori, P; Jover, E; Alzaga, R; Diez, S; Bayona, J. 





Transport of explosives TNT in soil and its 

1899 TNT in sand equilibrium vapor Headspace for 20min TEEM-GC/MS 

Proc SPIE Int Soc Opt Eng, 5415, #2, 1389-1399 immersion in GC/ECD 

Baez, B; Briano, J; Castro, M.; Correa, S; De Jes, M.; water extract 

Hernandez-Rivera, Samuel P.; Mina, Nairmen 

Oxidation of TNT by photo-Fenton process 

1900 Oxidation Chemosphere, 57, #9, 1107-1114 GC-MS 

byproducts of Chen, Jong-Nan; Liou, Ming-Jer; Lu, Ming-Chun 

TNT 

New developments in SPME. Part 2: analysis of 

1901 Ammonium ammonium nitrate-based explosives. Alkylchloroformate GC-MS 

nitrate J Forensic Sci, 49, #2, 215-221 derivative 

explosive Brown, H.; Kirkbride, K.*; Pigou, P. .; Walker, G. 

Laboratory and field experiments used to identify Canis 

1902 Signature odor lupus var. familiaris active odor signature chemicals 50µm CW/DVB GC/MS 

explosives from drugs, explosives, and humans PDMS coatings GC/ECD 

drugs, and Anal. Bioanal. Chem., 376, #8, 1212-1224 

humans Chow, M.; Furton, K.; Harper, R.; Hsu, Ya-Li.; 

Lorenzo, N.; Rose, S.; Wan,T. 

GC-MS analysis of triacetone triperoxide (TATP) degradation products 

2884 TATP Rapid Commun, Mass Spectrom 22, #7 950-958 (2008) headspace GC/MS 

degradation Armitt, David; Zimmermann, Peter; Ellis-Steinborner, Simon 

products 

Improved method for the detection of TATP after explosion 

1903 TATP in J Forensic Sci, 49, #5, 935-938 65µm PDMS-DVB GC/MS 

post Muller, D.; Levy, A.; Shelef, R.; Abramovich-Bar, S.; headspace 

explosives Sonenfeld, D.; Tamiri, T. 

Analysis of gamma-hydroxybutyric acid (GHB) in spiked 

1904 GHB in water water and beverage samples using SPME on fiber derivative on-fiber GC-MS 

derivatization/gas chromatography-mass spectrometry 

J Forensic Sci, 50, #1, 31-36 

Meyers, Jodi E.; Almirall, Jose R. 

Evaluation of a combined fractionation and speciation approach for 

2767 Organtin study of size-based distribution of organotin species on headspace GC-PFPD 

in landfill leachate environmental colloids 

Anal. Bioanal. Chem. 390, #7, 1805-1813 (April 2008) 

Dubascoux, S.; Heroult, J.; Le Hecho, I.; Lespes, G.; Potin-Gautier, M. 

Influence of the soil matrices on the analytical performance of 

2749 Organtin headspace SPME for organotin analysis by GC-pulsed FPD 100µm PDMS GC-PFPD 

in soil J. Chromatogr. A 1132, #1-2, 234-240 (2006-11-03) headspace 

Zuliani, T.; Lespes, G.; Milacic, R.; Scancar, J.; Potin-Gautier, M. 

Solid phase microextraction with GC/MS for the 

1905 Explosives trace analysis of explosives GC-MS 

in soil, water, Proc. 50th ASMS Conf. Mass Spectrom. Allied Top. GC-ECD 

and swab 2002, p669-670 

samples Maslanka, D; McDonald, J.; Miller, M. 

Wipe-test and patch-test for alcohol misuse based 

1906 FAEE from on the concentration ratio of fatty acid ethyl esters headspace GC-MS 

skin samples and squalene C FAEE / C SQ in skin surface lipids. LC-PDA 

Forensic Sci Intl, 143, #2-3, 77-86 

Pragst, F.; Auwaerter, V.; Kiessling, B.; Dyes, C. 

Headspace SPME for the GC analysis of methyl- 

1907 Methyl parathion in postmortem human samples: application 85µm polyacrylate GC-NPD 

parathion in a suicide case by intravenous injection. headspace 

in biological Forensic Sci Intl, 143, #2-3, 127-132 salt added 

samples Tsoukali, H.; Raikos, N.; Theodoridis, G.; Psaroulis, D. 

Detection of cocaine and cocaethylene in sweat 

1908 Cocaine in by SPME-GC-MS immersed in 0.2M GC-MS 

sweat J. Chromatogr. B, 811, #1, 37-40 sodium acetate buffer 

Follador, M; Moreau, R; Silva, O.; Yonamine, M. pH 5 

2750 Hydroxy 

Determination of hydroxy metabolites of PAHs by fully automated 

SPME derivatization and gas chromatography-mass spectrometry immersion GC-MS 

metabolites of J. Chromatogr. A 1173, #1-2, 37-43 (30 Nov 2007) BTSF derivative 





PAHs Luan, T.; Fang, S.; Zhong, Y.; Lin, L.; Chan, S. M. N.; Lan, C.; Tam, N. 

identification of gasoline soot in suspect arson 

1909 PAHs in cases by using headspace SPME-GC-MS 100µm PDMS GC-MS 

gasoline soot Analytical Letters, 236, #7, 1373-1384 75µm Carboxen 

Wu, Chia-Hao; Chen, Chin-Lien; Huang, Ching-Te; heaspace 

Lee, Maw-Rong; Huang, Chih-Ming 

Quantification of propane in biological materials 

1910 Propane in by headspace GC headspace GC-MS 

biological Forensic Science International, 151, #2-3, 165-170 

materials Park, J; Min, Ji-Sook; Heo, S.; Lim, Mi-Ae; Park, S 

The study of fingerprint characteristics of the emanations 

1911 Volatile from human arm skin using the original sampling headspace GC-MS 

organics system by SPME-GC-MS 30min sampling 

from human J. Chromatogr. B, 822, #1-2, 244-252 

skin Cai, Ji-Jin; Li, Gong-Ke; Ruan, Gui-Hua; Zhang, Zhuo-Min 

Extraction of capsaicin in aerosol defense sprays from fabrics 

1912 Capsaicin Talanta, 67, #2, 377-382 headspace GC 

from fabrics Almirall, Jose R.; Spicer Jr., Oliver 

Identification of dominant odor chemicals emanating from 

1913 Odor explosives for use in developing optimal training aid headspace GC-MS 

chemicals in combinations and mimics for canine detection GC-ECD 

explosive Talanta, 67, #2, 313-327 

Almirall, Jose R.; Furton, Kenneth G.; Harper, Ross J. 

Evaluation of sample recovery of malodorous gases from air 

2235 Odorous gases sampling bags, SPME, and sampling canisters 75µmCarboxen GC/MS 

from livestock Annu. Int. Meet., (2004) p5547-5562 headspace 

operations Koziel, J.; Kuhrt, F.; Lloyd, J.; Parker, D.; Spinhirne,J.; Wright,D. 

Evaluation of sample recovery of malodorous livestock gases from 

2265 Malodorous gases air sampling bags, SPME fibers, Tenax TA sorbent tubes, 75µm Carboxen GC/MS 

from livestock and sampling canisters headspace 

J. Air Waste Manage. Assoc. 55, #8, 1147-1157 (2005) 

Koziel, J.; Kuhrt, F.; Lloyd, J.; Parker, D.;Spinhirne, J.; Wright, D. 

2657 Volatiles found 

Headspace-SPME preconcentration of phenols, indoles and on-fibre 

derivatised volatile fatty acids in liquid and gas samples from cow slurries DVB/Car 50/30µm GC/MS 

in cow slurry J. Sep. Sci. 30, #14, 2293-2304 (September 2007) headspace 

Arana, G,; Larreta, J.; Vallejo, A.; Bilbao, U.; Alonso, A.; Zuloaga, O. 

Optimisation of the on-fibre derivatisation of volatile fatty acids in the 

MTBSTFA 

derivative 

2588 Volatiles found simultaneous determination together with phenols and DVB/Car 50/30µm GC 

in cow slurry indoles in cow slurries headspace 

Anal Bioanal Chem 389, #5, 1603-1609 (NOV 2007) MTBSTFA 

Larreta, J.; Usobiaga, A.; Etxebarria, N.; Arana, G.; Zuloaga, O. derivative 

Experimental design to optimise the analysis of organic volatile 

2459 Volatiles found compounds in cow slurry by headspace SPME-GC-MS 100µm PDMS GC/MS 

in cow slurry J. Chromatogr., A 1136, #1, 1-9 (2006-12-08) 75µm Carboxen 

Larreta, J.; Vallejo, A.; Bilbao, U.; Alonso, A.; Arana, G.; Zuloaga, O. headspace 

Methylation 

2477 Odor from 

Identification of volatile organic compounds in the manures of cow, 

hog and chicken by SPME-GC-MS 65µm PDMS-DVB GC-MS 

manures Se Pu 25, #3, 425-9 (2007 May) 30 min at 60°C 

Huang, Jun; He, Jin; Zhang, Jibin; Yu, Ziniu 

sat.NaCl 

headspace In chinese 

Multidimensional GC-olfactometry for the identification and 

2221 Malodors of prioritization of malodors from confined animal feeding operations GC-MS 

livestock operations J Ag Food Chem, 53, #22, 8663-8672 (2005) 

Wright, D.; Eaton, D..; Nielsen, L.; Kuhrt, F.; Koziel, J.,. 

Spinhirne, J.; Parker, D 

2316 Odor from 

Effect of ozonation on odor and the concentration of odorous 

organic compounds in air in a swine housing facility air sampling GC 

swine Trans. Am. Soc. Agric. Eng. 48 #6, 2297-2302 (2005) 

facilities Davies, S.H.; Hill, J.D.; Kim-Yang, H.; Von Bernuth, R.D. 





Analysis of odorous compounds in swine buildings and their 

2144 Odor from relationship to thermal environment, management and Air sample GC/MS 

swine categories of pigs 

facilities Livestock Environ. Proc. Seventh Int. Symp 334-340 (2005) 

Dahl, P.; Johnsen, J.; Maahn, M.; Segaard, H.;Takai, H.; Tegersen, F. 

Simultaneous chemical and sensory characterization of volatile organic 

2759 Odor from compounds and semi-volatile organic compounds emitted from swine 85µm Carboxen GC/MS 

swine manure manure using SPME and multidimensional GC-MS-olfactometry headspace 

J. Environ. Qual. 37, #2, 521-534 (2008) 

Cai, L.; Hoff, Steven J.; Jenks, W.; Koziel, Jacek A.; Lo, Yin-Cheung M.; 

Xin, Hongwei 

Characterization of volatile organic compounds and odorants 

2161 Volatiles in associated with swine barn particulate matter using SPME-MS- 75µm Carboxen GC-MS 

swine particulate olfactometry headspace 

matter J. Chromatogr. A, 1102, #1-2, 60-72 (2006) 

Cai, Lingshuang; Koziel, Jacek A.; Lo, Yin-Cheung; Hoff, Steven J. 

Environmental 

1914 Auto exhaust 

Formation and reaction of hydroxycarbonyls from the 

reaction of OH radicals with 1,3-butadiene and isoprene pentafluorobenzyl API-MS 

Environ. Sci. Technol., 39. #11, 4091-4099 hydroxyl amine GC/FID 

Arey, Janet; Atkinson, Roger; Baker, Jillian derivatives 

Photochemical sources of organic acids. 1. Reaction 

1915 Carboxylic of ozone with isoprene, propene, and 2-butenes headspace GC-MS 

acids under dry and humid conditions using SPME 

in air J Phys Chem A, 109, #24, 5358-5365 

Orzechowska, Grazyna; Paulson, Suzanne 

Rate coefficients for the gas-phase reaction of 

1916 Byproducts isoprene with N0 3 and NO 2 headspace GC/FID 

of reactions Int J Chem Kinet, 37, #2, 57-65 

Johnson, M.; Langer, S.; Stabel, J. 

1,4-Hydroxycarbonyl products of the OH radical initiated 

1917 Hydroxyl- reactions of C5-C8 n-alkanes in the prescence of NO on-fiber hydroxylamine GC-MS 

carbonyls Environ. Sci. Technol., 39. #12, 4447-4453 derivatives GC/FID 

in Air Arey, Janet; Aschmann, Sara M.; Atkinson, Roger; Reisen, F 

Occurrence and abatement of volatile sulfur 

1918 Volatile sulfur compounds during biogas production headspace GC-MS 

from biogas J. Air Waste Manage. Assoc, 54, #7, 855-861. 

production Andersson, F.; Ejlertsson, J.; Karlsson, A.; Svensson, B. 

Headspace SPME followed by GC/PFPD for the analysis of 

1920 Sulfur compd malodorous sulfur compounds liquid industrial effluents 65µm PDMS-DVB GC/PFPD 

industrial Anal and Bioanal Chemistry, 378, #1, 190-196 75µm Carboxen 

effluents Desauziers, V.; Fanlo, Jean-Louis; Lestremau, F. 5 or 60 min 

headspace 

Air/polymer distribution coefficients for 

1921 PAHs in PAHs by SPME sampling. PDMS coated fibers GC-MS 

air J Chromatography, A, 1029, #1-2, 263-266 

Kolar, K.; Ciganek, M.; Malecha, J. 

Selective extraction of trace levels of polychlorinated and 

1922 Organo- polybrominated contaminants by supercritical fluid-SPME and GC/MS/MS 

halogenated determination by GC-MS. Application to aquaculture fish 

in fish feed feed and cultured marine species 

Anal. Chem., 77, #7, 2259-2265 

Carro, A.M.; Lorenzo, R.A.; Rodil, R.; Torrijos, R. Cela 

Round-robin evaluation of a SPME-GC for reliable determination of 

2389 Ethylene oxide trace level ethylene oxide in sterilized medical devices GC 

in air Biomed Chromatogr: 22, #2, 136-48 (-2008 Feb) 

Harper, T.; Cushinotto, L.; Blaszko, N.; Arinaga, J.; Davis, F.; 

Cummins, C.; Dicicco, M. 

Laboratory and field validations of a SPME 

1923 Ethylene oxide device for the determination of ethylene oxide. 75µm Carboxen GC 

in air J Chromatogr A, 1026, #1-2, 25-30 HBr on-fiber derivative 





Tsai, S; Tsai, S; Wang, V; Lai, J 25°C 

Isotope dilution SPME GC/MS for the determination of 

2187 Methylmercury methylmercury in tuna fish samples headspace GC-MS 

in tuna fish J. Mass Spectrom. 41, #1, 77-83 (2006) 15 min 

Centineo, G.; Garcia A., J.; Gonzalez, E. Sanz-Medel, A. NaEt4B 

derivatives 

Blank correction considerations for isotope dilution and 

1924 Methyl reverse isotope dilution calibration: Determination of GC-ICP-MS 

mercury from methylmercury in fish tissue 

fish tissue J of Anall Atomic Spectrometry, 20, #8, 724-729 

Yang, Lu; Sturgeon, Ralph E. 

Selective determination of PCBs in waste oils using 

1925 PCBs in liquid-liquid partition followed by headspace SPME 65µm PDMS-DVB GC-AED 

waste oil and GC with atomic emission detection headspace 

J. Chromatogr. A,1056, #1-2, 263-266 

Cela Torrijos, R.; Ramil Criado, M.; 

Rodriguez Pereiro, I. 

Confirmation of the formation of dichlorodibenzo-p- 

1926 Degradation dioxin in the photodegradation of triclosan by photo-SPME 100µm PDMS GC-EI/MS 

byproducts Anal. Bioanal. Chem., 381,#6, 1294-1298 headspace 

of triclosan Cela, R.; GarciaJares, C.; Llompart, M.; 

Lores, M.; SanchezPrado, L. 

Degradation and corrosive activities of fungi in a diesel-mild 

1927 Acids from steel-aqueous system headspace @ 30°C GC 

diesel fuel World J Microbiology & Biotechnology, 21, #2, 135-142 

Bento, F.; Beech, I.; Gaylarde, C.; Englert, G.; Muller,I. 

Determination of PCBs in ash using dimethylsulfoxide 

1928 PCBs in microwave assisted extraction followed by SPME 65µm PDMS-DVB GC-ECD and GC-MS 

ash Talanta, 63, #3, 533-540 headspace 

Criado, M.; Pereiro, I. ; Torrijos, R. stirring 

Solid phase microextraction combined with gas chromatography - A 

2508 Chemical powerful tool for the determination of chemical warfare agents and related review article 

warfare agents CURR. ORG. CHEM. 11, #3, 241-253 (2007) 

Zygmunt, B.; Zaborowska, A.; Swiat&lstrok;owska, J.; Namiesnik, J. 

LC electrospray tandem MS and desorption electrospray 

2196 Chemical ionization tandem MS analysis of chemical warfare agents LC-MS 

warfare agents in office media typically collected during a forensic investigation 

(TEP, GB and GD) J. Chromatogr. A, 1110, #1-2,86-94 (2006) 

on office media Chenier, C.L.; D'Agostino, P.A.; Hancock, J.R.; Lepage, C.R. Jackson 

2165 Chemical warfare 

Closed tube sample introduction for gas chromatography-ion 

mobility spectrometry analysis of water contaminated with a headspace IMS 

agent surrogate chemical warfare agent surrogate compound 

from water Anal. Chim. Acta, 556, #2, 455-461 (2006) 

Erickson, R.; Tripathi, A; Maswadeh, W.; Snyder, A.; Smith, P. 

Detection of gas-phase chemical warfare agents 

1929 Chemical using field-portable GC-MS systems: instrument direct air sampling GC-MS 

warfare agemt and sampling strategy considerations. 

in air Trends in Anal Chem, 23, #4, 296-306 

Smith, P.; Lepage, C.; Koch, D.; Wyatt, H., Hook, G.; 

Betsinger, G.; Erickson, R., Eckenrode, B. 

Towards smaller and faster GC-MS systems 

1930 Chemical for field chemical detection




water J Env Sci and Health 42, #5, 491-498 (2007) 40 min @ 70°C 

Lancas, Fernando M.; Olivares, Igor R. B.; Alves, Priscila M. sat salt 

SPME-GC-MS for analysis of phenols and nitrophenols in rainwater, 

2381 Phenol and as their t-butyldimethylsilyl derivatives 50µm PA GC-MS 

nitrophenol in Analytical and Bioanalytical Chemistry 38, # 7; 40 min @ 22°C 

rainwater Conference 10. 2527-2535 (2007-04-15 ) t-butyldimethylsilyl 

Jaber, F., Schummer, C., Mirabel, P., Millet, M., Chami, J. derivatives 

75 g NaCl, ph 3 

Assessment of the matrix effect on the headspace (HS-SPME) 

2745 Chlorophenol in analysis of chlorophenols in wines. headspace GC-ECD 

wine J. Sep. Sci. 30, #5, 722-730 (2007-03) GC-MS 

Insa, S.; Besalu, E.; Salvado, V.; Antico, E. 

Recent trends in the use of organized molecular systems combined 

2858 Organics from with chromatographic techniques in environmental analysis Review article 

environmental Anal. Bioanal. Chem. 391, #3, 725-733 (June 2008) 

samples Ferrera, Zoraida Sosa; Moreno, Daura Vega; Padron, M. Esther Torres; 

Rodriguez, Jose Juan; Santana; Santana, Cristina Mahugo 

Implementation of SPME with micellar desorption method for 

2799 Phenols in priority phenolic compound determination in natural waters 

natural water J. Chrom Sci., 46, #4, 325-331 (APR 2008) 

Padron, M. ; Santana, C.; Ferrera, Z. Sosa; Rodriguez, J. 

2438 Chlorophenol in 

Development of a SPME method with micellar desorption for the 

determination of chlorophenols in water samples: Comparison with HPLC-DAD. 

water conventional SPME method 

J. Chromatogr., A 1140, #1-2, 13-20 (2007-01-26) 

Mahugo Santana, C.; Torres Padron, M.; Sosa Ferrera, Z.; 

Santana Rodriguez, J. 

Monitoring chlorophenols in industrial effluents by SPME-GC-MS 

2396 Chlorophenol in Int. J. Environ. Anal. Chem. 87, #3, 159-175 (2007-03-15) 85µm PA GC-MS 

water Pino, V.; Ayala, J. H.; Gonzalez, V.; Afonso, A. M. 50µm CW 

Experimental and statistical validation of SPME-GC-MS analysis of r 

2374 Phenol and phenol and chlorophenols in raw and treated wate 85µm PA GC-MS 

chlorophenol in Chemosphere 68, #3, 501-510 (JUN 2007) 40 min @ 35°C 

water Simoes, N.; Cardoso, V.; Ferreira, E.; Benoliel, M. 10% NaCl, pH 4.0 

Enhanced extraction capacity and chemical noise 

1932 Phenols from reduction in SPME review of fibers GC/MS 

water J Separation Science, 27, #17-18, 1517-1523 

Moeder, Monika; Schrader, Steffi 

SPME-GC-MS determination of nitrous oxide evolution to measure 

2560 Nitrous oxide denitrification in estuarine soils and sediments GC-MS 

in sediment J. Chromatogr. A, 1133, #1-2, 300-304 (2006-11-10) 

Drescher, S. R.; Brown, S. D. 

Identification of sulfur interferences during organotin 

1933 Sulfur determination in harbour sediment samples by GC-FPD 

compounds NaEt4B ethylation and GC-pulsed FPD NaEt 4B derivatives 

in sediment flame photometric detection 

J. Chromatogr. A, 1046, #1-2, 217-224 

Bravo, M; Gregori, I Lespes, G; Pinochet, H; Potin-Gautier, M 

Flavour profile of capers (Capparis spinosa L.) from the Eolian 

2581 Flavor volatiles Archipelago by HS-SPME/GC-MS headspace GC-MS 

from capers Food Chemistry 101, 1272-1278 #3, (2007) 

Romeo, V; Ziino, M.; Giuffrida, D.; Condurso, C.; Verzera, A. 

SPME method for the determination of volatile compounds 

2893 Volatiles in associated to oxidation of fish muscle 75µm Carboxen GC-MS 

fish muscle J. Chromatogr. A, 1192, #1, 9-16 (May 23 2008) headspace 

Iglesias, Jacobo; Medina, Isabel 30 min at 60 °C 

saline extraction 

Characterisation of the volatiles of yellowfin tuna (Thunnus albacares) 

2552 Volatiles in during storage by SPME- GC-MS and their relationship to headspace GC-MS 

tuna fish fish quality parameters 

Intl J Food Sci Tech 42, #10, 1139-1147 (2007) 

Edirisinghe, R. K. B.; Graham, A. J.; Taylor, S. J. 





Oxidatively derived volatile compounds in microencapsulated fish oil 

2278 Volatiles in monitored by SPME PDMS/DVB GC-FID 

fish oil J Food Science 70 #7, C433-C440 (2005) headspace 

Jonsdottir, Rosa; Bragadottir, Margaret; Arnarson, Gudmundur Orn 

Determination of mono- to octachlorobiphenyls in 

1934 Biphenyls fish oil using Florisil adsorption followed by 65µm PDMS-DVB GC-TOF-MS 

in fish oil headspace SPME-GC with TOF-MS headspace 

J. Chromatogr. Am 1085, #2, 278-284 

Agustin, M.; Hong, S; Lee, K.; Park, H.; Ryu, Jae-Ch 

The comparison of SPME-GC and static headspace-GC 

2805 Solvent residue in for determination of solvent residues in vegetable oils 85µm CAR/PDMS GC-FID 

vegetable oil Journal of Separation Science 31,#2, 364-371 (Feb 2008) headspace 

Ligor, Magdalena; Buszewski, Boguslaw 

Rapid validated method for the analysis of benzo a pyrene in vegetable 

2700 Benzo-a-pyrene in oils by using SPME-gas chromatography-mass spectrometry. headspace GC-MS 

vegetable oil J. Chromatogr., A 1176, #1-2, 231-235 (2007) 

Purcaro, G.; Moret, S.; Conte, L. S. 

Determination of PAHs in vegetable oils using SPME-comprehensive 

2453 PAHs in two-dimensional GC coupled with time-of-flight MS immersed GC-TOF-MS 

vegetable oil J. Chromatogr., A 1150, #1-2, 173-177 (2007-05-25) 

Wejnerowska, G.; Karczmarek, A.; Gaca, J 

Evaluation of spme conditions for the determination of PAHs 

2868 PAHs in in aquatic species using gas chromatography 65µm PDMS-DVB GC-MS 

aquatic species Anal. Bioanal. Chem. 391, #4, 1419-1424 (June 2008) 75°C for 60 min 

Aguinaga, N.; Campillo, N.; Hernandez-Cordoba, M.; Vinas, P. headspace 

A headspace SPME procedure coupled with for the analysis of 

2866 PAHs in volatile polycyclic aromatic hydrocarbons in milk samples 65µm PDMS-DVB GC-MS 

milk Anal. Bioanal. Chem. 391, #3, 753-758 (June 2008) 75°C for 60 min 

Aguinaga, N.; Campillo, N.; Hernandez-Cordoba, M.; Vinas, P. headspace 

Determination of 16 polycyclic aromatic hydrocarbons in milk and 

2448 PAHs in related products using SPME-GC-MS 65µm PDMS-DVB GC-MS 

milk Anal. Chim. Acta 596, #2, 285-290 (2007-07-23) immersed 

Aguinaga, N.; Campillo, N.; Hernandez-Cordoba, M. ; Vinas, P. 60 min at 55°C 

Analysis of polycyclic aromatic hydrocarbons in solid matrixes by 

2423 PAHs in solid-phase microextraction coupled to a direct extraction device 100µm PDMS GC-MS 

smoked meat Talanta 71, #2, 751-757 (2007-02-15) 65µm PDMS-DVB 

Martin, D.; Ruiz, J. 25°C for 60 min 

headspace 

Behaviour of polycyclic aromatic hydrocarbons in dissolved, 

2720 PAHs in colloidal, and particulate phases in sedimentary cores GC-MS 

sediment Intl J Env Analyt Chem 87, #3, 211-225 (2007) 

King, A. J.; Readman, J. W.; Zhou, J. L. 

Electronic nose and SPME techniques to monitor phenanthrene 

2782 Phenanthrene in biodegradation in soil headspace 

soil Sens Actuators, B Chem 131, #1, 63-70 (Apr 14 2008) 

De Cesare, F.; Macagnano, A.; Pantalei, S.; Zampetti, E. 

Comparison of techniques for estimating PAH bioavailability: uptake 

2650 PAHs in in Eisenia fetida, passive samplers and leaching using various s GC 

soil olvents and additives. 

Environ Pollut 145, #1, 154-60 (2007 Jan) 

Bergknut, M.; Sehlin, E.; Lundstedt, S.; Andersson, P.; 

Haglund, P.; Tysklind, M. 

SPME and GC-MS for the determination of PAHs in 

1935 PAHs in environmental solid matrices. 100µm PDMS GC-MS 

soil/seaweed Jl of Chromatographic Sci, 42, #6, 329-335 immersed liquid carrier 

Cam, D.; Gagni, S.; Lombardi, N.; Punin, M. 

SPME coupled with HPLC using on-line diode-array and 

2266 Fenitrothion electrochemical detection for the determination of fenitrothion and HPLC 

in water its main metabolites in environmental water samples 

J. Chromatogr. A, 1094 #1-2, 70-76 (2005) 

Barrio,R.; Goicolea, M.; Sampedro, M.; Sanchez-Ortega, A.; Unceta,N. 





Sensitive method for the determination of roxarsone using 


1936 Roxarsone w/ SPME multi-detector gas chromatography 65µm PDMS-DVB GC-MS 

in water J Chromatogr A, 1057, #1-2, 177-183 15min @ 70°C GC-PFPD 

Aldstadt III, Joseph H.; Roerdink, Aaron R. 

Speciation of volatile selenium species in plants using 

1,3-propanedithiol 

derivatives 

1937 Selenium GC-ICP-MS headspace GC-ICP-MS 

from plants Sepu, 22, #1, 16-19 

Meija, J.; Montes-Bayon, M.; Caruso, J.; Leduc, D.; Terry, N. 

Analysis of sulfur & nitrogen odorants using SPME and GC-MS 

1938 Sulfur & N2 Water Sci. Technol., 50, #4, 115-120 headspace GC-MS 

odorants in Chiu, P.C.; Dentel, S.K.; Hepner, S.; Turkmen, M. 

biomass 

Identification of metallic-smelling 1-octen-3-one and 1-nonen-3-one 

2303 Odorants from from solutions of ferrous sulfate headspace GC 

FeSO4 solutions. J Ag Food Chem, 53, #21, 8325-8327 (2005) (1, 5, and 16 h) 

Lubran, Meryl B.; Lawless, Harry T.; Lavin, Edward; Acree, Terry E. 22° and 37°C 

Characterization of odors from limed biosolids treated 

1939 Odors from with nitrate and anthraquinone headspace GC-MS 

biosolids J. Environ. Sci. Health, 40, #1, 139-149 

Abu-Orf, M; Choi, H.; Kim, H.; McConnell, L.; 

Peot, C.; Ramirez, M. 

Contamination of toxic volatile and semi-volatile compounds 

2214 Organics from from automobile materials 

automobile Bul Envn Contamination and Toxicology 76, #2, 301-305 (2006) 

materials Zhou, S.; Huang, J. X.; Kinkel, J.; Stark, W. 

Sampling and analysis of volatile organic pollutants emitted 

1940 Organics by an industrial stack 85µm polyacrylate GC-MS 

in stack Anal. Chim. Acta, 524, #1-2, 51-62 headspace 

emmisions Campo, L.; Domeno, C.; Martinez-Garcia, Fca.; Nerin, C. 

Quantitative determination of volatile organic compounds in 

1941 Volatile indoor dust using gas chromatography-UV spectrometry headspace GC-UV 

organics in Environ. Int., 31, #8, 1141-1148 

dust Bornehag, C; Lagesson, V; Nilsson, A; Sundell, J; Tagesson, C 

Analysis of volatile components in concrete by 

1942 Volatiles SPME-GC-Mass Spetrometry 50/30µm DVB/CAR GC-MS 

in concrete Zhipu Xuebao, 25, #4, 225-228 65°C, headspace 

Liao, K. 

Identification of volatile components in yunyan and yanmo 

1943 Volatiles concrete by SPME -GC-MS headspace GC-MS 

in concrete Zhipu Xuebao, 25, #1, 32-37 

Zhu, S. M.; Li, J.; Lin, P. 

Chlorophenols in leachates originating from different landfills 

1944 Chlorophenols and aerobic composting plants headspace GC-FID 

from landfills J. Hazard. Mater., 124. #1-3, 107-112 

Ozkaya, Bestamin 

GC analysis of organic marker compounds in fine particulate 

2694 Organics matter using solid-phase microextraction 75µm Carboxen GC-MS 

from J Air Waste Manag Assoc. 57, #1, 53-58 (2007 Jan,) 30min headspace 

particulate Lin, Lin; Lee, Milton L; Eatough, Delbert J 

Qualitative analysis of organics in atmospheric 

1945 Organics particulates by headspace SPME-GC/MS 100µm PDMS GC-MS 

from Atmos. Environ., 38, #40, 6917-6925 10min headspace 

particulate Khanal, O.; Shooter, D. 

Current trends in SPME techniques for the determination of 

2653 Pesticides pesticides in food and environment Review 

from soil J Biochem Biophysical Methods 70, #2, 117-131 (MAR 10 2007) 

Pico, Yolanda; Fernandez, Monica; Ruiz, Maria Jose; Font, Guillermina 

Determination of pesticides and their degradation products 

1946 Pesticides IN soil: Critical review and comparison of methods Review GC-MS 

from soil TrAC Trends Anal. Chem., 23, #10-11, 772-789 headspace SPME LC-MS 

Andreu, Vicente; Pico, Yolanda 

Coupled in-tube and on-fibre SPME for cleanup and preconcentration of 





2844 Organics organic micropollutants from aqueous samples and analysis by GC-MS DVB/Cab (30/50 μm) GC-MS 

in water Anal. Chim. Acta 618, #1, 61-69 (Jun 16 2008) 

Gupta, Manju; Jain, Archana; Pillai, Aradhana K.K.V.; Verma, K. 

Target and nontarget screening of organic micropollutants in water by 

2339 Organics SPMEs combined with GC-TOF-MS 

in water Anal Chem Vol. 79, # 24 9494-504 (2007 Dec 15) GC-TOF-MS 

Hernandez, F.; Portoloes, Tania; Pitarch, Elena; Loopez, F. 

2846 PAHs in 

SPME followed by HPLC with fluorimetric and UV detection for 

the determination of polycyclic aromatic hydrocarbons in water 65µm PDMS/DVB LC-UV 

water Analytical Letters 41, #1, 119-136 (2008) 60 min @ 70°C 

Ricardo Lucio-Gutierrez, J.; de la Luz Salazar-Cavazos, Maria; 

Waksman de Torres,Noemi H.; Castro-Rios, Rocio 

immersion 

2397 PAHs in 

Determination of PAHs in aqueous samples by microwave assisted 

headspace SPME-GC-FID 65µm PDMS/DVB GC-FID 

water Talanta 72, #4, 1269-1274 (2007-06-15) 

Wei, M. -C.; Jen, J. -F. 

30 min @ 20°C 

SPME-GC-MS analysis of PAHs Towards the European 

2345 PAHs in Union water directive 2006/0129 EC 65µm PDMS/DVB GC-MS 

water J Chromatogr A 1176, #1-2 , 48-56 (2007 Dec 28) immersion GC-MS-MS 

Fernoandez-Gonzoalez, V; Concha-Graona, E; Muniategui-Lorenzo, S; 

Loopez-Mahoa, P; Prada-Rodroguez, D 

Predicting PAH bioaccumulation and toxicity in earthworms exposed to 

2543 PAHs in manufactured gas plant soils with solid-phase microextraction 

earthworms Env Science & Tech 41, #21, 7472-7478 (NOV 1 2007) 

Jonker, T. O.; van der Heijden, S.; Kreitinger, J.; Hawthorne,S. 

2596 Organics 

Characterization of an urban landfill soil by using physicochemical . 

analysis and solid phase microextraction (SPME)-GC/MS 65µm PDMS/DVB GC-MS 

from soil Env. Monitoring Assessment 127, #1-3, 337-351 (APR 2007) headspace 

Banar, Mufide; Ozkan, Aysun; Vardar, Cigdem 15 min @ 50°C 

SPME to predict bioavailability and accumulation of organic 

1947 Organics micropollutants in terrestrial organisms after exposure 30µm PDMS GC-MS 

from soil to a field-contaminated soil headspace 

Environ. Sci. Technol., 38, #18, 4842-4848 10 days exposure 

Barendregt, A; Fleuren, R; Hermens, J.; Jager, T; Sinnige, T.; 

Van Der Wal, Leon; Van Gestel, Cornelis A. M. 

SPME coupled to GC-MS for determining PAH-micelle 

1948 PAHs in micelle partition coefficients 85µm polyacrylate GC-MS 

micelles Anal. Chem., 76, #15, 4572-4578 100µm PDMS 

Alfonso, Ana M.; Ayala, Juan H.; Gonzalez, V; Pino, V. 

Implementation of new methods to characterise 

1949 Odors from atmospheres in piggeries headspace GC-MS 

pig sheds Int. J. Environ. Anal. Chem., 84, #9, 647-659 

Begnaud, F.; Berdague, Jean-Louis; Lebost, J.; 

Murat, C.; Peres, C. 

In-tube solid-phase microextraction and online 

1950 Organics in coupling with high-resolution GC. 5 M X 0.53mm ID GC 

water LC-GC Europe, 17, #3, 144-151 1.2µm PDMS 

Wang, H. W.; Liu, W. M.; Guan, Y. F. 

Characterization of volatile organic compounds on 

1951 Odor from airborne dust in a swine finishing barn 75µm Carboxen GC 

swine Trans. Am. Soc. Agric. Eng., 47, #4, 1231-1238 100µm PDMS 

facilities Jeon, I.J.; Maghirang, R.G.; Razote, E.B.; Seitz, L.M headspace 

Water 


Solid Phase Microextraction of volatile organic compounds 

in environmental applications 100µm PDMS GC 

in environmental Am Laboratory (2001)33(4), 18-20 85µm Polyacrylate 

samples Van Longenhove, H; Dewulf, J. 15 min. 

858 Organic pollutants 

SPME - a convenient tool for the determination of organic 

pollutants in environmental matrices 





in environment Crit. Rev. Anal. Chem (2001) 31(1) 1-18 

Zygmunt, Bogdan; Jastrzebska, Anna; Namiesnik, Jacek 

2670 Toluene from 

Characterisation of absorptive sampling with SPME fibres in 

the EUPHORE photoreactor GC 

air Talanta 72, #5, 1757-1766 (JUL 31 2007) 

Alvarez E., Gomez 

Experimental confirmation of the dicarbonyl route in the photo-oxidation 

2601 Carbonyl product of benzen and toluene 

photo-oxidation Env Sci Tech 41, #24, 8362-8369 (DEC 15 2007) 

BTEX Alvarez, E. Gomez; Viidanoja, J.; Munoz, A.; Wirtz, K.; Hjorth, J. PFBHA derivatives 

Rapid analysis of tile industry gaseous emissions by ion mobility 

2717 Volatile emissions spectrometry and comparison with SPME-GC-MS GC-MS 

industrial gaseous J. Environ. Monit. 8, #12, 1219-1226 (2006-11-28) 

Pozzi, R.; Bocchini, P.; Pinelli, F.; Galletti, G. C. 

Comparative application of SPME fibre assemblies and semi-permeable 

2710 Semivolatile membrane devices as passive air samplers for semi-volatile chlorinated 

organic compounds. A case study on the landfill "Grube Antonie" in 

65µM CW/DVB GC 

chlorinated 

Bitterfeld, Germany passive air sample 

organics in air Environmental Pollution 144; # 2; 414-422 (2006-11-15) 

Paschke, A.; Vrana, B.; Popp, P.; Schueuermann, G. 

Modelling of toluene SPME for indoor air sampling. 

2602 Toluene from Anal Bioanal Chem 388, #1, 147-56 (2007 May) 75µm Carboxen GC 

air samples Mocho, Pierre; Larroque, Virginie; Desauziers, Valoerie 

1 BTEX compounds, 

The Application of Chemically Modified Fused Silica 

Fibers in the Extraction of Organics from Water Matrix uncoated fiber GC-FID 

PCBs, solvents Samples and Their Rapid Transfer to Capillary Columns 1 min 

in water Water Pollution Research J. Canada 24: 179 (1989) 

Belardi, R., Pawliszyn, J. 

2678 VOCs 

Development of a simple, accurate SPME-based method for assay 

of VOCs in column breakthrough experiments headspace GC 

in water CHEMOSPHERE 66, #1, 18-29 (2006) 

Salaices, Avila M. A.; Breiter, R.; Mott, H. 

5 min 

Multiple solid-phase microextraction: Theory and applications. 

2682 Review article Trends Anal. Chem 26, #3, 206-214 (2007-03) 

Tena, M. T.; Carillo, J. D. 

Developments in multiple headspace extraction 

2685 Review article J. Biochem. Biophys. Mehods 70, #2, 229-233 (10 MAR 2007) 

Hakkarainen, M. 

Sorbent- and liquid-phase microextraction techniques and membrane- 

2789 Review article assisted extraction in combination with GC analysis: A review 

Anal. Chim. Acta 614, #1, 27-37 (Apr 28 2008) 

Hyotylainen, Tuulia; Riekkola, Marja-Liisa 

3 VOCs 

Solid Phase Microextraction for the Direct Analysis of 

Water: Theory and Practice 100µm PDMS GC-FID 

in water LC-GC 10: 656-661 (1992) 2-5 min 

Arthur, C., Potter, D., Buchholz., K, Motlagh, S., Pawliszyn, J. salt added 

4 VOCs, PCBs, 

Practical and Theoretical Aspects of Solid Phase 

Microextraction for the Direct Analysis of Groundwater 100µm PDMS GC-FID 

solvents in water Proceedings 15th Annual EPA Conference-Analysis 5-14 min 

of Pollutants in Environment, Norfolk, VA, May 1992 

Arthur, C., Buchholtz, K., Motlagh, S., Killam, L., Pawliszyn, J. 

salt added 





Analysis of Substituted Benzene Compounds in 


6 BTEX, gasoline Groundwater Using SPME 56µm PDMS GC-FID 

in water J. Env. Sci. Technol. 26: 979-983 (1992) 2-6 min 

Arthur, C., Potter, D., Lim, M., Motlagh, S., 

Killam, L., Pawliszyn, J. 

stirring 

2616 BTEX compounds 

Determination of benzene, toluene, ethylbenzene, xylenes in water at 

sub-ng l(-1) levels by SPME coupled to cryo-trap GC-MS 75µm Carboxen GC-MS 

in water Chemosphere 69, #9, 1381-1387 (NOV 2007) 15 min @ 25°C 

Lee, Maw-Rong; Chang, Chia-Min; Dou, Jianpeng sat. salt 


Dynamics of Organic Compounds Extraction from 

Water Using Liquid-Coated Fused Silica Fibers 56µm PDMS GC-FID 

in water Anal. Chem. 64: 1187-1199 (1992) 2-6 min 

Louch, D., Motlagh, S., Pawliszyn, J. stirring 


Detection of Substituted Benzenes in Water at the pg/mL 

Level Using Solid Phase Microextraction and 100µm PDMS GC-FID 

in water GC-Ion Trap Mass Spectrometer 30 min 

J. Chromatogr. 625: 247-255 (1992) 

Potter, D., Pawliszyn, J. 

stirring 

11 Organics 

Environmental Analysis of Organic Compounds in 

Water Using Solid Phase Microextraction 100µm PDMS GC-MS 

in water J. High Res. Chromatogr. 15: 741-744 (1992) 14 min 

Arthur, C., Pratt, K., Belardi, R., Motlagh, S., Pawliszyn, J. stirring 

14 Phenols 

Determination of Phenols by SPME and GC Analysis 

J. Environ. Sci. Technol. 27 (13): 2844-2848 (1993) 85µm polyacrylate GC-FID, -MS 

in water Buchholz, K., Pawliszyn, J. 60 min 

stirring 

salt added, pH 2 

Determination of Phenolic Compounds in Waste Water 

230 Phenols by Solid-Phase Microextraction GC-MS 

in water Fresenius’ J. Anal. Chem. 357: 326-332 (1997) 

Moeder, M., Schrader, S., Franck, U., Popp, P. 

670 Phenols 

Sorption of phenols to dissolved organic matter 

investigated by SPME 

in water Sci. Total Environ. (2000), 253(1-3), 63-74 

Ohlenbusch, G., Kumke, M., Frimmel, F. 

922 Phenolic compounds 

SPME coupled to liquid chromatography for the analysis 

of phenolic compounds in water 50µm CW/TPR HPLC 

in water J. Chromatogr. A (2001) 923(1-2), p45-52 65µm DVB/PDMS 

Toledo, E., Prat, M., Alpendurada, M. 30min immersed 

salt added, pH 2 

951 Chlorinated phenolics 

Application of SPME in pre-concentration of chlorinated 

phenolic compounds from cellulose bleaching effluents 

in water J. Sep. Sci (2001), 24(4), 309-312 

Dos Santos, L.; Vale, M.; De Araujo, M. 

Bertrand C.; Caramao, E.; Oliveira, E. 

Recent Advances in Solid-Phase Microextraction 

15 VOCs, phenols, (SPME) of Environmental Samples 100µm PDMS GC-MS 

semivolatiles Proceedings Water Quality Technology Conference 5 min (volatiles) 

in water Miami, FL, Nov. 1993 10 min (semivolatiles) 

Arthur, C., Pratt, K., Belardi, R., Motlagh, S., Pawliszyn, J. headspace 


671 4-Quinolones 

Influence of pH and other modifying factors on the 

distribution behaviors of 4-Quinolones to Solid phase and CW/TPR HPLC 

in water humic acids studied by "negligible-depletion" SPME-HPLC 10min. 260NM 

Environ Sci Technol. 2000, 34, 4989-4994 pH 3-5.5 

Lutzhoft, H. Vaes, W., Freidig, A., Halling-Sorrensen, B. 

Hermens, J. 

stirred 





2644 Semivolatiles 

Determining chemical activity of (semi)volatile compounds by 

headspace solid-phase microextraction headspace GC 

varied matrices Anal. Chem. 79, #7, 2869-2876 (Apr 1 2007) 

Burken, J.; Karlson, U.; Legind, C.; Mayer, P.; Reichenberg, F 

30 min 


Analysis of semi-volatile organic compounds in aqueous samples by 

microwave-assisted headspace SPME Coupled with GC-ECD headspace GC-ECD 

in waste water J. Chromatogr., A 1140, #1-2, 35-43 (2007-01-26) 

Huang, Y. P.; Yang, Y. C.; Shu, Y. Y. 

30 min @ 70°C 

501 24 Semivolatiles 

Development of SPME-GC method for the determination of 

organic compounds in waste water GC 

in waste water Acta Hydrochim. Hydrobiol. 1999, 27(4), 1913-199 

Grote, C., Belau, E., Levsen, K., Wunsch, G. 

938 Organics 

An improved automatic analyzer for organic compounds in 

water based on headspace (SPME) coupled to GC GC 

in water Field Anal. Chem. Technol (2001) 5(1-2), 37-49 

Belau, E.; Grote, C.; Spiekermann, M.; Levsen, K. 


Polyacrylate-Coated SPME fibers as a tool to simulate body 

residues and target concentrations of complex organic 85µm polyacrylate GC-MS 

in fish, water mixtures for estimation of baseline toxicity 

Environ. Sci. Technol. 2000, 34, 324-331 

Verbruggen, E., Vaes, W., Parkerton, T., Hermens, J. 

5-150 min 

785 Halogenated 

Impact of a lignite seam on contaminated groundwater in the 

aquifer system of the Bitterfeld region 

hydrocarbons Water Air Soil Pollut (2000) 125(1-4), 157-170 

in water Christoph, G; Dermietzel, J. 

19 Chlorohydrocarbons 

Determination of Volatile Chlorinated Hydrocarbons in 

Air and Water with Solid-Phase Microextraction 100µm PDMS GC-ECD 

in water Analyst(Cambridge,UK) 118: 1501-5, Dec. 1993 20 min (immersion) 

Chai, M., Arthur, C., Pratt, K., Pawliszyn, J., Belardi, R. 10 min (headspace) 

436 Chlorohydrocarbons 

Analysis of Volatile Halogenated Hydrocarbons in Water by 

SPME and GC-MS 100µm PDMS GC-MS 

in water Chem. Listy (1998), 92(9), 633-642 20 min 

Janda, V., Viden, I. stirred 

2645 Aromatic 

Laboratory studies on the uptake of aromatic hydrocarbons by ice 

crystals during vapor depositional crystal growth headspace GC 

hydrocarbons in Atmos. Environ. 41, #29, 6156-6166 (Sept 2007) 

ice crystals Borrmann, S.; Fries, E.; Haunold, W.; Jaeschke, W.; Mitra, S.; 

Schmidt, M.; Starokozhev, E. 

Rapid Determination of Polyaromatic Hydrocarbons 

20 PAHs, PCBs and Polychlorinated Biphenyls in Water Using 15µm PDMS GC-MS 

in water Solid-Phase Microextraction and GC/MS 10 min 

J. Environ. Sci. Technol. 28(2): 298-305 (1994) stirring 

Potter, D., Pawliszyn, J. 

900 Aromatic compounds 

SPME of aromatic hydrocarbons from water samples 

Chemija (2000) 11(4) 206-210 

in water Seduikiene, I.; Vickackaite, V.; Kazlauskas, R 

672 PAHs 

Quantitative analysis of PAHs in water by SPME-HPLC 

Huanjing Huaxue (2000) 19(4), 382-384 HPLC 

in water Li, Y., Zhang, X., Xu, R., Cai, W., Wang, G., Song, Y. 

2831 Dissolved 

Allochthonous DOC in floodplain rivers: Identifying sources using 

using SPME with GC. 

organic carbon Aquatic Sciences 69m #4, 472-483 (2007) 





in rivers Zander, Alek; Bishop, Andrea G.; Prenzler, Paul D.; Ryder, Darren S. 

2740 Chlorinated 

Determination of chlorinated volatile organic compounds in water and 

municipal wastewater using headspace-SPME-GC headspace GC-MS 

volatils in water J. Chromatogr. A, 1132, #(1-2), 310-314 (2006-11-03) 

and wastewater Antoniou, V.; Koukouraki, E. E.; Diamadopoulos, E. 

2482 Volatiles and 

Analysis of volatile and semivolatile organic compounds in municipal 

wastewater using headspace SPME-GC headspace GC-MS 

semivolatiles from Water Environment Research 79, #8, 921-930 (AUG 2007) 

wastewater Antoniou, Chrysoula V.; Koukouraki, Elisavet E.; Diamadopoulos, Evan 

2540 VOCs 

Leaching of vocs from cement-based stabilized/solidified refinery oily 

sludge using solid phase microextraction headspace GC-FID 

in oil sludge Env Tech 28, #10, 1173-1185 (OCT 2007) 

Karamalidis, A. K.; Voudrias, E. A. 

Analysis of Organic Compounds in Environmental 

22 VOCs, BTEX, PAHs Samples Using Headspace Solid Phase Microextraction 100µm PDMS GC-MS 

in wastewater, J. High Res. Chromatogr. 16(12): 689-692 (1993) stirring, varied time 

sludge Zhang, A., Pawliszyn, J. saturated salt 

673 Jet fuels 

Source identification of underground fuel spills by 

SPME/High Resolution GC/genetic algorithms GC 

in ground water Anal. Chem. (2000), 72(2), 423-433 

Lavine, B., Ritter, J., Moores, A., Wilson, M., 

Faruque, A., Mayfield, H. 

Relative efficacy of intrinsic and extant parameters for modeling 

2824 Organic chemicals biodegradation of synthetic organic compounds in headspace GC-FID 

in sludge activated sludge: Steady-state systems 

Water Environ. Res. 75(2), 98-104 (2000) 

Bowyer, R.; Grady Jr., C.; Magbanua Jr., B.; Rodieck, Allison G.; 

Sanders II, R.; Smets, B.; Sowers, W.; Stolze, S. 

Quantification of synthetic organic chemicals in 

674 Organic chemicals biological treatment process effluent using SPME-GC 85µm polyacrylate GC-FID 

in waste water Water Environ. Res, (2000), 72(1), 98-104 

Magbanua, B., Mitchell, D., Gehniger, S., Bowyer, R., 

Grady, C., Leslie, J. 

675 Musk fragrances 

Optimization of SPME for the GC-MS determination of 

synthetic musk fragrances in water samples 65µm PDMS/DVB GC-MS 

in water J. Chromatogr. A, (2000) 903(1-2), 203-210 45 min @ 30°C 

Winkler, M., Headley, J., Peru, K. 

Occurrence and distribution of organic compounds in the 

headspace 

agitation 

502 Polycyclic musk aquatic system in Berlin, Germany. Part 3, Determination of GC-MS 

in surface water synthetic musks in Berlin surface water applying 

SPME and GC-MS 

Acta Hydrochim Hydrobiol (1999), 27(3), 150-156 

Heberer, T., Gramer, S., Stan, H. 

787 Polyolefins 

Ultrasonication and microwave assisted extraction of 

degradation products from degradable polyolefin blends GC-MS 

in soil aged in soil 

J. Appl. Polym. Sci (2001) 79(6), 1101-1112 

Contat-Rodrigo, L; Haider, N; Karlsson, S; Ribes-Greus, A 

2854 Fluorene from 

Kinetics of fluorene biodegradation by a mixed culture 

Proc. Second IASTED Int. Conf. Advanced Technol. Environ. Field GC-FID 

water samples pp84-87 (2007) 

Brito, A.G.; Gomes, R.C.B.; Nogueira, R.; Oliveira, J.M.; Peixoto, J. 

SPME as a tool to predict the bioavailahility and toxicity of pyrene to 





2775 Pyrene the springtail, Folsomia candida, under various soil conditions 

in soil Environl Scie & Tech, 42(4), 1332-1336 (2008) 

Styrishave, B.; Mortensen, M.; Krogh, P.; Andersen, Ole; Jensen, J. 

940 Pyrene 

Sorption of pyrene to dissolved humic substances and related 

model polymers. 1. Structure-property correlation 

on humic material Environl Scie & Tech (2001), 35(12), 2536-2542 

Kopinke, F.; Georgi, A.; Mackenzie, K. 

Influence of sorption to dissolved humic substances on transformation 

2586 PAHs reactions of hydrophobic organic compounds in water. 

in water I. Chlorination of PAHs 

Env Sci & Tech 41, #320, 7003-7009 (OCT 15 2007) 

Georgi, Anett; Reichl, Annett; Trommler, Ulf; Kopinke, Frank-Dieter 

676 PAHs 

SPME and headspace SPME for the determination of high 

molecular-weight PAHs in water and soil samples 100µm PDMS GC-FID 

in water/soil J. Chromatogr. Sci., (2000) 38(12) 528-534 85µm polyacrylate 

Doong, R., Chang, S., Yuh-Chang 20-60 min @60°C 

677 PAHs 

Determination of Distribution Coefficients of priority 

PAHs using SPME 100µm PDMS 

in water/soil Anal. Chem. 2000, 72(15), 3647-3652 85µm polyacrylate 

Doong, R., Chang, S., 20-60min. 

678 PAHs 

SPME FOR determining the Distribution of 16 USEPA 

PAHs in water 100µm PDMS GC-MS 

in water/soil J.. Chromatogr.. A 2000, 879(2), 177-188 85µm polyacrylate 

Doong, R., Chang, S., Sun,, Y. 20-60 min 

585 PAHs in 

Interaction between natural organic matter (NOM) and (PAH) 

comparison of fluorescence quenching and SPME. 7µm PDMS GC-MS 

water/humic material Fresenius'-J-Anal-Chem. Jun 1999; 364(4): 313-319 

Doll,-TE; Frimmel,-FH; Kumke,-MU; Ohlenbusch,-G 

20 min 

25 PAHs, semivolatiles 

Solid Phase Microextraction -- A Solventless Sample 

Preparation Method for Organic Compounds in Water 7µm PDMS (PAHs) GC-FID, -ECD 

in water American Environmental Lab April 1994, p 43-45 polyacrylate (semivol) 

Shirey, R., Mani, V., Savrock, J. 

Optimization of Extraction Conditions for Low-Molecular- 

15 min, stirring 

saturated salt 

679 Volatiles Weight analytes using SPME six different fibers GC-MS 

in water J. Chrom. Sci., Vol. 38, March 2000, 109-116 15 min headspace 

Shirey, R. sat. salt, pH2,7,11 

Optimization of Extraction Conditions and Fiber Selection for 

680 Semivolatiles Semivolatile Analytes using SPME seven different fibers GC-MS 

in water J. Chrom. Sci., Vol. 38, July 2000, 279-288 30 min, immersed 

Shirey, R. sat. salt, pH2,7,11 

Solvent-Free Method for the Determination of PAHs in 

440 PAHs in Wastewater by SPME-HPLC with Photodiode-Array Detector 100µm PDMS HPLC-PAD 

water J. Chromatogr. A (1998), 823(1+2), 211-218 45°C, 30 min 

Negrao, M., Alpenduradu, M. stirring 

Analysis of BTEX in Water by Commercially Available 

26 BTEX compounds SPME and CLOT Column Gas Chromatography 100µm PDMS GC-FID 

in water J. Chromatogr. 677: 201-205 (1994) 35 min 

Sama, L., Webster, G., Friesen-Fisher, M., Ranjai, R. stirring 

Determination of the Semi-Volatile Compounds 

30 Nitrobenzenes Nitrobenzene, Isophorone, 2,4-Dinitrotoluene and 100µm PDMS GC-FID 

in water 2,6-Dinitrotoluene in Water Using SPME with 15 min 

Polydimethylsiloxane-Coated Fiber stirring 

J. Chromatogr. A Vol 678(2): 313 (1994) saturated salt 

Horng, J., Huang, S. 

Rapid Analysis of Environmental Samples Using SPME 





31 VOCs, chloropesticides and Narrow Bore Capillary Columns 100µm PDMS GC-MS 

in water J High Res. Chromatogr. 18(8): 495-499 (1995) 15 min 

Shirey, R. stirring 



Determination of BTEX Compounds in Water by 

Solid-Phase Microextraction and Raman Spectroscopy 100µm PDMS GC-FID 

in water Anal. Chem. 67(3): 600-605 (1995) 

Wittkamp, B., Tilotta, D. 

681 Volatiles 

A new method for the rapid determination of volatile 

substances: the SPME-direct method Part 1: Apparatus 

and working conditions 

Sens, Acatuators, B. (2001) B72 (2) 184-187 

Bene, A., Fornage, A., Luisier, J., Pichler, P., Villettaz, J. 

830 Methyl, ethylmercury 

Direct hydride derivatization of methyl- and ethylmercury 

chlorides in acqueous solution with KBH4 GC-MS 

chlorides J Environ Sci (China) (2000) 12(3) 275-278 

in water Jiang Gui-bin; He Bin 


Methylmercury determination in biota by SPME matrix effect evaluation 

J Chromatogr A 1174, #1-2, 2-6 (2007 Dec 7) headspace GC-Py-AFS 

derivatives in 

biological matrix 

Carrasco, Luis; Doez, Sergi; Bayona, Josep M 

Determination of Methymercury in Fish and River Water 

NaBEtr derivative 

48 Methylmercury Samples Using in situ Sodium Tetraethylborate 100µm PDMS GC-MS 

derivatives Derivatization Followed by SPME and GC-MS 10 min 

in water and fish J. Chromatogr. 696: 113-122 (1995) stirring 

Cai, Y., Bayona, J. headspace 

407 Organomercury 

SPME and GC-MIP-AED for the Speciation Analysis of 

Organomercury Compounds 100µm PDMS GC-MIP-AED 

in water and soil J. High Resol. Chromatogr. 1999, 22 (3) 181-182 25°C 

Mothes, S., Wennrich, R. 

Solid Phase Microextraction of Metal Ions 

50 min (immersion) 

20 min (headspace) 

18 Bismuth III Microchim. Acta 112: 41-6 (1993) bare, or 100µm PDMS UV / VIS 

in water Otu, E., Pawliszyn, J. 

Speciation of dimethylarsinic acid and monomethyl- 

60 min 

immersion 

460nm 

682 Dimethylarsinic acid arsonic acid by SPME-GC-ion trap MS 100µm PDMS GC-MS 

arsonic acid J. Chromatogr.A 2000, 873(1), 129-135 

Mester, Z., Pawliszyn, J. 

40min @ 20°C 

thioglycol methylate derv. 

96 Organo Hg, Sn, Pb 

Sensitive, Simultaneous Determination of Organomercury 

Lead, and Tin Compounds with Headspace SPME 100µm PDMS ICP-MS 

in water Capillary GC Combined with Inductively Coupled Plasma MS 10 min 

Anal. Chem. 69: 1604-1611 (1997) headspace 

Moens, L., DeSmaele, T., Dams, R., VanDen Broeck, P., stirring 

Sandra, P. 

SPME-GC-glow discharge-optical emission detection for 

pH 5.3 


873 Tin & lead tin and lead speciation GC-OES 

in water J Anal At Spectrom (2001) 16(4), 376-381 

Orellana-Velado, N.G.; Pereiro, R.; Sanz-Medel, A 

Speciation of organotins in environmental samples by 


796 Organo Sn SPME-GC: comparison of four specific detectors: FPD, PFPD 

in water J. Anal. At. Spectrom (2001) 16(3), 263-269 MIP-AES 

Aguerre, S; Lespes, G; Desauziers, V; Potin-Gautier, M ICP-MS 

2764 Organotin and 

Optimisation of the headspace-SPME for organomercury and 

organotin compound determination in sediment and biota 30 µm PDMS MIP-AES 

organomercury in J. Sep. Sci. 31, #4, 768-774 (March 2008) Headspace 

sediments de Diego, A.; Delgado, A.; Madariaga, Juan M.; Prieto, Ailette; 3-24 min@ 20-90°C 





Usobiaga, Aresatz; Zuloaga, Olatz NaBEtr derivative 

2244 Organotin in 

Organotin speciation in Bizerte lagoon (Tunisia) 

Science of the Total Environment 349, #1-3, 211-222 (2005) headspace GC-PFPD 

marine sediments Mzoughi, N.; Lespes, G.; Bravo, M.; Dachraoui, M.; Potin-Gautier, M. 

Preconcentration and Determination of Sn- and Pb-Organic 

NaEt4B 

derivatives 

153 Organo Sn, Pb Species in Environmental Samples by SPME and GC-AED GC-AED 

in water Fresenius’ J. Anal. Chem. 354: 587-91 (1996) 

Tutschiku, S., Mothes, S., Wennrich, R. 

Determination of Organotin Compounds in Water Samples 

215 Organotin by Solid-Phase Microextraction (SPME) and GC-MS GC-MS 

in water Ann. Chim. (Rome) 87: 497-504 (1997) 

Guidotti, M., Vitali, M. 

152 Methyltin 

Rapid Determination of Methyltin Compounds in Aqueous 

Samples Using SPME and Capillary GC Followed by 100µm PDMS GC-FPD 

in water in situ Derivatization with Sodium Tetraethylborate 29°C, 2-35 min 

J. High Res. Chromatogr. 18: 767 (1995) headspace 

Morcillo, Y., Cai, Y., Bayona, J. 

Determination of Tetraethyllead and Inorganic Lead in Water 

stirring 


161 Lead derivatives by SPME-GC 100µm PDMS GC-MS 

in water Anal. Chem. 68: 3008 (1996) 10 min 

Gorecki, T., Pawliszyn, J. headspace 

683 Lead derivatives 

Determination of Tetraethyllead by SPME-thermal desorption 

quartz furnace atomic absorption spectrometry AA 

in water J. Anal. At. Spectrom. 2000, 15(16), 705-709 

Sandra Fraguairo, M, AlavapMoreno, F., Isela, B. 


Rapid Determination of Butyl, Phenyl and Cyclohexyl Tin 

23 Organotin compounds Compounds in Aqueous Samples Using SPME and 100µm PDMS GC-FPD 

in water Capillary Gas Chromatography Following in situ Derivatization 30 min 

with Sodium Tetraethylborate immersion 

CID-CSIC Jordi Girona, 18-26, E-8034, Barcelona, Spain stirring 

Morcillo, Y., Cai, Y., Porte, C., Bayona, J. NaBEt4 derivative 

503 Organo-tin, -lead, 

Determination of organometallic compounds in surface 

water and sediment samples with SPME-CGC-ICPMS 100µm PDMS GC-ICPMS 

-mercury Mikrochim. Acta (1999), 130(4), 241-251 10 min 

in water De Smaele, T., Moens, L., Sandra, P., Dams, R. headspace 

235 Rare earth elements 

Separation of Cerium from Other Rare-Earth Elements with 

Application to Samarium-Neodymium and Lanthanum- 

Cerium Chronometry 

Nucl. Instrum. Methods Phys.Res.Sect.B 117: 201-208 (1996) 

Rehkaemper, M., Gaertner, M., Galer, S., Goldstein, S. 

2742 Selenite and 

Comparison of two derivatizing agents for the simultaneous. 

determination of selenite and organoselenium species immersed vs GC-MS 

organoselenium by GC and atomic emission . headspace (20min) 

J. Chromatogr. A 1165, #1-2, 191-199 (Sep 21 2007) piazselenol 

Campillo, N.; Penalver, R.; Hernandez-Cordoba, M.; Perez-Sirvent, C.; 

Martinez-Sanchez, M. -J. 

derivative 

580 Selenite, selenate 

Selective determination of selenite and selenate using 

SPME and GC-MS GC-MS 

in water J-High-Resolut-Chromatogr. Jul 1999; 22(7): 414-416 35 min, agitation 

Guidotti,-M; Ravaioli,-G; Vitali,-M 

Compound-specific nitrogen and carbon isotope analysis of 

piazselenol derivative 

immersed 

2752 Nitroaromatics nitroaromatic compounds in aqueous samples using SPME-GC/IRMS GC/IRMS 

in water ANAL. CHEM. 79, #6, 2386-2393 (15 MAR 2007) 

Berg, M.; Bolotin, J.; Hofstetter, T. B. 





Analysis of nitroaromatic compounds in complex samples using SPME 


2640 Nitroaromatics and isotope dilution quantification GC-electron negative ionisation MS GC-MS 

in water J. Chromatogr. A 1164, #1-2, 65-73 (Sep 14 2007) 

van Bavel, B.; Gustavsson, L.; Jonsson, S 

49 Nitroaromatics 

Enrichment of Nitroaromatic Compounds from Water 

Samples by SPME 

in water GIT Spex Chromatogr. 14: 85-87 (1995) 

Schaefer, B., Engewald, W. 

809 Nitroarenes 

Analysis of nitroarenes by SPME/GC-Ion trap MS 

Chromatography (2000) 21(2),123-124 

Kataoka, Hiroyuki; Lord, Heather L.; Pawliszyn, Janusz 

GC-MS 

160 Hetero aromatics 

Trace Analysis of Hetero Aromatic Compounds in 

Water by SPME 85µm polyacrylate GC-MS 

in water J. High Res. Chromatogr. 19(11): 627-632 (1996) 60-200 min 

Johansen, S., Pawliszyn, J. stirring 


218 BTEX 

Determination of Benzene Derivatives in Water by SPME 

Anal. Chim. Acta 343: 101-108 (1997) 

in water Huang, S., Cheng, C., Sung, Y. 

Enrichment of Nitrophenols from Water by Means of SPME 

50 Nitrophenols Fresenius’ J. Anal. Chem. 352(5): 535-6 (1995) 100µm PDMS GC-NPD 

in water Schafer, B., Engewald, W. 5 min 

stirring 

pH




Nilsson, T., Ogaard-Madison, J., Montanrilla, L., Larsen, B., headspace 

Facchetti, S., Pelusioj, F. stirring 

685 MTBE 

Determination of MTBE in surface water by use of SPME 

Environ, Sci.Technol. (2000), 34(7), 1359-1364 Carboxen/DVB/PDMS GC-MS 

in surface water Achten, C., Puettmann, W. 

Sensitive methods for measuring methyl tert-butyl-ether 

69 min 

25% NaCl, stirred 

935 MTBE in water Carboxen/DVB/PDMS GC-MS 

in surface water Umwelt-Technol. Aktuell (2000) 12(1), 22-25 69 min 

Achten, C., Puettmann, W. 25% NaCl, stirred 

686 MTBE, Ethanol, other 

Trace Analysis of Ethanol, MTBE, and related Oxygenate 

Compounds in Water using SPME and GC-MS Carboxen/DVB/PDMS GC-MS 

oxygenates in water Anal. Chem. 2000, 72, 4654-4658 25 min immersed 

Cassada, D., Zhang, Y., Snow, D., Spalding, R. stirred 

Sat. salt, 

910 MTBE, TBE, BTEX 

High levels of monoaromatic compounds limit the use of 

SPME of MTBE and Tert butyl alcohol 75µm Carboxen/PDMS Ion trap 

in water Environ Sci Technol, 2001, 35 (15) 3190-3192 65µm DVB/PDMS GC-MS 

Black, L., Fine, D. 

Analysis of Water Samples for Trace Levels of Oxygenated 

1-25min. 


354 MTBE, EBE, BTEX and Aromatic Compounds Using Headspace SPME and 75µm Carboxen/PDMS GC-FID 

in water Comprehensive Two-Dimensional Gas Chromatography 40°C, 10 min 

J. Microcolumn Separations, 10 (7), 597-604 (1998) headspace 

Gaines, R., Ledford, E., Stuart, J. saturated salt 

952 MTBE 

Measurement of Henry's law constant for MTBE using SPME 

Environ. Toxicol. Chem (2001), 20(8), 1625-1629 

in water Bierwagen, B.G.; Keller, A.A. 

Role of humic acids in the titanium oxide-photocatalysed 

15°-40°C 

headspace 

581 Tetrachloroethene degradation of tetrachloroethene in water. 100µm PDMS GC-MS 

in water Water-Res. Jun 1999; 33(8): 1827-1836 

Selli,-E; Baglio,-D; Montanarella,-L; Bidoglio,-G 

Using SPME with GC to assess trihalomethane content in water 

2331 Trihalomethanes Abstracts of Papers Am Chem Society (2004) 227 Part1, U456 GC 

in water Rizzuti, Anthony M.; Rogers, Lisa N. 


Simultaneous analysis of 23 priority volatile compounds in water 

by SPME-GC-MS and estimation of the method's uncertainty 75µm Carboxen GC-MS 

in drinking water Int. J. Environ. Anal. Chem. 88, #3, 151-164 (March 2008) headspace 

Alpendurada, M.; Carvalho, J.; Goncalves, C.; Guimaraes, A. 15min @ 20°C 

Determination of trihalomethanes in drinking water of towns in 

2215 Trihalomethane the State of Minas Gerais, Brazil using headspace (HS)/SPME headspace GC-ECD 

in drinking water high resolution GC-ECD 

Ciencia Eng.) 11 #2, 57-62 (2002) 

Duarte, M.; Parreira, F; Rabelo De Carvalho, C. 

175 Trihalomethanes 

Detection and Quantification of Trihalomethanes in 

Drinking Water from Alexandria, Egypt 

in water Contam. Toxicol. 56: 397-404 (1996) 

Hassan, A., Benfenati, E., Fanelli, R. 

Analysis of dichlorobenzene in water by SPME 

687 Dichlorobenzene J. Chin. Chem. Soc (2000) 47(2) 415-420 100um PDMS GC-ECD 

in water Liu, Y., Ho, W. 30 min 

813 Chloroform 

Analysis of chloroform in drinking water by 

headspace solid-phase microextraction and GC 85µm Polyacrylate GC-FID 

in water Fenxi Shiyanshi (2000), 19(5), 65-67 45°C 

Liu, Z. L.; Wang, C. H.; Wang, X headspace 





858 Chloroform 

Chloroform formation during kraft pulp bleaching with 

chlorine and chlorinated compounds -determination of 

from Kraft pulp bleach chloroform amounts by solid phase microextraction 

Kami Pa Gikyoshi (2000) 54(11) 1555-1563 

Oi, Hiroshi; Masuzawa, Kiyoshi 

Application of Solid Phase Microextraction (SPME) in 

(Japanese) 

83 Benzene, halobenzene Combination with GC/FID: The Determination of Benzene and GC-FID 

in water Halogenated Benzenes in Pure and Octanol-Saturated Water 

Chem-Anal (Warsaw) 40: 897-904 (1995) 

Popp, P., Paschke, A., Schroeter, U., Oppermann, G. 

688 Benzene derivatives 

Matrix effect for several derivatives of benzene in water 

by SPME 

in surface water Chromatographia 2000, 51(suppl.) S328-S330 

Javorszky, E., Molnar, E., Torkos, K. Borossay, J 

Comparison of On-line SPE-HPLC and SPME-GC for 

86 Organics the Analysis of Microcontaminants in Water HPLC 

in water Chromatographia 41: 462-470 (1995) 

Rivasseau, C., Caude, M. 

Determination of Haloethers in Water by SPME 

217 Haloethers J. Chromatogr. A 769: 239-246 (1997) 100µm PDMS GC-FID 

in water Huang, S., Ting, C., Lin, C. 40 min, immersion 


Anaerobic biotransformation of trichlorofluoroethene in 

586 Trichlorofluoroether groundwater microcosms. 100µm PDMS GC-MS 

in water Environ-Sci-Technol. 15 Jun 1999; 33(12): 2040-2045 headspace 

Vancheeswaran,-S; Hyman,-MR; Semprini,-L salt, agitation 

Determination of Volatile Organic Compounds in Water 

90 Aromatics by Solid Phase Micro-Extraction and Infrared Spectroscopy parafilm, GC-FID 

in water Environ. Sci. Technol. 30: 1212-1219 (1996) 30 min 

Heglund, D., Tilotta, D. 

Poly(dimethylsiloxane) films as sorbent for SPME couple 

926 infrared spectroscopy PDMS IR 

J. Chromatogr. A (1998), 829(1-2) 377-384 

Merschman, S., Lubbad, S., Tilotta, D. 

Development of headspace SPME/attenuated total reflection 

942 Volatile organics infrared chemical sensing method for the determination o IR 

in water of volatile organic compounds in aqueous solutions 

Analytica Chimica Acta (2001), 436(1), 31-40 headspace 

Yang, Jyisy; Tsai, Shu-Sha 

505 Hydroxyaromatics 

Determination of hydroxyaromatic compounds in water by 

SPME coupled to HPLC PDMS/DVB or CW-TPR HPLC 

in water J. Chromatogr. A. (1999), 835(1+2), 127-135 

Wu, Y., Huang, S. 

280nm 

229 71 organics 

Calibration of a Commercial Solid-Phase Microextraction 

Device for Measuring Headspace Concentrations of 100µm PDMS GC-FID 

in gaseous mixture Organic Volatiles 25°C, 30 min 

Anal. Chem. 69: 364-372 (1997) 

Bartlet, R. 

headspace 

155 VOCs 

Sampling Volatile Organic Compounds Using a Modified 

Solid Phase Microextraction Device 100µm PDMS GC-MS 

in water J High Res. Chromatogr. 19(3): 155-60 (1996) 10 min 

Zhang, Z., Pawliszyn, J. 

Solid Phase Microextraction of Volatile Compounds Using 

headspace 

stirring, saturated salt 

205 Volatiles Carboxen-Polydimethylsiloxane Fibers 75µm Carboxen/PDMS GC-FID, ECD 

in water Chromatographia 46: 419-424 (1997) 30 min 

Popp, P., Paschke, A. headspace 

stirring 





Application of Solid-Phase Microextraction to the Analysis 


240 Volatiles of Volatile Organic Compounds in Water 100µm PDMS, GC-FID 

in water J. Chromatogr. A 742: 181-189 (1996) 85µm polyacrylate 

Santos, F., Galceran, M., Fraisse, D. 

Static headspace, SOME and headspace SPME for BTEX 

12 min 

stirring 

689 BTEX determination in aqueous samples by GC 100µm PDMS GC-FID 

in water Anal. Chim. Acta. 2000, 415(1-2), 9-20 

Menendex, J., Sanchez, M., Uria, J., Martinez, E., Medel, A. 

506 BTEX in 

In-tube SPME-GC of volatile compounds in aqueous solution 

Analyst (Cambridge, UK), 1999, 124(5), 651-655 1 meter capillary GC-FID 

water Tan, B, Marriott, P., Morrison, P., Lee, H. 

Carbon Isotope Analysis of Semivolatile Organic Compounds 

117 Solvents, C2-C4 acids in Aqueous Media Using SPME and Isotope Ratio polyacrylate, Carbowax, GC-MS 

in water Monitoring GC/MS cyclodextrin 

Anal. Chem. 69: 944-950 (1997) 10-30 min 

Dias, R., Freeman, K. stirring 


Application of Solid-Phase Microextraction to the Headspace 

GC Analysis of Semivolatile Organochlorine 100µm PDMS GC-ELCD 

semivolatiles in water Contaminants in Aqueous Matrices 87°C, 45 min 

J. Chromatogr. A 757: 173-182 (1997) headspace & 


Analysis of organochlorine compounds in water by SPME/GC 

immersion 

salt added 

507 Polar organics Fenxi Huaxue, 1999, 27(7), 768-772 100µm PDMS GC-ECD 

in water Zhang, D, Zhou, Z., Tang, Y., Wu, C., Zhen, W. Xu, Y. 

Protocol for the Analysis of High Concentrations of Benzene, 

70°C, headspace 

Chinese 

151 BTEX Toluene, Ethylbenzene, and Xylene Isomers in Water Using 100µm PDMS GC-FID 

in water Automated SPME-GC-FID 5 min 

Environ. Sci. Technol. 30: 1521 (1996) 

Thomas, S., Ranjan, S., Webster, G., Sarna, L. 

immersion 

154 Organics 

Solid Phase Microextraction Coupled to GC: A New Method 

for the Analysis of Organics in Water various fibers GC-MS, AED 

in water J. Chromatogr. A 733: 143 (1996) 

Eisert, R., Levson, K. 

and conditions 

Column siylation method for determining endocrine 

909 Endocrine disruptors from environmental water samples by SPME 

disruptors Talanta 2001, 54(6) 1039-1047 

in water Helaleh, M., Fujii, S., Korenaga, T. 

767 Ibuprofen, NBBS 

Elimination of Ibuprofen and NBBS in municipal purification 

plant analyzed by SPME 

in water Schiftenr (1999), 95, 1-148 

Huppert, N. 

(in german) 

162 Surfactants 

SPME Coupled with HPLC for Determination of Alkylphenol 

Ethoxylate Surfactants in Water Carbowax/TPR 100 HPLC 

in water Anal. Chem. 68: 1521-9 (1996) 50 min UV, 220nm 

Boyd-Boland, A., Pawliszyn, J. immersion 

stirring 

897 Surfactant 

Identification of alkyl dimethylbenzylammonium surfactants 

in water samples by SPME followed by ion trap LC/MS 

in water LC/MS and LC/MS/MS 

Environ. Sci. Technol 92001) 35(12) 2583-2588 

Ferrer, Imma; Furlong, Edward 


Identification and characterization of Fenton oxidation 

products of surfactants by EMS and SPME-GC-MS 





in water Fatty alcohol polyethoxy sulfates. 

Rapid Commun, Mass Spectrom 2000, 14(10), 834-839 

Cuzzola, A., Raffaelli, A., Saba, A., Salvadori, P. 


Assessment of polycystalline graphites as sorbents for 

SPME of nonionic surfactants 

in water J. Chromatogr. A (2000) 888(1-2) 35-41 

Aranda, R., Kruus, P., Burk, R. 

508 Diethylphthalate 

Trace determination of diethylphthalate in aqueous media 

by SPME-HPLC 60µm DVB/PDMS HPLC 

in water J. Chromatogr. A 841(1999) 177-185 15 min immersed UV, 226nm 

Kelly, M., Larroque, M. NaCl 

804 Phthalic diesters 

Determination of phthalic diesters in water by solid-phase 

microextraction-capillary gas chromatography 100µm PDMS 

in water Sepu (2000) 18(6), 568-570 

Liu, Z. L.; Xiao, C. H.; Wu, C. Y.; Han, H. M. 

Determination of diethylhexyl phthalate in water by SPME-HPLC 

headspace 

(in Chinese) 

2721 Diethylhexyl Talanta 69, #5, 1095-1099 (2006-07-15) HPLC 

phthalate in 

water 

Kayali, N.; Tamayo, F. G.; Polo-Diez, L. M. 

Determination of phthalates and adipate in bottled water by 

2449 Phthalates esters headspace SPME and gas chromatography/mass spectrometry 65µm DVB/PDMS GC-MS 

in bottled water Journal of Chromatography A 1178, #1-2, 231-238 (2008) headspace 

Xu-Liang Cao 

10 and 30% NaCl 

In-tube SPME-LC analysis of phthalate esters in 

588 Phthalates esters water samples 40m x 0.25mm capillary HPLC 

in water Chromatography. Jun 1999; 20(2): 124-125 

Saito,-Y; Nakao,-Y; Jinno,-K 

782 Butylphthalates 

Fiber-in-tube solid-phase microextraction: a fibrous rigid-rod 

heterocyclic polymer as the extraction medium HPLC 

in water Fresenius' J AnalChem (2000) 368(7), 641-643 

Saito, Y.; Nakao, Y.; Imaizumi, M.; Takeichi, T.; Kiso, Y.; Jinno, K 

20min. 

Distribution coefficients of phthalates between absorption fiber and 

2335 Phthalates esters water and its using in quantitative analysis 85µm polyacrylate GC-FID 

in wastewater Anal. Chim. Acta 560 #1-2, 110-117 (2006) 100µm PDMS 

Garbowska, Katarzyna; Isidorov, Valery A.; Kotowska, Urszula immersed 

691 Phthalates esters 

Determination of phthalate esters in water samples by 

SPME and GC with mass spectrometric detection 85µm polyacrylate GC-MS 

in water J. Chromatogr. A (2000), 872 (1&2), 191-201 90min @ 45°C 

Penalver, A., Pocurull, E, Borrull, F., Marce, R. NaCl added 

801 Phthalates esters 

Methods for routine analysis of phthalates in food 

and the environment GC-FID/MS 

in water Deutsche Lebensmittel-Rundschau (2000) 96(11), 411-417 

Baerwinkel, D.; Haufe, J.; Kroh, L. W 

178 4-Nonylphenol 

Determination of 4-Nonylphenol. Part 2: Orthogonal Array 

Design as a Chemometric Method for the SPME of 100µm PDMS GC-FID 

in sea water 4-Nonylphenol in Water 30 min 

J. Microcolumn Sep. 8 (2): 131-136 (1996) immersion 

Chee, K., Wong, M., Lee, H. stirring 

219 BTEX 

Direct Solid Phase Microextraction for the Determination 

of BTEX in Water and Waste Water 100µm PDMS GC-FID 

in water J. High Res. Chromatogr. 19: 472-474 (1996) 10 min 

Valor, I., Cortada, C., Molto, J. stirring 

A New Porous-Layer Activated-Charcoal-Coated Fused 





208 BTEX compounds Silica Fibre: Application for Determination of BTEX 100µm charcoal coated GC-FID 

in water Compounds in Water Samples Using Headspace SPME and fiber / PDMS 

Capillary Gas Chromatography 25°C, 15 min 

Chromatographia 45: 183-189 (1997) stirring 

Djozan, D., Assadi, Y. salt added 


Analysis of Chlorinated 1,3-Butadienes by SPME and GC-MS 

J. Chromatogr. A 737: 85-91 (1996) 100µm PDMS GC-MS 

1,3-butadienes Fattore, E., Benfenati, E., Fanelli, R. 30 min 

in water 

SPME method for the quantitative analysis of styrene in water 

immersion 

692 Styrene J. Chromatogr.Sci. (2000), 38(7), 315-318 85µm polyacrylate GC-FID 

in water Silva, F., DeCarvalho, C., Cardeal, Z. 10mn @ 55°C 

headspace 

2837 Furan in the 

Primary product distribution from the Cl-atom initiated atmospheric 

degradation of furan: Environmental implications air sample GC-MS 

atmospher Atmospheric Environment 41, #31, 8796-8810 (DEC 2007) 

Villanueva, F; Barnes, I.; Monedero, E.; Salgado, S;Gomez, M; Martin, P. 

776 Dioxin, Furans 

Determination of dioxins and furans in water sample by 

HRGC/HRMS and pretreatment using SPME GC-MS 

in water Organohalogen Compd (2000) 45, 68-71 

Eom, S; Ahn, So; Kim, M; Shin, J 

2367 Review 

Trends in solventless sample preparation techniques for 

environmental analysis 

J. BIOCHEM. BIOPHYS. METHODS 70,# 2, 275-288 (10 MAR 2007) 

Wardencki, W.; Cury&lstrok;o, J.; Namiesnik, J. 

Review article 


Trends in Extraction of Semivolatile Compounds from Water 

for Environmental Analysis 

in water Anal. Commun. 33 (9): 15H-17H 

Poole, S., Poole, C. 


Studies of the composition of distillates from leachate by 

GC-MS coupled to SPME GC-ms 

in water Rapid Commun. Mass Spectrom (1999), 13(10), 966-970 pH 4 or 10 

Saba, A., Pucci, S., Raffaekki, A., Salvadori, P. headspace/immersed 

2607 Monocarboxylic 

Structure and isotopic ratios of aliphatic side chains in the insoluble 

organic matter of the Murchison carbonaceous chondrite GC 

acids from Earth Planet. Sci. Lett. (Netherlands) 259, #3-4, 517-25 (2007) 

carbonaceous 

chondrite 

Yongsong Huang; Alexandre, M.R.; Yi Wang 

807 Petroleum 

Application of SPME chromatography with mass 

spectrometry to the analysis of gasoline content in water 

hydrocarbons Huaxue Fence (2000) 36(10) 465-466 

in water Chen, X. D.; Zhou, H 

216 Petroleum 

Water Analysis by Solid-Phase Microextraction Based on 

Physical Chemical Properties of the Coating 100µm PDMS GC-FID 

hydrocarbons Anal. Chem. 69(11): 1992-1998 (1997) 30 min 

in water Saraullo, A., Martos, P., Pawliszyn, J. 

Application Methods of SPME for the Classification of BTEX 

headspace 

stirring 

272 BTEX GIT Labor-Fachz. 41 (12): 1191-1195 (1997) 

Van der Heide, M., Petry, P. 

SPME as a Method for Preparing Environmental Samples 

273 Pol. J. Environ. Stud. 6 (5): 5-12 (1997) 

Ligor, M., Buszewski, B. 





SPME in Pretreatment of Environmental Samples 


274 Huaxue Jinzhan 10 (1): 74-84(1998) 

Jia, J., He, Y., Huang, J. 

Direct SPME of Complex Aqueous Samples with Hollow 

275 Aqueous samples Fiber Membrane Protection 

Anal. Commun. 33 (7): 219-221(1996) 

Zhang, Z., Poerschmann, J., Pawliszyn, J. 

The degradtion of humic substance using continuous 

2838 Organics from photocatalysis systems GC 

humic material Sep. Sci. Technol. 43, #1, 93-112 (January 2008) 

Areerachakul, N.; Duangduen, C.; Kandasamy, J.; Vigneswaran, S. 

Partitioning of selected environmental pollutants into organic matter 

2618 Organics from as determined by solid-phase microextraction GC 

humic material Chemosphere 66, #8, 1580-1589 (2007-01) 

Prosen, H.; Fingler, S.; Zupancic-Kralj, L.; Drevenkar, V. 

Bioavailability of PCBs from field-collected sediments: Application 

2801 PCBs in sediment of Tenax extraction and matrix-SPME techniques GC 

Chemosphere 71, #2, 337-344 (MAR 2008) 

Trimble, Tricia A.; You, Jing; Lydy, Michael J. 

Availability of polychlorinated biphenyls in field-contaminated sediment 

2631 PCBs in sediment Env Tox Chem 26, #9, 1940-1948 (SEP 2007) GC 

You, Jing; Landrum, Peter E.; Trimble, Tricia A.; Lydy, Michael J. 

Sorption of very hydrophobic organic compounds onto 

693 Alkanes, PCBs,PAHs PDMS and dissolve humic organic matter. 1. Adsorption or 7um, 30um PDMS GC-MS 

in humic material partitioning of VHOC on PDMS coated SPME fibers- 20 min SIMS 

never-ending story stirring 

Environ Sci Technol 2000, 34, 3824-3830 

Poerschmann, J., Gorecki, T., Kopinke, G. 

Sorption of hydrophobic organic compounds on nonpolar 

844 Hydrophobic organics SPME fibres and dissolved humic organic matter long dash PDMS, polyacrylate GC-MS 

in humic material Part III: Application of the solubility parameter concept to 

interpret sorption on SPME fibre coatings 

J Microcolumn Separations (2000) 12(12), 603-612 

Poerschmann, J. 

923 

Use of SPME for measuring oil-water partition coefficients and 

correlation with HPLC methods for lipophilicity 

J. Chromatogr A (1999) 864(2) 183-189 

Pollein, P., Roberts, D. 

HPLC 

276 Phenols, PAHs 

SPME for Determining Distribution of Chemicals in 

Aqueous Matrixes 100µm PDMS GC-MS 

in wastewater Anal. Chem. 69 (4): 597-600 (1997) 10 sec 

Zhang, A., Kopinke, G., Pawliszyn, J. stirring 

277 Chlorinated organics 

Water Solubility and Octanol/Water-Partitioning of 

Hydrophobic Chlorinate Organic Substances Determined 

in water by Using SPME/GC 

Fresenius’ J. Anal. Chem. 360 (1): 52-57 (1998) 

Paschke, A., Popp, P. 

278 Phenols 

Determination of Phenols by Solid-Phase Microextraction 

J. Chromatogr. A 767 (1+2): 171-175 (1997) 85µm polyacrylate GC-FID 

in water Bartak, P., Cap, L. 

Determination of Chlorophenols Using SPME and GC/MS 

25°C, 60 min 

headspace 


439 Chlorophenols Ann. Chim. (Rome) (1998), 88(9-10), 629-635 GC-MS 

in water Guidotti, M., Ravaioli, G. 

Determination of volatile organic compounds pollution sources in 





2617 Organics in Malaysian drinking water using multivariate analysis 100µm PDMS GC-MS 

drinking water Environ. Monit. Assess. 124, #1-3, 39-50 (January 2007) 

Abdullah, Pauzi; Soh, Shiau-Chian 


Evaluation of SPME as an alternative to the official method for the 

analysis of organic micro-pollutants in drinking water 65µm PDMS/DVB GC-MS 

drinking water J. Chromatogr. A, 1101, #1-2, 46-52 (2006) 

Guillot, Sophie; Kelly, Mary T.; Fenet, Helene; Larroque, Michel 

30 min @ 60°C 

777 Organics 

Solid phase extraction techniques for drinking water 

abstraction monitoring and investigation of pollution GC-MS 

in drinking water incidents 

J Water Supply Res and Tech (2000) 49(2), 103-109 

Gardner, M.; Comber, S. ; Rogers, H. 

944 Organics 

Determination of water contaminants at trace levels using 

large volume sampling techniques: Comparison of LVPTVI, 

in water LVOCI, and SPME. 

American Laboratory (2001) 33(11), 45-47 

Trisciani, A.; Munari, F.; Anelli, L.; Castanho, J. 

279 VOCs 

Pollution of Ground and Drinking Water with Volatile 

Organic Compounds, SPME and GC/MS Analysis GC-MS 

in water Toxicol. Environ. Chem. 55 (1-4): 73-81 (1996) 

Hassan, A., Benfenati, E., Facchini, G., Fanelli, R. 

280 Trihalomethanes 

Determination of Trihalomethanes in Drinking Water by 

SPME-GC with Electron-Capture Detection GC-ECD 

in water Toxicol. Environ. Chem. 60(1-14): 39-45 (1997) 

Chen, M., Mao, I., Hsu, C. 

Determination of Chlorinated Acetic Acids in Drinking 

281 

Chloroacetic acid 

esters Water by in situ Derivatization and Solid Phase 30µm PDMS GC-ECD 

in water Microextraction 1 min 

Int. J. Environ. Anal. Chem. 66 (3): 215-224(1997) headspace 

Aikawa, B., Burk, R. 

Studies on the application of SPME for analysis of volatile 

stirring 

methanolic HCl added 

510 Sulfur compounds in organic sulfur compounds in gaseous and liquid samples FPD-GC 

water, N2 & propane Chem. Anal. (Warsaw), 1999, 44(3A), 485-493 

Wardencki, W., Namiesnik, J. 

339 Geosmin, 2-MIB 

Rapid Analysis of Geosmin and 2-Methylisoborneol in Water 

Using SPME Procedures 100µm PDMS GC-MS 

in water Water Research Vol. 32, No. 7, 2140-2146 (1998 40°C, 30 min 

Lloyd, S., Lea, J., Zimba, P., Grimm, C. 

Analysis of 2-Methylisoboreneol and Geosmin in Catfish 


salt added 

362 2-MIB, geosmin by Microwave Distillation-SPME 100µm PDMS GC-MS 

in catfish J. Agri. Food Chem., 47, No. 1, pg. 164-169, 1999 40°C, 30 min 

Lloyd, S., Grimm, C. 

Determination of Geosmin and 2-Methylisoboreneol in Water 


salt added 

80µm 

446 MIB & geosmin Using SPME and GC-Chemical Ionization/Electron Impact 

Carboxen/DVB/PDMS GC-MS 

in water Ionization Ion Trap MS 60°C, 30 min 

Analyst (Cambridge, U.K.) (1998), 123 (10), 2155-2160 headspace 

McCallum, R., Pendleton, P., Scumann, R., Trinh, M. stirring 

salt added 

2778 Ozone in air 

Passive sampling of ambient ozone by SPME with on-fiber derivatization 

Analytica Chimica Acta: 610, #2, 149-155 (MAR 10 2008) 65µm DVB/PDMS GC-ECD 

Lee, I-Su; Tsai, Shih-Wei PFBHA & DPE 

derivatives @ 25°C 





Tacoma controls tastes and odours with ozone 


2375 Odor compounds Water Science and Technology 55, # 5, 137-144 ( 2007) 

in water Carlson, M.; Chen, T.; McMeen, C.; Suffet, I. H.; Zhang, M 

511 34 Odor compounds 

Headspace SPME for the determination of trace levels of 

taste and odor compounds in water samples 65µm DVB/PDMS GC-Ion trap 

in water Analyst (Cambridge, UK) 1999, 123(4), 459-466 40 min @ 20°C MS 

Bao, M., Mascini, M., Griffini, O., Burrini, D., Santianni, D., NaCl, stirring 

Barbieri, K. immersion/headspace 


On-Site Sample Work-Up Procedures to Isolate Chemical 

Warfare-Related Compounds, Using SPE & SPME Technology 

compounds Analytical Chemistry Associated with the Destruction of 

Chemical Weapons NATO ASI Ser., Ser. 1 13: 65-76 (1997) 

Alcaraz, A., Hulsey, S., Whipple, R., Andresen, B. 

2349 Nerve agents 

Synthetic methods applied to the detection of chemical 

warfare nerve agents 

CURR. ORG. CHEM. 11, #3, 255-265 

Giordano, B. C.; Collins, G. E 

Review article 

116 Nerve agents 

Determination of Chemical Warfare Agents in Natural 

Water Samples by SPME 65µm PDMS/DVB GC-FID 

in water Anal. Chem. 69: 1866-1872 (1997) 30 min GC-MS 

Lakso, H., Ng, W. headspace 


762 Lewisite oxide 

Determination of Lewisite oxide in soil using SPME 

followed by GC w/FPD or Mass spectormetric detection 100µm PDMS GC-FPD/or 

in soil J. Chromatogr-A, 909 (2001) 13-28 20min. GC-MS 

Tomkin, B., Sega, G., Ho, C. agitated 

1,3-propanedithiol derv. 


In-situ derivatisation of degradation products of chemical 

warfare agents in water by SPME and GC-MS analysis 65µm Carboxen/PDMS GC-MS 

agents in water J. Chromatogr-A, Feb 1999, 832(1+2), 173-182 20°C, 

Sng, M., Ng., W. 

Rapid Determination of Volatile Organic Compounds in 

N-methyl-N-(tert-butyl 

dimethylsilyl) trifluoroacetamide 

derivative 

283 Volatiles Environmentally Hazardous Wastewaters, Using SPME 

in wastewater Anal. Chem. 358 (7-8): 833-837 (1997) 

James, K., Stack, M. 

284 TNT, DNT salt 

Trace salt Signatures from World War II 

Unexploded Undersea Ordinance 65µm PDMS/DVB directly 

in seawater/ Environ. Sci. Technol. 32 (9): 1354-1358 (1998) 15 min into MS 

sediment Darrach, M., Chutjian, A., Plett, G. pH 8 

agitation 

285 Aromatic amines 

Determination of Aromatic Amines by SPME-GC-MS 

in Water Samples 65µm Carbowax/DVB GC-MS 

in water J. Chromatogr. A 791(1+2): 221-230 (1997) 30 min 

Muller, L., Fattore, E., Benfenati, E. 

SPME coupled with HPLC for the determination of 

stirring 

pH 7.6, salt added 

65µm PDMS/DVB, CW- 

578 Aromatic amines aromatic amines. 

TPR HPLC-UV 

in water Anal-Chem. 15 Jan 1999; 71(2): 310-318 

Wu,-Y-C; Huang,-S-D 

280nm 

286 Volatiles 

Inter-Laboratory Studies for the Validation of SPME for 

the Quantitative Analysis of Volatile Organic Compounds 100µm PDMS GC-ECD 

in water Compounds in Aqueous Samples 30 min 

Anal. Chim. Acta 356 (2-3): 113-123 (1997) headspace & 

Nilsson, T., Ferrari, R., Facchetti, S. immersion 





Solid-phase micro-extraction of volatiles from water 

Conditions 

stirring 

Instrument 

597 Volatiles (BTEX) using open cap vials 100µm PDMS GC-FID 

in water Chromatographia. May 1999; 49(9-10): 513-519 5 min. @ 25C 

Matisova,-E; Sedlakova,-J; Simon,-P; Welsch,-T stirred 

287 VOCs, pesticides 

Capabilities for the Direct Determination of Triphenyland 

Triethylarsine in Water by SPME Followed by GC-A Carboxen/PDMS, GC-MS 

in water and air Amer. Environ. Lab, 9 (10): cover, 5-6 (1997) 100µm PDMS 

Mothes, S., Wennrich. R. various conditions 

374 Organoarsenicals 

Determination of Organoarsenicals in the Environment by 

SPME-GC-MS 100µm PDMS GC-MS 

in water and soil J. Chromatogr. A 807 (1998) 253-263 10 min 

Szostek, B., Aldstadt, J. immersion 

methyl thioglycolate 

(derivative) 

879 Organoarsenicals 

SPME method for GC w/MS and pulsed Flame photometric 

detection: studies of organoarsenical speciation 100µm PDMS GC-MS 

in water J. Chromatogr. A 918(2001) 169-175 10 min GC- PFPD 

Killelea, D., Aldstadt, J. immersion 

methyl thioglycolate 

(derivative) 

Speciation of organoarsenic compounds by poly(pyrrole)- 

790 Organoarsenicals coated capillary in-tube SPME coupled with HPLC-EI-MS Polypyrrol capillary LC-EI-MS 

in water Analytica Chimica Acta (2000) 424(2), 211-222 

Wu, J. C.; Mester, Z.; Pawliszyn, J. 

815 Metal hydrides 

Sampling and determination of metal hydrides by SPME 

thermal desorption inductively coupled plasma MS Carboxen/PDMS, ICP-MS 

in water J. Analytical Atomic Spectrometry (2000) 15(11) 1461-1465 

Mester, Z.; Sturgeon, R. E.; Lam, J. W Sodium Borohydride/HCl 

2894 Disinfection 

Emerging technologies for identification of disinfection byproducts: 

GC/FT-ICR MS characterization of solvent artifacts GC/FT-ICR MS 

byproducts Environ Sci& Tech 41, #15, 5419-5425 (AUG 1 2007) 

in water Heffner, C.; Silwal, I.; Peckenham, J..; Solouki, T. 

288 Iodinated volatiles 

SPME with Temperature-Programmed Desorption for the 

Analysis of Iodinated Disinfection Byproducts 85µm polyacrylate GC-ECD 

in water Anal. Chem. 70 (3): 638-644 (1998) 15 min 

Frazey, P., Barkley, R., Siever, R. immersion 

stirring 


Determination of Chloroethers in Aqueous Samples, 

Using SPME GC-FID or MS 

in water Acta Hydrochim. Hydrobio. 25 (6): 329-334 (1997) 

Wennrich, L., Engewald, W., Popp, P. 


GC trace analysis of haloethers in water: Comparison of 

different extraction techniques GC-FID or MS 

in water Int. J. Environ.Anal. Chem (1999), 73(1), 31-41 

Wennrich, L., Engewald, W., Popp, P. 

514 Aliphatic aldehydes 

Influence of extraction parameters and medium on efficiency 

of SPME sampling in analysis of aliphatic aldehydes 100µm PDMS GC-MSD 

in water/oil J. Chromatogr., A 1999, 845(1+2), 337-347 30 min @ 40°C 

Keszler, A., heberger, K. immersed/headspace 

515 Glycerol ethers 

Improved extraction of glycerol ethers from water by SPME 

by Carboxen-PDMS coated fiber 75µm Carboxen/PDMS GC-FID 

in water Chromatogrophia, 1999, 50 (3/4), 155-159 25°C, sat. NaCl 





Bensoam, J., Cicolella, A., Durjardin, R. immersed 

516 Amines/alcohols 

Evaluation of SPME for the anlaysis of hydophilic 

compounds 75µm Carboxen/PDMS 

in water J. Exposure Anal.Environ. Epidemiol. 1999, 9(3) 181-191 

Shoemaker, J. Munch, J., Behmer, T. 

517 Polar volatiles 

SPME of volatile polar compounds in water 

J. High Resolut. Chromatogr. (1999), 22(2), 109-115 85µm polyacrylate GC-MS 

in water Matisova, E, Sedlakova, J., Slezackova, M., Welsch, T. 

On-Site Sampling for Volatiles and Pesticides, Using SPME 

50°C 

headspace 

290 VOCs, pesticides Amer. Environ. Lab. 10 (2): 21-22 (1998) 100µm PDMS, GC-MS 

in water and air Shirey, R., Mani, V, Mindrup, R. 75µm Carboxen/PDMS 

2-3 min, headspace 


291 Petroleum 

Solvent-Free and Rapid Determination of Petroleum 

Hydrocarbons in Water by SPME 

hydrocarbons UFZ-Ber. Optimierung Umweltvertiraeglicher 

in water Analysenverfahren fuer Mineraloelkohlenwasserstoff 

IM Boden 12: 14-17 (1997) 

Christall, B. 

Partition Infrared Method for Total Gasoline Range Organics 

367 C3-C16 hydrocarbons in Water Based on SPME 130µm Teflon film IR 4000-2690 

in water Environ. Sci. Technol, 1999, 33, 814-819 30 min cm-1 

Stahl, D., Tilotta, D. immersion 

518 MMT in 

Determination of methylcyclopentadienylmanganese 

tricarbonyl (MMT) in aqueous samples by SPME-GC-AED 100µm PDMS GC-AED 

water Analyst (Cambridge, UK), (1999), 124(1), 71-73 15 min @ 20°C 

Yang, F., Chau, Y. headspace 

SPME combined with GC-AED for the determination of cyclopentadienyl- 

2665 MMT in manganese tricarbonyl and (methylcyclopentadienyl)manganese headspace GC-AED 

water tricarbonyl in soils and seawaters 

J. Chromatogr. A 1173, #1-2, 139-145 (Nov 30 2007) 

Campillo, N.; Hernandez-Cordoba, Manuel; Penalver, Rosa 

849 MMT in 

Determination of methylcyclopentadienylmanganesel 

tricarbonyl by SPME-direct thermal desorption-quartz GC-AED 

water furnace atomic absorption spectrometry 

Spectrochim. Acta, Part B (2001) 56B(2) 215-222 

Fragueiro, M. S.; Alava-Moreno, F.; Lavilla, I.; Bendicho, C 

Uncertainty associated to the analysis of organochlorine pesticides in 

2706 Organochlorine water by SPME-GC-ECD-Evaluation using two different approaches headspace GC-ECD 

pesticides in Analytica Chimica Acta; Vol. 573-574, 202-208 (2006-07-28) 

water Ratola, Nuno 

Analytical methods for PCBs and organochlorine pesticides in 

2852 Review article environmental monitoring and surveillance: A critical appraisal 

Anal. Bioanal. Chem. 386, #4, 769-789 (October 2006) 

Muir, Derek; Sverko, Ed 

2409 Pesticides, PCBs 

Simultaneous analysis of PCBs and organochlorine pesticides in water 

by headspace SPME with GC-MS 100µm PDMS GC-ECD 

from water J. Chromatogr., A 1138, #1-2, 231-243 (2007-01-05) 

Derouiche, A.; Driss, M. R.; Morizur, J. -P.; Taphanel, M. -H. 

headspace 

519 VOCs, BTEX, 

Efficiency of direct SPME from water: Comparison of 

different fiber types including a new C8-coating variety of fibers 





pesticides, PCBs Chromatographia, 1999, 49(11/12), 686-690 

from water Popp, P., Paschke, A. 

904 pesticides 

Analysis of fire ant pesticides in water by SPME and GC-MS 

and LC-MS GC-MS & 

in water Analytica Chimica Acta 2001, 436(1) 11-20 

Reyzer, M., Brodbelt, J. 

LC-MS 

Optimisation and validation of a SPME method for simultaneous 

2413 Pesticides determination of different types of pesticides in water by GC-MS 60µm PDMS/DVB GC-MS 

in water J. Chromatogr., A 1141, #2, 165-173 (2007-02-09) 

Beceiro-Gonzalez, E. ; Concha-Grana, E.; Guimares, A.; Goncalves, C.; 

Muniategui-Lorenzo, S.; Alpendurada, M. 

45 min @ 60°C 

770 Chlorine, nitrogen 

Multiresidual method for determination of chlorine, 

nitrogen, and phosphorus containing pesticides in surface GC/ECD/NPD 

phosphorus and drinking water by SPME and GC/ECD/NPD 

pesticides Boll. Chim. Ig., Parte Sci. (2000) 51(S3), 99-103 

in water de Luca, Giuseppe; Mura, Michele 

(in Italian) 

512 Iodinated THMs 

SPME for the determination of iodinated trihalomethanes in 

drinking water 65µm CW/DVB/PDMS GC-ECD 

in drinking water J. Chromatogr., A (1999), 841(2), 197-206 10 min @ 20°C 

Cancho, B., Ventura, G., Galceran, M. NaCl used 

292 Iodinated organics 

Solid Phase Microextraction and Analysis of Iodinated 

Organic Compounds 85µm polyacrylate GC-ECD 

in water Avail. UMI, Order No. DA9812871 from: 

Diss. Abstr. Int., B 58 (10): 5364 (1998) 

Frazey, P. 

288 Iodinated volatiles 

SPME with Temperature-Programmed Desorption for the 

Analysis of Iodinated Disinfection Byproducts 85µm polyacrylate GC-ECD 


Frazey, P., Barkley, R., Siever, R. 

Simultaneous determination of cyanogen chloride and 

immersion 

stirring 

694 Cyanogen chloride cyanogen bromide in treated water at sub-ug/L levels by a Carboxen/DVB/PDMS GC-ECD 

in water new SPME-GC-ECD method 15 min, headspace 

J. Chromatogr. A 897(2000) 307-315 

Cancho, B., Ventura, F., Galceran, M. 

2-3pH, 25% salt added 

Determination of acetic acid in aqueous samples, by 

695 Acetic acid water-phase derivatization, SPME, and GC 85µm Polyacrylate GC-FID 

in water J. Chromatogr. A., (2000), 874(2), 225-234 headspace 

Wittmann, G., Van Langenhove, H., Dewulf, J. benzenal bromide derv. 

Determinationof Chlorinated Acetic Acids in Drinking 

411 Chloroacetic acids Water by in-situ Derivatization-SPME 

in water Interri J. Environ. Anal. Chem. 66: 215-224 (1997) 

Aikawa, B., Burk, R. 

SPME coupled with GC-ion trap mass spectrometry for the 

520 Haloacetic acids analysis of haloacetic acids in water GC-Iontrap 

in water J. Chromatogr., A 1999, 859(2), 159-172 MS 

Sarridon, M., Santos, F., Galceran, M. 

696 Haloacetic acids 

In situ derivatization/SPME for the determination of 

haloacetic acids in water Carboxen/PDMS GC-ITMS 

in water Anal. Chem. 2000 Oct. 15, 72(20), 4865-4873 

Sarrion, M. Santos, F., Galceran, M. 

Using SPME to Determine Partition Coefficients to Humic Acids 

headspace 

dimethyl sulfate derv. 

353 Chlorobenzenes and Bioavailable Concentrations of Hydrophobic Chemicals 7µm PDMS GC-FID 

in water Environ.Sci Technol, 1998, 32, 3430-3435 20 min 

Ramos, E., Meijer, S., Vaes, W., Verhaar, H., Hermens, J. 

SPME-capillary GC determination of chlorobenzene 

immersion 

pH 7 





576 Chlorobenzenes compounds in water 100µm PDMS GC-ECD 

in water Lihua-Jianyan,-Huaxue-Fence. Mar 1999; 35(3): 103-105 5 min, agitated 

Yang,-HB 

Trace analysis of ten chlorinated benzenes in water 

0.5gm NaOH 

immersed 

697 Chlorinated by headspace SPME 100µm PDMS GC-MS 

benzenes in J. Chromatogr. A (2000) 874(1), 149-154 headspace 

water He, Y., Wang, Y., Lee, H. salt, agitated 

698 Fungicides 

Determination of fungicides in natural waters using SPME and 

GC coupled with ECD and MS detection 100µm PDMS GC-MS 

in water J. Chromatorgr A., 893 (2000), 143-156 30 min, agitated 

Lambropoulou, D., Konstantinou, I., Albanis, T. 

New cloud vapor zone (CVZ) coupled headspace SPME technique 

20% NaCl, pH 4 

immersed 

2527 Chlorothalonil Anal Bioanal Chem 388, #2, 377-83 (2007 May) 100µm PDMS 

in water Huang, Yi-Ching; Su, Yi-Song; Muniraj, Sarangapani; Zhang, W.; Jen, J. 5°C 

headspace 

699 Chlorothalonil 

Determination of aqueous chlorothalonil with SPME-GC 

J. Chromatogr. A, 896 (2000) 105-110 100µm PDMS GC-ECD 

in water Chen, S., Su, Y., Jen, J. 40 min, 

800 Alachlor 

Optimization of alachlor solid-phase micro-extraction from 

water samples using experimental design. 60µm PDMS/DVB HPLC 

in water J. Chromatogr. A (2000) 896(1-2), 373-379 120min @ 25°C 

Gonzalez-Barreiro, C.; Lores, M.; Casais, M. C.; Cela, R. stirred 

2786 Pyrethroids in 

Simultaneous determination of traces of pyrethroids, organochlorines 

and other main plant protection agents in agricultural soils 85µm polyacrylate GC-µECD 

soil by headspace SPME-GC-MS headspace 

J. Chromatogr. A, 1188, #2, 154-163 (Apr 25 2008) 100 °C 

Cela, R.; Dagnac, Thierry; Fernandez-Alvarez, M.; Garcia-Jares, C.; 

Lamas, J.; Llompart, Maria; Lores, Marta 

Application of SPME for determination of pyrethroids in groundwater 

2787 Pyrethroids in using LC with post-column photochemically induced 60µm PDMS/DVB LC fluorescencene 

groundwater fluorimetry derivatization and fluorescence detection fluorimetry 

J. Chromatogr. A, 1188, #2, 61-68 (Apr 25 2008) 

Galera, M. Martinez; Mughari, Ahmed R.; Vazquez, P. Parrilla 


2403 Chloroacetanilide 

Analysis of chloroacetanilide herbicides in water samples by SPME-GC-MS 

Anal. Chim. Acta 591, #1, 87-96 (2007-05-15) GC-MS 

herbicides in 

water 

Xu, X. Q.; Yang, H. H.; Wang, L.; Han, B.; Wang, X. R.; Lee, F. S.-C 

Gas-Phase Post-Derivatization Following SPME for 

293 Acidic herbicides Determining Acidic Herbicides in Water 85µm polyacrylate GC-MS 


Lee, M., Lee, R., Lin, Y., Chen, C., Hwang, B. immersion, stirring 


diazomethane (deriv.) 

905 Acidic herbicides 

Derivatisation/SPME followed by GC-MS for the analysis 

of phenoxy acid herbicieds in aqueous samples GC-MS 

in water J. Chromatogr. A (1998),826(2), 211-216 

Nilsson, T., Baglio, D., Miguez, I., Madsen, J., Facchetti, S. 

898 Acidic herbicides 

Automated on-line in-tube SPME followed by LC/electrospray 

ionization mass spectrometry for the determination of LC-MS 

in water chlorinated phenoxy acid herbicides in environmental waters 

Analyst (Cambridge, U. K.) 2001 , 126(5) 602-608 

Takino, Masahiko; Daishima, Shigeki; Nakahara, Taketoshi 





763 Profoxydim 

Application of on-site SPME in aquatic dissipation studies 

of profoxydim in rice 50µm Carbowax-TPR HPLC-UV 

in water J. Chromatogr A, 909 (2001) 29-36 30min. 

Eisert, R, Jackson, S., Krotzky, A. 

SPME of the antifouling Irgarol 1051 and fungicides 

salt added 

immersed 

521 Fungicides dichlofluanid and 4-chloro-3-methylphenol in water samples 85µm polyacrylate GC-MS 

in water J. Chromatogr. A, (1999), 839(1+2), 253-260 1 hr. @ 60°C 

Penalver, A., Pocurull, E., Borrull, F., Marce, R. immersion, salt added 

568 T2 mycotoxin 

Determination of trichothecene (T2 mycotoxin) in aqueous 

sample with solid-phase microextraction technique 85µm polyacrylate GC-FID 

in water followed by GC-FID 75 min, immersed 

J-High-Resolut-Chromatogr. Jul 1999; 22(7): 424-426 satr. salt 

Lee,-PK; Kee,-SYK; Ng,-W; Gopalakrishnakone,-P stirred 

294 PAHs 

SPME of PAHs from Aqueous Samples, Using Fibers Coated 

with HPLC Chemically Bonded Silica Stationary Phases 100µm silica/epoxy GC-FID, -MS 

in water Anal. Chem. 69 (24): 5001-5005 (1997) 60°C, 30 min 

Liu, Y., Lee, M., Hageman, K., Yang, Y, Hawthorne, S. headspace 

295 PAHs 

Separation and Determination of Polycyclic Aromatic 

Hydrocarbons by SPME/Cyclodextrin-Modified Capillary 

Electrophoresis 

Anal. Chem. 69 (9): 1726-1731 (1997) 

Nguye, A., Luong, J. 

700 PAHs 

Monitoring of PAH in water using headspace SPME 

and capillary GC 

in water Microchem J. (1999), 63(2), 276-284 

Djozan, D., Assadi, Y. 

701 PAHs 

SPME for determining the distribution of sixteen USEPA 

polycyclic aromatic hydrocarbons in water samples 

in water J. Chromatogr. A. (2000) 879, 177 

Doong, R., Chang, S., Sun, Y. 

Determination of Aromatic Compounds in Water by SPME 

296 Aromatics and Ultraviolet Absorption Spectroscopy PDMS chip UV spectroscopy 

in water Anal. Chem. 69 (1): 1197-1203 (1997) 30-50 min 220-300nm 

Wittkamp, B., Hawthorne, S., Tilotta, D. immersion 

Trace Analysis of salt in Seawater Using SPME and 

344 RDX, TNT metabolites GC-Ion Trap Mass Spectrometry Carbowax/DVB GC-MS 

in salt water Anal. Chem., Vol. 70, No. 14, July 15, 1998, pg. 3015-3020 10 min 

Barshick, S., Griest, W. immersion 

stirring 

Characterization of Water-Soluble Components of Slurries 

297 Phthalates, surfactants Using SPME Coupled to LC-MS 65µm Carbowax/TPR LC-MS 

in water J. Microcolumn Sep. 10 (2): 225-234 (1998) 1-15 hr. 

Moder, M., Popp, P., Pawliszyn, J. pH 2, satr. salt 


Comparative studies of the leachate of an industrial landfill 

by GC-MS,LC-nuclear magnetic resonance and LC-MS GC-MS 

compounds J-Chromatogr,-A. 29 Jan 1999; 831(2): 243-256 

in leachate Benfenati,-E; Pierucci,-P; Fanelli,-R; Preiss,-A 

Godejohann,-M; Astratov,-M; Levsen,-K; Barcelo,-D 

Development of a headspace SPME procedure for the 

702 Fatty acids determination of free volatile fatty acids in waste wate 85µm Carboxen/PDMS GC-FID, MS 

in waste water J Chromatogr. A,(2000) 873(1), 107-115 headspace 

Abalos, M., Bayona, J., Pawliszyn, J. stirring 

703 Fatty acids 

Application of GC coupled to chemical ionisation MS following 

headspace SPME for the determination of free volatile 85µm Carboxen/PDMS GC-CI-MS 

in water fatty acids in aqueous samples. 20 min headspace 





J. Chromatogr. A 891 (2000) 387-294 3.75 g NaCl, pH 1.5 

Abalos, M., Bayona, J. 

Analysis of volatile fatty acids in waste water 

593 Fatty acids collected from a pig farm by a SPME method. 65µm Carbowax/DVB GC-MS 

in waste water Chemosphere. Feb 1999; 38(4): 823-834 20 min 

Yo,-S-P immersion 

stirred 

SPME with pH adjustment for the determination of aromatic 

913 Aromatic acids/bases acids and bases in water 

in water J. Chromatogr. A (1998) 829(1-2) 223-233 

van Doorn, H., Grabanski, C., Miller, D., Hawthorne, S. 

704 Volatile, 

Solid Phase microextraction: a promising technique for 

sample preparation in environmental analysis review article 

semivolatiles J. Chromatogr. A 889 (2000) 3-14 

in water & soil Alpendurada, M. 

2529 Antibiotics in 

SPME of macrolide, trimethoprim, and sulfonamide antibiotics 

in wastewaters HPLC-MS-MS 

wastewater J Chromatogr. A 1169, #1-2, 53-62 (OCT 26 2007) 

McClure, Evelyn L.; Wong, Charles S. 

Simultaneous extraction and analysis of 11 tetracycline and 

2296 Antibiotics in sulfonamide antibiotics in influent and effluent domestic wastewater LC-MS 

wastewater by SPME and LC electrospray ionization tandem mass spectrometry 

J. Chromatogr. A, (2006) 1097, #1-2, 40-53 

Carlson, Kenneth; Cha, Jongmun; Yang, Shinwoo 

Determination of volatile alkyl sulfides in wastewater. 

972 Alkyl sulfides in water J.Chromatogr. A (2002) 963(1-2), 249-257 

Abalos, M.; Prieto, X.; Bayona, J.M. 

PDMS/carboxen GC-MS 

975 MTBE in water 

Determination of MTBE in water by GC-FID 

J.Chromatogr. A (2002) 963(1-2), 259-264 

Dron, J.; Garcia, R.; Millan, E. 

65 um PDMS/DVB GC-FID 

Current perspectives in analyte extraction strategies for tin 

2238 review of trends and arsenic speciation 

J Chromatogr. A 1153, #1-2, 114-29 (2007 Jun 15) 

Dietz, C.; Sanz, Jon; Sanz, Estrella; Muonoz-Olivas, Rian; Coamara, C. 

976 Butyltin in water 

Rapid determination of butyltin species in water samples by multicapillary GC 

J.Chromatogr. A (2002) 963(1-2), 195-203. 

Carpinterio Botana, J.; Rodriguez Pereiro, I.; Cela Torrijos, R. 

GC-AED 

978 BHT in bottled water 

Determination of butylated hydroxytoluene in bottled drinking water. 

J.Chromatogr. A (2002) 963(1-2), 179-183 

Tombesi, N.B.; Freije, H. 

GC-MS 

2641 Nonylphenols in 

Analysis or nonylphenol in water samples by automatic SPME-GC 

Zhongshan Daxue Xuebao 46, #5, 45-48 (Sept 2007) 65µm DVB/PDMS GC 

water Chen, Ling; Deng, Qin-Ying; Liu, Lan; Zhou, Hai-Yun 20 min. 

979 Nonylphenols in 

Determination of short ethoxy chain nonylphenols and their brominated analogs 

in raw and treated water. 

J.Chromatogr. A (2002) 963(1-2), 159-167 DVB/carboxen/PDMS GC-MS 

water Diaz, A.; Ventura, F.; Galceran, M.T. 

Method for the analysis of thirty phenolic pollutants in water samples. 

980 

Phenolic pollutants in 

water J.Chromatogr. A (2002) 963(1-2), 137-148 

Llompart, M.; Lourido, M; Landin, P.; Garcia-Jares, C.; Cela, R. 

75 um carboxen/PDMS GC-MS 

Comparison of SPE and SPME for carbofuran in water. 





981 Carbofuran in water J.Chromatogr. A (2002) 963(1-2), 117-123 HPLC 

Lopez-Blanco, M.C.; Cancho-Grande, B.; Simal-Gandara, J. 

983 

Quantification of volatile sulfur compounds in complex gaseous matrices by 


Sulfur in gaseous 

matrices J.Chromatogr. A (2002) 963(1-2), 57-64 

Nielsen, S.T.; Jonnson, S. 

75 um carboxen/PDMS GC-MS 

Optimization of SPME method for synthetic musk compounds in water. 

993 

Musk compounds in 

water. J.Chromatogr. A (2002) 963(1-2), 277-285 

Garcia-Jares, C.; Llompart, M.; Polo, M.; Salgado, C.; Macias, S.; Cela, R. 

Various GC 

Determination of volatile organic compounds (VOC) in water and soil using solid 

phase microextraction. 

1001 VOC's in water/soil Chemia Analityczna (2002) 47 (4), 507-530. PDMS GC-MS 

Wypych, J.; Manko, T 

Determination of estrogenic short ethoxy chain nonylphenols and metabolites in 

river and treated water by SPE (solid phase extraction) and SPME (solid phase 

microextraction) 

1005 Nonylphenols in water Water Sc. Technol. Water Supply (2003) 3 (1-2), 329-334. 

Diaz, A.; Galceran, M.T.; Ventura, F. 


Determination of MTBE in a recreational harbor using solid-phase 


Chemosphere (2003) 51 (8), 805-810. 

Ganske, Jane A.; Green, David B.; Zuccarello, Joseph L. 

GC-MS 

y yp p p 

1023 Nonylphenol in water 

ethinylestradiol in wastewater using solid-phase microextraction and gas 

J.Chromatogr. A (2003) 988(1), 41-51. 

Braun, P.; Engewald, W.; Kuschk, P.; Moeder, M.; Popp, P.; St. Schrader 

Various GC-MS 

Improved analysis of MTBE, TAME, and TBA in petroleum fuel-contaminated 

groundwater by SPME using deuterated internal standards with GC-MS 

MTBE, TAME and TBA 

1026 in water. Environmental Science & Technology (2003) 37 (7), 1392-1397. 

Dewsbury, Paul; Lerner, David N.; Thornton, Steven F. 

PDMS-carboxen GC-MS 

Headspace solid phase microextraction for the analysis of the new antifouling 

agents Irgarol 1051 and Sea Nine 211 in natural waters. 

Antifouling agents in 

1029 water Analytica Chimica Acta (2002) 468 (1), 171-180. 

Lambropoulou, D. A.; Sakkas, V. A.; Albanis, T. A.* 

65 um PDMS-DVB GC-MS 

Characterization and source identification of hydrocarbons in water samples 

using multiple analytical techniques. 

1041 Hydrocarbons in water Journal of Chromatography, A (2002) 971 (1-2), 173-184. GC-MS 

Wang, Z. D.; Li, K.; Fingas, M.; Sigouin, L.; Menard, L. 

1042 

Characteristics of poly(methylphenylvinylsiloxane) fibre probe for solid-phase 


Aromatic amines and 

PAH in water. Fenxi Shiyanshi (2002) 21 (5), 75-78. 

Zeng, Z. R.; Wang, Y. L.; Yang, M.; Tian, S. Z. 

poly(methylphenylvinylsiloGC 

Determination of methamidophos residues in water by SPME-CGC-MS. 

Methamidophos in 

1043 water. Fenxi Shiyanshi (2002) 21 (5), 28-30 

Li, Q.; Liu, H. L.; Wang, J. L.; Chen, H. 

100 µm PDMS GC-MS 


Identification of MTBE in water by SPME and GC-MS. 

American Laboratory (2002) 34 (21), 34. 

Guidotti, M.; Blasi, G.; Lucarelli, E.; Onorati, B.; Ravaioli, G.; Stella, D. 

75 µm Carboxen/PDMS GC-MS 

Determination of chlorophenols in waste water using direct solid-phase 

microextraction-GC 


1058 




Chlorophenols in 

water. Fenxi Kexue Xuebao (2002) 18 (5), 421-423. 85 µm polyacrylate GC-ECD 

Zhang, H. Y.; Zhang, J.; Huang, X. H. 260°C, 5 minutes 

1059 Phenols in water 

Determination of phenols in water by solid-phase microextraction-gas 


Fenxi Huaxue (2002) 30 (10), 1240-1242. 

Zhao, R. S.; Liu, R. M.*; Cui, Q. X 

GC-MS 

Coating of solid-phase microextraction fibers with chemically bonded silica 

particles: selective extraction of polycyclic aromatic hydrocarbons from drinking 

water samples. 

PAHs from drinking 

1069 water. Journal of Chromatographic Science (2002) 40 (9), 489-494. 

Rodrigues, R.; Lacerda, C. A.; Lancas, F. M.* 

Various 

1093 Cedrol in sea water 

Determination of cedrol in sea water by SPME-GC-MS and its content variations 

in redtide sea water. 


Zhao, M. Q.; Li, G. K.; Chen, H.; Zhang, Z. X. 

Various GC-MS 

Infra-red reflection-absorption method for the detection of aromatic compounds 

in aqueous solutions with limited sample volumes. 

Aromatic compounds 

1095 in aqueous solutions. Analytical Sciences (2002) 18 (11), 1247-1252. 

Yang, J.; Chen, P. Y.* 

Analysis of n-alkanes at sub microgram per liter level after direct solid phase 

microextraction from aqueous samples. 

n-alkanes from 

1100 aqueous samples Analytical Sciences (2002) 18 (11), 1221-1226. 

Farajzadeh, M.; Hatami, M. 

GC-FID 

Gas-phase analysis of trimethylamine, propionic and butyric acid, and sulfur 

compounds using solid-phase microextraction 

1103 Organic acids in water Analytical Chemistry (2002) 74(5), 1054-1060 

Kim, H.; Nochetto, C.; McConnell, L. L. 

Hollow-fibre liquid-phase microextraction of phthalate esters from water 

Phthalate esters from 

1110 water. Journal of Chromatography A (2003) 999 (1-2), 145-153. 

Kalogerakis, Nicolas; Psillakis, Elefteria 

Simultaneous determination of "earthy-musty" odorous haloanisoles and their 

corresponding halophenols in water samples using solid-phase microextraction 

coupled to gas chromatography with electron-capture detection 

1111 Haloanisoles in water. Journal of Chromatography A (2003) 999 (1-2), 135-144. 

Bruchet, Auguste; Dugay, Jose; Hennion, Marie-Claire; Malleret, Laure 

GC-ECD 

Factorial design optimization of SPME conditons for (GC-MS) 

2194 Alkylbenzenes analysis of linear alkylbenzenes (LABs) in detergents headspace GC-MS 

in detergents Anal. Chim. Acta 562. #2, 152-157 (2006) 

Bruns, Roy E.; De Carvalho, Lilian R. Franco; Penteado, Jose C. 

Determination of linear alkylbenzensulfonates in aqueous matrices by ion-pair 

solid-phase microextraction-in-port derivatization-gas chromatography-mass 

spectrometry 

Alkylbenzenesulfonate 

1116 s Journal of Chromatography A (2003) 999 (1-2), 51-60. 

Alzaga, Roberto; Bayona, Josep Maria; Ortiz, Laura; Pena, Araceli 

GC 

Improved determination of chlorophenols in water by solid-phase 

microextraction followed by benzoylation and gas chromatography with electron 

capture detection. 





1122 Chlorophenols in water Chromatographia (2002) 55(9-10), 595-600 

Bianchi, F.; Careri, M.; Mucchino, C.; Musci, M. 

65um DVB/PDMS, 

pentafluorobenzoyl 

chloride derivatization 

GC-ECD 

MultiSimplex optimization of the solid-phase microextraction-gas 

chromatography-mass spectrometric determination of polycyclic aromatic 

hydrocarbons, polychlorinated biphenyls and phthalates from water samples. 

PAH, PCB and 

1151 phthalates in water. Journal of Chromatography, A (2002) 978 (1-2), 165-175. 

Cortazar, E.; Zuloaga, O. *; Sanz, J.; Raposo, J. C.; Etxebarria, N.; Fernandez, 

L. A. 

PDMS GC-MS 

1153 Endosulfan in water. 

Optimization of solid-phase extraction and solid-phase microextraction for the 

determination of small alpha - and small beta -endosulfan in water by gas 

chromatography-electron-capture detection. 

Journal of Chromatography, A (2002) 976 (1-2), 293-299. 

Lopez-Blanco, M. C.; Reboreda-Rodriguez, B.; Cancho-Grande, B.; Simal- 

Gandara, J. * 

GC-ECD 

1154 PAH's in water 

Application of the novel benzo-15-crown-5 sol-gel coating for solid-phase 

microextraction in rapid determination of trace PAHs in water at non-equilibrium 

situations. 

Fenxi Kexue Xuebao (2003) 19 (2), 109-112. 

Wang, D. H.; Xing, J.; Wu, C. Y.* 

GC 

Application of time-resolved luminescence methodology to the determination of 

phthalate esters. 

1155 Phthalate esters Analytical Letters (2003) 36 (5), 1017-1027. 

Casas-Hernandez, A. M.; Aguilar-Caballos, M. P.; Gomez-Hens, A. * 

2549 Butyltin in 

Headspace SPME-GC-ion trap tandem mass spectrometry method for 

butyltin analysis in sediments: Optimization and validation headspace GC-MS 

sediments Microchemical Journal 87, #2, 147-153 (DEC 2007) 

Carvalho, P.; Pinto, L.; Basto, A..; Vasconcelos, A.. 

1164 Butyltin 

SPME-GCMS for speciation of butyltin compounds in marine environment 

Journal De Physique. IV : JP (2003) 107 (II), 1313-1316. 

Mahapatra, S.; Puranik, V.D.; Sadasivan, S.; Tripathi, R.M. 

PDMS GC-MS 

Fibre introduction mass spectrometry: fully direct coupling of solid-phase 

microextraction with mass spectrometry. 

VOC, SVOC in 

1071 aqueous solutions. Analytical Chemistry (2002) 74 (21), 5688-5692. 

Meurer, E. C.; Tomazela, D. M.; Silva, R. C.; Augusto, F.; Eberlin, M. N.* 

PDMS FIMS 

Extractions with superheated water. 

1072 Journal of Chromatography, A (2002) 975 (1), 31-46. 

Smith, R. M. 


Rapid determination of organotin compounds by headspace solid-phase 



Le Gac, Marjorie; Lespes, Gaetane; Potin-Gautier, Martine 

GC 

Determination of siloxane-water partition coefficients by capillary extraction-highresolution 

gas chromatography. Study of aromatic solvents. 

1228 BTEX Journal of Chromatography, A (2003) 985 (1-2), 39-45. 

Nardi, L. 

1167 Glycol ethers 

Optimization of the headspace solid-phase microextraction for determination of 

glycol ethers by orthogonal array designs. 

Journal of Chromatography, A (2002) 977(1), 11-15 

Huang, C. T.; Su, Y. Y.; Hsieh, Y. Z. 

75µm Carboxen PDMS GC-FID 

Simultaneous determination of oestrogenic short ethoxy chain nonylphenols 

and their acidic metabolites in water by an in-sample derivatization/solid-phase 

microextraction method. 


1168 




Oestrogenic short 

ethoxy chain 

nonylphenols in water 

Analytical Chemistry (2002) 75(15), 3869-3876 

Diaz, A.; Ventura, F.; Galceran, M. T. 

1182 Biocides in water 

Comparison of the performance of analytical methods based on solid-phase 

extraction and on solid-phase microextraction for the determination of antifouling 

booster biocides in natural waters. 


Konstantinou, I. K.; Hela, D. G.; Lambropoulou, D. A.; Sakkas, V. A.; Albanis, 

T. A.* 

GC-MS 

1184 Phthalates in water 

Solid-phase microextraction of phthalates from water. 


Luks-Betlej, K.; Janoszka, B.; Paschke, H.; Popp, P. 

70µm Carbowax/DVB 

Speciation of mercury compounds by gas chromatography with atomic emission 

detection. Simultaneous optimization of a headspace solid-phase 

microextraction and derivatization procedure by use of chemometric techniques. 

1188 Mercury in sea water. Chromatographia (2002) 56 (11-12), 733-738. 

Carro, A. M.; Neira, I.; Rodil, R.; Lorenzo, R. A. 

PDMS GC-MIP AES 

Optimization and application of SPME for the gas chromatographic 

determination of endosulfan and its major metabolites in the ng L-1 range in 

aqueous solutions. 

Endosulfan in aqueous 

1189 samples. Analytical and Bioanalytical Chemistry (2003) 376 (1), 61-68. 

Frimmel, F. H.; Deger, A. B.; Gremm, T. J.; Mendez, L. 

PDMS GC-ECD 

Methyl tert-butyl ether (MTBE) in urban and rural precipitation in Germany. 

1206 MTBE in water Atmospheric Environment (2001) 35(36), 6337-6345 

Achten, Christine; Kolb, Axel; Puettmann, Wilhelm 

75um Carboxen PDMS GC-MS 

1213 VOC's in groundwater. 

Monitoring and evolution of the pollution by volatile organic compounds (VOCs) 

in the groundwaters of the Najerilla River Basin (Spain) 

International Journal of Environmental Analytical Chemistry (2003) 83 (6), 495- 

506. 75 um Carboxen/PDMS GC-FID 

Fernandez-Torroba, Miguel A.; Ortiz, Gustavo; Pons, Begona; Tena, Maria 

Teresa 

In-tube solid-phase microextraction sampler for long-term storage. 


Nardi, L. 

1222 PAHs 

Determination of polycyclic aromatic hydrocarbons in water by capillary solidphase 

microextraction coupled with high-performance liquid-chromatography. 

Fenxi Huaxue (2003) 31 (2), 171-174. 

Chen, S.; Hahn, J. H.; Quan, X.; Lim, K. S.; Yang, F. L. 

HPLC 

1223 Phthalates in water 

Solid-phase microextraction coupled with high performance liquid 

chromatography-UV detection for the determination of di- n -propyl-phthalate, diiso 

-butyl-phthalate, and di-cyclohexyl-phthalate in environmental water 

samples. 

Analytical Letters (2003) 36 (2), 389-404. 

Cai, Y. Q.; Jiang, G. B.*; Liu, J. F. 

HPLC 


Validation, using a chemometric approach, of gas chromatography-inductively 

coupled plasma-atomic emission spectrometry (GC-ICP-AES) for organotin 

determination. 

Analytical and Bioanalytical Chemistry (2003) 376 (1-2), 226-235. 

Lespes, Gaetane; Aguerre, Sandrine; Pecheyran, Christophe 

GC-ICP-AES 

Solid-phase microextraction for the analysis of short-chain chlorinated paraffins 

in water samples. 




Matrix 

Chlorinated paraffins in 

Literature Reference Conditions Instrument 

1241 water. Journal of Chromatography, A (2003) 984 (1), 1-8. 

Castells, P.; Santos, F. J.; Galceran, M. T.* 

Various. GC-ECD 

1256 Dioxin in water 

Rapid determination of 2,3,7,8-tetrachlorodibenzo- p -dioxin in water samples 

by using solid-phase microextraction followed by gas chromatography with 

tandem mass spectrometry. 

Journal of AOAC International (2003) 86 (1), 44-49. 

Landin, P.; Llompart, M.; Lourido, M.; Garcia-Jares, C.; Carro, N.; Cela, R. 

Various GC-TMS 

1258 Beta-endosulfan 

Application of single-drop microextraction and comparison with solid-phase 

microextraction and solid-phase extraction for the determination of small alpha - 

and small beta -endosulfan in water samples by gas chromatography-electroncapture 

detection. 

Journal of Chromatography, A (2003) 984 (2), 245-252. GC-ECD 

Lopez-Blanco, M. C.; Blanco-Cid, S.; Cancho-Grande, B.; Simal-Gandara, J. * 

1260 PCBs in water. 

Analysis of polychlorinated biphenyls in aqueous samples by microwaveassisted 

headspace solid-phase microextraction 


Huang, Yaping; Shu, Youn Yuen; Tardif, Mylaine; Wang, Shu Shing 

Headspace GC-FID 

Determination of PCBs in the Housatonic River, MA by SPME and GC-ECD. 

1263 PCBs in water Abstracts of Papers American Chemical Society (2003) 225 (1-2), CHED 317. 

Wells, James; Schaumloffel, John C. 

1264 n-alkanes in water 

A new selective SPME fiber for some n-alkanes and its use for headspace 

sampling of aqueous samples 

Journal of Separation Science (2002) 26 (9-10), 802-808. 

Farajzadeh, Mir Ali; Hatami, Mehdi 

Cellulose acetate, PVC 

1265 PAHs from water 

Extraction of polycyclic aromatic hydrocarbons and organochloride compounds 

from water: A comparison between solid-phase microextraction and stir bar 

sorptive extraction 

Journal of Separation Science (2002) 26 (9-10), 961-967. GC-MS 

Bauer, Coretta; Hauser, Barbara; Keil, Petra; Popp, Peter; Wennrich, Luise 

Experimental design applied to the determination of several contaminants in 

Duero River by solid-phase microextraction. 

Solvents from 

1267 varnishes. Analytica Chimica Acta (2003) 477 (2), 257-267. 

Salafranca, J.; Domeno, C.; Fernandez, C.; Nerin, C. * 

Various GC-MS 

Development and validation of a solid-phase microextraction method for the 

analysis of volatile organic compounds in groundwater samples. 

1278 VOCs in groundwater. Chromatographia (2003) 41 (6), 301-304. 

Alonso, A.; Fernandez-Torroba, M. A.; Tena, M. T.; Pons, B. * 

Various GC 

1298 

Development of an SPME-GC-MS method for trace organic compounds in 

waste water from a petrochemical refinery. 

Trace organic 

compounds in waste 

water. Sepu (2003) 21 (1), 76-80. 

Xiao, K.; Wang, Y.; Lu, X.; Kong, H. W.; Yao, Q. H.; Xu, G. W.* 

GC-MS 

1300 Triazines in water. 

Optimization of a solid-phase microextraction procedure for the determination of 

triazines in water with gas chromatography-mass spectrometry detection. 


Frias, S.; Rodriguez, M. A.*; Conde, J. E.; Perez-Trujillo, J. P. 

Various GC-MS 

1322 Aldehydes in water 

Analysis of aldehydes in water by solid-phase microextraction with on-fiber 



Chang, Chun-Ming; Tsai, Shih-Wei 






Determination of iodinated phenol species at parts-per-trillion concentration 

levels in different water samples by solid-phase microextraction/offline GC-ICP- 

MS 

Phenol species in 

1335 water. Journal of Analytical Atomic Spectrometry (2003) 18 (9), 1119-1124. 

Caruso, Joseph A.; De Wuilloud, Jorgelina C.A.; Vonderheide, Anne P.; 

Wuilloud, Rodolfo G. 

Various GC-ICP-MS 

1340 PAH's in water. 

Solid-phase microextraction to monitor the sonochemical degradation of 

polycyclic aromatic hydrocarbons in water. 

Journal of Environmental Monitoring (2003) 5 (1), 135-140. GC-MS 

Psillakis, E.; Ntelekos, A.; Mantzavinos, D.; Nikolopoulos, E.; Kalogerakis, N. 

1351 Phenols from water. 

Investigations on the sorption of phenols to dissolved organic matter by a QSAR 

study. 

Chemosphere (2001) 45(3), 323-327. 

Ohlenbusch, G.; Frimmel, F. H. 


1357 Phthalates in water. 

Miniaturized solid-phase extraction as a sample preparation technique for the 

determination of phthalates in water. 


Saito, Y.; Nakao, Y.; Imaizumi, M.; Morishima, Y.; Kiso, Y.; Jinno, K. * 

HPLC 

Sorptive sample preparation long dash a review. 

PAH, PCB, pesticides 

1358 and VOC Analytical and Bioanalytical Chemistry (2002) 373(1-2), 3-22. 

Baltussen, E.; Cramers, C. A.; Sandra, P. J. F. 

PDMS 

1374 Tin and lead. 

Determination of tin- and lead-organic compounds by SPME-GC-atomicemission 

detection (SPME-GC-AED) after in situ propylation with sodium 

tetrapropylborate. 

Journal of Analytical Atomic Spectrometry (2001) 16(10), 1160-1166. 

Crnoja, M.; Haberhauer-Troyer, C.; Rosenberg, E. *; Grasserbauer, M. 

GC-AED 

Simultaneous determination of traces of hydrophilic and volatile compounds in 

water by solid-phase microextraction and GC/MS. 


1376 water. Bunseki Kagaku (2001) 50(10), 685-693. 

Miyazaki, T.; Kadokami, K.; Tukamoto, H. 

GC-MS 

Determination of phenylurea herbicides in natural waters at concentrations 

below one nanogram-per-litre using solid-phase extraction, derivatization, and 

solid-phase microextraction-gas chromatography-mass spectrometry. 

Phenylurea herbicides 

1383 in water. Journal of Chromatography, A (2001) 930(1-2), 9-19. 85µm Polyacrylate GC-MS 

1405 

Organophosphorous 

pesticides in water. 

Gerecke, A. C.; Tixier, C.; Bartels, T.; Schwarzenbach, R. P.; Mueller, S. R.* 

Comparison between solid-phase extraction methods for the chromatographic 

determination of organophosphorus pesticides in water. 

Journal of Environmental Science and Health Part B Pesticides Food 

Contaminants and Agricultural Wastes (2001) B36(5), 517-527. 

Lancas, Fernado M.; Carvalho, Dermeval; Queiroz, Maria E. C.; Silva, Silvana M 

1407 Butyltin in water 

Occurrence of butyltin compounds in the waters of selected lakes, rivers and 

coastal environments from China. 

Environmental Pollution (2001) 115(1), 81-87. 

Jiang Gui-bin; Liu Ji-yan; Wu Di-jing; Zhou Qun-fang 

GC-FID 

Alkylphenols and bisphenol-A in the coastal environment of Singapore and their 

rapid extraction from seawater and biological materials. 

Alkylphenols and 

1408 bisphenol-A Abstracts of Papers American Chemical Society (2001) 222(1-2), ENVR155. 

Lee, Hian Kee; Chanbasha, Basheer 




Matrix 

Nitroaromatic 


Screening method for nitroaromatic compounds in water based on solid-phase 

microextraction and infrared spectroscopy. 


1416 compounds in water. Environmental Science & Technology (2001) 35(17), 3507-3512. 

Tilotta, David C.; Stahl, Danese C. 

IR 

Comparison of different fibers for the solid-phase microextraction of phthalate 

esters from water. 

Phthalate esters from 

1419 water. Journal of Chromatography A (2001) 922(1-2), 377-384. 

Pocurull, E.; Borrull, F.; Marce, R. M.; Penalver, A. 

65µm PDMS/DVB GC-MS 


A rapid and sensitive method for methyl tert-butyl ether analysis in water 

samples by use of solid phase microextraction and gas chromatography-mass 

spectrometry. 

Chemosphere (2001) 44(4), 539-544. DVB/carboxen/PDMS GC-MS 

Roda, Aldo; Barbieri, Anna; Piazza, Francesco; Violante, Francesco Saverio 

Optimisation of the hyphenation between solid-phase microextraction , capillary 

gas chromatography and inductively coupled plasma atomic emission 

spectrometry for the routine speciation of organotin compounds in the 

environment 

1431 Organotin compounds J Anal At Spectrom (2001) 16(12), 1429-1433. GC-ICP-AES 

Aguerre, S.; Donard, O.F.X.; Krupp, E.; Lespes, G.; Pecheyran, C.; Potin- 

Gautier, M. 

Speciation without chromatography: Part I. Determination of tributyltin in 

aqueous samples by chloride generation, headspace solid-phase 

microextraction and inductively coupled plasma time of flight mass 

spectrometry 

1432 Tributyltin J Anal At Spectrom (2001) 16(11), 1313-1316. PDMS/DVB ICP-TOFMS 

Lam, J.W.; Maxwell, P.S.; Mester, Z.; Peter, L.; Sturgeon, R.E. 

Comparison of SPME/Transmission IR and SPME/ATR-IR spectroscopic 

methods in detection of chloroanilines in aqueous solutions 

1436 Chloroanilines in water Applied Spectroscopy (2001) 55(7), 919-926. 

Tsai, F.-P.; Yang, J. 

Analysis of carcinogenic aromatic amines in water samples by solid-phase 

microextraction coupled with high-performance liquid chromatography 

1444 Amines in water Anal. Chim. Acta (2003) 495(1-2) 109-122 Various fibers compared HPLC 

Chang, Wei-Yan; Huang, Shang-Da; Sung, Yu-Hsiang 

Determination of aliphatic amines using N-succinimidyl benzoate as a new 

derivatization reagent in gas chromatography combined with solid-phase 


1449 Amines in water Journal of Chromatography A (2003) 1021 (1), 175-181 

Cai, Ling-Shuang; Jing, Zhi-Zhong; Wang, Hong; Yu, Jian-Xin; Zhang, Hua- 

Shan; Zhao, Yuan-Yuan 

Reevaluation of headspace solid-phase microextraction and gas 

chromatography-mass spectrometry for the determination of methyl tert-butyl 

ether in water samples 

Headspace after 

derivatization with Nsuccinimidyl 

benzoate 

1450 MTBE in water Journal of Chromatography A (2003) 1021(1), 157-164 

Bucciferro, Anthony; Chu, Shaogang; Fang, Fu; Hong, Chia-Swee; Kou, 

Wenpeng 

GC-MS 

Strategically designed sample composition for fastest screening of 

polychlorinated biphenyl congeners in water samples. 

1460 PCBs in water Journal of Environmental Monitoring (2002) 4(4), 490-497 

Martinez, E.; Llompart, M. P.; Landin, P.; Cela, R.; Carro, A. M. 


GC-FID, GC-MS




State of the art in the determination of MTBE in natural waters & soils 

2232 MTBE in water Crit. Rev. Anal. Chem.35 #4, 317-337 (2005) headspace FID 

and soil Aragon, P.; Atienza, J.; Herrero, M; M., Angel; Aragon, P.; Atienza, J.; 

Herrero, Ma. Asuncion; Maquieira, A.; Puchades, R. 

Sensitive method for determination of methyl tert-butyl ether (MTBE) in water by 

use of headspace-SPME/GC-MS. 

1475 MTBE in water Fresenius' Journal of Analytical Chemistry (2001) 371(4), 519-525 

Achten, Christine; Kolb, Axel; Puettmann, Wilhelm 

75um Carboxen/PDMS, 

headspace 

Methyl tert-butyl ether (MTBE) in finished drinking water in Germany 

2230 MTBE in Environ. Pollut 140 #2, 294-303 (2006) 

drinking water Kolb, Axel; Puttmann, Wilhelm 

GC-MS 

1480 MIB in drinking water 

Correlation of musty odor and 2-MIB in two drinking water treatment plants in 

South Taiwan. 

Science of the Total Environment (2002) 289(1-3), 225-235 

Lin, Tsair-Fuh; Kao, Hsiao-Pin; Wong, Jiun-Yue 

GC-MS 

1484 

1488 

1493 

Gas chromatographic determination of 2-hydroxy-4-methoxybenzophenone and 

octyldimethyl-p-aminobenzoic acid sunscreen agents in swimming pool and 

bathing waters by solid-phase microextraction 

2-hydroxy-4methoxybenzophenone 

and octyldimethyl-p- 


aminobenzoic acid 

sunscreen agents in 

water 

Organochlorines in 

water 

Albanis, T. A.; Giokas, D. L.; Karayannis, M. I.; Lambropoulou, D. A.; Sakkas, 

V. A. 

Determination of organochlorides in water using solid-phase microextraction 

coupled to gas chromatography. 

100µm PDMS, 85µm 

Polyacrylate 

American Laboratory (2002) 34(17), 12-14 GC 

Ou Qing-Yu; Liang Bing; Li Ju-bai; Huang Min-jia 

Method based on solid-phase microextraction-high-performance liquid 

chromatography with UV and electrochemical detection to determine estrogenic 

compounds in water samples. 

Estrogenic compounds 


in water 

Pocurull, E.; Borrull, F.; Marce, R. M.; Penalver, A. 

85um Polyacrylate HPLC-UV, HPLC-ED 

Application of SPME for the quantitative determination of methylmercury in 


1504 Mehylmercury in water Abstracts of Papers American Chemical Society (2002) 223(1-2) CHED 125 

1536 

1538 

Phthalic acid esters in 

water 

Phenolic compounds 

in water 

Moore, J. Taylor; McDowell, Derek R.; Ambler, Rich B. 

Development of a solid-phase microextraction method for the determination of 

phthalic acid esters in water. 

Analytica Chimica Acta (2002) 457(2), 211-223 Various fibers compared GC-ECD 

Holadova, Katerina; Hajslova, Jana; Poustka, Jan; Prokupkova, Gabriela 

Solid-phase microextraction coupled to high-performance liquid 

chromatography to determine phenolic compounds in water samples. 

Journal of Chromatography A (2002) 953(1-2), 79-87 85um Polyacrylate HPLC-UV 

Marce, R. M.; Borrull, F.; Penalver, A.; Pocurull, E. 

Vial position in the determination of chlorophenols in water by SPME 

2154 Chlorophenols J. Chromatogr. A, 1103, #1, 29-34 (2006) headspace GC-MS 

in water Portillo, A; Prohibas, N.; Salvado, V.; Simonet, B. M. 

Determination of chlorophenols by solid-phase microextraction and liquid 

chromatography with electrochemical detection. 





1552 Chlorophenols in water Journal of Chromatography A (2002) 947(2), 155-165 Various fibers compared HPLC-ELCD 

1354 

Aldehydes in drinking 

water 

Galceran, M. T.; Santos, F. J.; Sarrion, M. N. 

Determination of aldehydes in drinking water using 

pentafluorobenzylhydroxylamine derivatization and solid-phase microextraction 


Ventura, Francesc; Cancho, Beatriz; Galceran, Ma. Teresa 

65um DVB PDMS, onfiber 


PFBHA 

GC-ECD 

1156 Chlorophenols 

Solid-phase microextraction liquid chromatography/tandem mass spectrometry 

for the analysis of chlorophenols in environmental samples. 

Rapid Communications in Mass Spectrometry (2002) 17 (1), 39-48. 

Sarrion, M. N.; Santos, F. J.; Moyano, E.; Galceran, M. T.* 

Carbowax/TPR LC-TMS 

1166 

Simultaneous mercury and tin speciation in environmental samples by GC- 

MIP/AES after preconcentration by solid phase microextraction 

Mercury and tin in 

environmental 

samples. Journal De Physique. IV : JP (2003) 107 (II), 1423. PDMS GC-MIP/AES 

Carrera, R.; De Diego, A.; Delgado, A.; Madariaga, J.; Sanz, J.; Zuloaga, O. 

1074 Tributyltin 

Improvement of measurement precision of SPME-GC/MS determination of 

tributyltin using isotope dilution calibration. 

Analytical Chemistry (2002) 74 (21), 5606-5613. 

Bancon-Montigny, C.; Maxwell, P.; Yang, L.; Mester, Z.; Sturgeon, R. E. 

GC-MS 

Determination of methylphosphonic acid in water by SPME-GC 

1952 Methyl Fenxi Ceshi Xuebao, 23, #1, 106-108 GC 

phosphoric Yuan, L.; Xu, D. N. 

acid in wate 

Electrochemically controlled (EC) SPME based 

1953 Nickle-cadmium on over oxidized sulfonate polypyrrole sulfortated polypyrrole ETAAS 

from water Talanta, 67, #1,, 245-251 coated fiber 

Ertas, N; Pekmez, K; Sahin, Y; Tamer, U Udum, Y.; immersed 

Yildiz, A. 

Risk assessment of domestic and industrial effluents 

1954 Industrial unloaded into a freshwater environment GC-MS 

effluent in Ecotoxicology & Environmental Safety, 61, #3, 380-391 

freshwater Di Marzio, W.; Saenz, M.; Alberdi, J.; 

Tortorelli, M.; Silvana, G. 

Low part per trillion determination of reactive 

1955 Alkanethiols alkanethiols in wastewater by in situ derivatization- N-ethylmaleimide GC-MS 

in wastewater SPME followed by GC/MS derivatives 

Anal. Chem., 77, #18, 6012-6018 immersion sampling 

Alzaga, R.; Bayona, J.M.; Garcia-Jares, C.; 

Llompart, M.; Salgado-Petinal, C. 

2876 Alcohol 

Sediment toxicity of a rapidly biodegrading nonionic surfactant: 

Comparing the equilibrium partitioning approach with GC-MS 

ethoxylates in measurements in pore water 

marine sediment Env Sci & Tech. 42, #11, 4215-4221 (Jun 1 2008) 

Droge, Steven T. J.; Hermens, Joop L. M.; Postma, Jaap F. 

Analysis of freely dissolved alcohol ethoxylate homologues in various 

2443 Ethoxylates seawater matrixes using solid-phase microextraction headspace GC 

in seawater Anal. Chem. 79, #7, 2885-2891 (2007-04-01) 

Droge, S. T.; Sinnige, T. L.; Hermens, J. L. M. 

Determination of total chromium in seawater by 

1956 Chromium in isotope dilution sector field ICPMS using GC s PDMS fiber ICPMS 

seawater sample introduction TFA derivatives 

Anal. Chem., 76, #13, 3510-3516 headspace 

Abranko, L; Mester, ; Sturgeon, .; Yang, L 





Determination of chromium(III) in water by SPME 

1957 Chromium in w/ polyimide-coated fiber and GC-FPD polyimide fiber GC-FPD 

Water J. Chromatogr. A, 1062, #1, 49-55 TFA derivatives 

Ding, Tzuoo-Huei; Lin, Huang-Huei; Whang, Chen-Wen 

SPME: A powerful sample preparation tool prior to 

1958 Organics mass spectrometric analysis review article GC-MS, LC-MS 

in water J. Mass Spectrom.(2004) 39(3), 233-254 

Vas, Gyorgy; Vekey, Karoly 

Comparison between headspace and aqueous phase SPME 

1959 Butyltin in method for speciation analysis of butyltin compounds headspace & GC 

sea water in sea water immersion sampling 

J Food and Drug Analysis, 12, #3, 205-211 

Hsia, Meng-Pei; Hsu, Tau-Being; Liu, Shiu-Mei 

Multielemental speciation analysis of organometallic 

1960 Hg,Pb,Tn compounds of mercury, lead, and tin in natural water Various fibers GC-MS 

in water & samples by headspace-SPME followed by GC-MS NaEt 4B derivatives 

seawater J. Chromatogr. A, 1034,#1-2, 191-197 headspace 

Centineo, G; Gonzalez, E; Sanz-Medel, A 

Reevaluation of headspace SPME-GC-MS for the 

1961 MTBE in determination of methyl tert-butyl either in water samples headspace GC-MS 

water J. Chromatogr. A, 1021, #1-2, 157-164 

Fang, Fu; Hong, Chia-Swee; Chu, S; Kou, W; Bucciferro, A 

Identification of 2,3-butanedione (diacetyl) as the 

1962 Diacetyl Odor compound causing odor events at trace levels in the 75µm Carboxen GC-MS 

in water Llobregat River and Barcelona's treated water (Spain 30min @ 60°C 

J. Chromatogr. A, 1034, #1-2, 175-182 NaEt 4B derivative 

Diaz, A.; Galceran, Ma. Teresa; Ventura, F. Headspace 

Simultaneous determination of 22 volatile organic compounds, 

1963 Odors/volatiles methyl-tert-butyl ether,1,4-dioxane, 2-methylisoborneol and 100µm PDMS GC-MS 

in water geosmgeosmin in water by headspace SPME-GC-MS headspace 

Anal. Chim. Acta, 548, #1-2, 79-85 

Daishima, Shigeki; Nakamura, Sadao 

Determination of musty odorants, 2-methylisoborneol and geosmin, 

2807 Geosmin and in environmental water by headspace GC-MS 65µm PDMS-DVB GC-MS 

2-methyisoborneol J. Chromatogr. A, 1186, #1-2, 434-437 (Apr 4 2008) Headspace 

in water Kataoka, Hiroyuki; Okamura, Kota; Saito, Keita 70 °C for 30 min. 

Study of alkyl lead speciation by Head Space (HS)- 

1964 Alkyl lead SPME coupled with GC-MS Headspace GC-MS 

in water Fenxi Shiyansh, 23, #2, 14-17 

Shuai, Q.; Zheng, C; Shuai, Q.; Yang, W.; Zheng, Y. 

Effects of riboflavin-photo sensitization on the formation of volatiles 

2666 Volatiles from in linoleic acid model systems with sodium azide or D2O Headspace GC-MS 

linoleic acid Food Chemistry 105, #4, 1375-1381 (2007) 

Yang, Seungk; Lee, JaeMin; Lee, JaeChul; Lee, JaeHwan 

Volatile fatty acids as malodorous compounds in 

1965 C2-C7 Fatty wool scouring water and lanolin. Origin and headspace GC-CI-MS 

acids in characterization. 

water/lanolin Env Technology, 24, #12, 1465-1470 

Jover, E.; Abalos, M.; Ortiz, L.; Bayona, J. 

SPME of volatile oxidation compounds in oil-in-water 

1966 Volatile emulsions headspace GC-FID. 

oxidative Food Chemistry, 92, #3, 401-406 50°C for 20 min. 

products in Beltran, G; Aguilera, M; Gordon, Michael H. 

oil-water 

Full automation of derivatization:SPME-GC-MS 

1967 Organometallic with dual-arm system for the determination of phenyl derivative GC-MS 

derivatives organometallic compounds in aqueous samples. headspace 

in water J Chromatogr A, 1025, #1, 77-84 

Parkinson, D; Bruheim, I; Christ, I; Pawliszyn, J 

1968 Methyl 

Determination of methylmercury and mercury(II) in a marine 

ecosystem using SPME--GC-MS headspace GC-MS 

mercury from Anal. Chim. Acta, 551, #1-2, 192-198 Na(C6H5) 4B 

seawater Bhalke, S.; Mishra, S.; Puranik, V.D.; Shukla, V.K.; Tripathi, R.M. derivative 





Speciation analysis of mercury by SPME and multicapillary 

1969 Mercury GC hyphenated to ICP-TOF spectrometry. 75µm Carboxen ICP-TOF-MS 

from wate/ J Chromatogr A, 1055, #1-2, 197-207 NaEt 4B derivatives 

sediment Jitaru, P.; Adams, F. C.* headspace 

Diffusion-based calibration for SPMEof benzene, 

1970 BTEX in toluene, ethylbenzene, p-xylene and chlorobenzenes headspace GC 

water from aqueous samples 

J Chromatogr A, 1025, #1, 11-16 

Paschke, A.; Popp, P. 

Indirect determination of low vapour pressures using SPME - 

1971 Chlorinated Application to tetrachlorobenzenes & trachlorbenyltoluenes minutes to hour GC 

benzenes J Chromatogr A, 1072, #1, 93-97 headspace 

Paschke, Albrecht; Schroter, Uwe; Schuurmann, Gerrit 

LC-MS-based procedures for monitoring of toxic organophosphorus 

2890 Organo- compounds and verification of pesticide and nerve agent poisoning review article LC-MS 

phosphorus Anal. Bioanal. Chem. 391, #1, 97-116 (May 2008) 

compounds John, Harald; Thiermann, Horst; Worek, Franz 

Determination of organophosphorus pesticides in 

1972 Organo- spiked river water samples using SPME-GC With immersed sampling GC-MS 

phosphorus EI-MS and ICP-MS detection GC-ICP-MS 

pesticides J Anal At Spectrom, 20, #9, 876-882 

in water Blanco-Gonzalez, E; Fidalgo-Used, N; Montes-Bayon, M; 

Sanz-Medel, A 

SPME for the determination of pyrethroids in cucumber and watermelon 

2404 Pyrethroids using HPLC combined with post-column photochemically induced HPLC-PIF-FD 

in cucumber fluorimetryderivatization and fluorescence detection 30 min @ 65°C 

and watermelon Anal. Chim. Acta 607, #1, 74-82 (21 JAN 2008) fluorimetry 

Vazquez, P. P.; Mughari, A. R.; Galera, M. M. derivatization 

Alternative sample preparation method for photochemical studies 

2609 Pyrethroids based on SPME: Synthetic pyrethroid photochemistry headspace GC-MS 

photodegradation J. Chromatogr. A 1152, #1-2, 156-167 (Jun 8 2007) 

Cela, R.; Fernandez-Alvarez, M.; Garcia-Jares, C.; Llompart, M.; 

Lores, M.; Sanchez-Prado, L. 

The photochemical behaviour of five household pyrethroid insecticides 

2591 Pyrethroids and a synergist as studied by photo-solid-phase microextraction headspace GC-MS 

photodegradation Anal. Bioanal. Chem. 388, #5-6, 1235-1247 (2007-07) 100µm PDMS 

Fernandez-Alvarez, M.; Lores, M. ; Llompart, M.; Garcia-Jares, C.; Cela, R 

Occurrence and bioavailability of pyrethroids in a mixed land 

2625 Pyrethroids use watershed 

in sediment J. Environ. Qual. 36, #4, 1006-1012 (July/August 2007) 

Bondarenko, S.; Budd, R.; Gan, J.; Haver, D.; Kabashima, J. 

Analysis of pyrethroids in sediment pore water by SPME 

2594 Pyrethroids Environ Toxicol Chem 26, #12, 2587-93 (2007 Dec) 

in sediment Bondarenko, Svetlana; Spurlock, Frank; Gan, Jianying 

Development of a SPME-GC with micro ECD detection method for 

2865 Pyrethroids and a multiresidue analysis of pesticides in bovine milk 65µm PDMS-DVB GC-ECD 

organochlorinated Anal. Chim. Acta 617, #1-2, 37-50 (Jun 9 2008) 30min @ 100°C 

pesticides in Cela, Rafael; Dagnac, Thierry; Fernandez-Alvarez, Maria; stirred 

bovine milk Garcia-Jares, Carmen; Lamas, J.: Pablo; Llompart, Maria; Lores, M. 

Effects of sample pretreatment and storage conditions in the 

2537 Pyrethroids etermination of pyrethroids in water samples by SPME-GC-MS headspace GC-MS 

in water Anal Bioanal Chem 387, #5, 1841-1849 (2007) 40°C 

Casas, V.; Llompart, M.; Garcia-Jares, C.; Cela, R.; Dagnac, T 

Determination of enantiomers of synthetic 

1973 Pyrethroids pyrethroids in water by SPME GC 

in water enantioselective gas chromatography. 

J Agrl Food Chem, 52, #4, 736-741 

Liu, W. P.; Gan, J. J.* 

Ultrasound-assisted emulsification-microextraction of emergent 





2908 Pesticides in contaminants and pesticides in environmental waters 10min immersion GC-MS 

water J. Chromatogr. A 1190, #1-2, 27-38 (May 9 2008) 

Cela, R.; Garcia-Jares, C.; Garcia-Monteagudo, J.; Llompart, M.; 

Regueiro, J. 

Strategies for the microextraction of polar organic contaminants in 

2172 Polar organics water samples GC-MS 

in water Anal. Bioanal. Chem. 384, #7-8, 1447-1461 (2006) 

Quintana, Jose Benito; Rodriguez, Isaac 

Photochemical studies of a polybrominated diphenyl ethers (PBDES) 

2268 Polybrominated technical mixture by SPME 

diphenyl ethers Chemosphere 60 #7, 922-928 (2005) 

from water Sanchez-Prado, L.; Gonzalez-Barreiro, C.; Lores, M.; Llompart, M.; 

Garcia-Jares, C.; Cela, R. 

Development of a SPME-GC-MS method for poly- 

1974 Polybrominate brominated diphenyl ethers and polybrominated headspace GC-MS 

diphenyls/ biphenyls in water sample 

biphenyls Analytical Chemistry, 76, #4, 1054-1062 

in water Polo, M.; Gomez-Noya, G.; Quintana, J. B.; Llompart, M.; 

Garcia-Jares, C.; Cela, R. 

Photochemical studies of a polybrominated diphenyl 

1975 Polybrominate ethers (PBDES) technical mixture by SPME GC 

diphenyl ether Chemosphere, 60, #7, 922-928 

from water Cela, R.; Garcia-Jares, C.; Gonzalez-Barreiro, C.; 

Llompart, M.; Lores, M.; Sanchez-Prado, L. 

Determination of PDMS-seawater distribution 

1976 PCBs in coefficients for PCBs and chlorinated biphenyls 100µm PDMS GC-MS 

water and chlorinated pesticides by SPME-GC-MS 12 day extraction 

J. Chromatogr. A,1066, #1-2, 165-175 immersion 

Zeng, E; Tsukada, D; Noblet, J.; Peng, J 

Multivariate optimization of a SPME method for the 

1977 Phthalate analysis of phthalate esters in environmental waters Various fibers GC-MS 

esters in J. Chromatogr. A,1072, #1, 63-72 direct immersion & 

water Cela, R; Garcia-Jares, C; Llompart, M Polo, M headspace 

New approach of SPME improving the extraction 

1978 Tin compounds yield of butyl and phenyltin compounds by combining Ethylate derivatives GC 

in water the effects of pressure and type of agitation headspace 

J. Chromatogr. A,1072, #1, 19-27 agitated 

Bueno, M; Darrouzes, J; Holeman, M; Pecheyran, C; 

Potin-Gautier, M 

Determination of aliphatic amines using N-succinimidyl 

1979 Aliphatic benzoate as a new derivatization reagent in 60min @ 80°C GC-MS 

amines GC combined with SPME headspace GC-FID 

in water J. Chromatogr. A,1021, #1-2, 175-181 succinimidyl benzoate 

Zhao, Y.; Cai, L.; Jing, Z.; Wang, H.; Yu, J.; Zhang, H. derivatives 

Analytical methods applied to the determination of heterocyclic 

2834 Aromatic aromatic amines in foods Review article 

amines in J. Chromatogr. B,862, #1-2, 15-42 (Feb 1 2008) 

food Afonso, A.M.; Ayala, J.H.; Gonzalez, V.; Sanz Alaejos, M. 

In situ derivatization/SPME determination of polar 

1980 Aromatic aromatic amines. 65µm PDMS-DVB GC-MS 

amines in Analytical Chemistry, 76, #4, 1028-1038 diazotation/ iodination 

water Zimmermann, T.; Ensinger, W. J.; Schmidt, T. C.* 

Determination of aromatic amines in waste water by 

1981 Aromatic SPME-GC GC 

amines in Fenxi Ceshi Xuebao, 23, #3, 18-21 

water Peng, J. G.; Wang, D. H.; Wu, C. Y. 

Comparative study of the use of flow-through 

1982 Phenols in systems with and without air segmentatio 80µm polyacrylate GC 

water determination of phenols by SPME-GC 100µm PDMS 

Chromatographia, 59, #5-6, 387-391 immersed 

Nome, R. C.; Carasek, E. * 

1983 Aldehydes 

Determination of low-molecular mass aldehydes by automated 

headspace spme with in-fibre derivatisation headspace GC-FID 





in water J. Chromatogr. A, 1071, #1-2, 147-154 PFBHA derivatives 

O'Reilly, John; Pawliszyn, Janusz; Wang, Qing 

Determination of low-molecular mass aldehydes by automated 

1984 Aldehydes in headspace SPME with in-fibre derivatization PFBHA derivatives GC-FID 

water J. Chromatogr. A, 1071, #1-2,147-154 headspace 

Wang, Qing; O'Reilly, John; Pawliszyn, Janusz 

Concentration and fate of persistent organochlorine pesticides 

2197 Organochlorine in estuarine sediments using headspace SPME headspace 

pesticides in Chemosphere 62, #11,1869-1878 (2006) 

sediments Chang, Sue-Min; Doong, Ruey-An 

Determination of organochlorine pesticides in ground water samples 

2388 Organochlorine using SPME by GC-ECD 50/30µm DVB/CAR GC-ECD 

pesticides in Talanta 72, #5, 1833-1841 (2007-07-31) immersion 

water Raposo, J. L., Jr.; Re-Poppi, N. 

Analysis of organochlorine pesticides in water by 

1985 Organochlorine novel activated carbon fiber SPME coupled w/GC-MS GC-MS 

pesticides J. Environ. Sci. Health Part B, 39, #2, 235-248 

in water Fang, N; Jia, J; Sun, T; Wang, Y; Yu, J 

Development and validation of a methodology for the determination 

2240 Tebuthiuron and of pesticides in water by SPME-LC/DAD 85µm polyacrylate LC/DAD 

diuron in water J. Liq. Chromatogr. 28 #18, 2909-2919 (2005) 50 minutes, 

Brondi, Silvia H. G.; Lancas, Fernando M.; Rodrigues Da Silva, Jose C. 

Optimization of a methodology for the determination 

1986 Organochlorine of organochlorine pesticides in surface water by 85µm polyacrylate GC-MS 

pesticides SPME-GC-MS 40min @ >20°C 

in water J. Environ. Sci. Health Part B, 40, #4, 513-523 agitation 

Brondi, Silvia Helena G.; Lancas, Fernando M. immersed sampling 

GC-MS methodology using SPME for the multiresideu 

1987 Pesticides in determination of pesticides in surface waters. 65µm PDMS-DVB GC-SIM-MS 

surface water Intl J Env Analytical Chem, 84, #14-15, 1079-1092 

Albanis, T; Hela, D.; Lambropoulou, D.; Sakkas, V. 

Pesticides in Esteros del Ibera (AR): Evaluation of 

1988 Endosulfan, impacts and proposal of guidelines for water immersed sampling GC-MS 

carbofuran quality protection 

in water Ecol. Model., 86, #1, 85-97 

Boia, C; Borrego, C; Silva, C; Valente, J 

Optimization and application of SPME for the GC 

1989 Endosulfan, determination of endosulfan and its major metabolites 100µm PDMS GC-ECD 

in water in the ng L/sup-1 / range in aqueous solutions 30% NaCl GC-MS 

Anal. Bioanal. Chem., 376, #1, 61-68 

Deger, A.B.; Frimmel, F.H.; Gremm, T.J.; Mendez, L. 

Determination of membrane permeability without calibration 

2306 PAHs in using (SPME) PDMS GC 

water J. Membr. Sci. 68 #1, 65-73 (2005) 

Liu, Xinyu; Pawliszyn, Janusz 

Application of membrane techniques to water 

1990 Phthalates purification. Removal of phthalates 65µm CW/DVB GC-FID 

in water Desalination, 162, #1-3, 121-128 

Bodzek, M; Dudziak, M; Luks-Betlej, K 

Degradation of PAHs in aqueous solutions by 

1991 PAHs ultrasonic irradiation 20°C & 40°C GC-MS 

in water J. Hazard. Mater., 108, #1-2, 95-102 immersed sampling 

Goula,G; Kalogerakis,N; Mantzavinos,D; Psillakis, E sonicated 

Oxidative microbial transformation of vinyl chloride 

1992 Vinyl chloride under anaerobic conditions in ground water headspace GC-MS 

in water Proc. of the Third Int. Conf. on Rem. of Chlorinated 

and Recalcitrant 2002, pp1571-1578 

Banwart, S; Holliger, C; Morgan, Pl; Shah, N.; Szynalski, K. 

Determination of adipate in water with 

1993 Adipate in headspace SPME and single ion monitoring GC-MS Headspace GC-MS 

water Fenxi Shiyanshi, 23, #4, 77-80 





Zhang, W. Y.; Wang, C. Y.; Yang, Z. J. 

SPME coupled with HPLC w/ fluorimetric detection 

1994 Bisphenol in for the determination of bisphenol A, 4-n-nonylphenol and 50µm CW-TPR HPLC-Fluorimetric 

water 4-t-octylphenol in environmental water samples. 

Analytical Letters, 37, #4, 739-753 

Cai, Y. Q.; Jiang, G. B.*; Liu, J. F.; Liang, X.; Yao, Z. W.; 

Liu, J. M.; Liu, J. Y.; Zhou, Q. X. 

Electronic nose technology for the detection of microbial 

1995 Volatiles from and chemical contamination of potable water headspace @ 25°C GC 

Bacteria Sens Actuators, B Chem, 106, #1, 3-6 

in water Canhoto, O.; Magan, N. 

On-fibre silylation following SPME for the determination of 

1996 Herbicides acidic herbicides in water samples by GC 85µm polyacrylate GC-MS 

in water Anal. Chim. Acta, 537, #1-2, 259-266 MTBSTFA derivative 

Cela, R.; Gonzalez, R.; Quintana, J.; Rodriguez, I.; Rubi, E. stirred 

Analysis of the chloroacetanilide herbicides in water using 

1997 Herbicides SPME with CAR/PDMS and GC/ECD 75µm Carboxen GC-ECD 

in water J of AOAC Intl, 88, #4, 1236-1241 immersed sampling 

Hwanc, Ying-Ming; Wong, Yih-Gang; Ho, Wu-Hsiung 

Sonochemical degradation of triclosan in water and wastewater 

2790 Triclosan in Ultrason. Sonochem.15, #5, 689-694 (July 2008) GC-ECD 

water Barro, R.; Garcia-Jares, C.; Kalogerakis, N.; Llompart, M.; Lores, M.; GC-MS 

Mantzavinos, D.; Petrakis, C.; Psillakis, E.; Sanchez-Prado, L. 

2171 Triclosan in 

Further research on the photo-SPME of triclosan 

Anal. Bioanal. Chem.384, #7-8, 1548-1557 (2006) PDMS fiber GC-MS 

water Cela, R.; Fernandez-Alvarez, M.; Garcia-Jares, C.; Llompart, M.; 

Lores,Marta; Sanchez-Prado, L. 

Optimization of SPMEconditions for the determination of 

1998 Triclosan in triclosan and possible related compounds in water samples 85µm polyacrylate GC-MS 

water J Chromatogr A, 1072, #1, 107-115 MTBSTFA derivative 

Canosa, P.; Rodriguez, I.; Rubi, E.; Cela, R. 30min extraction 

immersed sampling 

Application of strategic sample composition to the screening 

1999 Anti- of anti-inflammatory drugs in water samples using SPME 85µm polyacrylate GC-MS 

inflamatory Anal. Chim. Acta, 524, #1-2, 63-71 silylated esterfication 

drugs in Carpinteiro, J.; Carro, A.; Cela, R.; Lorenzo, R.; headspace 

water Martinez, E.; Quintana, J.; Rodriguez, I. 

Determination of anti-inflammatory drugs in water samples, by in situ 

2793 Anti-inflamatory derivatization, SPME-GC-MS 100µm PDMS GC-MS 

drugs in Talanta 75, #1, 111-115 (MAR 15 2008) headspace 

water Araujo, L.; Wild, J.; Villa, N.; Camargo, N.; Cubillan, D.; Prieto, A. dimethyl sulphate, 

derivatives 

Recently developed GC/MS and LC/MS methods for determining 

2499 Anti-inflamatory NSAIDs in water samples LC-MS 

drugs in Anal Bioanal Chemistry 387, #4, 1203-1214 (FEB 2007) derivatives GC-MS 

water Farre, M.; Petrovic, M.; Barcelo, D. 

A combination of statistical and analytical evaluation methods as 

2784 Phamaceutical a new optimization strategy for the quantification of pharmaceutical GC-MS-MS 

resideu in sewage residues in sewage effluent 2.5-7 pH 

effluent Anal. Chim. Acta, 613, #2, 169-176 (Apr 21 2008) 

Budziak, D.; Carasek, E.; Costa, L..; Martendal, E.; Suchara, E. 

Applicability of SPME followed by on-fiber silylation for the 

2000 Estrogens in determination of estrogens in water samples by GC-MS-MS 85µm polyacrylate GC-MS-MS 

sewage J Chromatogr A, 1056, #1-2, 179-185 MSTFA derivatives 

water Carpinteiro, J.; Carro, A.; Cela, R.; Lorenzo, R.A.; immersed sampling 

Quintana, J.; Rodriguez, I. 

Determination of odorous mixed chloro-bromoanisoles in 

2001 Chloro-brom- water by SPME-GC-MS headspace GC-MS 

anisole in J Chromatogr A, 1064, #1-2, 97-106 100µm PDMS 

water Diaz, A.; Ventura, F.; Galceran, M. 

Estimation of measurement uncertainty for the 





2002 Nonylphenol determination of nonylphenol in water GC-MS 

in water using SPME and SPME procedures. 

Analytica Chimica Acta, 506, #1, 71-80 

Diaz, A.; Vazquez, L.; Ventura, F.; Galceran, M. 

Predicting organic contaminant concentrations in sediment porewater 

2523 Organics in using solid-phase microextraction 

sediment Chemosphere 66, #8, 1408-1414 (JAN 2007) 

Yang, Ze-Yu; Zeng, Eddy Y.; Maruya, Keith A.; Mai, Bi-Xian; Ran, Yong 

Validation, using a chemometric approach, of GC- 

2003 Organotin inductively coupled plasma-atomic emission GC-ICP-AES 

in water and spectrometry (GC-ICP-AES) for organotin determination 

sediment Anal. Bioanal. Chem., 376, #2, 226-235 

Aguerre, S.; Lespes, G.; Pecheyran, C. 

Development of a novel SPME element for 

2004 Bethrodine thermal desorption GC analysis 30µm PDMS GC-MS 

herbicide in J. Chromatogr. A, 1035, #2, 277-279 

water Hosaka, A.; Ohtani, H.; Tsuge, S.; Wang, L.; Watanabe, C. 

Application of SPME for the determination of soil fumigants 

2005 Fumigants in water and soil samples soil headspace or GC/ECD/NPD 

in soil/water Journal of Separation Science, 28, #1, 98-103 immersed in water 

Fuster, S.; Beltran, J.; Lopez, F. J.; Hernandez, F. 

Impurity analysis of 1,4-dioxane in nonionic surfactants and 

2006 Surfactants cosmetics using headspace SPME coupled w/GC & GC-MS headspace GC, GC-MS 

in water J. Chromatogr. A, 1071, #1-2, 141-145 

Fuh, C. Bor; Lai, M.; Tsai, H. Y.; Chang, C. M. 

Rapid screening for trace nonyl-phenyl 

2007 Surfactants polyethylene glycol ether in water by SPME 14 hour SALDI-MS 

in water combining with laser desorption ionization MS polycrystaline 

Proc. 50th ASMS Conf. Mass Spectrom. Allied Top. graphite coated fiber 

2002, p597-599 

Chen, Yu-Chie; Sun, Mei-Chuan 

Analysis of methylamine by SPME and HPLC after 

2008 Methylamine on-fiber derivatization with 9-fluorenylmethyl chloroformate 9-fluorenylmethyl HPLC 

in water Anal. Chim. Acta, 513, #2, 425-433 chloroformate 

Campins-Falco, P.; Chafer-Pericas, C.; Herraez-Hernandez, R derivative 

immersion sampling 

A new selective method for dimethylamine in water analysis 

2009 Methylamine by LC using SPME and two-stage derivatization with 50µm CW-TPR HPLC 

in water o-phthalaldialdehyde and 9-fluorenylmethyl chloroformate 9-fluorenylmethyl 

Talanta, 66, #5, 1139-1145 chloroformate 

Chafer-Pericas, C; Herraez-Hernandez, R.; Campins-Falco, P derivative 

immersion sampling 

Determining leaching of bisphenol A from plastic 

2010 Bisphenol A containers by SPME-GC-MS 85µm polyacrylate GC-MS 

from water Anal. Chim. Acta, 539, #1-2, 41-47 50min @ 65°C 

Chang, Chia-Min; Chou, Chi-Chi; Lee, Maw-Rong BSTFA derivative 

headspace 

Determination of trace bisphenol-A in leachate by 

2011 Bisphenol A SPME coupled with HPLC HPLC-UV 

from water Fenxi Kexue Xuebao, 20, #5, 461-464 

Deng, L.; Zhang, W. H.; Feng, X. H.; Deng, N. S.* 

Fibre selection based on an overall analytical feature comparison for the 

2426 Trihalomethanes solid-phase microextraction of trihalomethanes from drinking water 65µm PDMS-DVB GC-MS 

in drinking water J. Chromatogr., A 1139, #1, 27-35 (2007-01-12) headspace 

San Juan, P. M.; Carrillo, J. D.; Tena, M. T. 40°C, 0.36 g mL salt 

Novel analytical methods for the determination of fuel oxygenates 

2857 Fuel oxygenates in water review article 

in water HANDBOOK OF ENVIRONMENTAL CHEMISTRY pp1-30 (2007) 

Jochmann, Maik A.; Schmidt, Torsten C. 

Measurement of fuel oxygenates in tap water using SPME-GC-MS 

2758 Fuel oxygenates J Chrom Sci, 46, #5, 381-387 (MAY-JUN 2008) headspace GC-MS 

in tap water Cardinali, Frederick L.; Blount, Benjamin C.; Schmidt, Rachael; Morrow, J. 

2012 THM & TBE 

Measurement of trihalomethanes and methyl 

tertiary-butyl ether in tap water using SPME-GC-MS. headspace GC-MS 





in tap water J Chrom Sci, 42, #4, 200-206 

Cardinali, F.; Ashley, D.; Morrow, J.; Moll, D.; Blount, B. 

Methods for sampling and analysis of tropospheric 

2013 Ethanol in ethanol in gaseous and aqueous phases. headspace from GC-FID 

air & water Chemosphere, 52, #8, 1307-1319 cryocooled sample 

Monod, A.; Bonnefoy, N.; Kaluzny, P.; Denis, I.; 

Foster, P.; Carlier, P. 

Determination of aniline in water by microwave- 

2014 Aniline assisted headspace SPME-gas chromatography. 65µm PDMS-DVB GC-FID 

in water Chromatographia, 59, #7-8, 517-520 headspace 

Yan, C. T.; Jen, J. F.* pH12, salt added 

Coupling of a modified in-tube spme technique w/ 

2015 PAHs HPLC-fluorescence detection for the ultra-trace PDMS capillary tube HPLC 

in water determination of PAHs in water samples. 

Chromatographia, 59, #7-8, 501-505 

Bagheri, H.; Salemi, A. 

Quantitation of formate in plants and its enhancement in response 

2773 Formate in to environmental stresses GC/MS 

plants J Applied Biological Chem 50, #4, 211-214 (DEC 2007) 

Kim, Jae-Kwang; Cho, Myoung-Rae; Baek, Hyung-Jin; Ryu, Tae-Hun; 

Kim, Jung-Bong; Kim, Jun-Heong; Kim, Myong-Jo; Yu, Chang-Yeon; 

Fukusaki, Ei-Ichiro; Kobayashi, Akio 

Improved method for the in vitro assessment of antioxidant activity of 

2458 Antioxidants plant extracts by headspace SPME-GC-ECD GC-ECD 

in plants J. Chromatogr., A 1152, #1-2, 150-155 (2007-06-08) headspace 

Gioti, E. M.; Fiamegos, Y. C.; Skalkos, D. C.; Stalikas, C. D. hydrazone derivative 

Development of malonaldehyde assay using headspace -SPME) 

2263 Malonaldehyde and its application for antioxidants headspace GC/MS 

Abstracts of Papers Am Chem Society (2005) 229 #1, U57 

Fujioka, Kazutoshi; Shibamoto, Takayuki 

SPME for qualitative and quantitative determination of 

2016 Aromatic migrated degradation products of antioxidants in an headspace GC 

compounds organic aqueous solution 

in 10% alcohol J. Chromatogr. A, 1080, #-2, 107-116 

water mixture Albertsson, Ann-Christine; Burman, L.; Hoglund, A. 

Analysis of anatoxin-a using polyaniline as a sorbent in SPME 

2017 Anatoxin coupled to GC-MS 32µm polypyrrole film GC-MS 

in water J. Chromatogr. A, 1078, #1--2, 120-127 10% salt 

Davarani, H.; Fallahi, M.; Ghassempour, A.; 30min w/agitation 

Mehdinia, A.; Najafi, N.; Nakhshab, M. 

SPME-HPLCdetermination of Nabam, Thiram, and 

2018 agrochemicals Azamethiphos in water samples with UV detection: PDMS fiber HPLC-UV 

in water preliminary data headspace 

Talanta, 66, #1, 266-270 

Aulakh, Jatinder Singh; Malik, A. K.; Mahajan, R. K. 

Headspace single-drop microextration for the 

2019 Orgaonotin detection of organotin compounds headspace GC 

in water Talanta, 63, #3, 555-560 

Bancon-Montigny, C; Colombini, V; Maxwell, P; 

Mester, Z; Sturgeon, R: Yang, Lu 

Determination of organotin compounds in water by headspace 

2020 Orgaonotin SPMEwith GC-MS NaEt 4B derivatives GC-MS 

in water J. Chromatogr. A, 1064 #1, 1-8 30min @ 45°C, pH 5 

Chou, Chi-Chi; Lee, Maw-Rong headspace 

Automated headspace-SPME-retention time locked- 

2021 Organotin isotope dilution GC-MS for the analysis of organotin NaEt 4B derivatives GC-MS 

in water/ compounds in water and sediment samples headspace 

sediment J. Chromatogr. A, 1079, #1-2, 408-414 

David, F; Devos, C; Moens, L; Sandra, P.; 

Vliegen, M; Willaert, B 

2022 Phthalate 

Monitoring the sonochemical degradation of 

phthalate esters in water using SPME immersion sampling GC 

esters in Chemosphere, 54, #7, 849-857 21°C & 50°C 





water Psillakis, E.; Mantzavinos, D.; Kalogerakis, N. NaCl addition 

SPME-GC-MS for the analysis of selective serotonin 

2023 Drugs from reuptake inhibitors in environmental water 65µm PDMS-DVB GC-MS 

water J. Chromatogr. A, 1045, #1-2, 241-247 100°C, direct extract 

Cela, R; Garcia-Jares, C; Gomez, Mo; Llompart, M; in situ acetylation 

Pablo Lamas, J.;Salgado-Petinal, Carmen 

Analysis of earthy and musty odors in water samples 

2024 Musty odors bySPME coupled with GC-ion trap MS headspace GC-ITMS 

in water Talanta, 65, #2, 518-524 

Huang, Shang-Da; Li, Tzu-Ying; Sung, Yu-Hsiang 

Determination of trace triazine and chloroacetamide herbicides in 

2913 Triazine tile-fed drainage ditch water using SPME coupled with GC-MS 100 µm PDMS GC-MS 

herbicides in Environ. Pollut.152, #1, 239-244 (March 2008) headspace 

ground water Huang, Chi-hua; Pappas, Elizabeth A.; Rocha, Cleonice 40 min, 

83% NaCl, 

Optimization of a SPME procedure for the 

2025 Triazine detemination of herbicides by micellar electrokinetic 65µm PDMS-DVB SPME-MEKC 

herbicides in chromatography. 120 min 

ground water J Separation Sci, 27, #9, 660-666 10% NaCl, stirring 

Frias-Garcia, S.; Sanchez, M..; Rodriguez-Delgado, M 

Analysis of triazine in water samples by SPME-HPLC 

2026 Triazine Talanta, 64, #4, 887-893 50µm CW-TPR HPLC 

herbicides in Huang, Hsin-I; Huang, Shang-Da; Sung, Yu-Hsiang 100µm PDMS 

water 

Applications of chitosan beads and porous crab shell powder combined 

2823 Organics in with for detection and the removal of colour from textile wastewater PDMS fiber GC-MS 

wastewater Carbohydr Polym 72, #3, 550-556 (May 16 2008) headspace 

Lu, Li C.; Sye, Wen F.; Tai, Jia W.; Wang, Cheng I. 

A laboratory batch reactor test for assessing nonspeciated 

2027 Volatiles in volatile organic compound biodegradation in activated sludge headspace GC 

wastewater Water Environ. Res., 75, #4, 342-354 

Allen, C.; Cano, M.; Huot, M.; Rhodes, I.; Saterbak, A; 

Van Compernolle,Remi; Williams, M. 

Determination of organic contaminants in 

2028 Organics coastal water LC-MS 

in seawater Trends in Anal Chemistry, 23, #4, 341-350 

Gimeno, R. A.; Marce, R. M.*; Borrull, F. 

Study of the photoinduced degradation of polycyclic 

2029 Musk musk compounds by SPME and GC-MS PDMS fiber GC-MS 

compounds Rapid Comm in Mass Spec, 18, #111, 1186-1192 headspace 

in water Sanchez-Prado, L; Llompart,M; Lores,M; 

Garcia-Jares,C; Cela, R 

Development of a SPME method for the analysis of phenolic flame 

2569 Phenolic retardants in water samples. 75µm Carboxen GC-MS 

fire retardants J. Chromatogr., A 1124, #1-2, 11-21 (2006-08-18) headspace 

in water Polo, M.; Llompart, M. ; Garcia, C.; Gomez-Noya, G.; Bollain, M.; Cela, R. 100°C 

Determination of organophosphorus fire retardants and plasticizers in 

2509 Organophosphorus wastewater samples using MAE-SPME with GC-ICPMS and GC-TOFMS 

fire retardants GC-TOFMS detection 30min @ 65°C GC-ICPMS 

in wastewater JEM 9, #12, 1329-1336 (2007) 10% NaCl 

Ellis, Jenny; Shah, Monika; Kubachka, Kevin M.; Caruso, Joseph A. 

Recent developments in the analysis of brominated flame retardants 

2483 Brominated and brominated natural compounds 

compounds J. Chromatogr. A 1153, #1-2, 145-171 (15 JUN 2007) 

Review article Covaci, A.; Voorspoels, S.; Ramos, L.; Neels, H.; Blust, R 

Microwave-assisted extraction followed by headspace SPME-GC-MS 

2464 Polybrominated detection for determination of polybrominated compounds in headspace GC-MS/MS 

compounds in aquaculture samples 

water Anal. Bioanal. Chem. 388, #5-6, 1021-1029 (2007-07) 

Carro, A. M.; Lorenzo, R. A.; Phan-Tan-Luu, R.; Cela, R. 

2571 Polybrominated 

Simple approach for the determination of brominated flame retardants 

in environmental solid samples based on solvent extraction and SPME headspace GC-MS/MS 

compounds in followed by gas chromatography-tandem mass spectrometry 





sewage sludge J. Chromatogr., A 1124, #1-2, 139-147 (2006-08-18) 

Salgado, C.; Llompart, M. ; Garcia-Jares, C.; Gares-Chao, M.; Cela, R 

Investigation of photodegradation products generated 

2030 PBDEs in after UV-irradiation of five polybrominated diphenyl PDMS fiber GC-MS 

water ethers using photo SPME 

Journal of Chromatography A, 1071, #1-2, 85-92 

Sanchez-Prado, L.; Llompart,M.; Lores,M.; 

Garcia-Jares,C.; Cela, R. 

Determination of organic contaminants in coastal water 

2031 Organics in TrAC Trends Anal. Chem., 23, #4, 341-350 GC 

water Borrull, F.; Gimeno, R.A.; Marce, R.M. 

Determination of the acaricide fenbutatin oxide in water 

2032 Acaricide samples by automated headspace-SPME-GC/MS headspace GC-MS 

fenbutatin J. Sep. Sci., 26, #7, 665-668 NaEt 4B derivatives 

oxide in water Devos, Christophe; Moens, Luc; Sandra, Pat 30min @ 80°C 

Linear alkylbenzensulphonic acids (LAS) oxidation by 

2033 Alkylbezene- H2O2 and O2: An investigation by GC & LC coupled w/MS headspace GC-MS 

sulphonic acid Appl. Catal. B Environ.59, #1-2, 113-120 

in water Cuzzola, Angela; Raffaelli, Andrea; Salvadori, Piero 

SPME for the evaluation of partition coefficients of a 

2034 Dioxin, hexa- chlorinated dioxin and hexachlorobenzene into immersed GC-ECD 

chlorobenzene humic substances 

in water Analytical Sciences, 20, #5, 787-791 

Yabuta, H.; Fukushima, M. *; Tanaka, F.; 

Ichikawa, H.; Tatsumi, K. 

Influence of chemical characteristics of humic substances on 

2035 Dioxin, hexa- the partition coefficient of a chlorinated dioxin headspace GC-ECD 

chlorobenzene Chemosphere, 58,#10, 1319-1326 

in water Fukushima, Masami; Ichikawa, Hiroyasu; Kikuchi, Atsunori 

Tanaka, Fumiko; Tatsumi, Kenji; Yabuta, Hikaru 

A case study of molinate application in a Portuguese 

2036 Molinate rice field: Herbicide dissipation and proposal of a immersed sampling GC-FPD 

herbicides clean-up methodology 

in water Chemosphere, 59, #7, 1059-1065 

Castro, M; Manaia, C.; Nunes, O.; Silva-Ferreira, A. 

Determination of organic contaminants in coastal water 

2037 Organics in Trends in Analytical Chemistry, 23, #4, 341-350 LC-MS 

seawater Gimeno, R. A.; Marce, R. M.; Borrull, F. 

Development of SPME-HPLC method for the determination of 

2816 Copper II from copper(h) in environmental samples using morpholine-4-carbodithioate 100µm PDMS LC-MS 

environmental Annali di Chimica 97, #11-12, 1279-1290 (NOV-DEC 2007) derivatives 

samples Kaur, Varinder; Malik, Ashok Kumar 

Simultaneous multi-elemental speciation analysis 

2038 Organometals of organometallic compounds by SPME and multi- 65µm PDMS-DVB ICP-TOF-MS 

in water capillary GC hyphenated to ICP-time-of-flight-MS 75µm Carboxen 

J Anal At Spectrom, 19, #7, 867-875 headspace 

Adams, Freddy C.; Infante, Heidi G; Jitaru, Petru NaEt 4B derivatives 

Speciation analysis of mercury by SPME and multi- 

2039 Mercury capillary GC- inductively coupled plasma-TOF-MS 75µm Carboxen GC-ICP-MS 

in water J. Chromatogr. A,1055, #1-2, 197-207 headspace 

Adams, Freddy C.; Jitaru, Petru NaEt 4B derivatives 

Fast speciation analysis of iodophenol compounds 

2040 Iodophenols in river waters by capillary electrophoresis- immersion sampling ICP-MS 

in river water ICP-MS with off-line SPME 

Electrophoresis, 25, #12, 1843-1851 

Kannamikumarath, Sasi S.; Wuilloud, Rodolfo G.; 

Jayasinghe, Sarath; Caruso, Joseph A. 

Determination of oil pollutants in aqueous samples with the use of 

2195 Oil pollutants steam carrier gas chromatography 

in water Pet. Chem.46, #1, 60-64 (2006) 

Chuikin, A.V.; Grigor'ev, S.V.; Velikov, A.A. 





Optimization of SPME for the GC-MS analysis of 

2041 Organic persistent organic pollutants varios fibers GC/MS 

pollutants J AOAC Int, 87, #4, 1021-1027 

from water Alpendurada, M.; Gago-MARTINEZ, A; Nogueiras, M, 

Prado, Juan; Rellan, Satvdra;Vetter, Walter 

Use of headspace SPME to characterize odour 

2042 Amines, fatty compounds in subsurface flow constructed wetland headspace GC/MS or GC/NPD 

acids, alky- for wastewater treatment 

sulfides in Water Sci. Technol., 49, #9, 89-98 

wastewater Aguirre, P.; Bayona, J.M.; Garcia, J.; Huang, Y.; 

Mujeriego, R.; Ortiz, L. 

Development of a simple and sensitive method for the 

2043 Odourous characterization of odorous waste gasemissions by 75µm Carboxen GC/MS or GC/FID/O 

compounds means of SPME-GC-MS/olfactometry headspace 

from waste Waste Manage., 25, #9, 872-879 

gas Jans, M.; Kleeberg, K.K.; Liu, Y.; Schlegelmilch, M.; 

Stegmann, R.; Streese, J. 

Comparison of strategies for extraction of high 

2044 PAHs in molecular weight PAHs from drinking waters immersion sampling HPLC-FLD 

drinking water J Agr Food Chem, 52, #23, 6897-6903 

Garcia-Falcon, M. S.; Perez-Lamela, M.; 

Simal-Gandara, J. 

Determination of PAHs in water by SPME-HPLC 

2045 PAHs in Analytical Sciences, 20, #10, 1383-1388 35min immersed extract HPLC-FLD 

water Chen, H. W. added 1.5M sodium 

monochloroacetate 

Determination of organochlorides in water using 

2046 organochlorides solid-phase microextraction coupled to GC 65µm PDMS-DVB GC 

in water Am Lab, 34. #17, 12-14 45sec @ 50°C 

Huang, Min-Jia; Li, Ju-Bai; Liang, Bing; Ou, Qing-Yu 

SPME measurement of parent and alkyl PAHs in 

2047 PAHs in milliliter sediment pore water samples and immersion sampling GC/ MS 

water determination of K' values 

Environ. Sci. Technol,.39, #8,2795-2803 

Grabanski, C.; Hawthorne, S.; Kreitinger, J..; Miller, D. 

Coupling of SPME with MCC/UV-IMS as a tool for rapid on-site 

2048 Organics in detection of groundwater and surface water contamination headspace UV-IMS 

groundwater Anal. Bioanal. Chem., 382, #8, 1842-1847 

Baumbach, J.I.; Klockow, D.; Walendzik, G. 

Simultaneous picogram determination of "earthy-musty" odorous 

2292 Trichloroanisoles compounds in water using SPME-GC-MS coupled with initial cool DVB/CAR 50/30µm GC/MS 

and gesomin in programmable temperature vaporizer inlet headspace 

water J. Chromatogr. A 1098, #1-2, 7-13 (2005) 

Hu, Ruikang; Yang, Zhaoguang; Zhang, Lifeng 

Detection of 2,4,6-trichloroanisole in chlorinated water at 

2049 2,4,6-Trichloro- nanogram per litre levels by SPME-GC-ECD 100µm PDMS GC-ECD 

anisole in Anal. Bioanal. Chem., 382, #2, 341-346 headspace 

chlorinated Da Silva, Joaquim C. G. Esteves; Pinheiro, Paula B. M. 

water 

SPME and headspace derivatization of clenbuterol followed 

2050 Clenbuterol by GC-FID and GC-SIMMS quantification 85µm polyacrylate GC-FID, GC-MS 

in water Anal. Bioanal. Chem., 375, #3, 460-464 HMDS derivative 

Engelmann, M.D.; Hinz, D.; Wenclawiak, B.W. headspace 

Use of SPME-GC-ECD for the determination of energetic 

2051 Explosives chemicals, in marine samples 65µm CW/DVB GC-ECD 

in water J Chromatogr A, 1066, #1-2, 177-187 30% salt added 

Monteil-Rivera, Fanny; Beaulieu, Chantale; Hawari, J. 

SPME ion mobility spectrometer interface for explosive 

2051 Explosives and taggant detection headspace Ion mobility 

in water J Sep Science, 28, #2, 177-183 spectrometry 

Perr, Jeannette M.; Furton, Kenneth G.; Almirall, J. 


Determination of explosives in environmental water samples 

by SPME-liquid chromatography 50µm CW-TPR HPLC-UV 

in water J. Chromatogr. A, 1048, #2, 213-221 

Beaulieu,C.; Deschamps,S.; Hawari,J.; 

immersed 





Monteil-Rivera,F.; Paquet,L. 

In-tube capillary solid-phase microextraction coupled 

2053 Anthracen on-line to micro-HPL In-tube capillary HPLC 

in water Fenxi Shiyanshi, 24, #2, 41-43 

Shu, X.; Yang, B. C.; Tan, F.; Guan, Y. F. 

Optimization of a sensitive method for the determination of nitro musk 

2521 Nitro musk fragrances in waters by SPME-GC with micro ECD using factorial 75µm Carboxen GC-ECD 

fragrance in experimental design 65µm PDMS/DVB 

water Anal Bioanal Chem 388, #8, 1789-1798 (AUG 2007) headspace @ 100°C 

Polo, Maria; Garcia-Jares, Carmen; Llompart, Maria; Cela, Rafael 

Further SPME-GC-MS applications: "On-fibre" and 

2054 Volatiles and aqueous photodegradation of nitro musks immersion sampling GC-MS 

from musks J. Chromatogr. A, 1048. #1, 73-80 

Cela, R.; Garcia-Jares, C.; Llompart, M.; Lores, M.; 

Lourido, M.; Sanchez-Prado, L. 

Analysis of volatile organic compounds (VOCs) in sediments using in . 

2341 Volatiles situ SPME sampling headspace GC 

from sediment J Environ Monit 9 # 5, 411-418 (2007 May) 

Bravo-Linares, Claudio M; Mudge, Stephen M 

SPME for predicting the bioavailability of 

2055 2,4,6-trinitro- 2,4,6-trinitrotoluene and its primary transformation 85µm polyacrylate GC-MS 

toluene in products in sediment and water 

water & Environ. Toxicol. Chem., 24, #5, 1059-1066 

sediment Conder, Jason M.; La Point, Thomas W. 

Rapid analysis of aromatic contaminants in water samples 

2056 Aromatics by means of laser ionization mass spectrometry GC-MS 

in water Anal. Bioanal. Chem, 377, #7-8, 1124-1132 

Globig, Daniel; Weickhardt, Christian 

Coupling of SPME and capillary isoelectric focusing 

2057 phycoerythrin w/ laser-induced fluorescence whole column imaging 10 min sampling CIEF-WCID 

in water detection for protein analysis. 

Analytical Chemistry, 77, #1, 165-171 

Liu, Z.; Pawliszyn, J. * 

Spme fibers for estimating the toxicity of nitroaromatic 

2058 Nitroaromatics compounds 85µm polyacrylate GC 

in sediment, Aquatic Ecosystem Health & Mgmt, 7, #3, 387-397 immersion sampling 

water Conder, J. M.; Lotufo, G. R.; Bowen, A. T.; Turner, P. K.; 

La Point, T. W.; Steevens, J. A. 

Determination of perfluorocarboxylic acids in aqueous 

2059 Perfluoro- matrices by ion-pair SPME in-port derivatization GC headspace CI-MS 

carboxylic negative ion chemical ionization mass spectrometry butyl ester derivative 

acod in J Chromatogr, A, 1042, #1-2, 155-162 

water Alzaga, R.; Bayona, J. M.* 

Development of a procedure for the determination of 

2060 perfluoro- perfluorocarboxylic acids in sediments by pressurised headspace CI-MS 

carboxylic fluid extraction, headspace SPME followed by GCMS 

acod in Journal of Chromatography, A, 1083, #1-2, 1-6 

water Alzaga, R.; Bayona, J.M.; Jover, E.; Salgado-Petinal, C. 

Determination of fuel dialkyl ethers and BTEX in water 

2061 Dialkyl ethers using headspace SPME and GC-FID 65µm PDMS-DVB GC-FID 

in water J Chromatogra A, 1033, #2, 193-203 headspace 

Arambarri, I.; Lasa, M.; Garcia, Rosa; Millan, E. 10min @ 10°C 

Identification of MTBE in water by SPME and GC-MS 

2062 MTBE Am Lab, 34, #21, 34 headspace GC/MS 

in water Blasi, G.; Guidotti, M.; Lucarelli, E.; Onorati, B.; 

Ravaioli, G.; Stella, D. 

Analysis of taste- and odor-causing compounds 

2063 Taste/odor in drinking water using solid-phase microextraction review technique GC 

in water Am Lab, 35, #17, 42-46 

Voit, Jim 

2064 MTBE 

Interlaboratory comparison study for the determination 

of methyl tert-butyl ether in water various fibers GC/MS 





in water Anal. Bioanal. Chem., 377, #7-8, 1140-1147 GC-FID 

Fuhrer, M.; Kandler, W.; Krska, R.; 

Schuhmacher, R.; Stadlmann, C. 

Comparison of SPME headspace analysis to U.S. 

2065 MTBE, TBA EPA Method 5030/8260B for MTBE monitoring 75µm Carboxen GC-MS 

in water Ground Water Monit. Rem., 25, #2, 52-58 headspace 

Oh, Keun-Chan; Stringfellow, William T. 

Observations on SPME for MTBE analysis 

2066 MTBE Chemosphere, 57, #6, 523-527 headspace GC-MS 

in water Bergendahl, J.; Erdem-Senatalar, Ayse; Thompson, Robert W. 

Sources, distribution and behaviour of methyl tert-butyl 

2067 MTBE ether (MTBE) in the Tamar Estuary, UK 75µm Carboxen GC-MS 

in water Chemosphere, 57, #6, 429-437 75% salt added 

Bayona, Josep M.; Guitart, Carlos; Readman, James W. headspace 

Spme for the determination of chromium in sea-water. 

2068 Chromium in J of Anal Atomic Spectrometry, 19, #9, 1098-1103 100µm PDMS GC-ECD 

sea water Abranko, L.; Yang, L.; Sturgeon, R. L.; Fodor, P.; Mester, Z. headspace derivatives ICP-MS, EI-MS 

(trifluoroacetylacetone) 

Micro-solid-phase extraction with helical-solid-sorbent in 

2069 Saccharides the presence of organic solvent for GC-MS analysis of - headspace GC-MS 

from water & per-O-methylated mono and disaccharides. per- O -methylation 

juices Analytica Chimica Acta, 519, #1, 93-101 

Ciucanu, I.; Swallow, K. C.; Caprita, R. 

Analysis of compound-specific carbon isotopic compositions 

2070 Volatiles in of trace-level volatile organic compounds in aqueous phases. cryofocused injection GC 

water Sepu, 22, #4, 439-441 headspace sampling 

Liu, G. Q.; Zhang, G.; Huang, S. Q.; Peng, X. Z.; Chen, H. H. 

On-line coupling of in-tube SPME to capillary GC 

2071 Volatiles in for trace analysis of aqueous samples. GC 

water Sepu, 22, #4, 354-357 

Guan, Y. F.; Wang, H. W.; Liu, W. M. 

SPE versus SPME for the determination of chlorinated 

2071 Chlorinated paraffins in water using GC-negative chemical ion MS immersed fiber GC-NCI-MS 

parafins in J Chromatography, A, 1025, #2, 157-162 

water Castells, P.; Santos, F. J.; Galceran, M. T.* 

Headspace SPME GC-ECD determination of organic chlorinated 

2175 Chlorinated hydrocarbons in soils headspace GC-ECD 

hydrocarbons in Annali di Chimica 95, #11-12, 741-756 (2005) water solution 

soils Pastore, Paolo; Favaro, Gabriella; Badocco, Denis; Lavagnini, Irma 

Development of a SPME-based method for sampling 

2073 Chlorinated of persistent chlorinated hydrocarbons in an 100µm PDMS GC 

hydrocarbons urbanized coastal environment in situ sampling 

in water Environ. Sci. Technol., 38, #21, 5737-5743 18 to 43 days 

Diehl, Dario W.; Tsukada, David; Zeng, Eddy Y. 

An automated headspace SPME-GC-ITMS technique for 

2074 Odors from taste and odor compound identification 65µm PDMS-DVB GC-ITMS 

water Water Qual. Res. J. Can., 39, #3, 213-222 headspace 

Davies, John-Mark; Furtula, Vesna; Mazumder, Asit 

Determination of PAHs in water by SPME-GC-MS 

2075 PAHs in Anal. Chim. Acta, 523, #2, 259-267 agitation applied GC-MS 

water King, A.J.; Readman, J.W.; Zhou, J.L. immersed 

Determination of phenolic compounds in wastewater 

2076 Phenols samples using a novel fiber by SPME coupled to GC 85µm polyacrylate GC-FID 

in waste Analytica Chimica Acta, 538, #1-2, 63-70 

water Zhou, Furong; Li, Xiujuan; Zeng, Zhaorui 

SPME - capillary GC combined w/ microwave-Inducted 

2077 Selenite plasma atomic-emission spectrometry for selenite NaEt 4B derivatives GC-MIP-AED 

in water determination headspace 

Anal& Bioanalytical Chem, 379, #5, 842-848 

Dimitrakakis, E.; Haberhauer-Troyer, C. *; Abe, Y.; 

Ochsenkuhn-Petropoulou, M. T.; Rosenberg, E. 




Matrix 

Pesticides 


Determination of Pesticides in Aqueous Environmental 


441 Pesticides Samples via SPME (Solid-Phase Microextraction) 

in water GIT Frachz. Lab. 39: 25-26 (1995) 

Eisert, R., Levsen, K. 


Quantitative analysis of pesticides in water by SPME 

coupled with Mass Spectrometry 100µm PDMS, 65µm GC-MS 

in water Spectra. Anal. 1999, 28(208), 23-29 DVB/PDMS 

Massat, F. Laurent, A. 

A Systematic Approach to Optimize SPME determination 

30 min 

agitated 

523 Organochlorine & of Pesticides in Ethanol/Water mixtures 

organophosphorus used as Food Simulates 

in water/ethanol Anal. Chem. (1999), 71(13), 2417-2422 

Batlle, R, Sanchez, C., Nerin, C. 

Solid-Phase Microextraction (SPME) 

442 GIT Frachz. Lab. 39: 325-331 (1995) 

Popp, P., Kauert, A., Kalbitz, K. 


Determination of organophosphorus insecticides in natural 

waters using SPE-disks and SPME followed by 85µm polyacrylate GC-FTD and 

pesticides GC-FTD and GC-MS GC-MS 

in water Fresenius' J Anal Chem (2000) 368(6) 616-623 

Lambropoulou, D.; Sakellarides, T.; Albanis, T. 


Optimization of headspace SPME conditions for the 

determination of organophorus insecticides in natural water 

pesticides J. Chromatogr. A (2001) 922(1-2) 243-255 

in water Lambropoulou, D.; Albanis, T. 


Pesticide Analysis by SPME 

Am. Env. Lab. April 1997, pp 20-22 100µm PDMS GC-FID 

pesticides Eisert, R., Gorecki, T., Pawliszyn, J. 60 min 

in water immersion 

2487 Benzimidazole 

SPME of benzimidazole fungicides in environmental liquid samples and 

HPLC-fluorescence determination 75µm Carboxen HPLC 

Fungicides Anal Bioanal Chemistry 387, #6, 1957-1963 (2007) fluorescence 

in water Lopez-Monzon, A.; Vega-Moreno, D.; Torres-Padron, M. E.; 

Sosa-Ferrera, Z.; Santana-Rodriguez, J. J. 

104 Insecticides, 

Influence of Ethanol on Pesticide Extraction in 

Aqueous Solutions by SPME 100µm PDMS GC-MS 

fungicides J. Agric. Food Chem. 44: 3871-3877 (1996) 30 min 

in water Urruty, L., Montury, M. headspace 


Simultaneous Determination of 60 Pesticides in Water 

Using SPME and GC/MS 100µm PDMS GC-MS 

in water Analyst 121: 929-938, July 1996 50 min 

Boyd-Boland, A., Magdic, S., Pawliszyn, J. 

Solid-Phase Microextraction of Nitrogen- and Phosphorusimmersion 


241 Nitrogen- & phosphate- Containing Pesticides from Water and GC Analysis 100µm PDMS GC-NPD 

pesticides Environ. Sci. Technol. 30: 3259-3265 (1996) 60 min 

in water Choudhury, T., Gerhardt, K., Mawhinney, T. immersion 

52 Pesticides 

Determination of Organophosphorus, Triazine, and 

2,6-Dinitroanailine Pesticides in Aqueous Samples via 100µm PDMS, GC-NPD 

in water SPME and GC with NPD Detection 85µm polyacrylate 

Fresenius J. Anal. Chem. 351: 555-562 (1995) 25 min 


Simple Extraction of Organophosphate Pesticides Using 

immersion 






443 Organophosphate (SPME) Before Capillary Gas Chromatography GC-NPD, -MS 

pesticides Hochudoku 13 (2): 122-123 (1995) 

in water Lee, X., Kumazawa, T., Taguchi, T., Sato, K., Suzuki, O. 


Analysis of Organophosphorus Insecticides from 

Environmental Samples Using SPME 85µm polyacrylate GC-NPD 

insecticides J. Chromatogr. A 736: 219-228 (1996) 60°C, 60 min 

in water Magdic, S., Boyd-Boland, A., Jinno, K., Pawliszyn, J. 

Solventless sample preparation procedure for 

immersion 

salt added 

861 Organophosphorus organophosphorus pesticides analysis using SPME and HPLC 

pesticides on-line supercritical fluid extraction/HPLC technique. 

in water Analytica Chimica Acta (2001) 433(2) 207-215 

Jinno, K; Kiso, Yoshiaki; S, Yoshihiro; S, Shamsul H 


Matrix Effects on SPME of Organophosphorus 

Pesticides from Water 85µm polyacrylate GC-NPD 

pesticides J. Chromatogr. A 767: 195-203 (1997) 60°C, 45 min 

in water Valor, I., Molto, J., Apraiz, D., Font, G. 

SPME of 52 pesticides and polychlorinated biphenyls: 

immersion 

stirring 

839 52 Pesticides, PCBs efficiencies of the SPME coatings PDMS, polyacrylate, 

PDMS/DVB, Carboxen/PDMS, and Carbowax/DVB 

J. Sep. Sci. 2001) 24(1), 39-48 

Valor, I; Perez, M; Cortada, C; Apraiz, D; Molto, J; Font, G 

65µm PDMS/DVB 


Solid Phase Microextraction of Organophosphorus 

Pesticides from Water 65µm PDMS/DVB 

pesticides J. Chromatogr. A 759: 225-230 (1997) 30 min 

in water Sng, M., Lee, F., Lakso, H. immersion 


Determination of organophosphorus pesticides in water 

using GC-MS 100µm PDMS GC-MS 

pesticides Qim. Nova (1999), 22(2), 197-200 

in water Silva, F., Cardeal, Z., De Carvalho, C. Portuguese 

Headspace solid-phase microextraction for the gas chromatographic 

2579 Organophosphorus analysis of organophosphorus insecticides in vegetables 100µm PDMS GC-FPD 

pesticides J AOAC Int 90, #6, 1677-81 (2007 Nov-Dec) headspace 

in vegetables Fytianos, K.; Drimaropoulou, G.; Raikos, N.; Theodoridis, G.; Tsoukali, H. 


The Application of SPME in the Analysis of 

Organophosphorus Pesticides in a Food Plant 100µm PDMS GC-FPD 

pesticides Environ Sci. Technol. 1998, 32, 3816-820 90 min 

in food plant Chen, W., Poon, K., Lam, M. immersion (water) 

525 Pyrethrins in 

Heterogenic catalytic hydrolysis and analysis of natural 

pyrethrins in subcritcal water coupled w/SPME-GC-MS 100µm PDMS GC-FID or 

insect spray, Fresenius'J. Anal. Chem. 1999, 364(7), 625-630 20 min @ pH 2 MSD 

shampoo, flowers Krappe, M, Hawthorne, S., Weclawiak, B. immersed 

705 Pyrethroids 

SPME of pyrethroid pesticides from water at low and 

sub-ppt levels at different temperature 100µm PDMS GC-ECD 

in water J.High Resolut.Chromatogr. (2000), 23(7/8), 485-488 5 min 

Barrionuevo, W., Lancas, F. 40-90°C 

837 Pyrethroids 

Solid-phase extraction (SPE) and solid-phase microextraction 

( SPME ) of pyrethroids in water 

in water Quim. Nova (2001), 24(2), 172-175 

Barrionuevo, W., Lancas, F. 


Online Determination of Organophosphorus Pesticides in 

Water by SPME and GC with Thermionic-Selective Detection 30µm PDMS GC-TCD 

pesticides J. High Resolut. Chromatogr. 20 (9): 487-492(1997 30 min 

in water Lopez-Avial, V., Young, R., Becker, W. immersion 




Matrix Literature Reference Conditions 

stirring 

Instrument 


SPME for quantitative analysis of organophosphorus 

Pesticides in Environmental Water Samples 100µm PDMS, GC-NPD 

pesticides J. Chromatogr. A 808 (1998) 257-263 85µm polyacrylate 

in water Beltran, J., Lopez, F., Hernandez, F. 

SPME for the determination of systemic and non-volatile 

30 min 


706 Pesticides pesticides in river water using GC with NPC and ECD 100µm PDMS GC-NPD 

in water J. Chromatogr. A 893(2000) 347-358 15min ECD 

Sampedro, M.; et al immersed 


Determination of herbicides in natural waters using (SPME) 

and GC coupled with flame thermionic and MS detection GC-MS 

in water Int. J. Environ. Anal. Chem (2000) 78(3-4), 223-240 

Lambropoulou, D.; Konstantinou, I; Albanis, T. 

707 Nitrogen herbicides 

Use of SPME for the Quantitative determination of 

Herbicides in soil and water samples Carbowax DVB GC-MS 

in water Anal. Chem. 2000, 72, 2313-2322 30 min SIM mode 

Hernandez, F., Beltran, J., Lopez, F, Gaspar, J. salt added, stirred 

28 Nitrogen herbicides 

Solid Phase Microextraction of Nitrogen-Containing 

Herbicides 85µm polyacrylate GC-NPD 

in water J Chromatogr. 704: 163-172 (1995) 50 min 

Boyd-Boland, A., Pawliszyn, J. immersion 


53 Triazine herbicides 

Automated Determination of S-Triazine Herbicides 

Using Solid-Phase Microextraction 100µm PDMS GC-NPD 

in water J. Chromatogr. 705: 305-312 (1995) 15 min (manual) 

Barnabas, I., Dean, J., Fowlis, I., Owen, S. 

Determination of Triazine Herbicides in Environmental Samples 

3 min (automated) 

immersion 

177 Triazine herbicides J. Chromatogr. 733: 295-335 (1996) (review) 100µm PDMS GC-NPD 

Dean, J., Wade, G., Barnabas, I. 

Validation of SPME for the Analysis of Triazine Herbicides 

10 min 

immersion (water) 

111 Triazine herbicides at ppt Level in Aqueous Samples Carbowax/DVB GC-NPD, 

in water J. Chromatogr. A. 795 (1998) 371-376 30 min GC-MS 

Nilsson, T., Ferrari, R., Basta, R., Dellavedova, P. immersion, stirring 

salt added 

708 Urea herbicides 

Indirect analysis of urea herbicides from environmental 

water using solid phase microextraction 85µm polyacrylate GC-NPD 

in water J. Chromatogr. A. 890 (2000) 303-312 immersed 

Berrada, H., Font,G., Molto, J. sat. salt, pH 4 

Depletion SPME for the evaluation of fiber-sample partition 

2162 Pesticides coefficients of pesticides headspace GC-MS 

J. Chromatogr. A, 1102, #1-2, 51-59 (2006) 

Zimmermann, Thomas; Ensinger, Wolfgang J.; Schmidt, Torsten C. 


Minimization of Solvent Consumption in Pesticide 

Residue Analysis overview 

J. Chromatogr. A 754: 43-47 (1996) 

Wan, H., Wong, M. 

article 


Determination of chlorine-containing pesticides in aqueous 

media by solid-phase microextraction method 

pesticides Zh. Prikl. Khim (2000) 73(11), 1877-1882 

in water Stolyarov, B. V.; Boiko, V. V 


Online Determination of Organochlorine Pesticides in Water 

by SPME and GC-ECD 100µm PDMS GC-ECD 

pesticides J. High Res. Chromatogr. 19(5): 24756 (1996) 20 min 





in water Young, R., Lopez-Avila, V., Beckert, W. immersion 

stirring 

Development and validation of a novel method for the analysis 

2307 Chlorinated of chlorinated pesticides in soils using microwave-assisted headspace GC/MS 

pesticides extraction- headspace SPME-GC-MS 

in soils Anal. Bioanal. Chem. 384 #3, 810-816 (2006) 

Alves, A.; Herbert, P.; Morais, S.; Paiga, P.; Santos, L. 

Optimization of a Technique of SPME and Capillary GC with 

180 Chlorinated pesticides ECD for the Determination of Nine Organochlorine Pesticides GC-ECD 

in water in Drinking Water 

Analusis 25 (3): 51-54 (1997) 

Almeida, M., Conceicao, P., Alpendurada, M. 


Application of SPME and GC with ECD for the 

analysis of chlorinated pesticides in water 100µm PDMS GC-ECD 

pesticides Spectra Anal (2000) 29(213) 20min. 

in water Boussahel, R., Bouland, S., Montiel, A., Moussaoui, K 


Comparison of three analytical procedures for determination 

of organochlorine pesticides and their by-products in water GC-ECD 

pesticides suspension during photocatalytic oxidation GC-MS 

in water Chemia Analityczna (Warsaw) (2000) 45(6) 901-910 

Wiergowski, M.; Zaleska, A.; Biziuk, M.; Hupka, J. 


Monitoring organochlorine pesticides from landfill leachates 

by GC-ECD detection after solid phase microextraction 100µm PDMS GC-ECD 

pesticides J. Chromatogr. A 891 (2000) 305-311 30 min @ 55°C 

in water Bras, I., Santos, L., Alves, A. immersion 

stirring 


Pesticide analysis in herbal infusions by SPME-GC-AED. 

Talanta 71, #3, 1417-1423 (2007-02-28) 100µm PDMS GC-AED 

in herbal teas Campillo, N.; Penalver, R.; Hernandez-Cordoba, M. immersion 


SPME for organochlorine pesticides residues analysis in 

Chinese herbal formulations 100µm PDMS GC-MS 

pesticides J. Chromatogr. A 898 (2000) 245-256 

in herbs Hwang, B. H.; Lee, M. R 


Element-Selective Detection of Pesticides by Gas 

Chromatography-Atomic Emission Detection and SPME 100µm PDMS GC-AED 

pesticides J. Chromatogr. A 683: 175-183 (1994) 20 min 

in water Eisert, R., Levsen, K., Wunsch, G. immersion 


Determination of organophosphorus pesticides in water 

by SPME 85µm polyacrylate GC-FPD 

in water Talanta (1999), 49(2), 393-402 

Su, P., Huang, S. 


Solid Phase microextraction in pesticides residue analysis 

J. Chromatogr. A 885 (2000) 389-404 review article 

various matrices Beltran, J., Lopez, F., Hernandez, F. 


An approach to solventless sample preparation 

procedure for pesticide analysis using SPME/supercritical HPLC 

in water fluid extraction technique 

Analytica Chimical Acta 2000, 418(1), 69-77 

Salleh, S., Saito, Y., Jinno, K. 


Solventless sample preparation procedure for organophosphorus 

pesticides analysis using SPME and on-line HPLC 

pesticides supercritical fluid extraction/HPLC technique 

in water Analytica Cheimica Acta 2001, 433(2), 207-215 





Salleh, S., Saito, Y., Kiso, Y., Jinno, K. 


87 Pesticides 

Determination of Pesticides in Aqueous Samples by SPME 

In-Line Coupled to Gas Chromatography-Mass Spectrometry GC-MS 

in water Am. Soc. Mass Spectrom. 6: 1119-1130 (1995) 


157 Contaminants 

Development of a Prototype System for Quasi-Continuous 

Analysis of Organic Contaminants in Surface or Sewage 85µm polyacrylate GC-FID 

in water Water Based on In-Line Coupling of SPME to GC 10 min 

J. Chromatogr. A 737: 59 (1996) 

Eisert, R., Levsen, K., Wuensch, G. 

immersion 

77 Metolachlor 

Solid Phase Microextraction of the Herbicide Metolachlor 

in Runoff and Tile Drainage Water Samples 100µm PDMS GC-ECD 

in water J. Chromatogr. A 725: 129 (1996) 15 min 

Webster, G., Gaynor, J., Ng, H., Graham, J., Sama, L. 

Comparative SPE, SPME, and Immunoassay Analysis 

immersion 

stirring 

193 Metolachlor of Metolachlor in Surface Runoff and Tile Drainage 100µm PDMS GC-ECD 

in water J. Agric. Food Chem. 44: 2736-2741 (1996) 15 min 

Graham, K., Ng, H., Tan, C., Gaynor, J., Cancilla, D., immersion 

Webster, G., Drury, C., Welacky, T., Sarna, L. stirring 

112 Polar herbicides 

Application of SPME Coupled with HPLC for Analysis 

of Polar Herbicides 

Request from Environmental Institute, European Commission 

Joint Research Centre, 21020 Ispra (Va) Italy 

Nilsson, T. 

HPLC 


Analysis of Pesticides in Environmental Water Sample 

by SPME-HPLC 85µm polyacrylate HPLC-UV 

in water J. Chromatogr. A754: 137-144 (1996) 60°C, 60 min 220nm 

Jinno, K., Muramats, T., Saito, Y., Kiso, Y., Magdic, S., immersion 

Pawliszyn, J. salt added 


Pesticides by Solid-Phase Microextraction: Results of 

Round Robin Test 100µm PDMS GC-MS 

in water Analyst (Cambridge) 121: 1381-1386 (1996) 45 min 

Gorecki, T., Mindrup, R., Pawliszyn, J. immersion 

stirring 


SPME and GC for Rapid Analysis of Pesticides 

Aanalusis (1998), 26(6), M137-M143 Review GC-MS 

water Miege, C., Dugay, J. 

Analysis of Organochlorine Pesticides by SPME 

298 Chlorinated pesticides J. Chromatogr. A 723(1): 111-112 (1996) 100µm PDMS GC-MS, -NPD 

Magdic, S., Pawliszyn, J. 

Optimization of SPME conditions using a response surface 

90 min 

immersion 

salt added 

527 Organochlorine methodology to determine organochlorine pesticides in 85µm polyacrylate GC-ECD 

pesticides water by GC-ECS 45 min @ 60°C 

in water J. Chromatogr. A (1999), 844(1+2), 425-432 immersed 

Aguilar, C., Penalver, A, Pocurull, E., Ferre, J., Borrull, F., 

Marce, R. 

agitated 


Effect of Various Parameters Governing SPME for the Trace 

Determination of Pesticides in Water 65µm PDMS/DVB GC-NPD 

in water J. Chromatogr., A 795 (1): 27-42 (1998) 25°C, 30 min 

Dugay, J., Miege, C., Hennion, M. 

SPME and GC-MS Detection for the Determination of 

immersion 


301 Pesticides Pesticides in Aqueous Samples 85µm polyacrylate GC-MS 





in water J. Chromatogr. A. 795 (1): 105-115 (1998) 55°C, 45 min 

Aguilar, C., Penalver, S., Pocurull, E., Borrull, F., Marce, R. 

Analysis of some pesticides in water samples using SPMEimmersion 


528 Pesticides GC with different Mass Spectrometric techniques GC-MS 

in water J. Chromatogr, A, 859(2): 193-202 (1999) 

Natangelo, M., Tavazzi, S., Fanelli, R., Befenatti, E. 

714 Fentin 

Headspace SPME capillary GC-ICP-MS for the 

determination of the organotin pesticide fentin in 100µm PDMS GC-ICP-MS 

in environmental environmental samples 10-20 min 

samples J.Anal. At. Spectrom. (2000), 15(6), 651-656 75-85°C 

Vercauteren, J., DeMeester, A, DeSmaele, T. NaBEt4 

Vanhaecka, F., Moens, L., Dams, R., Sandra, P. pH 8 


Analysis of Pesticides in Environmental Water Samples by 

SPME-HPLC 85µm polyacrylate HPLC-UV 

in water J. Chromatogr. A 754 (1+2): 137-144 (1996) 60°C, 60 min 220nm 

Jinno, L., Muramatsu, T., Saito, Y., Kiso, Y., Magdic, S., immersion 

Pawliszyn, J. stirring, salt added 


Study on solventless sample preparation of pesticides with 

SPME-SFE technique. 85µm polyacrylate HPLC-UV 

Chromatography. Jun 1999; 20(2): 126-127 

Selleh,-SH; Saito,-Y; Jinno,-K 

3 hr @ 60°C 

2329 Biologically active 

Bioanalytical applications of solid-phase microextraction 

Trends Anal. Chem. 26, #1, 36-45 (2007-01) Review article 

substance 

in water 

Musteata, F. M.; Pawliszyn, J. 

SPME-GC-MS of biologically active substance in 

715 Biologically active water samples 85µm polyacrylate GC-MS 

substance J. Chromatogr. A., (2000) 873(1), 95-106 65µm Carbowax/DVB 

in water Moeder, M., Schrader, S., Winkler, M., Popp, P. 30 min 

223 PCBs in 

SPME and Headspace SPME for the Determination of PCBs 

in Water Samples 100µm PDMS GC-MSD 

water Anal. Chem. 1998, 70, 2510-2515 100°C, 30 min 

Llompart, M., Fingas, M., Li, K. headspace/immersion 

stirring 

Determination of organochlorine pesticides in ground water. 

973 


pesticides in water J.Chromatogr. A (2002) 963(1-2), 95-105 

Perez-Trujillo, J.P.; Frias, S.; Conde, J.E.; Rodriguez-Delgado, M.A. 

Various 


Comparison of different fibers for the analysis of pesticides in water. 

J.Chromatogr. A (2002) 963(1-2), 19-26 

Goncalves, C.; Alpendurada, M.F. 

Various 


Monitoring of pesticides in the Kalamas River (Greece) 

J.Chromatogr. A (2002) 963(1-2), 107-116 

Lambropoulou, D. A.; Sakkas, V.A.; Hela, D.G.; Albanis, T.A. 

100 um PDMS GC-MS 

Comparison of microextraction procedures to determine pesticides in oranges 

by liquid chromatography-mass spectrometry. 

998 Pesticides in oranges J.Chromatogr. A (2002) 970(1-2), 201-212 

Blasco, C.; Font, G.; Pico, Y. 

LC-MS 

Multiresidue method for the simultaneous determination of four groups of 

pesticides in ground and drinking waters, using solid-phase microextraction-gas 

chromatography with electron-capture and thermionic specific detection. 

Pesticides in drinking 

1000 water J.Chromatogr. A (2002) 968(1-2), 177-190. PDMS/DVB GC 





Goncalves, C.; Alpendurada, M. F.* 



Monitoring of priority pesticides using SPME (solid phase microextraction) in 

river water from Greece 

Water Sc. Technol. Water Supply (2003) 3 (1-2), 335-342. 

Albanis, T.A.; Hela, D.; Lambropoulou, D.A.; Sakkas, V.A. 

PDMS GC-MS 

Determination of atrazine and four organophosphorus pesticides in ground 

water using solid phase microextraction ( SPME ) followed by gas 

chromatography with selected-ion monitoring. 

Pesticides in 

1009 groundwater J.Chromatogr. A (2002) 972(2), 183-194. 

Tomkins, B. A.; Ilgner, R. H. 

65 um PDMS/DVB GC-SIM 

An enzyme-linked immunosorbent assay (ELISA) for the detection of acetochlor 

1011 Acetochlor in water International Journal of Environ. Anal. Chem. (2002) 82 (11-12), 879-891. GC-MS 

Belai, Ivan; Eremin, Sergei; Hegedus, Gyongyver; Krikunova, Vitalia; Szekacs, 

Andras 

1019 

1046 

1047 

Evaluation of an enzyme immunoassay for the detection of the insect growth 

regulator fenoxycarb in environmental and biological samples. 

Fenoxycarb in 

environmental samples Pest Management Science (2003) 59 (4), 410-416. GC-MS 

Szekacs, Andras; Le, Hong T. M.; Szurdoki, Ferenc 

Organonitrogen 

pesticides in water. 


pesticides. 

Application of solid-phase microextraction for the determination of 

organonitrogen pesticides in aqueous samples by gas chromatography with 

nitrogen-phosphorus detector. 

International Journal of Environmental Analytical Chemistry (2002) 82 (10), 

691-703. 

Le Calvez, N.; Bodineau, L.; Fischer, J. C. 

Various GC 

Analysis of organochlorine pesticides by solid-phase microextraction followed 

by gas chromatography-mass spectrometry. 

International Journal of Environmental Analytical Chemistry (2002) 82 (10), 

651-657. 

Zambonin, C. G.; Aresta, A.; Nilsson, T. 

Various GC-MS 

Application of solid-phase microextraction for monitoring the photocatalytic 

decomposition of fenthion and parathion in aqueous TiO 2 suspensions. 

1048 Fenthion and parathion Analytica Chimica Acta (2002) 467 (1-2), 233-243. GC-MS 

Sakkas, V. A.; Lambropoulou, D. A.; Sakellarides, T. M.; Albanis, T. A.* 

1096 

1113 

Validation of an SPME method, using PDMS, PA, PDMS-DVB, and CW-DVB 

SPME fiber coatings, for analysis of organophosphorus insecticides in natural 

waters. 


insecticides in water. Analytical and Bioanalytical Chemistry (2002) 374 (5), 932-941. 


Various 

Solid-phase microextraction for herbicide determination in environmental 

samples 

Herbicides in 

environmental 

samples. Journal of Chromatography A (2003) 999 (1-2), 103-121. 

Krutz, L.J.; Sciumbato, A.S.; Senseman, S.A. 

GC 


Determination of herbicides, including thermally labile phenylureas, by solidphase 

microextraction and gas chromatography-mass spectrometry 


Carabias-Martinez, R.; Garcia-Hermida, C.; Hernandez-Mendez, J.; Rodriguez- 

Gonzalo, E.; Soriano-Bravo, F.E. 






Determination of dichlorvos by online microwave-assisted extraction coupled to 

headspace solid-phase microextraction and gas chromatography-electroncapture 

detection. 


1148 Dichlorvos Journal of Chromatography, A (2002) 976 (1-2), 349-355. 

Chen, Y. I.; Su, Y. S.; Jen, J. F.* 

GC-ECD 

Analysis of polar pesticides in water and wine samples by automated in-tube 

solid-phase microextraction coupled with high-performance liquid 


Polar pesticides in 

1152 water and wine. Journal of Chromatography, A (2002) 976 (1-2), 357-367. 

Wu, J. C.; Tragas, C.; Lord, H.; Pawliszyn, J. * 

ESI-MS 

1172 

1177 

1192 

Oxidation residues of 

herbicides 

Pesticides in water 

samples. 

Atrazine and 

organophosphorus 

pesticides in soil 

Determination of oxadiazon residues by headspace solid-phase microextraction 

and gas chromatography-mass spectrometry 


Araujo, Lilia; Navalon, Alberto; Prieto, Avismelsi; Vilchez, Jose Luis 

Solventless sample preparation for pesticides analysis in environmental water 

samples using solid-phase microextraction-high resolution gas 

chromatography/mass spectrometry (SPME-HRGC/MS) 

Journal of Environmental Science and Health - Part B Pesticides, Food 

Contaminants, and Agricultural Wastes (2003) 48 (4), 417-428. Various 

Lancas, Fernando M.; Souza, Dalva A. 

Solid-phase microextraction method for the determination of atrazine and four 

organophosphorus pesticides in soil samples by gas chromatography. 

Journal of Chromatography A (2001) 939(1-2), 13-21 GC-MS 

Camara, C.; Bouaid, A.; Fernandez, P.; Gonzalez, M. J.; Ramos, L. 

1219 DDT 

On-fiber photodegradation after solid-phase microextraction of p,p '-DDT and 

two of its major photoproducts, p,p '-DDE and p,p '-DDD. 


Llompart, M.; Lores, M.; Lourido, M.; Sanchez-Prado, L.; Cela, R. 

GC-MS 

Determination of organophosphorus insecticide residues by solid-phase 

microextraction coupled with gas chromatography-mass spectrometry. 


1299 insecticide residues. Sepu (2003), 21 (3), 273-276. 

Shuai, Q.; Yang, W.; Zheng, Y. J.; Zheng, C. G. 

PDMS or polyacrylate. GC-MS 

1309 

Solid-phase microextraction coupled with high-performance liquid 

chromatography for the determination of phenylurea herbicides in aqueous 

samples 

Phenylureas herbicides 

in aqueous samples. Journal of Chromatography, A (2003) 1012 (1), 57-66. 

Huang, Shang-Da; Lin, Hsin-Hang; Sung, Yu-Hsiang 

PDMS-DVB, CW-TPR HPLC 

Pesticide vapours in confined atmospheres. Determination of dichlorvos by 

SPME-GC-MS at the mg m-3 level. 

Dichlorvos in 

1316 pesticides. Journal of Environmental Monitoring (2003) 5 (4), 574-577. 

Sanusi, Astrid; Montury, Michel; Ferrari, Federico; Millet, Maurice 

PDMS GC-MS 

2440 Acaricides 

GC-MS determination of acaricides from honey after a new fast 

ultrasonic-based SPME sample treatment 85µm polyacrylate GC-MS 

from honey Talanta 71, #5, 1906-1914 (2007-03-30) 

Rial-Otero, R. ; Gaspar, E. M.; Moura, I.; Capelo, J. L. 

30 min 

1355 Pesticides in honey. 

A solid-phase microextraction-gas chromatography-mass spectrometry 

approach for antivarroa acaricides and pesticide residues in honey. 


Volante, M.; Galarini, R.; Miano, V.; Cattaneo, M.; Pecorelli, I.; Bianchi, M.; 

Marinoni, M. T.; Cossignani, L.; Damiani, P 





Matrix 



Application of solid-phase microextraction for the determination of 

organophosphorus pesticides in aqueous samples by gas chromatography with 

flame photometric detector. 


1364 pesticides Talanta (2001) 55(4), 807-814. 

Yao, Z. W.; Jiang, G. B.*; Liu, J. M.; Cheng, W. 

Various GC-FID 

Focused microwave assistance for extracting some pesticide residues from 

strawberries into water before their determination by SPME/HPLC/DAD. 

Pesticides in 

1369 strawberries. Journal of Agricultural and Food Chemistry (2001) 49(11). 

Falqui-Cao, C.; Wang, Z.; Urruty, L.; Pommier, J. -J.; Montury, M. * 

60µm PDMS/DVB HPLC 


Analysis of acidic pesticides using in situ derivatization with alkylchloroformate 

and solid-phase microextraction ( SPME ) for GC-MS. 

Chemosphere (2001) 44(7), 1531-1539. 

Henriksen, T.; Svensmark, B.; Lindhardt, B.; Juhler, R. K. 

PDMS GC-MS 


Formation of volatile halogenated by-products during chlorination of isoproturon 


Chemosphere (2001) 45(3), 269-274. 

Lopez, A.; Ciannarella, R.; Mascolo, G.; Tiravanti, G. 

85 µm polyacrylate GC-MS 

Factors affecting multiresidue determination of priority herbicides when using 

solid-phase microextraction. 

1439 Herbicides in water Journal of AOAC International (2002) 85(2), 486-493 

1445 

1459 

1483 

Organochlorine pest. 

In water 

Methyl parathion in 

apples 

triazole in wine and 

strawberries 


pesticides in water 

1495 

Pesticides in bee 

products 

Albanis, Triantafyllos A.; Konstantinou, Ioannis K.; Lambropoulou, Dimitra A. 

Determination of organochlorine pesticides in water using microwave assisted 

headspace solid-phase microextraction and gas chromatography 

100µm PDMS and 85µm 

Polyacrylate 

GC-FID, GC-MS 

Journal of Chromatography A (2003) 1012(2), 129-137 Various fibers compared GC-ECD 

Jen, Jen-Fon; Li, Gwo-Chen; Li, Hong-Ping 

Field study for degradation of methyl parathion in apples cultivated with 

integrated crop management system. 

Bulletin of Environmental Contamination and Toxicology (2002) 69(6), 771- 

778 

Tsatsakis, A. M.; Danis, T. G.; Nikitovic, D. P.; Stratis, I. A.; Toutoudaki, M.; 

Tsakiris, I. N. 

Solid-phase microextraction and gas chromatography-mass spectrometry for 

the rapid screening of triazole residues in wine and strawberries. 


Zambonin, C. G.; Cilenti, A.; Palmisano, F. 

Determination of organochlorine pesticides in ground water using solid-phase 

microextraction followed by dual-column gas chromatography with electroncapture 

detection. 

Journal of Chromatography A (2002) 964(1-2), 21-33 30µm PDMS GC-ECD 

Tomkins, Bruce A.; Barnard, Angela R. 

Analytical methods for pesticide residue determination in bee products. 

Journal of Food Protection (2002) 65(9), 1502-1511 

Fernandez, M.; Manes, J.; Pico, Y. 

Identification of dimethylchloroarsine near a former herbicide factory by 

headspace solid-phase microextraction gas chromatography-mass 

spectrometry. 

1505 Dimethylchloroarsine Chemosphere (2002) 48(9), 1003-1008 

Aldstadt, Joseph H., III; Killelea, Daniel R. 


85µm Carboxen PDMS 

Stableflex 

GC-MS

1522 

1531 

1554 

1551 




Chlorinated pesticides 

in water 

Organophosphorus 

pesticides in cherry 

and strawberry juice 

Determination of chlorinated pesticides in water by SPME/GC. 

Water Research (2002) 36(7), 1909-1911 100µm PDMS GC-ECD 

Boussahel, R.; Baudu, M.; Bouland, S.; Montiel, A.; Moussaoui, K. M. 

Headspace solid phase microextraction applied to the analysis of 

organophosphorus insecticides in strawberry and cherry juices. 

Journal of Agricultural and Food Chemistry (2002) 50(12), 3359-3365 Various fibers compared GC-MS 


Evaluation of Solid Phase Microextraction-gas chromatography in the analysis o 

some pesticides with different mass spectrometric techniques: Application to 

environmental waters and food samples. 

Pesticides in water and 

Analytical Letters (2002) 35(2), 327-338 

food 

Benfenati, E.; Natangelo, M.; Tavazzi, S. 

GC-ITMS 

Pesticides in human 

blood 

Headspace solid-phase microextraction in combination with gas 

chromatography and tandem mass spectrometry for the determination of 

organochlorine and organophosphorus pesticides in whole human blood. 

Journal of Chromatography B (2002) 769(1), 65-77 GC-MS 

Hernandez, F.; Beltran, J.; Lopez, F. J.; Pitarch, E. 


Applications of solid-phase microextraction ( SPME ) in the determination of 

residues of certain herbicides at trace levels in environmental samples. 

Journal of Environmental Monitoring (2001) 49(9), 505-508. 

Ramesh, A.; Ravi, P. E. 

65µm Carobwax/DVB GC-ECD 

Determination of tebufenpyrad and oxadiazon by solid-phase microextraction 

and gas chromatography-mass spectrometry. 

Tebufenpyrad and 

1384 oxadiazon. Chromatographia (2001) 54(5-6), 377-382. 

Navalon, A.; Prieto, A.; Araujo, L.; Vilchez, J. L.* 

100µm PDMS GC-MS 

2550 2-aminoaceto- 

Analysis of 2-aminoacetophenone by direct-immersion SPME-GC-MS 

and its sensory impact in Chardonnay and Pinot gris wines. immersion GC-MS 

phenone Food Chemistry 105, #3, 1144-1150 (2007) 

in wine Wenlai Fan; I-Min Tsai; Qian, M. C. 

2815 Phthalates 

Determination of phthalates in wine by headspace SPME followed 

by GC-MS use of deuterated phthalates as internal standards headspace GC-MS 

in wine J Chromatography A 1181, #1-2, 125-130 (FEB 15 2008) 

Carrillo, J. D.; Martinez, M. P.; Tena, M. T. 

2535 Phthalates 

Determination of phthalates in wine by headspace SPME followed by . 

GC-MS. Fibre comparison and selection 65µm PDMS-DVB GC-MS 

in wine J Chromatography A 1164, #1-2, 248-261 (2007) 

Carrillo, J. D.; Salazar, C.; Moreta, C.; Tena, M. T. 

headspace 

2746 guaiacols, phenols 

Determination of Brett character responsible compounds in wines by 

using multiple headspace solid-phase microextraction 65µm CW-DVB GC-MS 

in wine J Chromatography A 1143, #1-2, 176-181 (2007) 

Pizarro, C.; Perez-del-Notario, N.; Gonzalez-Saiz, J. M. 

headspace 

2526 Ethylphenols 

Determination of ethylphenols in wine by in situ derivatisation and 

headspace solid-phase microextraction-GC-MS 50/30 DVB/CAR GC-MS 

in wine Anal Bioanal Chem 387, #7, 2547-2558 (2007) headspace 

Carrillo, J. D.; Tena, M. T. 

Automated analysis of 2-methyl-3-furanthiol and 3-mercaptohexyl . 

70C for 70 min 

acetic anhydride 

2573 Polyfunctional acetate at ng L minus 1 level by headspace SPME with on-fibre . 65µm PDMS-DVB GC-MS 

thiols in wine derivatisation.and GC-negative chemical ionization MS determination headspace 

J. Chromatogr., A 1121, #1, 1-9 (2006-07-14) 5 min 





Mateo-Vivaracho, L.; Ferreira, V. ; Cacho, J. 

Gas phase post derivitization following SPME for rapid analysis of polyphenols 

in wine by GC-MS. 

pentafluorobenzyl 

bromide 

1558 Polyphenols in wine. Zhongshan Daxue Xuebao, Ziran Kexueban 40(1) 54-57. 

Luan, Tian-gang; Li, Gong-ke; Zhang, Zhan-xia. Chinese 

Fast screening determination of some ubiquitous 

2078 Pesticides pesticides with SPME in water samples 85µm polyacrylate GC-MS 

in water Analytical Letters, 37, #7, 1427-1436 immersion sampling 

Moreira Vaz, J.; Komatsu, E. 

Multiresidue method using SPME for the determination 

2079 Pesticides in of various pesticides with different volatility in 100µm PDMS GC-MS 

air confined atmospheres 40min 

Anal and Bioanal Chemistry, 379, #3, 476-483 dynamic air sampling 

Ferrari, F; Sanusi, Ad; Millet, M; Montury, M 

Pesticides analysed in rainwater in Alsace region (Eastern France): 

2855 Pesticides in Comparison between urban and rural sites 100µm PDMS GC-MS/MS 

rainwater Atmospheric Environment 41, #34, 7241-7252 (NOV 2007) 65µm PDMS-DVB 

Scheyer, Anne; Morville, Stephane; Mirabel, Philippe; Millet, Maurice PFBBr derivatives 

Development of an SPME-GC-MS/MS method for the determination 

2241 Pesticides in of pesticides in rainwater: Laboratory and field experiments GC-MS/MS 

rainwater Environ. Pollut. 139 #1, 133-142 (2006) 

Mirabel, Philippe; Sauret-Szczepanski, Nathalie; Wortham, Henri 

Analysis of trace levels of pesticides in rainwater using SPME and 

2223 Pesticides in GC tandem mass spectrometry PDMS GC-MS-MS 

rainwater Anal. Bioanal. Chem. 384, #2, 475-487 (2006) 

Millet, Maurice; Mirabel, Philippe; Morville, Stephane; Scheyer, Anne 

Analysis of trace levels of pesticides in rainwater by SPME and 

2467 Pesticides in GC-tandem mass spectrometry after derivatisation with PFBBr. 65µm PDMS-DVB GC-MS 

rainwater Anal Bioanal Chem 387, #1, 359-68 (2007 Jan) headspace 

Scheyer, A.; Briand, O.; Morville, S.; Mirabel, P.; Millet, M. PFBBr derivative 

60 min at 68°C 

Interactions of chlorpyrifos with colloidal materials 

2080 Chlorpyrifos in aqueous systems GC 

from water J of Environmental Quality, 33., #5, 1765-1770 

Wu, Jigang; Laird, David A. 

SPME-GC-(tandem) MS as a tool for pesticide residue 

2081 Pesticides in analysis in water samples at high sensitivity and 65µm PDMS-DVB GC-MS-MS 

water selectivity w/ confirmation capabilities immersed fiber 

J Chromatogr A, 1026, #1-2, 239-250 

Goncalves, C.; Alpendurada, M. F. 

Transport and fate of dieldrin in poplar and willow 

2082 Dieldrin in trees analyzed by SPME headspace GC 

trees Chemosphere, 61, #1,, 85-91 

Anderson, Larry G.; Ramaswami, Anu; Skaates, S. 

Pesticide residue analysis in waters by SPME 

2083 Pesticides coupled to GC-tandem mass spectrometry. 100µm PDMS GC-MS-MS 

in water Analytical Letters, 37, 1, 99-117 65µm PDMS-DVB 

Arrebola, F. ; Cortes Aguado, S.; Sanchez-Morito, N.; 

Garrido Frenich, A.; Martinez Vidal, J. 

Determination of pesticides and some metabolites in 

2084 Pesticides different kinds of milk by SPME and low-pressure GC-MS-MS headspace/ immersed GC-MS-MS 

in milk Anal. Bioanal. Chem., 381, #1, 164-172 acidified sample 

Frenich, A. Garrido; Gonzalez-Rodriguez, M.J.; Liebanas, F. J. Arrebola; Lopez, 

F. J. Sanchez; Vidal, J. L. Martinez 

Evaluation of SPME conditions for the determination of chlorophenols 

2741 Chlorophenol in honey samples using gas chromatography 100µm PDMS GC-AED 

in honey J Chromatogr A, 1125, #1, 31-37 (2006-08-25) headspace 

Campillo, N.; Penalver, R.; Hernandez-Cordoba, M. 15 min @ 75°C 

acetylation 

Comparison of SPME and stir bar sorptive 

2085 Organo- extraction for determining six organophosphorus 100µm PDMS LC-MS 

phosphorus insecticides in honey by LC-MS 

insecticides J Chromatogr A, 1030, #1-2, 77-85 





in honey Blasco, C.; Fernandez, M.; Pico, Y.; Font, G. 

Application of SPME for the determination of pyrethroid 

2086 Pyrethroid residues in vegetable samples by GC-MS immersion sampling GC/MS 

In vegetables Anal. Bioanal. Chem., 376, #4, 502-511 

Beltran, J.; Hernandez, F.; Lopez, F.J.; Peruga, A.; Pitarch, E. 

Water quality and presence of pesticides in a 

2087 Pesticides in tropical coastal wetland in southern Mexico immersion sampling GC 

water Mar. Pollut. Bull., 48, #11-12, 1130-1141 

Bello-Mendoza, R; Hernandez-Romero, A.; Malo, E.; Tovilla-Hernandez, C 

2348 p,p'-DDT 

Spatial and temporal variations and possible sources of (DDT) and a 

its metabolites in rivers in Tianjin, Chin GC 

in water Chemosphere 68, #1,10-6 (May-2007) 

Tao, S; Li, B G; He, X C; Liu, W X; Shi, Z 

Determination of dichlorodiphenyltrichloroethane in 

2088 p,p'-DDT water using automated SPME-GC-ECD 100µm PDMS GC-ECD 

in water Fenxi Huaxue, 32, #4, 500-502 immersion sampling 

Luan, T. G.; Lan, C. Y.; Zhou, H. L.; Wong, M. H. 

Evaluation of an SPME and GC-MS method for 

2089 Fluazifop analysis of fluazifop in water. 100µm PDMS GC-MS 

in water Acta Chromatographica, 14, #1, 231-236 stirring 

Olszewska, E. 

Cost analysis of ELISA, solid-phase extraction, and 

2090 Pesticides SPME for the monitoring of pesticides in water comparison of cost GC 

in water Environmental Research, 98, #1, 143-150 

Dalvie, M.; Sinanovic, E.; London, L; Cairncross, E; 

Solomon, A.; Adam, H. 

Advanced method using microwaves and SPME 

2091 Prethroid coupled w/GC-MS for the determination of pyrethroid 100µm PDMS GC-MS 

residue on residues in strawberries 30min immersed 

strawberries J. Chromatogr. A, 1046, #1-2, 35-40 water/acetornitrile 

Guillet, Valerie; Montury, Michel; Sanusi, Astrid preextraction 

Analysis of pesticide residues in juice and beverages "review" 

2092 Pesticides in Crit. Rev. Anal. Chem., 34, #2, 121-131 Review article GC-MS 

beverages Albero, B; Gonzalez, L; Sanchez-Brunete, C; Tadeo, J. 

Combining SPME and on-line preconcentration-capillary 

2093 Pesticides electrophoresis sensitive analysis of pesticides in foods CE-UV 

in water Electrophoresis, 26, #4-5, 980-989 

Hernandez-Borges, J.; Cifuentes, A.; 

Garcia-Montelongo, F.; Rodriguez-Delgado, M. 

Highly sensitive analysis of multiple pesticides in foods 

2094 Pesticides in combining SPME, capillary electrophoresis-MS & chemometrics NH 2HCO 3 buffer CE-MS 

food Electrophoresis, 25, #13, 2065-2076 pH 4 CE-UV 

Hernandez-Borges, Javier; Rodriguez-Delgado, M.; 

Garcia-Montelongo, Francisco J.; Cifuentes,A. 

Application of SPME to the study of the photochemical 

2095 Pesticides behaviour of five priority pesticides: "On-fiber" 100µm PDMS GC-MS 

in water and aqueous photodegradation 30min extract 

J. Chromatogr. A, 1047, #2, 271-279 immersion sampling 

Sanchez-Prado, Lucia; Llompart, Maria; Lores, Marta; 

Garcia-Jares, Carmen; Cela, Rafael 

Applicability of headspaceSPME to the determination 

2096 Pesticides in of multi-class pesticides in waters. 30µm polyacrylate GC-MS 

water J Chromatogr A, 1028, #1, 63-74 30° to 100°C 

Sakamoto, Mitsushi; Tsutsumi, Taizou headspace 

Soil 

Application of SPME and GC with Electron-Capture and Mass 

36 HexachlorocyclohexaneMass Spectrometric Detection for the Determination of 100µm PDMS GC-ECD, 

in soil Hexachlorocyclohexanes in Soil Solutions 20-30 min GC-MS 

J. Chromatogr. 687: 133-140 (1994) immersion 





Popp, P., Kalbitz, K., Opperman, G. stirring 

74 Diesel fuel 

Solid Phase Microextraction-GC for Analysis of Diesel Fuel 

Residues in Soil 100µm PDMS GC-FID 

in soil Request from Dept. Soil Science, University of Manitoba 55°C, 30 min 

Winnipeg, MB, Canada R3T 2N2. 

Graham, K., Webster, B., Sarna, L. 

headspace 

716 THF, methanol 

Analysis of THF and methanol in distillation residue 

samples by automated headspace SPME-GC with FID 65µm PDMS/DVB GC-FID 

in distillate J Chromatogr. Sci. (2000), 38(3), 117-121 9min. 

Gavlick, W. headspace 

870 PAHs in 

The use of SPME and GC-MS for the chemical characterization 

and assessment of PAH pollution in aqueous 

environmental environmental samples 

samples Int. J. Environ. Anal. Chem (2000) 78(3-4) 205-221 

Havenga, Willem J.; Rohwer, Egmont R 

717 PAHs 

Solid Phase Microextraction of PAHs from soil 

Chem. Ana., 2000 (45 No.6) 835-842 

in soil Sedukiene, I., Vickackaite, V., Kazlauskas, R. 

567 PAHs 

Chemical characterization and screening of hydrocarbon 

pollution in industrial soils by headspace SPME 100µm PDMS GC-MS 

in soil J-Chromatogr,-A. 2 Jul 1999; 848(1-2): 279-295 40 min 

Havenga,-WJ; Rohwer,-ER headspace 

865 PAHs 

Solid phase microextraction of PAHs from soil 

Chemia Analityczna (Warsaw) (2000) 45(6) 835-842 

in soil Seduikiene, I.; Vickackaite, V.; Kazlauskas, R. 

Extraction of Pesticides by Solid Phase Microextraction 

30min @ 60°C 

heaspace 

75 Pesticides (from Soil) 100µm PDMS GC-ECD, -NPD 

in soil Request from: Dept. Environmental Assessment, Swedish immersed, 

University of Agricultural Sciences, PO Box 7050, 

Uppsala, Sweden 

Bengsson, S., Berglof, T. 

water solution 

Distribution coefficients of aliphatic alcohols, carbonyl compounds 

2336 Alcohols, esters, and esters between air and Carboxen/PDMS fiber coating Carboxen/PDMS GC/MS 

carbonyls in air Anal. Chim. Acta. 560 #1-2, 103-109 (2006) air sample 

Isidorov, V.; Modzelewska, A.; Purzynska, A.; Serowiecka, M. 15-30°C 

2149 Amides in Air 

Analysis of amides in the air by sampling with SPME and detection 

by GC-FID passive air sampling GC-FID 

J. Sep. Sci., 29, #3, 346-350 (2006) 65µm PDMS-DVB 

de Lourdes Cardeal, Z.; de Souza Bergo, P.; Parreira, F.; 

Rabelo de Carvalho, C. 

90min @25°C 

2718 Triazine 

On-fibre SPME coupled to conventional HPKC versus in-tube 

SPME coupled to capillary LC screening analysis of triazines 65µm PDMS-DVB LC 

in water in water samples. 

J. Chromatogr., A 1125, #2, 159-171 (2006-09-01) 

Chafer-Pericas, C.; Herraez-Hernandez, R.; Campins-Falco, P. 

855 Triazine, amides 

Determination of triazines and amides in water using 

solid-phase microextraction coupled with GC-MS. GC-MS 

in water Chromatographia (2001) 53(5-6), 306-310 

Hu, R.; Elia, D.; Berthion, J. -M.; Poliak, S. 

529 Triazines, 

Determination of polar pesticides in soil by SPME couple to 

HPLC-MS 85µm polyacrylate HPLC-MS 

carbamates Fresenius'J. Anal. Chem. (1999), 363(7), 680-685 salt added 

in soil leachates Moder, M., Popp, P., Eisert, R., Pawliszyn, J. 





Determination of triazines in soil leachates by SPME 


718 Triazines, coupled to GC-MS 85µm polyacrylate GC-MS 

in soil leachates J. Chromatogr. A 2000, 874(2), 247-255 30min @ 20°C 

Zambonin, C.., Palmisano, F. aggitation 


Determination of organophosphorus pesticides in soil 

by headspace SPME 85µm polyacrylate GC-FID 

pesticides in Fresenius'J. Anal. Chem (1999), 363(7), 673-679 1 hr @ 80°C 

soil Ng, W., Teo, M., Lakso, H. headspace over soil 

76 Lindane 

Analysis of Lindane in Water and Soil by Solid Phase 

Microextraction 30µm & 100µm PDMS GC-ECD 

in water and soil Request from: Dept. Soil Science, University of Manitoba, 58°C 

Winnipeg MB, Canada R3T 2N2. 40 min (headspace) 

Anderson, K., Sarna, L., Webster, B. 15-20 min (immersion) 

A novel headspace SPME method for the exact determination 

2170 Organochlorine of organochlorine pesticides in environmental soil samples GC-ECD 

pesticides in Anal. Bioanal. Chem. 384, #7-8, 1584-1589 (2006) 

soil Fu, Shan; Jiang, Ting; Wang, Xia; Xu, Xiaobai; Yuan, Jinpeng; Zhao, R. 


Determination of organochlorine pesticides and their 

metabolities in soil samples using headspace SPME 100µm PDMS, GC-ECD 

pesticides in J.Chromatogr. A (2001) 918(1), 177-188 65µm DVB/PDMS 

soil Doong, R., Liao, P. 60min@70°C 

heahspace 

stirred 

881 Fipronil in 

Determination of fipronil by SPME and GC-MS 

J chromatogr. A 919(2001) 215-221 85µm polyacrylate GC-MS 

water, soil, urine Vilchez, J., Prieto, A., Araujo, L., Navalon, A. 

Determination of metolachlor volatile flux from 

30min. @ 60°C 

stirred 

9.5 pH 

857 Metochlor soil using SPME 

from soil Prepr. Ext. Abstr. ACS (2001) 41(1) 307-311 

McConnell, L.; Kim, H; Nochetto, C; Gish, T; Prueger, J 

833 Halobenzenes 

Gas chromatography/ion-trap tandem mass spectrometry 

for the analysis of halobenzenes in soils by SPME 100µm PDMS GC-MS 

in soil and water Rapid Commun Mass Spectrometry (2000) 14(23) 2271-2281 

Sarrion, M. N.; Santos, F. J.; Galceran, M. T. 

45min 

92 Chlorobenzenes 

Analysis of Chlorobenzenes in Soils by Headspace SPME 

and GC-Ion Trap MS 100µm PDMS GC-Ion Trap 

in soil and water J. Chromatogr. A 771: 181-189 (1997) 

Santos, F., Sarrion, M., Galceran, M. 

headspace MS 

921 Chlorobenzenes 

Strategies for the analysis of chlorobenzenes in soils using 

SPME coupled with GC-ion trap mass spectrometry GC-Ion Trap 

in soil J. Chromatogr. A (1998), 819(1-2), 197-209 

Sarrión, M., Santos, F., Galceran, M. 

MS 

238 Chlorobenzenes, 

Analysis of Chloro- and Nitroanilines and Benzenes in Soil 

by Headspace Solid-Phase Microextraction 85µm polyacrylate GC-ECD 

nitrobenzenes, J. Chromatogr. A 746: 71-81 (1996) headspace 

anilines in soil, water Fromberg, A., Nilsson, T., Larsen, R., Montanarella, L., 

Facchetti, S., Madsen, J. 

50°C, 30 min 


Coupled Subcritical Water Extraction with SPME for 

Determining Semivolatile Organics in Environmental Solids 100µm PDMS GC-MS 

in solids Anal. Chem. 68: 3892-3898 (1996) 15 min 

Hageman, K., Mazeas, L., Grabanski, C., Miller, D., Hawthorne, S. immersion 

793 Phenols 

Fast determination of phenols in contaminated soils 

J. Chromatogr., A (2001) 911(1), 135-141 85µm polyacrylate GC-FID 





in soil Baciocchi, R.; Attina, M.; Lombardi, G.; Boni, M. R 

Determination of chlorophenols in soil using accelerated 

60min. @ 20°C 

immersion, pH 1 

719 Chlorophenols solvent extraction combined with SPME 85µm polyacrylate GC-MS 

in soil Anal. Chem. (2000), 72(3), 46-551 20min. @ 20°C 

Wennrich, L, Popp, P., Moeder, M. 

Headspace SPME for the determination of volatile and 

immersion, pH 2 

satr NaCl 

531 Volatiles and semivolatile pollutants in soils 100µm PDMS GC-MSD 

semivolatiles Talanta (1999), 48(2), 451-459 30 min @ 20°C 

in soils/water Llompart, M., Li, K., Fingas, M. headspace 

532 PAHs, hydrocarbons 

Investigation by SPME and GC-MS of organic films on 

stone monuments GC-MS 

in pollutant crust Rapid. Commun. Mass Spectrom. (1999), 13(10), 895-900 

Angelis, F., Di Tullio, A., Mellerio, G., Quaresima, R, Volpe, R 

533 Aldehydes, acids 

Degradation of palmitic (Hexadecanoic) acid deposited on 

TiO2 coated self cleaning glass: kinetics of disappearance, 

from palmitic acid intermediate products and degradation pathways 

New J. Chem (1999), 23(4), 365-374 

Romeas, V., Pichat, P., Guillard, C., Chopin, T., Lehaut, C. 

534 PAHs in 

Interaction between natural organic matter (NOM) and 

polycyclic aromatic compounds, Comparison of 85µm polyacrylate GC-MS 

organic matter fluorescence quenching and SPME 30 min 

Fresenius'J. Anal. Chem. (1999), 364(4), 313-319 pH3, immersed 

Myung, S., Kim, M., Min, H., Yoo, E. Kim, K. alkyl formate derivative 

172 Elemental analysis 

Elemental and Organometallic Analysis of Soil Using 

Glow-Discharge MS and GC-MS 100µm PDMS GC-MS 

of soil Rapid Commun. Mass Spectrom. 10: 341-346 (1996) 50°C, 10 min 

Barshick, C., Barshick, S., Mohill, M., Britt, P., Smith, D. salt added 

174 Mercury species in 

Performance Improvements in the Determination of Mercury 

Species in Natural Gas Condensate Using Online GC-ICP 

natural gas condensate Amalgamation Trap or SPME with Capillary GC-Microwave- 

Induced Plasma Atomic Emission Spectrometry 

Analyst 121: 1055-1060 (1996) 

Snell, J., Frech, W., Thomassen, Y. 

535 Organomercury 

SPME and GC-MIP-AED for the speciation analysis of 

organomercury compounds GC-MIP-AED 

in soil and water J. High Resolut. Chromatogr. (1999), 22(3), 181-182 

Mothes, S., Wennrich, R. 

Headspace solid-phase microextraction (HS-SPME) for the 

2314 BTEX in determination of BTEX in foundry molding sand 75µm Carboxen GC/MS 

sand Analytical Letters 38 #14, 2393-2405 (2005) headspace 

Dungan, Robert S. 

239 BTEX, chlorinated 

The Determination of Volatile Organic Compounds in Soils 

Using SPME with Gas Chromatography-Mass Spectrometry 100µm PDMS GC-MS 

hydrocarbons J. High Res. Chromatogr. 19: 515-519 (1996) 5 min 

in soil James, K., Stack, M. headspace 

197 VOCs in 

Environmental Analysis of Volatile Organic Compounds in 

Water and Sediment by GC overview 

water and sediment J.Chromatogr. A 733A 733: 119-141 (1996) (review) 

Kuran, P., Sojak, L. 

article 

536 VOCs in 

Determination of VOC contamination in borehole sediments 

by headspace SPME-GC analysis 

sediment Fresenius' J. Anal. Chem 1999, 364(7), 645-647 water solution 

Dermietzel, Jurgen, Strenge, G. headspace 





768 Tributyltin 

Determination of tributyltin by automated in-tube 

SPME with HPLC-ES-MS In-tube SPME LC-ES-MS 

in water J Anal At Spectrom (2001) 16(2), 159-165 

Wu, J; Mester, Z; Pawliszyn, J. 

Supel-Q PLOT 

720 Butyltin 

Determination of butyltin compounds in aqueous 

samples by GC w/FPD and headspace SPME after GC-FID 

in water in-situ hydride derivatization 

Aanl. Sci. 2000, 16(6), 585-588 

Jiang, G, Liu, J. 

Determination of butyltin compounds in sediments 

NaBEt4 

Japanese 

771 Butyltin by headspace SPME and capillary GC w/FPD using quartz GC-FPD 

in sediment surface induced luninescence 

Fenxi Huaxue (20001) 29(2), 158-160 

Liu, J; Jiang, G. KBH-4 

in Chinese 

721 Butyltin 

Determination of butyltin species in water and 

sediment by SPME-GC-FID GC-FID 

in water J.Chromatogr. A (2000), 873(1), 61-71 

Millan, E., Pawliszyn, J. NaBEt4 

Solid phase microextraction as a tool for trace 

888 element speciation 

Spectrochim. Acta, Part B (2001) 56B(3), 233-260 

Mester, Z.; Sturgeon, R.; Pawliszyn, J. 

852 Butyltin 

Speciation of butyltin compounds in marine sediments with 

headspace SPME and gas chromatography: MS 100µm PDMS GC-MS 

in marine sediment Fresenius' J. Anal. Chem 2001, 369(6), 510-515 

Cardellicchio, N.; Decataldo, A.; Di Leo, A.; Giandomenico, S. headspace 

NaBEt4 derivative 

722 Butyl-, phenyltin 

SPME: a new procedure for the control of butyland 

phenyltin pollution in the environment by GC-FID 100µm PDMS GC-FID 

in water Analyst (Cambridge, UK) 2000, 125(2), 263-268 60 min, immersed 

Aguerre, S., Montigny, C, Lespes, G., Gaultier, M. NaBEt4 

199 Organotin 

in humic organic 

Solid Phase Microextraction to Study the Sorption of 

Organotin Compounds onto Particulate and Dissolved 100µm PDMS GC-MS 

matter Humic Organic Matter 30 min 

Environ. Sci. Technol. 31: 3629-3636 (1997) 

Poerschmann, J., Kopinke, F., Pawliszyn, J. 

immersion 


Development of a Technique for the Analysis of Inorganic 

Mercury salts in Soils by GC-MS 100µm PDMS, GC-MS 

derivative Intl. J. Mass Spectrometry 178 (1998) 31-41 65µm PDMS/DVB 

in soil Barshick, C., Barshick, S., Britt, P., Lake, D., Vance, M., 50°C, 5 min 

Walsch, E. 

Determination of methylmercury by SPME-ICP-MS: a new 


methyl bis(dimethylgloximate) 

pyridinecobalt 

(III) 

723 Methylmercury sample introduction method for volatile metal species ICP-MS 

derivative J. Anal. AT. Spectrom (2000) 15(7), 837-842 

in soil Mester, Z., Lam, J., Sturgeon, R, Pawliszyn, J. 

Applications of Sorbent Extraction in Environmental Analysis 

209 Chem. Anal. (Warsaw) 42 (3): 297-314 (1997) 

Gorlo, D., Namiesnik, J., Zygmunt, B. 

Coupled Subcritical Water Extraction with SPME for 


303 



Matrix 

PAHs, amines, 


aromatic Determining Semivolatile Organics in Environmental Solids 100µm PDMS GC-ECD 

from soil & particulate Anal. Chem. (1996) 68, 3892-3898 15 min 

Hageman, K., Mazeas, L., Grabanski, C, Miller, D., 

Hawthorne, S. 

immersion 

884 Phenyl compounds 

Determination of phenyl compounds in drinking water by 

solid phase microextraction coupled with capillary GC/MS 

in water Huanjing Huaxue (2001) 20(2) 191-195 

2572 PCBs 

Rapid screening of polychlorinated biphenyls in sediments using 

non-equilibrium SPME and fast gas chromatography with ECD 100µm PDMS GC-ECD 

in sediment J. Chromatogr., A 1124, #1-2, 43-50 (2006-08-18) 10 min @ 100°C 

Montes, R.; Ramil, M.; Rodriguez, I. ; Rubi, E.; Cela, R. headspace 

920 PCBs 

Simple method for estimating PCH concentratons on soils 

and sediments using subcritical water extraction coupled 

in soil with SPME 

J. Chromatogr. A (1998), 814(1-2) 151-160 

Hawthorne, S., Grabanski, C., Hageman, K. Miller, D. 

304 PCBs 

Solid-Phase Microextraction of Polychlorinated Biphenyls 

J. Chromatogr. A 800 (2): 257-266 (1998) 100µm PDMS GC-ECD 

in soil Yang, Y., Miller, D., Hawthorne, S. 

Adsorption versus Absorption of PCBs onto SPME Coatings 

15 min 

immersion 

370 PCBs Anal. Chem. 1998, Vol. 70, 1866-1869 7µm PDMS GC-ECD 

in soil Yang, Y., Hawthorne, S., Miller, D. 

Headspace SPME for the determination of PCBs in soils 

5 hr 

immersion 


537 PCBs in and sediments 100µm PDMS GC-MS 

soil & sediment J. Microcolumn Sep. (1999), 11(6), 307-402 30 min @ 100°C 

water slurry Llompart, M., Li, K., Fingas, M. headspace 

724 PAHs 

Determination of PAHs in sediment using SPME w/GC-MS 

J. Chromatogr. Sci. (2000), 38(2), 55-60 100µm PDMS GC-MS 

in sediment Cam, D., Gagni, S., Meldolesi, L., Galletti, G. 

538 Bisphenol A 

An attempt by SPME with on-column silylation for a rapid 

and highly sensitive determination of bisphenol A GC-MS 

in water Bunseki Kagaku (1999) 48(6), 589-593 BSTFA derivative 

Takao, Y. Lee, H., Arizono, K. Japanese 

305 Organics 

SPME of Semivolatile Organic Compounds from 

Odoriferous Samples 

from odoriferous Hazard. Ind. Wastes (28th) 734-738 (1996) 

samples Wojtowicz, C., Clifton, A., Willy, D. 

Assessment of tin and butyltin species in estuarine superficial sediments from 

Gipuzkoa, Spain 

Tin and butyltin in 

1014 sediment Chemosphere (2003) 51 (8), 643-649. 

Arambarri, I.; Garcia, R.; Millan, E. 

PDMS GC-FID 

Determination of methylmercury and butyltin compounds in marine biota and 

sediments using microwave-assisted acid extraction, solid-phase 

microextraction, and gas chromatography with microwave-induced plasma 

atomic emission spectrometric detection. 

Methylmercury and 

1028 butyltin in sediments Analytical Chemistry (2002) 74 (18), 4694-4701. 

Tutschku, S.; Schantz, M. M.; Wise, S. A.* 

GC-MIP-AES 

Application of headspace solid-phase microextraction and gas chromatographymass 

spectrometry for detection of the chemical warfare agent bis(2-chloroethyl) 

sulfide in soil. 




Matrix 

Bis(2-chloroethyl) 


1040 sulfide in soil. Journal of Chromatography, A (2002) 971 (1-2), 185-191. 

Kimm, G. L.; Hook, G. L.; Smith, P. A.* 


Direct determination of chlorophenols in landfill leachates by solid-phase microextraction-gas 


Chlorophenols in 

1068 landfill leachates Journal of Chromatography, A (2002) 975 (2), 267-274. 

Ribeiro, A.; Neves, M. H.; Almeida, M. F.; Alves, A.; Santos, L. * 

GC-MS 

1108 

Determination of musk compounds in sewage treatment plant sludge samples 

by solid-phase microextraction 

Musk compounds in 

sludge. Journal of Chromatography A (2003) 999 (1-2), 185-193. Various GC-MS 

Cela, Rafael; Garcia-Jares, Carmen; Llompart, Maria; Polo, Maria; Salgado, 

Carmen 

1193 VX in soil 

Detection of VX contamination in soil through solid-phase microextraction 

sampling and gas chromatography/mass spectrometry of the VX degradation 

product bis(diisopropylaminoethyl)disulfide. 


Smith, Philip A.; Ding, Bangwei; Hook, Gary L.; Kimm, Gregory; Koch, David; 

Savage, Paul B. 

PDMS GC-MS 

1220 Triazines in soil. 

Determination of triazines in soil by microwave-assisted extraction followed by 

solid-phase microextraction and gas chromatography-mass spectrometry. 


Shen, G.; Lee, H. K.* 

GC-MS 

2713 PAHs in sediment 

New cold-fiber headspace Spme device for quantitative extraction of 

polycyclic aromatic hydrocarbons in sediment. 

Journal of Chromatography, A 1124, #1-2, 35-42 

Ghiasvand, A. R.; Hosseinzadeh, S.; Pawliszyn, J. 


1240 PAHs in sediment 

Micellar microwave-assisted extraction combined with solid-phase 

microextraction for the determination of polycyclic aromatic hydrocarbons in a 

certified marine sediment. 

Analytica Chimica Acta (2003) 477 (1), 81-91. 

Pino, V.; Ayala, J. H.; Afonso, A. M.; Gonzalez, V. * 

PDMS, polyacrylate. GC-MS 

Detection of O -ethyl- S -(2-diisopropylaminoethyl) methylphosphonothiolare 

(VX) contamination in soil through solid-phase microextraction sampling and 

gas chromatography/mass spectrometry of the VX degradation product 

bis(diisopropylaminoethyl)disulfide. 

1255 VX nerve agent in soil. Journal of Chromatography, A (2003) 992 (1-2), 1-9. GC-MS 

Hook, G. L.; Kimm, G.; Koch, D.; Savage, P. B.; Ding, B. W.; Smith, P. A.* 

1297 Isocarbophos in soil. 

Determination of isocarbophos in soil samples by gas chromatography-mass 

spectrometry with combination of microwave-assisted extraction and solidphased 



Yang, Y.; Li, G. K.* 

GC-MS 

1320 

Determination of antifouling compounds in marine sediments by solid-phase 

microextraction coupled to gas chromatography-mass spectrometry. 



GC-MS 

Determination of petroleum hydrocarbons in contaminated soils using solidphase 

microextraction with gas chromatography-mass spectrometry. 

Petroleum 

1363 hydrocarbons in soil Journal of Chromatographic Science (2001) 39(11), 481-486. 

Cam, D.; Gagni, S. 






1385 n-alkanes in soil. 

A new PVC-activated charcoal fibre coated on silver wire: application in 

determination of n-alkanes in the headspace of soil samples by SPME-GC. 

Analytical Sciences (2002) 18(1), 77-81. 

Farajzadeh, M.; Matin, A. A. 

Activated charcoal/PVC GC 

1394 Hydrocarbons in soil. 

Determination of hydrocarbons in old creosote contaminated soil using 

headspace solid-phase microextraction and GC-MS. 

Chemosphere (2001) 44(7), 1641-1648. 

Eriksson, M.; Faeldt, J.; Dalhammar, G.; Borg-Karlson, A. -K. 


Headspace solid-phase microextraction of butyltin species in sediments and 

their gas chromatographic determination. 

Butyltin species in 

1411 sediment. Journal of Separation Science (2001) 24(6), 459-464. 

Gui-bin, Jiang; Ji-yan, Liu; Ke-wu, Yang; Qun-fang, Zhou 

100 µm PDMS 

Determination of chlorophenols in soil samples by microwave-assisted 

extraction coupled to headspace solid-phase microextraction and gas 

chromatography - Electron-capture detection 

1446 Chlorophenols in soil Journal of Chromatography A (2003) 1012(2), 111-118 


pesticides in soil 

1462 

Tributyltin in water and 

soil 

Jen, Jen-Fon; Wei, Ming-Chi 

Solid-phase microextraction coupled to gas chromatography- mass 

spectrometry for the study of soil adsorption coefficients of organophosphorus 

pesticides 

85µm Polyacrylate, 1g 

soil in 6mL water, pH 2, 

9mins. Headspace 

GC-ECD 

Journal of Environmental Monitoring (2002) 4(4), 477-481 GC-MS 

Zambonin, C. G.; Palmisano, F.; Losito, I.; Cilenti, A. 

Gas phase detection of tributyltin chloride arising from aqueous and solid 

matrices. 

Journal of Analytical Atomic Spectrometry (2002) 17(11), 1506-1510 GC-MS 

Bancon-Montigny, Chrystelle; Lam, Joseph W.; Maxwell, Paulette; Mester, 

Zoltan; Sturgeon, Ralph E.; Yang, Lu 

1464 Aromatic acids in soil 

Separation and identification of aromatic acids in soil and the Everglades 

sediment samples using solid-phase microextraction followed by capillary zone 

electrophoresis. 


Deng, Yiwei; Fan, Xiaofang 

85µm Polyacrylate CZE 

1486 Monoaromatic 

hydrocarbons in soil 

Solid-phase microextraction-gas chromatographic determination of volatile 

monoaromatic hydrocarbons in soil. 

Fresenius' Journal of Analytical Chemistry (2002) 370(8), 1096-1099 100µm PDMS GC-MS 

Zygmunt, Bogdan; Namiesnik, Jacek 

Improvement in measurement precision with SPME by use of isotope dilution 

mass spectrometry and its application to the determination of tributyltin in 

sediment using SPME GC-ICP-MS. 

1490 Tributyltin in sediment Journal of Analytical Atomic Spectrometry (2002) 17(8), 944-949 

Yang, Lu; Mester, Zoltan; Sturgeon, Ralph E. 

100µm PDMS, sodium 

tetraethylborate 

derivative 

Trace element speciation using solid phase microextraction 

2243 Organometallic Spectrochimica Acta Part B: 60 #9-10, 1243-1269 (2005) Review article 

in water Mester, Zoltan; Sturgeon, Ralph 

Gas phase sampling of volatile (organo)metallic compounds above solid 

samples. 

GC-IDMS 

1491 Organometallics in soil Journal of Analytical Atomic Spectrometry (2002) 17(8), 868-871 ICP-MS 

Mester, Zoltan 

Determination of tributyltin compounds in surface sediments of harbour by gas 

chromatography with headspace solid-phase microextraction 





1150 Tributyltin in sediment Fenxi Ceshi Xuebao (2003) 22 (2), 28-30. 

Lei, Z.; Huang, C. J.; Jia, L.; Shi, H. H. 

GC-FPD 

Removal of two polycyclic musks in sewage treatment plants: freely dissolved 

and total concentrations. 

Polycyclic musks in 

1326 sewage. Environmental Science and Technology (2003) 37 (14), 3111-3116. 

Artola-Garicano, E.; Borkent, I.; Hermens, J. L. M.; Vaes, W. H. J. 

GC-MS 

SPME as a tool to predict internal concentrations 

2097 Chloro- of soil contaminants in terrestrial organisms after 30µm PDMS GC 

benzenes exposure to a laboratory standard soil 1 day sample 

in soil Chemosphere, 54, #4, 561-568 headspace 

van der Wal, L.; van Gestel, C.; Hermens, J. 

Applicability of SPME combined with GC-MIP AED for the 

2098 Butyltin in determination of butyltin compounds in sediment samples. ethylated derivative GC-MIP AED. 

sediment Analytical and Bioanalytical Chemistry, 380, #5-6, 853-857 headspace 

Carpinteiro, J.; Rodriguez, I. *; Cela, R. sonication 

Surface geochemical results complement 

2099 Hydrocarbons conventional development approaches headspace GC 

in soil World Oil, 225, #12, 54-65 

Quinlan, W.; Wood, James; Wylie, Albert 

Plant-assisted degradation of phenanthrene as 

2100 Phenanthrene assessed by solid-phase microextraction (SPME) headspace GC-FID 

in soil Intl J of Phytoremediation, 6, #3, 253-268 

Hynes, Russell K.; Farrell, Richard E.; Germida, James J. 

Determination of prometryn in soil by GC-MS using 

2101 Prometryn microwave-assisted extraction associated with SPME microwave heated GC-MS 

in soil Fenxi Huaxue, 32, #6, 775-778 

Yang, Y.; Luan, W.; Luo, X. J.; Li, G. K.* 

Soil volatile fungistasis and volatile fungistatic compounds 

2102 Fungistasis Soil Biol. Biochem.,36, #12, 1997-2004 Headspace GC-MS 

in soil Chuankun, Xu; Keqin, Zhang; Leming, Zhang; Minghe, Mo 

Determination of benzene, toluene, ethylbenzene 

2103 BTEX and xylenes in soils by multiple headspace SPME 75µm Carboxen GC-FID 

in soil J. Chromatogr. A, 1035, #1, 17-22 30min @ 30°C 

Ezquerro, O; Ortiz, G; Pons, B; Tena, M headspace over soil 

suspended in water 

Determination of the fungicides vinclozolin and 

2104 Fungicides in dicloran in soils using ultrasonic extraction coupled 85µm polyacrylate GC-MS 

soil with SPME 5% acetone/water 

Anal. Chim. Acta, 514, #1, 125-130 


Determination of pyrimethanil and kresoxim-methyl 

2105 Fungicides in in soils by headspace SPME and GC-MS 85µm polyacrylate GC-MS, SIM 

in soil Anal. Bioanal. Chem., 379, #7-8, 1100-1105 headspace 

Araujo, L; Navalon, A; Prieto, A; Vilchez, J 

The moss Physcomitrella patens releases a 

2106 Tetracyclic tetracyclic diterpene headspace GC-MS 

diterpene Plant Cell Rep., 22, #10, 780-786 

from moss Kassner, H.; Schultze, W.; VonSchwartzenberg, K. 

Static headspace versus head space SPME for the 

2107 Chlorinated for the determination of volatile organochlorine headspace GC-MS 

solvents in compounds in landfill leachates by GC 

Talanta, 63, #4, 809-814 

Fernandez Martinez, E.; Fernandez Sanchez, M.; 

Florez Menendez, J.; Sanchez Uria, J.;Sanz-Medel, A. 

Optimization of microwave-assisted extraction 

2108 Organics followed by SPME-GC-MS detection for the assay GC-MS 

in sebum of some semi-volatile organic 

J. Chromatogr.B, 825, #1, 11-20 

Diaz-Vazquez, Liz; Garcia, Oscar; Marrero, I.; 

Rosario, Osvaldo; Velazquez, Zorangelys 





Sediment dilution method to determine sorption 

2109 Organic coefficients of hydrophobic organic chemicals Immersed extract from GC 

chemicals in Environ. Sci. Technol., 39. #11, 4220-4225 sediment in water 

sediment Busser, F; Hermens, J.; Klamer, H.; Mayer, P; Ter Laak, T 

2698 Dioxin congeners 

Microbial dehalogenation of trichlorinated dibenzo-p-dioxins by a 

Dehalococcoides-containing mixed culture is coupled to headspace GC-MS 

from cultures carbon isotope fractionation 

Environ. Sci. Technol.41, #22, 7744-7751 (15 NOV 2007) 

Ewald, E. -M.; Wagner, A.; Nijenhuis, I.; Richnow, H. -H.; Lechner, U. 

Simple device for the SPME screening of 

2110 PCDDs/PCDF polychlorodibenzo-p-dioxins and polychlorodibenzo- 100µm PDMS GC-MS 

in soil furans in heavily contaminated soil samples. headspace 

Analytica Chimica Acta, 527, #2, 157-162 sonicated 

Chia, K. J.; Lee, T. Y.; Huang, S. D.* 

Air 

725 Organic vapors 

Application of SPME for determination of organic vapors in 

gaseous matrices review article 

in gaseous matrices J. Chromatogr. A, 885(2000) 405-418 

Namiesnik, J., Zygmunt, B., Jastrzebska, A. 

846 Solvent vapors 

Solvent vapour monitoring in work space by SPME 

J Hazardous Materials (2001) 83(1-2), 83-91 100µm PDMS 

in air Li, K.; Fingas, M.; Goldthorp, M.; Lambert, P.; 

Santilli, A.; Whiticar, S. 

75µm Carboxen/PDMS 

Diffusive sampling of methylene chloride with SPME 

2563 Methylene chloride J. Chromatogr., A 1137, #2, 138-144 (2006-12-29) 85µm Carboxen/PDMS GC-ECD 

in air Chen, C. Y.; Hsiech, C. M.; Lin, J. M. diffuse sampling 


Characterization of sorption mechanisms of SPME with volatile organic 

compounds in air samples using a linear solvation energy relationship 

approach 100µm PDMS GC 

in air J. Chromatogr. A 1179, #1, 24-32 (25 JAN 2008) 

Prikryl, P.; Sevcik, J. 

85µm polyacrylate 

726 Volatiles 

Airflow Rate in the Quantitation of Volatiles in Air Streams 

by Solid Phase Microextraction 100µm PDMS GC-FID 

in air Anal. Chem 2000, 72, 3949-3955 

Bartelt, R., Zilkowski, B. 

30 min 


Sorbent trapping of volatile organic compounds from air 

J. Chromatogr. A, 885 (2000) 120-151 75µm Carboxen/PDMS GC-FID 

in air Harper, M. review article 


Air sampling with porous SPME fibers compounds 

Anal. Chem. 2000, 72, 5178-5186 75µm Carboxen/PDMS GC-FID 

in air Koziel, J., Jia, M., Pawliszyn, J. 

Air sampling and Analysis of Volatile Organic compounds 

65µm DVB/PDMS 

5-10 sec air sampling 

754 Volatile organic with Solid Phase Microextraction 100um PDMS GC-FID 

in air J. Air & wasteManage. Assoc 51: 173-184 

Koziel, J., Pawliszyn, J. 

55 BTEX 

Analysis of Environmental Air Samples by Solid Phase 

microextraction and GC/Ion Trap Mass Spectrometry 100µm PDMS GC-MS 

in air Environ. Sci. Technol. 29: 693-701 (1995) 3 min 

Chai, M., Pawliszyn, J. gas sampling 

226 Petroleum 

Estimation of Air-Coating Distribution Coefficients for SPME 

Using Retention Indexes from Linear Temperature-Programmed 100µm PDMS, GC-FID 

hydrocarbons Capillary Gas Chromatography. Application to the Sampling 30µm PDMS 

in air and Analysis of Total Petroleum Hydrocarbons in Air 

Anal. Chem. 69: 402-408 (1997) 

30-480 min 





Martos, P., Saraullo, A., Pawliszyn, J. 


375 Formaldehyde 

Sampling and Determination of Formaldehyde Using SPME 

with On-Fiber Derivatization 65µm PDMS/DVB GC-MS 

derivatives Anal. Chem. 198, 70, 2311-2320 10-150 sec 

in air Martos, P., Pawliszyn, J. 

Determination of Amines in Air and Water Using Derivatization 

gas sampling 

PFBHA derivatives 

110 Amines Combined with SPME 65µm Carbowax/DVB GC-FID 

in air J. Chromatogr. A 773: 249-260 (1997) 30 min 

Pan, L., Chong, M., Pawliszyn, J. 

Evaluation of SPME for sampling of volatile organic sulfur 

gas sampling 

DPTFA derivatives 

539 Thiol and sulfides compounds in air for subsequent GC analysis with 75µm Carboxen/PDMS GC-AED 

in air samples atomic emission detection 

J. Chromatogr., A 1999, 848(1+2), 305-315 

Haberhauer-Troyer, C., Rosenberg, E., Grasserbauer, M 

540 Sulfur compounds 

Studies on the application of SPME for analysis of volatile 

organic sulfur compounds in gaseous and liquid samples 100µm PDMS FPD-GC 

in water/ N2 & Chem. Anal. (Warsaw), 1999, 44(3A), 485-493 10 min 

propane Wardencki, W., Namiesnik, J. 

Calibration of Solid-Phase Microextraction for Air Analyses 

233 C5-C11 hydrocarbons, Based on Physical Chemical Properties of the Coating 30µm & 100µm PDMS GC-FID 

BTEX Anal. Chem. 69: 206-215 (1997) 15-450 sec 

in air Martos, P., Pawliszyn, J. gas sampling 

On Calibration of SPME-GC-MS system for analysis of 

541 Chlorobenzen and organic air contaminants using gaseous standard mixtures Optimization of sampling GC-MS 

p-xylene Chem. Anal. (Warsaw) (1999), 44(2), 201-213 

in air Namiesnik, J., Gorlo, D, Wolska, L, Zygmunt, B. 

SPME in environmental analysis 

2851 Review article Anal. Bioanal. Chem. 386, #4, 1059-1073 (Oct 2006) 

Ouyang, Gangfeng; Pawliszyn, Janusz 

Standard-free kinetic calibration for rapid on-site analysis by SPME 

2903 PAHs J. Sep. Sci.31, #6-7, 1167-1172 (April 2008) GC-MS 

Cai, Jibao; Li, Hui; Ouyang, Gangfeng; Pawliszyn, Janusz; Zhang, Xu 

2297 PAHs 

Calibration of SPME for quantitative analysis by gas chromatography 

J. Chromatogr. A, 1097, #1-2, 9-16 (2006) 

Chen, Yong; Ouyang, Gangfeng; Pawliszyn, Janusz; Setkova, Lucie 

GC 


Calibration Procedure for SPME-GC Analysis of Organic 

Vapors in Air 

in air Talanta 44 (9): 1543-1550 (1997) 

Gorlo, D., Wolska, L., Zygmunt, B., Namiesnik, J. 


Diffusion-Based Calibration for SPME Analysis of 

Aqueous samples Carboxen/PDMS 

in air Anal. Chem. 2001, 73 (1), 13-18 DVB/PDMS 

Sukola, K., Koziel, J., Augusto, F., Pawliszyn, J. 10sec. Passive sampling 

Determination of absolute amount extracted by SPME 

828 different approaches under examination 

J.Microcolumn Separations (2000) 12(10), 550-557 

Tuduri, L.; Desauziers, V.; Fanlo, J. L 

757 Aerosols, particulate 

Sampling and Analysis of Airbourne Particulate matter 

and aerosols using In-Needle Trap and SPME fiber devices 7um PDMS GC-MS 





in air Anal. Chem., 2001, 73(1), 47-54 

Koziel, J., Odziemkowski, M., Pawliszyn, J. 

10 sec 

739 Aerosols, particulate 

Sampling and Raman Confocal Microspectroscopic Analysis 

of Airborne Particulate Matter Using Poly(dimethylsiloxane PDMS Raman 

in air Solid-Phase Microextraction Fibers 

Anal. Chem (2001) 73(13), 3131-3139 

Odziemkowski, M.; Koziel, J.; Irish, D.; Pawliszyn, J. 

Study of preservation of polydimethylsiloxane/carboxen SPME fibres 

2714 Volatiles in before and after sampling of volatile organic compounds in indoor air. 75µm Carboxen GC-MS 

Indoor air J. Chromatogr. A 1124, #1-2, 106-111 (2006-08-18) 

Larroque, V.; Desauziers, V. ; Mocho, P 

Volatile organic compounds in indoor environments 

2236 Volatiles in HANDBOOK OF ENVIRONMENTAL CHEMISTRY, (2004) p1-35 book 

Indoor air Ayoko, Godwin A. 

574 Solvents 

Application of SPME to monitoring indoor air quality. 

Fresenius'-J-Anal-Chem. Apr 1999; 363(7): 696-699 100µm PDMS GC-MS 

in air Gorlo,-D; Zygmunt,-B; Dudek,-M; Jaszek,-A; Pilarczyk,-M; Namiesnik,-J 15 min 


Application of SPME to monitoring indoor air quality 

Fresenius' J. Anal. Chem. (1999), 363(7), 696-699 100µm PDMS GC-MS 

in air Gorlo, D., Zygmunt, B., Dudek, M., Jaszek, A, Pilarczyk, M., 

Maniesnik, J. 

Time-weighted average water sampling with a SPME device 

2293 PAHs in Anal. Chem. 77 #22, 7319-7325 (2005) PDMS GC 

water Chen, Yong; Ouyang, Gangfeng; Pawliszyn, Janusz 


Time-Weighted Average Sampling with SPME Device; 

Implications for Enhanced Personal Exposure Monitoring to 100µm PDMS 

in Air Airborne Pollutants 

Anal. Chem. (1999), 71(8), 1513-1520 

Martos, p. Pawliszyn, J. 


Time-weighted average sampling of volatle and semivolatile 

airborne organic compounds by the SPME device 

in Air J. Chromatogr. A (2000), 892(1-2), 455-467 

Khaled, A, Pawliszyn, J. 

306 VOCs 

Application of Solid Phase Microextraction for Determination 

of Volatile Halogenated Hydrocarbons in Air and Water 

in water and air of an Indoor Swimming Pool 

Fresenius’ Environ. Bull. 5 (1+2): 55-60 (1996) 

Czerwinski, J., Zygmunt, B., Namiensnik, J. 

307 Pollution 

A Case Study of Indoor Pollution by Chinese Cooking 

Toxicol. Environ. Chem. 65 (1-4): 217-224 (1998) 

in air Benfenati, E., Pierucci, P., Niego, A. 

347 VOCs 

Nonequilbrium Quantitation of Volatiles in Air Stream by SPME 

Anal. Chem. Vol. 71, January 1, 1999, pg. 92-101 7µm, 30µm, 100µm GC-FID 

in air Bartelt, R., Zilkowski, B. PDMS 

27°C, 30 min 

gas sampling 


High-molecular products analysis of VOC destruction in atmospheric 

pressure discharge 65µm CW/PDMS GC-FID 

atmosphere J. Phys., Conf. Ser. (UK) 63, #1, 6 (2007) Car/DVB 30/50µm 

Grossmannova, H.; Ciganek, M.; Krcma, F. gas sampling 


The sampling and analysis of volatile organic compounds 

in the atmosphere 





atmosphere React. Hudrocarbons Atmos. (1999), 119-157 

Boob, Academic, Coden: 67ERAQ 

Cao, X, Hewitt, C. 

851 Toluene diisocyanate 

Determination of gaseous toluene diisocyanate by use of 

solid-phase microextraction with on-fibre derivatisation. 65µm DVB/PDMS LC-MS-MS 

Fresenius' J. Anal. Chem. (2001), 369(6), 524-529 60min. 

Nilsson, U.; Batlle, R.; Colmsjo, A. dibutylamine derivative 

752 VOC, formaldehyde 

Field air analysis with SPME device 

Analytica Chimiera Acta 400 (1999) 153-162 varied fibers GC-FID 

in air Koziel, J., Jia, M., Khaled, A., Noah, J., Pawliszyn, J. 

Field Sampling and Determination of Formaldehyde in Indoor 

1-75 min 

air samples 

753 VOC, formaldehyde Air with SPME and On-Fiber Derivatization 65µm DVB/PDMS GC-FID 

in air Environ Sci Technol 2001, Vol 35, pg. 1481-1486 10min. Headspace 

Koziel, J., Noah, J., Pawliszyn, J. PFBHA Derivative 

2702 Aromatic VOCs 

Field analysis of benzene, toluene, ethylbenzene and xylene in water by 

portable GC-micro-FID combined with headspace SPME 65µm DVB/PDMS GC-FID 

in water Talanta 69, #4, 894-899 (2006-06-15) 

Ji, J.; Deng, C. H.; Shen, W. W.; Zhang, X. M. 


sat. salt 

755 Aromatic VOCs 

Design of Validation of Portable SPME devices for 

rapid field air sampling and diffusion-based calibration 65µm DVB/PDMS GC-FID 

in Indoor air Anal. Chem. 2001,73(3), 481-486 

Augusto, F., Koziel, J., Pawliszyn, J. 

30 sec air sampling 

759 VOCs 

Fast field sampling/sample preparation and quantification 

of volatile organic compounds in indoor air by SPME 65µm DVB/PDMS GC-FID 

in Indoor air and portable GC 

Field Analytical Chem. And Tech 4(2-3): 73-84,2000 

Jia, M., Koziel, J., Pawliszyn, J. 



Analysis of volatile organic compounds in the ambient air of 

Algiers by GC with a beta-cyclodextrine capillary column 

in air J. Chromatogr A, 1999, 846(1+2), 287-293 

Yassaa, N., Meklati, B., Cecinato, A. 

984 VOC's in air 

Dynamic versus static sampling for quantitative analysis of VOC's in air. 

J.Chromatogr. A (2002) 963(1-2), 49-56 

Tuduri, L.; Desauziers, V.; Fanlo, J.L. 

PDMS/carboxen 

1062 

Volatile organics from 

steel. 

Analysis of airborne volatile organic compounds of a steel industry by solid 

phase microextraction and gas chromatography/mass spectrometry. 

Bulletin of Environmental Contamination and Toxicology (2003) 70 (5), 957- 

963. GC-MS 

de Lourdes Cardeal, Z.; de Carvalho, C. R.; Parreira, F. V. 

Solid phase microextraction with analysis by gas chromatography to determine 

short term hydrogen cyanide concentrations in a field setting. 

Hydrogen cyanide in 

1070 air Journal of Separation Science (2002) 25 (14), 917-921. 

Smith, P. A.; Sheely, M. V.; Kluchinsky, T. A, Jr. 

GC-NPD 

1114 

Development of a quantification method for the analysis of malodorous sulphur 

compounds in gaseous industrial effluents by solid-phase microextraction and 

gas chromatography-pulsed flame photometric detection 

Malodorous sulphur 

compounds in effluents Journal of Chromatography A (2003) 999 (1-2), 71-80. PDMS/carboxen GC-PFPD 

Desauziers, Valerie; Fanlo, Jean-Louis; Lestremau, Francois; Roux, Jean- 

Claude 





Discrimination of combustion fuel sources using gas chromatography-planar 

field asymmetric-waveform ion mobility spectrometry 


1144 Smoke plumes Journal of Separation Science (2003) 26 (6-7), 585-593. 

Eiceman, Gary A.; Funk, Paul A.; Hughs, S. Edgar; Miller, Raanan A.; Nazarov, 

Erkijon G.; Tarassov, Alexander 

GC-MS 

Potential of solid-phase microextraction fibers for the analysis of volatile organic 

compounds in air. 

1175 VOCs in air Journal of Chromatographic Science (2001) 39(12), 521-529 Various fibers compared 

Tuduri, Ludovic; Desauziers, Valerie; Fanlo, Jean Louis 

Sampling and sample-preparation strategies based on solid-phase 

microextraction for analysis of indoor air. 

1187 Trends in Analytical Chemistry (2002) 21 (12), 840-850. 

Koziel, J. A.; Novak, I. 

1194 PAHs 

Screening direct analysis of PAHs in atmospheric particulate matter with SPME 

Talanta (2003) 60 (4), 687-693. 

Vaz, Jorge Moreira 

PDMS 

PAHs in air 

2606 

Monitoring of PAHs in air by collection on XAD-2 adsorbent then 

microwave-assisted thermal desorption coupled with headspace 65µm PDMS/DVB GC-MS 

SPME and GC with mass spectrometric detection. headspace 

Anal. Bioanal. Chem. 387, #3, 999-1005 (2007-02) 35°C for 40 min. 

Wei, M. C.; Chang, W. T.; Jen, J. F. sat. salt 

Determination of benzene at trace levels in air by a novel method based on solid 

phase microextraction gas chromatography/mass spectrometry. 

1200 Benzene in air Rapid Communications in Mass Spectrometry (2001) 15(24), 2404-2408 GC-ITMS 

Salvadori, Piero; Cuzzola, Angela; Pucci, Sergio; Raffaelli, Andrea; Saba, 

Alessandro 

Determination of volatile aliphatic amines in air by solid-phase microextraction 

coupled with gas chromatography with flame ionization detection 

Volatile aliphatic 

1305 amines in air. Journal of Chromatography, A (2003) 1016 (1), 1-9. 

Jastrzebska, Anna; Namiesnik, Jacek; Zygmunt, Bogdan 

GC-FID 

Solid phase microextraction sampling and gas chromatography/mass 

spectrometry for field detection of the chemical warfare agent O-ethyl S-(2diisopropylaminoethyl) 

methylphosphonothiolate (VX) 

Chemical warfare 

1313 agents Journal of Separation Science (2003) 26 (12-13), 1091-1096. 

Betsinger, Geoffrey; Hook, Gary L.; Kimm, Gregory; Logan, Tom; Savage, Paul 

B.; Smith, Philip A.; Swift, Austin 

Various GC-MS 

Characterisation of odorants emissions from landfills by SPME and GC/MS 

Odorant emissions 

1334 from landfills. Chemosphere (2003) 51 (5), 357-368. DVB/Carboxen/PDMS GC/MS 

Davoli, E.; Gangai, M.L.; Morselli, L.; Tonelli, D. 

1342 

A simple calibration procedure for volatile organic compounds sampling in air 

with adsorptive solid-phase microextraction fibres. 

Analyst (2003) 128 (9), 1028-1032. PDMS/CAR GC-FID 

Tuduri, L.; Desauziers, V. *; Fanlo, J. L. 

Screening for sarin in air and water by solid-phase microextraction-gas 


1373 Sarin in air and water. Journal of Chromatographic Science (2001) 39(10), 420-424. 

Schneider, J. F.; Boparai, A. S.; Reed, L. L. 

GC-MS 

Determination of perfume oil in household products by headspace solid-phase 

microextraction and fast capillary gas chromatography. 




Matrix 

Perfume oil in 


1186 household products. Chromatographia (2003) 57 (Supp), S199-S206. 

Bothe, F.; Dettmer, K.; Engewald, W. * 

Various FCGC 

Volatile organic compounds produced during irradiation of mail. 

VOC's from irradiated 

1141 mail. AIHA Journal (2003) 64 (2), 189-195. 

Smith, Philip A.; Hakspiel, Shelly J.; Miller, Stephen; Sheely, Michael V. 

Evaluation of solid-phase microextraction for time-weighted average sampling of 

volatile sulfur compounds at ppb concentrations 

1126 Sulfur compounds Analytical Chemistry (2003) 75 (11), 2626-2632. 

Andersson, Fras Annika T.; Desauziers, Valerie; Fanlo, Jean-Louis; Lestremau, 

Francois 

Carboxen/PDMS 

Determination of low-level residual ethylene oxide by using solid-phase 


1098 Ethylene oxide Journal of AOAC International (2002) 85 (6), 1205-1209. 

Ayoub, K.; Harris, L.; Thompson, B. 

1447 


air 

Characterization of volatile effluents of livestock buildings by solid-phase 


Int. J. Environ. Anal. Chem. (2003) 83(10), 837-849 75um Carboxen PDMS GC-MS 

Begnaud, Frederic; Berdague, Jean-Louis; Peres, Christophe 

Development of a personal isocyanate sampler based on DBA derivatization on 

solid-phase microextraction fibers. 

1476 Isocyanates in air Fresenius' Journal of Analytical Chemistry (2001) 371(4), 514-518 

Nilsson, Ulrika; Batlle, Ramon; Colmsjo, Anders 

Traditional sampling with laboratory analysis and solid phase microextraction 

sampling with field gas chromatography/mass spectrometry by military industrial 

hygienists. 

1478 Volatiles in air AIHAJ (2002) 63(3), 284-292 

Thomas, Richard J.; Smith, Philip A.; Lee, Arthur P.; Kluchinsky, Timothy A., 

Jr.; Erickson, Richard P.; Savage, Paul B.; Stevens, Michael; Williams, 

Kenneth 

1479 VOCs in air 

Solid phase microextraction : Measurement of volatile organic compounds 

(VOCs) in Dhaka City air pollution. 

Journal of Environmental Science and Health Part A Toxic-Hazardous 

Substances & Environmental Engineering (2002) A37(7), 1223-1239 

Hussam, A.; Alauddin, M.; Bhattacharjee, M.; Bibi, H.; Chowdhury, D.; Khan, A. 

H.; Sultana, S. 

Gas chromatographic determination of glutaraldehyde in the workplace 

atmosphere after derivatization with O-(2,3,4,5,6pentafluorobenzyl)hydroxylamine 

on a solid-phase microextraction fibre. 

1523 Glutaraldehyde in air Journal of Chromatography A (2002) 955(1), 117-124 

1524 

Valeraldehyde in air 

(TWA) 

1543 Nicotine in air 

Pieraccini, Giuseppe; Bartolucci, Gianluca; Boccalon, Pierpaolo; Dugheri, 

Stefano; Focardi, Leonardo; Pacenti, Marco 

Time-weighted average sampling of airborne n-valeraldehyde by a solid-phase 

microextraction device. 


Tsai, S.-W.; Chang, T.-A. 

Trace analysis of nicotine in indoor air by a SPME method. 

Bulletin of Environmental Contamination and Toxicology (2002) 68(4), 485- 

489 

Shuokui, H.; Huali, Y.; Jianfang, F.; Songting, G. 


65um PDMS/DVB, 

dibutylamine (DBA) 

derivative 

On-fiber derivatization 

with PFBHA 

65um DVB PDMS, onfiber 


PFBHA 

HPLC-MS 

GC-MS 

GC 

GC-FID

1528 




Dynamic air sampling of volatile organic compounds using solid phase 


VOCs in air (dynamic 

sampling) 

Journal of Environmental Science and Health Part B Pesticides Food 

Contaminants and Agricultural Wastes (2002) B37(4) 365-378 

Razote, Edna; Chobpattana, Wannee; Jeon, Ike; Maghirang, Ronaldo 

Configurations and calibration methods for passive sampling techniques 

2674 passive sampling J. Chromatogr. A 1168, #1-2, 226-235 (19 OCT 2007) 

Ouyang, G.; Pawliszyn, J. 

75um Carboxen PDMS GC-MS 


Compound-specific carbon isotope analysis of volatile organic 

compounds in water using solid-phase microextraction 75um Carboxen GC-MS 

in water J. CHROMATOGR. A 1163, #1-2, 260-268 (07 SEP 2007) headspace and 

Palau, J.; Soler, A.; Teixidor, P.; Aravena, R. 

immersion 

2656 Volatiles in water 

Time-weighted average water sampling with a diffusion-based SPME 

J. Chromatogr. A 1138, #1-2, 42-46 (Jan 5 2007) PDMS coatings GC 

passive sampling Alaee, Mehran; Ouyang, Gangfeng; Pawliszyn, Janusz; Zhao, Wennan 

2638 Volatiles in water 

Time-weighted average water sampling in Lake Ontario with 

SPME passive samplers PDMS coatings GC 

passive sampling Environ. Sci. Technol. 41, #11, 4026-4031 (Jun 1 2007) 

Alaee, M.; Bragg, L.; Ouyang, G.; Pawliszyn, J.; Qin, Z.; Zhao, W. 

1547 

Evaluation of indoor exposition to benzene, toluene, ethylbenzene, xylene, and 

styrene by passive sampling with a solid-phase microextraction device. 

Volatiles in air (passive 


sampling) 

Cardeal, Zenilda de L.; de Carvalho, Ciomara R.; Parreira, Fabricio V. 

100um PDMS, 65um 

DVB PDMS 

1388 Perfumes 

Atmospheric lifetimes and fates of selected fragrance materials and volatile 

model compounds. 

Environmental Science and Technology (2001) 35(18), 3595-3600. 

Aschmann, S. M.; Arey, J.; Atkinson, R. *; Simonich, S. L 

PDMS GC-MS 

Measuring the effect of photocatalytic purifiers on 

2111 Hydrocarbons indoor air hydrocarbons and carbonyl pollutants 15 min sampling GC 

in air J. Air Waste Manage. Assoc., 55, #1, 88-96 

Disdier, Jean; Mas, Denis; Pichat, Pierre 

Air sampling of aromatic hydrocarbons in the 

2112 BTEX presence of ozone by SPME 100µm PDMS GC-FID, GC-MS 

in air J Chromatogr A, 1025, #1, 57-62 headspace 

Xiong, G; Koziel, J.; Pawliszyn, J. 

Sampling and analysis of PCBs in indoor air by 

2113 PCBs in sorbent enrichment followed by headspace headspace GC-MS 

indoor air SPME and GC-MS 

J. Chromatogr. A,1072, #1, 99-106 

Ares, S; Barro, R; Cela, R; Garcia-Jares, C; Llompart, M 

Air sampling of organophosphate triesters using 

2114 Organo- SPME under non-equilibrium conditions. 100µm PDMS GC 

phosphate Anal & Bioanalytical Chem, 378, #7, 1847-1853 1 hr. sampling 

triesters in Isetun, S.; Nilsson, U.; Colmsjo, A.; Johansson, R. 

air 

Evaluation of SPME w/ PDMS for air sampling of 

2115 Organo- gaseous organophosphate flame-retardants 100µm PDMS GC 

phosphate and plasticizers 8 hrs. sampling 

triesters in Anal & Bioanalytical Chem, 380, #2, 319-324 

Air Isetun, Sindra; Nilsson, Ulrika; Colmsjo, Anders 

Suitability of SPME for the determination of organophosphate 

2328 Flame retardants flame retardants and plasticizers in water samples 65µm PDMS-DVB GC-NPD 

& plasticizers J. Chromatogr. A 1108 #2, 158-165 (2006) Direct extraction 

in water Calvo, F.; Cela, R.; Quintana, J.B.; Rodil, R.; Rodriguez, I.; Rubi, E. 40 min @ 21°C 

NaCl added 

Investigation of artefact formation during analysis 

2116 Volatile of volatile sulfur compounds "in air" using SPME 75µm Carboxen GC 

sulfur Chromatographiam 59, #9-10, 607-613 direct air sample 





compounds Lestremau, F.; Andersson, F.; Desauziers, V. * 

in air 

Determination of benzene, toluene, ethylbenzene and 

2117 BTEX in xylenes in air by SPME-GC-MS 75µm Carboxen GC-MS 

air Analytical & Bioanalytical Chem, 380, #5-6, 824-830 30 min sampling 

Tumbiolo, S.; Gal, J. -F.*; Maria, P. -C.; Zerbinati, O. 

SPME sampling of BTEX before GC/MS analysis:Examples of outdoor 

2174 BTEX in and indoor air quality measurements in public and private sites GC-MS 

air Annali di Chimica 95, #11-12, 757-766 (2005) 

Tumbiolo, S.; GAL, Jean-Francois; Maria, P.; Zerbinati, O. 

Use of SPME for the detection of acetic acid by ion-trap 

2118 Acetic acid GC-MS and application to indoor levels in museums GC-ITMS 

in air J. Chromatogr. A, 1067, #1-2, 331-336 

Godoi, Ana F.L.; Van Grieken, Rene; Van Vaeck, Luc 

Development of a sensitive methodology for the 

2119 Chloro- analysis of chlorobenzenes in air bycombination of 65µm PDMS-DVB GC-MS 

benzenes SPE and headspace SPME 65µm CW GC-ECD 

in air J. Chromatogr. A, 1045, #1-2, 189-196 headspace 

Ares,S; Barro,R; Cela,R; Garcia-Jares,C; Llompart,M 

Dynamic SPME for sampling of airborne sarin with 

2120 Sarin in Air GC-MS for rapid field detection and quantification Direct sampling of air GC-MS 

J. Sep. Sci., 27,#12, 1017-1022 

Hook, G.; Lepage, C; Miller, S.; Smith, P. 

Analysis of sulfur-containing compounds in ambient air 

2121 Sulfur compd using SPME-GC with pulsed FPD direct sampling GC-FPD 

in air Int. J. Environ. Anal. Chem., 84, #10, 749-760 

Li, Kwong-Chi; Shooter, David 

Determination of aniline in silica gel sorbent by one-step 

2122 Aniline in situ microwave assisted desorption coupled to 65µm PDMS-DVB GC-FID 

in air headspace SPME and GC-FID headspace 

Talanta, 64, #3, 650-654 3 min extraction 

Jen, Jen-Fon; Shih, Ton-Sheng; Yan, Cheing-Tong 

Propylene glycol vapor contamination in controlled 

2123 Popylene environment growth chambers: Toxicity to corn and headspace MD-GC-MS 

glycol in soybean plants 

air J. Environ. Sci. Health Part B, 40, #3, 443-448 

McConnell, Laura; Niu, Genhua; Reddy, Vangimalla R. 

Theory / Technique 

856 Volatiles 

An automated method for the determination of some volatile 

organic compounds in water samples after extraction by GC-ECD 

in water SPME and CGC-ECD analysis 

Rev. Port. Farm (2000) 50(4) 141-149 

Cunha, E.; Goncalves, C.; Alpendrurada, M. F. (Portuguese) 

2 VOCs, BTEX, PAHs 

Solid Phase MicroExtraction with Thermal Desorption Using 

Fused Silica Optical Fibers 56µm PDMS GC-FID, 

in water Anal. Chem. 62: 2145-2148 (1990) 2 min GC-ECD 

Arthur, C., Pawliszyn, J. stirring, salt added 

5 BTEX 

Solid Phase MicroExtraction: An Attractive Alternative 

Environmental Lab. 11, Dec/Jan 1992/1993 pp 10-15 100µm PDMS GC-FID 

in water Arthur, C., Killam, L., Chai, M., Buchholdz, K., Potter, D., 14 min 

Zhang, Z., Pawliszyn, J. 

Automation and Optimization of Solid Phase MicroExtraction 

stirring 

salt added 

9 BTEX Anal. Chem. 64: 1960-1966 (1992) 56µm & 100µm PDMS GC-FID 

in water Arthur, C., Killam, L., Buchholz, K., Pawliszyn, J. 2-40 min 


2392 PAHs 

Automation of solid-phase microextraction on a 96-well plate format 

J. Chromatogr., A 1149, #2, 127-137 (2007-05-18 ) PDMS fibers 

in water Hutchinson, J. P.; Setkova, L.; Pawliszyn, J. 





Strategies for interfacing SPME with liquid chromatography 

2446 Review article J. Chromatogr., A 1152, #1-2, 2-13 (2007-06-08) 

Lord, H. L. 

Automation of solid-phase microextraction 

2337 Review article J. Sep. Sci. 28 #15, 2010-2022 (2005) GC & LC 

Chen, Y.; Hutchinson, J..; Linton, C..; Lord, H.; O'Reilly, J.; 

Pawliszyn, Janusz; Setkova, Lucie; Wang, Qing 

820 Jasmine plant 

A versatile Robotic Arm for Static headspace 

sampling with SPME 85µm Polyacrylate GC-MSN 

beer LC-GC Europe, April 2001, 215-222 30min. 

Pham-Tuan, H., Vercammen, J., Sandara, P. headspace 

12 BTEX 

Solventless Injection Technique for Microcolumn Separations 

J. Microcolumn Sep. 5: 51-56 (1993) 100µm PDMS GC-MS 

in water Arthur, C., Chai, M., Pawliszyn, J. 

13 BTEX, PAHs 

Headspace Solid Phase MicroExtraction 

Anal. Chem. 65(14): 1843-1852 (1993) 56µm PDMS GC-FID 

in water Zhang, Z., Pawliszyn, J. 

Practical Use of Automated Solid Phase Extraction 

1-5 min 

headspace 

16 Nitroaromatics Amer. Lab. Nov. Vol. 25,1993, p18-24 100µm PDMS GC-FID 

in water Berg, J. 1-20 min 

immersion 

17 Toluene 

On-Line Monitoring of Flowing Samples Using SPME-GC 

Anal. Chim. Acta 284: 265-273 (1993) 56µm PDMS GC-FID 

in water Motlagh, S., Pawliszyn, J. 

Optimization of Solid Phase MicroExtraction (SPME) Conditions 

20 min 


21 Phenols for Phenol Analysis 85µm polyacrylate GC-MS 

in water and air Anal. Chem. 66: 160-167 (1994) 40 min 

Buchholz, K., Pawliszyn, J. 

Determination of Phenols by Solid-Phase Microextraction 

immersion & headspace 


acetate derivatives 

204 Phenols J. Chromatogr. A 767: 171-175 (1997) 

Bartak, P., Cap, L. 

391 Phenols, PAHs 

SPME for Determining the Binding State of Organic Pollutants 

in Contaminated Water Rich in Hujic Organic Matter 7µm PDMS GC-MS 

in water J. Chromatogr. A, 816 (1998) 159-167 50°C, 90-180 min 

Porschamann, J., Kopinke, F., Pawliszyn, J. headspace, stirring 

Silica-Fiber microextraction for Laser Desorption Ion Trap 

24 PAHs Mass Spectrometry Trimethlysilyl coated fiber MS 

in soil and water Anal. Chem. 66: 1897-1901 (1994) 

Cisper, M., Earl, W., Nogar, N., Hemberger, P. 

3 min 

27 PAHs 

Solid Phase microextraction Coupled to HPLC 

Anal. Chem. 67: 2530-2533 (1995) 15µm PDMS HPLC-UV 

in water Chen, J., Pawliszyn, J. 6-60 min 

immersion 

222 

Potential Applications of Coupled SPME-HPLC 

LaborPraxis 20 (11): 66-68, 71 (1996) 

Haag, I. 

HPLC 

33 Fatty acids, PAHs, 

Solvent-free Sample Introduction for Supercritical Fluid 

Chromatography Using Polymer Coated Fibers 15µm PDMS, GC-FID 





pesticides in J. Microcolumn Res. 42: 1925-1930 (1994) 85µm polyacrylate 

methanol/water Hirat, Y., Pawliszyn, J. 

Headspace SPME vs. Purge & Trap for the Determination of 

5 min 

immersion 

35 BTEX Substituted Benzenes in Water 100µm PDMS GC-FID 

in water J. Chromatogr. Sci. 32(8): 317-322 (1994) 40°C, 50 min 

MacGillevra, B. 

Quantitative Extraction Using an Internally Cooled Solid 

headspace 

stirring, salt 

38 BTEX Phase MicroExtraction Device 50µm PDMS GC-MS 

in water Anal. Chem. 67(1): 34-43 (1995) 22-80°C, 2-5 min 

Zang, Z., Pawliszyn, J. headspace 


Element-Selective Detection of Pesticides by Gas 

Chromatography Atomic Emission Detection 100µm PDMS GC-AED 

pesticides and Solid Phase MicroExtraction 20 min 

in water J. Chromatogr. 683: 175-183 (1994) 

Eisert, R., Levser, K., Winsch, G. 

immersion 

44 BTEX 

Solid-Phase Microextraction: A Solvent-Free Alternative for 

for Sample Preparation polyacrylate, PDMS GC-FID 

in water Anal. Chem. 66(17): 844A-853A (1994) 

Zang, Z., Yang, M., Pawliszyn, J. 

immersion, salt 

45 BTEX 

New Solvent-Free Sample Preparation Techniques 

ES &T 28 (13): 569A-574A (1994) Various fibers and GC-FID,E1858 

in water and air Boyd-Boland, A., Chai, M., Luo, Y. Zhand, Z. Yang., M., 

Pawliszyn, J. 

extraction conditions GC-MS 

A New Separation and Extraction Method -- Solid-Phase 

213 Microextraction 

Sepu (Chinese) 15 (2): 118-119 (1997) 

Liu, J. 


56 GIT Fachz. Lab. 39: 325-362 (1995) 

Popp, P. 


Sample-introduction systems coupled to ion-mobility spectrometry 

equipment for determining compounds 

present in gaseous, liquid and solid samples IMS 

gases, liquid, TrAC Trends Anal. Chem. 27, #2, 139-150, (Feb. 2008) 

solids Arce, L.; Garrido-Delgado, R.; Menendez, M.; Valcarcel, M. 

57 BTEX 

Sample Introduction Approaches for Solid Phase 

MicroExtraction-Rapid GC 

in water Anal. Chem. 67: 3265-3274 (1995) 

Gorecki, T., Pawliszyn, J. 

GC-FID 

58 BTEX 

Solid Phase MicroExtraction/Isothermal GC for Rapid 

Analysis of Complex Organic Samples 15µm PDMS GC-FID 

in water J.High Res.Chromatogr. 18 (2): 161-166 (1995) 2 min 

Gorecki, T., Pawliszyn, J. headspace, stirring 

Examination of analyte partitioning to monocationic and dicationic 

2659 Semivolatiles imidazolium-based ionic liquid aggregates using SPME-GC 

in water J. Chromatogr. A 1148, #1, 92-99 (Apr 27 2007) 

Anderson, Jared L.; Baltazar, Quinner Q.; Pino, Veronica 


Estimating the octanol-water partition coefficients of NPAHs and PAHs 

by SPME and gas chromatography-ion trap detector immersion, stirring GC-MS 

in water Analytical Letters 40, #2, 307-319 (JAN 2007) 

Wang, Yiru; Wang, Yonghong 


SPME as a Method for Estimating the Octanol Water Partition 

Coefficient 85µm polyacrylate GC-FID 





in water Anal. Chem. 68: 130-133 (1996) min to 20 hr 

Dean, J., Tomlinson, W., Makovskaya, V., Cumming, R., 

Hetheridge, M., Comber, M. 


546 PAHs 

Solubility and partitioning studies with PAHs using an 

optimized SPME procedure 100µm SPME GC-MS 

in water and Fresenius' J. Anal. Chem. (1999), 363(4), 426-428 stirred 

octanol-water Paschke, A., Popp, P., Schueuermann, G. 

728 PAHs 

Determination of PAHs in waste water by off-line coupling 

SPME with column liquid chromatography 100µm PDMS HPLC 

in waste water J. Chjromtogr. A, 897(2000) 153-159 

Popp, P., Bauer, C., Moder, M., Paschke, A. 

60 min fluorescence 


Extracted amounts by SPME: a realistic approach to the 

partition coefficient K. 

water J. Chromtogr. Sci. 1999, 37(8), 277-282 

Urruty, L., Montury, M 

548 Volatiles 

Determination of Henry's law coefficient by combination of 

the equilibrium partitioning in closed systems and 100µm PDMS GC-FID 

in water SPME techniques 

J. Chromatogr, A., (1999), 830(2), 353-363 

Dewulf, J., Van Langenhove, H., Everaert, P 

30 min @ varied temp. 


Partitioning of Organic Chemicals to Polyacrylate-Coated 

Solid-Phase Microextraction Fibers: Kinetic Behavior and 85µm polyacrylate GC-FID, -ECD 

water and air Quantitative Structure-Property Relationships immersion GC-MS 

Anal. Chem. 68: 4458-4462 (1996) 

Vaes, W., Hamwik, C., Ramos, E., Verhaar, H., Hermens, J. 

stirring 

Solid Phase Microextracting Using Fused-Silica Fibers Coated 

84 with Graphitized Carbon Black 

Chromatographia 41: 678-684 (1995) 

Mangani, R., Cenciarini, R. 

88 Overview 

New Direction in Sample Preparation for Analysis of 

Organic Compounds 

Trends Anal. Chem. 14 (3): 113-122 (1995) 

Pawliszyn, J. 

Multiple applications 

121 Eugenol, 

Solid Phase Microextraction for Quantitative Analysis in 

Nonequilibrium Situations 85µm polyacrylate GC-MS 

2,4-dimethylphenol, Anal. Chem. 69: 1230-1236 (1997) 1-160 min 

2-phenylethanol Ali, J. immersion, stirring 

in water 

SPME in Headspace Analysis, Dynamics in Non-Steady State 

salt added 

360 2-Octanol Mass Transfer 85µm polyacrylate, GC-MS 

in water Anal. Chem., 70: 4822-4826, (1998) 100µm PDMS 

Ali, J. headspace 


Analysis of volatile compounds from Malaysian durians (Durio zibethinus) 

using headspace SPME coupled to fast GC-MS headspace GC-MS 

Malaysian durians J. Food Compos. Anal. (UK) 20, #1, 31-44 (Feb. 2007) 

Nazimah, S.; Chin, S.; Quek, S.; Man, Y.; Rahman, R.; Hashim, D. M. 


Characterization of volatile compounds in selected citrus fruits from 

Asia. Part I: freshly-squeezed juice headspace GC-MS 

citrus fruit Flavour and Fragrance J. 22, #3, 228-232 (MAY-JUN 2007) 

Dharmawan, Jorry; Kasapis, Stefan; Curran, Philip; Johnson, Jeffrey R. 


Postharvest survey of volatile compounds in five tropical fruits 

using headspace-solid phase microextraction (HS-SPME). headspace GC-MS 

tropical fruit HortScience 42, #2, 309-314 (2007) 

Natta Laohakunjit; Orapin Kerdchoechuen; Matta, F.; Silva, J.; Holmes, W. 

sat. salt 






Screening of Tropical Fruit Volatile Compounds Using SPME Fibers 

and Internally Cooled SPME Fiber PDMS coating GC-MS 

tropical fruit J. Agric. Food Chem. 54, #23, 8688-8696 (2006-11-15) 

Carasek, E.; Pawliszyn, J. 

214 Strawberries 

Solid-Phase Microextraction: Artifact Formation and Its 

Avoidance 85µm polyacrylate GC-MS 

and apples Chromatographia 46: 63-66 (1997) 30 sec 

in fruit homogenate Verhoeven, H., Beuerle, T., Schwab, W. immersion 

2518 Isophorone 

Determination of isophorone in food samples by SPME-GC-MS 

J Chromatography A 1155, #1, 100-104 (2007) 65µm PDMS/DVB GC/MS 

in food samples Kataoka, H.; Terada, Y.; Inoue, R.; Mitani, K. 60°C, 45 min 

headspace 

Study of barrier properties and chemical resistance of recycled PET 

2327 Organics from coated with amorphous carbon through a plasma enhanced headspace GC/MS 

PET coating chemical vapour deposition (PECVD) process 

Food Additives and Contaminants 23 #1, 100-106 (2006) 

Cruz, S. A.; Zanin, M.; Nerin, C.; De Moraes, M. A. B. 

139 McReynolds probes 

Studying Activity Coefficients of Probe Solutes in Selected 

Liquid Polymer Coatings Using SPME 7µm PDMS GC-FID 

in methanol J. Phys. Chem. 100: 17648 (1996) 25-100°C, 15 min 

Zhang, Z., Pawliszyn, J. headspace 

729 Lidocane 

Multiple solid phase microextraction 

J. Chromatogr. A. (2000) 878, 27-33 100µm PDMS HPLC 

from water Koster, E., de Jong, G. 45min 

Fibers coated with molecularly imprinted polymers for SPME 

939 Anal. Chem (2001) 73(13) 3140-3145 

Koster, E; Crescenzi, C; den Hoedt, W; Ensing, K; de Jong, G 

579 BTEX and solvents 

Study of polymer coatings for solid-phase microextraction 

Sepu. Jan 1999; 17(1): 10-13 88µm PDMS 

in water Zhang,-DN; Wu,-CY; Ai,-F 

148 Maillard reaction 

A Study of the Behavior of Maillard Reaction Products 

Analyzed by SPME-GC-Mass Selective Detection 100µm PDMS GC-MS 

products J. Chromatogr. Sci. 34: 213 (1996) 5 min 

in water Coleman III, W. 

A Study of the Behavior of Polar and Nonpolar SPME Fibers 

immersion 

stirring 

207 Alkyl & alkoxy aroma & J. Chromatogr. Sci. 35 (6): 245-258 (1997) 100µm PDMS GC-MSD 

flavor compounds Coleman, W. 5 min 

in water immersion & 

headspace 


730 Inorganic anions 

SPME of inorganic anions based on polypyrrole film 

Analyst (Cambridge, UK), 2000, 125(3), 391-394 Polypyrrole film Ion Chrom. 

in water Wu, J., Yu, Z, Lord, H., Pawliszyn, J. 


Preparation and appplication of polypyrrole films in SPME 

J. Chromatogr. A (2001) 909(1) 37-52 Polypyrrole film In-tube GC-FID 

PAHs, amines Wu, J., Pawliszyn, J. 20min. LC-UV 

in water/air mixture headspave 

163 Mercury, 

SPME Combined with Electrochemistry 

Anal. Commun. 33(10): 361-364 (1996) 10µm gold on GC-MS 

mercury compounds Guo, F., Gorecki, T., Irish, D., Pawliszyn, J. carbon steel electrode 

in water 5 min 

gas phase sampling 





Use of SPME with Ion Mobility Spectrometry 

Conditions 

stirring, KNO3 added 

Instrument 

182 Anal. Lett. 30 (7): 20-22 (1997) 

Orzechowsa, G., Poziomek, E., Tersol, V. 

GC-MS 

2610 VOCs 

Occurrence of volatile organic compounds (VOCs) in Liverpool 

Bay, Irish Sea headspace GC-MS 

in seawater Mar. Pollut. Bull. 54, #11, 1742-1753 

Bravo-Linares, C.M.; Loyola-Sepulveda, R.H.; Mudge, S.M 

228 VOCs 

SPME of Volatile Organic Compounds. Estimation of the 

Sorption Equilibrium from the Kovats Index Effect of Salinity 100µm PDMS GC-FID 

in seawater and Humic Acids and the Study of the Kinetics by the 45 min 

Development of an "Agitated/Static Layer" Model immersion 

J. Chromatogr. A 761: 205-217 (1997) stirring 

Dewulf, J., Everaert, M., Van-Langenhove, H. salt added 

840 Squalene 

Determination of squalene in seawater by SPME-GC-MS and 

the concentration variation of squalene in redtide seawater. 100µm PDMS GC-MS 

in seawater Fenxi Huaxue (2000) 28(11) 1326-1330 45 min 

Zhao, M. Q.; Li, G. K.; Luan, T. G.; Zhang, Z. X. 

Development of a Prototype System for Quasi-Continuous 

immersion 

stirring 

165 Triazines, organic Analysis of Organic Contaminants in Surface or Sewage 85µm polyacrylate GC-ECD, -FID 

pesticides Water Based on In-Line Coupling of SPME to GC 10 min 

in sewage water J. Chromatogr. A 737 (1): 59-65 (1996) 


300mL/min flow 


Design of Automated SPME for Trace Analysis of 

Organic Compounds in Aqueous Samples 100µm PDMS GC-FID 

in water J. Chromatogr. A 776: 293-303 (1997) 30 min 

Eisert, R., Pawliszyn, J. stirring 

184 BTEX, 

Sample Preparation for GC with SPE & SPME 

Chromatogr. 37: 205-236 (1997) 100µm PDMS GC-FID 

pesticides Penton, Z. 2-20 min 

in water 

Porous-Layer Solid-Phase Microextraction Using Silica 


salt added 

236 Aromatic Bonded Phase 30µm C8 silica bonded GC-FID 

hydrocarbons Anal. Chem. 69: 190-195 (1997) metal fiber 

in water Liu, Y., Shen, Y., Lee, M. 

High Temperature Water Extraction Combined with SPME 

20 min 

stirring 

189 PAHs in Anal. Commun. 33: 421-424 (1996) 30µm PDMS GC-FID 

water extract Daimon, H., Pawliszyn, J. 

Initial Bandwidth Resulting from Splitless and Solid-Phase 

70 min 

stirring 

220 C6-C11 hydrocarbons Microextraction Gas Chromatographic Injections 100µm PDMS GC-FID 

in water J. High Res. Chromatogr. 20 (2): 77-80 (1997) 10 min 

Snow, N., Okeyo, P. 

Optimizing Split/Splitless Injection Port Parameters for SPME 

immersion 

stirring 

138 PAHs in J. Chromatogr. A 740 (1): 139-145 (1996) 7µm & 100µm PDMS GC-FID 

water Langenfeld, J., Hawthorne, S., Miller, D. 

Nitro Musks in Cosmetic Products: Determination by 

5 hr 


211 Nitro musk compounds Headspace SPME and GC with Atomic Emission Detection: 100µm PDMS GC-AID 

in cosmetic products Dynamics of Organic Compound Extraction from Water, 1-60 min 

Using Liquid-Coated Fused Silica Fibers 

Chromatogrphia 45; 138-144 (1997) 

Struppe, C., Schaefer, B., Engewald, W. 

headspace 

Dynamics of Organic Compound Extraction from Water, Using 





243 Liquid-Coated Fused Silica Fibers 

Anal. Chem. 66: 1186-1199 (1994) 

Arthur, C., Pawliszyn, J. 

437 Review 

SPME and Its Utilization in Environmental Analysis 

Chem. Listy (1998), 92(8), 633-642 

Sedlakova, J., Matisova, E., Slezackova, M. 

New materials in sorptive extraction techniques for polar compounds 

2592 Review articles J. CHROMATOGR. A 1152, #1-2, 14-31 (08 JUN 2007) 

Fontanals, N.; Marce, R. M.; Borrull, F. 

549 Review of 52 refs. 

Trends in SPME for determining organic pollutants in 

environmental samples 

Trends Anal. Chem. 1999, 18(8), 557-568 

Penalver, A., Pocurull, E., Borrull, F., Marce, R. 

Varied 

Advances in Extraction Technology: A report from Extech '99 

550 Proceeding of Extech LC-GC Current Trends and development in Sample Prep, 

Sept. 1999, Vol. 17., No. 90, S25-S30 


Varied 

551 Overview of SPME 

Sample Preparation for GC with SPE and SPME 

Advances in Chromatography, Vol. 37, 1966, 205-236 

Book chapter by M. Dekker, New York, 1996 

Penton, Z. 

Solid Phase Microextraction -- A Unique Tool for 

244 Chemical Measurements 

Can. J. Chem. 74: 1297-1308 (1996) 

Gorecki, T., Boyd-Boland, A., Zhang, Z., Pawliszyn, J. 

Solvent Free Sample Preparation Techniques Based on Fiber 

245 and Polymer Technologies 

Environ. Sci. Technol. 28: 569A-574A (1994) 

Boyd-Boland, A., Chai, M., Luo, Y., Zhang, Z., Yang, M., 


246 BTEX, 

Solid Phase Microextraction 

Tech. Aquat. Toxicol. 459-477 (1996) 100µm PDMS GC-FID, -ECD 

pesticides Webster, G., Sarna, L., Graham, K. 10-30 min 

in water 

Solid Phase Microextraction Technique for Gas 

immersion 

stirring 

247 Chromatography overview 

Huaxue 54 (3): 119 (1996) 

Huang, S. 

article 

248 BTEX, 

Sample Preparation for Gas Chromatography with SPE 

and SPME 100µm PDMS GC-FID 

pesticides Adv. Chromatogr. (N.Y.) 37: 205-236 (1997) 2-20 min 

in water Penton, Z. 

Solid Phase Microextraction-SPME, State of the Art 


salt added 

249 BTEX, Chromatography Kaiser, O. (Ed.) Incom, Dusseldorf, 100µm PDMS GC-FID 

pesticides pp153-166 (1997) 2-20 min 

in water Kern, H., Penton, Z. immersion, stirring 

2493 Contaminants 

Potential sources of background contaminants in 

solid phase extraction and microextraction 70µm CW/DVB 

in SPME process J Separation Sci. 30, #7, 1029-1036 (MAY 2007) 

Stiles, R.; Yang, Ill; Lippincott, R.; Murphy, E.; Buckley, B. 

250 Reference book 

Solid Phase Microextraction: Theory and Practice 

VCH, New York, 275pp (1997) various fibers 





Pawliszyn, J. and conditions 

Applications of Solid Phase Microextraction 

731 Reference book Edited by Janusz Pawliszyn 

RSC Chromatography Monographs 

732 Overview 

Theory of solid phase microextraction 


Pawliszyn, J. 

35 applications 

described 

Researchers are giving SPME a second look 

733 R&D Magazine, February 1999, 44-45 

Sample Preparation and Solid-Phase Extraction 

30:50 

Carboxen/DVB/PDMS 

headspace 

GC-FID 

251 Overview LC-GC 15: 1106, 1108, 1110-1113, 1116-1117 (1997) no fibers or 

Majors, R., Raynie, D. conditions shown 

252 Formaldehyde, 

Recent Advances in Solid Phase Microextraction 

LC-GC May Supplement, ppS41-S46 (1998) 65µm PDMS/DVB, GC-MS, 

surfactants in Lord, H., Pawliszyn, J. Carbowax/TPR fiber HPLC-UV 

air and water varied conditions 

2494 VOCs in air and 

Sample preparation for the analysis of volatile organic compounds in 

air and water matrices review article 

water matrices J. Chromatogr. A 1153, #1-2, 130-144 (JUN 15 2007) 

Demeestere, Kristof; Dewulf, Jo; De Witte, Bavo; Van Langenhove, H. 


Sample handling strategies for the determination of persistent trace 

organic contaminants from biota samples 

sample handling ANAL. CHIM. ACTA 590, #1, 1-16 (02 MAY 2007) 

methods Fidalgo-Used, N.; Blanco-Gonzalez, E.; Sanz-Medel, A. 

255 Thiophenes 

Application of SPME/GC-MS to Characterize Metabolites in 

the Biodesulfurization of Organosulfur Model Compounds 85µm polyacrylate GC-MS 

in water in Gitumen 20 min 

Environ. Sci. Technol. 32 (3): 421-426 (1998) immersion 

MacPherson, T., et al. pH 2 

Construction of an Interface for SPME-PC-SFC 

256 J. High Resolut. Chromatogr. 34 (10): 275-277 (1997) 

Medvedovici, A., Sandar, P. 

Automated In-Tube SPME Coupled to HPLC 

257 Phenylurea pesticides Anal. Chem., Vol. 69, No. 16, August 15, 1997, 3140-3147 Omegawax 250 HPLC-UV, 

in water Eisert, R., Pawliszyn, J. 25µL, 10 flush cycles 245nm 

258 PAHs 

Effect of Heating the Interface on Chromatographic 

Performance of SPME Coupled to HPLC 100µm PDMS HPLC-UV, 

in water Anal. Commun. 34 (11): 365-369 (1997) 60 min 254nm 

Daimon, H., Pawliszyn, J. 

Effect of Heating the Interface on Chromatographic 

immersion 

heat desorb 22-180°C 

259 PAHs Performance of SPME Coupled to HPLC 100µm PDMS HPLC-UV, 

in water Analyst (Cambridge) 122 (11): 365-369 (1997) 60 min 254nm 

Daimon, H., Pawliszyn, J. immersion 

heat desorb 22-180°C 

Development of an improved heated interface for coupling SPME to 

2181 Heated interface high-performance liquid chromatography 

for HPLC J. Chromatogr. A, 1105, #1-2, 208-212 (2006) 

Alves, C.; Contadori, A..; Fernandes, C.; Lancas, F.; Neto, A. 

Santos; R., Jose C. 

SPME Combined with HPLC for the Determination of Metal Ions 





260 Hg (II) ion Using Crown Ether as Selective Extracting Reagent polypropylene hallow HPLC-UV, 

in water J. Microcolumn Sep. 167-173 (1998) fiber, 30 min 254nm 

Jia, C., Luo, Y., Pawliszyn, J. immersion 

derivative: 

dibenzo-18-crown-6 

734 Dopamine in 

Analysis of biogenic amines by SPME and HPLC with 

electrochemical detection Carbowax-TPR HPLC 

biological matrix J. Chromatogr. A, (2000) 873, 396 

Auger, J., Boulay, R., Jaillais, B., Delion-Vancassel, S. 

electrochem 


SPME Coupled with HPLC for the Determination of Aromatic 

Amines 50µm Carbowax/TPR, HPLC-UV, 

in wastewater Anal. Chem., Vol. 71, No. 2, January 15, 1999, 310-316 65µm PDMS/DVB, 280nm 

Wu, Y., Huang, S. 30 min or 20 min 

Na2SO4 buffer added 

Automated In-Tube SPME Coupled to HPLC 

407 Phenylurea pesticides Anal. Chem., Vol. 69, No. 16, August 15, 1997, 3141-3147 Omegawax 250 UV, 245nm 

in water Eisert, R., Pawliszyn, J. 25uL, 10 flush cycles 


Headspace SPME in pesticide residues analysis: 2. Apple samples. 

Pesticidi i Fitomedicina 22, #2, 173-176 (2007) 100µm PDMS GC-MS 

apple samples Durovic, R.; Milinovic, J.; Markovic, M.; Markovic, D. 60 min @ 60°C 

headspace 

2177 Carbamate 

Behaviour of carbamate pesticides in GC and their determination 

with SPE and SPME as preconcentration steps 85µm polyacrylate GC-MS 

pesticides J SepSci. 28, #16, 2130-2138 (2005) 

Carabias-Martinez, R.; Garcia-Hermida, C.; Rodriguez-Gonzalez, E.; 

Ruano-Miguel, Luis 

735 Carbamate 

Automated in-tube SPME-HPLC for Carbamate 

pesticide analysis Intube capillaries HPLC 

pesticides J. Chromatogr. A, (2000) 873(1), 137-147 

in water Gou, Y, Eisert, R., Pawliszyn, J. 

736 Carbamate 

In-tube SPME coupled to capillary LC for Carbamate 

analysis in water samples Intube capillaries HPLC 

pesticides Anal. Chem. 2000, 72(13), 2774-2779 

in water Gou, Y., Pawliszyn, J. 

737 Carbamate 

On-line coupling of in-tube SPME to HPLC for analysis 

of carbamates in water samples: comparison of Intube capillaries HPLC 

pesticides two commercially available autosampler 

in water J. Microcolumn Sep. (2000), 12(3), 125-134 

Gou, Y., Tragas, C., Lord, H., Pawliszyn, J. 

789 

Development of effective sample pretreatment by in-tube 

SPME and its application 

Chromatography (2000) 21(4), 276-279 

Kataoka, Hiroyuki; Wu, Jingcun; Lord, Heather L.; Pawliszyn, J. 

Intube capillaries 

Sample preparation technique using fiber-in-tube SPME 

810 Chromatography (2000), 21(4), 284-285 

Jinno, K; Kawazoe, M; Saito, Y; Hayashida, M 

571 175 references 

On-line combination of aqueous-sample preparation and 

capillary gas chromatography various references of 

review J-Chromatogr,-A. 21 May 1999; 842(1-2): 391-426 

Louter,-AJH; Vreuls,-RJJ; Brinkman,-UAT 

SPME & SPE 

552 

Solid phase microextraction turned inside out 

Che. Aust. 1999, 66(6), 9-11 

Tan, D., Marriott, P., Lee,H., Morrison, P. 

Intube capillaries 





412 

Solventless Analytical Separation Method -- 

SPME/Microcolumn LC 

Chromatography (1998), 19(2), 6063 

Jinno, K. 

HPLC 

261 Fatty acid 

Derivatization/SPME: New Approach to Polar Analytes 

Anal. Chem. 69(2): 196-205 (1997) 85µm polyacrylate GC-FID 

methyl esters Pan, L., Pawliszyn, J. 2 hr 

in air and water headspace, pH 6 

derivative: 1-pyrenyldiazomethane 

819 Formaldehyde 

Solid phase analytical derivatization: enhancement of 

sensitivity and selctivity of analysis 

J.Chromatogr. A., 843, 19-27 

Rosenfeld, J. 

On-fiber derivatization 

553 9 references 

New Gas chromatographic approach to polar compounds 

by derivatization-SPME 

Bunseki, 1999 (7), 595-597 

Takauchi, M. Japanese 

262 Alcohol and ketones 

Strategies for the Analysis of Polar Solvents in Liquid Matrixes 

Anal. Chem. 70 (1): 19-27 (1998) Nafion fiber GC-ECD 

in water Gorecki, T., Martos, P., Pawliszyn, J. 10 min 


738 Phenanthrene, PCB 

Absorption of hydrophobic compounds into the 

poly(dimethylsiloxane) coating of SPME fibers: high 7µm PDMS GC-MS 

pentachlorobenzene partition coefficients and fluorescence 10min 

in water microscopy images 

Anal. Chem. (2000) 72(3), 459-464 

Mayer, P., Vaes,W., Hermens, J. 

739 Hydrophobic 

Nonequilibrium SPME for determination of the freely 

dissolved concentration of hydrophobic organic 7µm PDMS GC-ECD 

compounds (PCBs) compounds: matrix effects and limitations 0.5-60min @ 37°C 

in water Anal. Chem 2000, 72(13), 2802-2808 

Oomen, A., Mayer, P., Tolls, J. 

263 nC8 to nC14, 

Methodological Aspects of Headspace SPME. Application 

J. High Resolut. Chromatogr. 20 (4): 217-221 (1997) various fibers GC-FID 

neat Schafer, B. Hennig, P., Engewald, W. 

Headspace SPME. Dynamics and Quantitative Analysis Before 

80°C, 5 min 

headspace 

264 Phenol, alcohols Reaching a Partition Equilibrium 85µm polyacrylate GC-MS 

in water Anal. Chem. 69 (16): 3260-3266 (1997) 1-80 min at 25°C, 

Ali, J. 1-40 min at 80°C 


413 Tetraethyllead 

SPME as a Sample Introduction Technique for Radio Frequency 

Glow Discharge MS 30µm PDMS radio frequency 

in water Anal. Commun. (1997), 34(10), 275-277 5 min glow discharge 

Gorecki, T., Belkin, M., Caruso, J., Pawliszyn, J. headspace, stirred MS 

Effect of Sample Volume on Quantitative Analysis by SPME, 

265 Part 1 - Theoretical Considerations 

Analyst (Cambridge) 122 (10): 1079-1086 (1997) 


Steady-state diffusion regime in solid-phase microextraction kinetics 

2835 Theory Anal Chim Acta 609, #1, 113-119 (Feb 18 2008) 

ter Laak, Thomas L.; van Leeuwen, Herman P.; Benhabib, Karim 





Kinetics of SPE and SPME in thin adsorbent layer with 


740 Theory saturated sorption isotherm 

J.Chromatogr. A (2000) 873(1), 39-51 

Emenov, S, Koziel, J., Pawliszyn, J. 

769 BTEX 

The use of polymeric fullerenes as a new coating for SPME 

Chromatographia (2000) 52(11/12), 803-809 GC-FID 

from water Xiao, C.; Liu, Z. ; Wang, Z.; Wu, C.; Han, H. headspace 

266 Organics 

SPME as a Tool to Determine Membrane/Water Partition 

Coefficients and Bioavailable Concentrations in vitro 85µm polyacrylate GC-FID 

in water Systems 9-17 min 

Chem. Res. Toxicol. 10 (10): 1067-1072 (1997) 

Vae, W., et al. 


267 PAHs, phenols, 

Sol-Gel Coating Technology for the Preparation of SPME Fibers 

of Enhanced Thermal Stability Solgel coating GC-FID 

anilines Anal. Chem. 69 (19): 3889-3898 (1997) 30 min 

in water Chong, S. et al. stirring 

A review on SPME- HPLC as a novel tool for the analysis of 

2231 Metallic species toxic metal ions review article HPLC 

Talanta 68 #3, 842-849 (2006) 

Kaur, Varinder; Malik, Ashok Kumar; Verma, Neelam 

2150 Organometallic 

Applications of SPME for the determination of metallic and 

organometallic species headspace GC-FID 

J. Sep. Sci., 29, #3, 333-345 (2006) 

Kaur, Varinder; Malik, Ashok Kumar; Verma, Neelam 

NaBEt4 derivatives 

A new method for simultaneous determination of Co(II), Ni(II) and Pd(II) 

2615 Co(II), Ni(II), Pd(II) as morpholine-4-carbodithioate complex by SPME-HPLC-UV system HPLC-UV 

in water Talanta 73, #3, 425-430 (Sep 30 2007) 

Kaur, Varinder; Malik, Ashok Kumar 

2491 Co(II), Ni(II), Pd(II) 

A new approach for simultaneous determination of Co(II), Ni(II), Cu(II), 

and Pd(II) using 2-thiophenaldehyde-3-thiosemicarbazone (TPTS) . PDMS fiber HPLC-UV 

in water as reagent by SPME-HPLC 

Anal Chim Acta 603, #1, 44-50 (2007 Nov 5) 

Kaur, Varinder; Aulakh, Jatinder Singh; Malik, Ashok Kumar 

TPTS derivative 

911 Organometalics 

Development of new SPME fibers by sol-gel technology 

for SPME-HPLC determination of organometals 

Analytica Chimica Acta 1999, 402(1-2) 67-69 

Gabatu, T., Sutton, K., Caruso, J. 

Solgel coatings HPLC 

741 BTEX, herbicides 

High-performance polyethylene glycol-coated SPME fibers 

using sol-gel technology PAG sol-gel fiber 

in water J. Chromatogr. A 893 (2000) 157-168 30°C, headspace 

Wang, Z., Xiao, C., Wu, C., Han, H. salt added, pH adjusted 

554 

Sol-gel method for the preparation of SPME fibers 

Anal. Lett., 1999, 32(8), 1675-1681 

Zhou, Z., Wang, Z., Qu, C., Zhan, W., Xu, Y. 

Solgel coatings 

268 BTEX 

Field-Portable SPME/Fast GC for Trace Analysis 

Field Anal. Chem. Technol. 1 (5): 277-284 (1997) 30µm PDMS GC-FID, -PID 

in soil Gorecki, T., Pawliszyn, J. 2 min, 


555 

Optimization of the SPME device design for field 

applications 

Fresenius' J. Anal. Chem. 1999, 364(7), 610-616 

Muller, L., Gorecki, T., Pawliszyn, J. 

varied coatings 





Fiber Conditioners for SPME: Design, Testing, and application 


742 Equipment design J.High Resol. Chromatogr. 2000, 23(4) 343-347 

Koziel, J., Shurmur, B., Pawliszyn, J. 


SPME- a convenient tool for the determination of 

organic pollutants in environmental matrices review article 

environmental Anal Chem (2001) 31(1), 1-18 

matrices Zygmunt, B.; Jastrzebska, A.; Namiesnik, J. 


New Trends in SPME 

Crate. Rev. Anal. Chem. 27 (2): 103-135 (1997) various fibers GC, HPLC 

air and water Eisert, R., Pawliszyn, J. and conditions 

556 Review of technique 

Solid Phase Microextraction 

TrAC, Trends Anal. Chem. (1999), 18(4), 272-282 

Prosen, H., Zupancic-Kralj, L., 

806 Review of technique 

Solid-phase microextraction (SPME) with direct detection 

a new analytical dimension 

Mitt. Lebensmittelunters. Hyg (2000) 91(6), 690-699 

Luisier, J; Villettaz, J; Azodanlou, R; Amado, R 

GC 

Optimizing SPME-GC Injections 

270 C6-C16 hydrocarbons LC-GC 15 (12): 1130-1136 (1997) 

7µm, 30µm, 100µm 

PDMS GC-FID 

in water Okeyo, P., Snow, N. 

Theoretical and Practical Comparison of SPME and 

10 min 

stirring 

403 PAHs Liquid-Liquid Extraction with Large Volume Injection for overview GC-FID 

in water Analysis of Aqueous Samples by GC 

Book chapter 

Snow, N. 

article 

Rate constants for the reactions of OH radicals with a series of 

2313 1,4-hydroxy- 1,4-hydroxyketones headspace GC-FID 

ketones J Photochemistry and Photobiology B:176 #1-3, 143-148 (2006) hydroxylamine 

Baker, Jillian; Arey, Janet; Atkinson, Roger derivatives 


Use of bench top photochemical reactor and SPME 

to measure semivolatile organic compound-hydroxyl 

in water radical rate constants 

Environ. Toxicol. Chem 2000, 19(7), 1705-1710 

Bernhard, M., Simonich., S. 

271 PCBs 

Adsorption versus Absorption of Polychlorinated Biphenyls 

onto SPME Coatings 100µm & 7µm PDMS GC-ECD 

in water Anal. Chem. 70 (9): 1866-1869 (1998) 5 hr 

Yang, Y., Hawthorne, S., Miller, D., Liu, Y., Lee, M. stirring 

744 PCBs 

Response to comments on adsorption versus absorption 

of polychlorinated biphenyls onto SPME coatings 100µm PDMS GC-ECD 

in water Anal. Chem. 72 (3): 642-6643 (2000) 5 hr 

Yang, Y., Hawthorne, S., Miller, D., Liu, Y., Lee, M. stirring 

817 Aroclor 1254 

Application of SPME-GC-MS to characterize intermediate 

in a joint solar-microbial process for total mineralization 85µm polyacrylate GC-MS 

of Aroclor 1254 40min. 

J.Chromatogr A 873 (2000) 53-61 stirring 

Rhofr, C., Hawari, J. 2pH w/H3PO4 Atomic spectrometry update. Clinical and biological materials, 

2168 Review article foods and beverages 

J Anal At Spectrom 21, #4, 439-491 (2006) 

Branch, S.; Day, .; Patriarca, M.; Taylor, A.; White, M. 


Evolution of solid phase microextracton technology 

J. Chromatogr. A 885(2000) 153-193 various 






Recent developments in headspace microextraction techniques for the 

2488 Review article analysis of environmental contaminants in different matrices 

J. Chromatogr. A 1152, #1-2, 70-96 (JUN 8 2007) 

Lambropoulou, D.; Konstantinou, Ioannis K.; Albanis, Triantafyllos A. 

2505 Off-gassing 

Thermal degradation in a trimodal poly(dimethylsiloxane) network 

studied bymultiple quantum NMR headspace GC-MS 

products from J Phys Chem B 111, #45, 12977-12984 (Nov 15 2007) 

siloxanes Alviso, C.; Chinn, S.; Giuliani, J.; Gjersing, E.; Herberg, J.; Jones, T.; 

Maxwell, R.; Pearson, M.; Wilson, T. 

2667 Standarization 

Equilibrium in-fiber standardization method for determination of 

sample volume by solid phase microextraction PDMS fiber GC-MS 

method Analyst 132, #5, 425-30 (2007 May) 

Niri, Vadoud H; Pawliszyn, Janusz 

headspace 

557 Benzene, 

Theory of analyte extraction by selected porous polymer 

SPME fibers PDMS/DVB, CW/DVB 

4-methylpentan-2one Analyst (Cambridge, UK) (1999), 124(5), 643-649 

in water Gorecki, T., Yu, Z., Pawliszyn, J. 

2390 VOCs from 

SPME-GC-TOFMS utilized for the evaluation of the new-generation 

super elastic fiber assemblies. headspace GC-TOFMS 

water, pump oil Anal. Chim. Acta 581, #2, 221-231 (2007-01-09) 

Setkova, L.; Risticevic, S.; Linton, C.; Ouyang, G. ; Bragg, L.; Pawliszyn, J. 

558 Organics 

New SPME fibers, Not only for aqueous systems 

LaborPraxis (1999), 23(3), 30-32, 34 PDMS/Carboxen/DVB 

in solvents Haag, Ingo Nafion 

573 BTEX in 

New coating surfaces of fibers for SPME 

J-Microcolumn-Sep. May 1999; 11(5): 377-383 evaluation of various 

Methanol Ligor,-M; Scibiorek,-M; Buszewski,-B coatings 

589 Coffee 

SPME application in GC/olfactometry dilution analysis 

J-Agric-Food-Chem. Apr 1999; 47(4): 1616-1618 PDMS fibers GC-FID 

sample Deibler,-KD; Acree,-TE; Lavin,-EH 

SPME with Rotation of the Microfiber 

15 min 

headspace 

355 Terbutryn Anal. Chem 1998, 70, 3981-3982 30µm PDMS GC-FID 

in water Geppert, H. 

Partitioning of Organic Chemicals to Polyacrylate-Coated SPME 

immersion 

stirring 

409 Organics Fibers: Kinetic Behavior and Quantitative Structure 85µm polyacrylate GC-FID, -ECD, 

in water Property Relationship 35 min MS 

Anal. Chem. 68: 4458-4462 (1996) immersion 

Vaes, W., Harnwijk, C., Urreatarazu, R., Verhaar, H. stirring 

pH 7.5 


Application of Isotope Dilution to Ion Trap GC-MS 

Anal. Chem 71, No. 2, Jan. 15, 1999, pg. 483-488 65µm PDMS/DVB GC-MS 

iodide in Barshick, C., Barshick, E., Walsch, E., Vance, M., Britt, P. 5 min 

soil and water immersion 

stirring 

2748 Anatoxin-a 

Improved conditions for the application of SPME prior to HPLC-FLD 

analysis of anatoxin-a. NBD-F derivative HPLC-FLD 

in water J Separation Sci. 30, #15, 2522-2528 (2007) 

Rellan, S.; Gago-Martinez, A. 

Various fibers 

Analysis of anatoxin-a in aqueous samples by SPME using on fibre 

derivitization 

974 

Anatoxin-a in aqueous 

samples J.Chromatogr. A (2002) 963(1-2), 295-302 HPLC 





Namera, A.; So, A.; Pawliiszyn, J. 


Photolysis of polychlorinated biphenyls by SPME 

987 

Polychlorinated 

biphenyls J.Chromatogr. A (2002) 963(1-2), 37-47 

Lores, M.; Llompart, M.; Gonzalez-Garcia, R.; Gonzalez-Barreiro, C.; Cela, R. 

994 Germanium 

Comparison of chloride- and hydride-generation for quantitation of germanium 

by headspace SPME inductively coupled plasma-mass spectrometry. 

Analytical and Bioananalytical Chemistry (2002) 373(8), 849-855 

Guo, X.M.; Mester, Z.; Sturgeon, r.e. 

ICP TOF MS 

Sample preparation in chromatography for long dash concentration, purification 

and filtration: guide to choice of equipment. 

995 Laboratorio 2000 (2002) 16 (6), 34-50 

Polesello, A. 

The development of selective and biocompatible coatings for solid phase 


1008 Journal of Separation Science (2003) 26 (3-4), 251-260. 

Mullett, Wayne M.; Pawliszyn, Janusz 

1010 

Rearrangement of p -menthane terpenes by Carboxen during HS-SPME. 


Zabaras, D.; Wyllie, S. G. 

75µm Carboxen GC-MS 

Headspace analysis in modern gas chromatography. 

1030 Review Trends in Analytical Chemistry (2002) 21 (9-10), 608-617. 

Snow, N. H.; Slack, G. C. 

1045 

Time-weighted average passive sampling with a Solid-Phase Microextraction 

device 


Chen, Yong; Pawliszyn, Janusz 

Various 

Research progress in solid-phase microextraction. 

1061 Review article Fenxi Kexue Xuebao (2002) 18 (5), 429-435. 

Chen, M.; Yuan, D. X.; Xu, P. X.; Chang, D. H. 

1075 

High concentration 


Extending the solid-phase microextraction technique to high analyte 

concentrations: measurements and thermodynamic analysis. 

Analytical Chemistry (2002) 74(5), 1031-1037 

Gill, K.; Brown, W. A. 

2897 Flavors from 

Interactions between flavour release and rheological properties in model 

custard desserts: 

Effect of starch concentration and milk fat headspace GC/MS 

custard desserts Food Chemistry 108, #4, 1183-1191 (JUN 15 2008) 

Kersiene, M.; Adams, An; Dubra, A. De Kimpe, N.; Leskauskaite, D. 

Properties of oregano (Origanum vulgare L.), citronella 

2309 Flavors from (Cymbopogon nardus G.) and marjoram (Majorana hortensis L.) 65µm PDMS/DVB GC/MS 

milk protein flavors encapsulated into milk protein-based matrices 85µm polyacrylate 

Food Res. Int. 39 #4, 413-425 (2006) headspace 

Baranauskiene, R.; Dewettinck, K.; Venskutonis, P.; Verhe, R. 10 min 

1102 

Static and dynamic 

sampling 

Comparison of different methods: static and dynamic headspace and solidphase 

microextraction for the measurement of interactions between milk 

proteins and flavour compounds with an application to emulsions. 


Fabre, M.; Aubry, V.; Guichard, E. 

On-site calibration method based on stepwise solid-phase microextraction 





1117 Journal of Chromatography A (2003) 999 (1-2), 43-50. 

Chen, Yong; Pawliszyn, Janusz; Xiong, Guohua 

75 um Carboxen/PDMS 

1118 

Solid-phase microextraction fibre-water distribution constants of more 

hydrophobic organic compounds and their correlations with octanol-water 

partition coefficients 


Paschke, A.; Popp, P. 

Various 

Optimization of solid-phase microextraction of volatiles. 

1134 VOCs Journal of Chromatography, A (2002) 960(1-2), 159-164 

Matisova, E.; Medved apostrophe ova, M.; Vraniakova, J.; Simon, P. 

1203 

Anodized zinc wire as a solid-phase microextraction fiber. 


Djozan, D.; Abdollahi, L. 

GC 

1229 

Monolithic silica column for in-tube solid-phase microextraction coupled to highperformance 

liquid chromatography. 


Shintani, Y.; Zhou, X. J.; Furuno, M.; Minakuchi, H.; Nakanishi, K. 

HPLC 

1230 PAH's in water 

Thin-film microextraction. 


Bruheim, I.; Liu, X. C.; Pawliszyn, J. * 

GC-MS 

Coupling solid-phase microextraction to liquid chromatography. A review. 

1245 Review Analytical and Bioanalytical Chemistry (2003) 375 (1), 73-80. 

Zambonin, C. G. 

1277 

A new solid-phase microextraction adsorbent of polyphenylethylene-butyl 

acrylate and its application. 

Fenxi Shiyanshi (2003) 22 (3, 1-4.) 

Shen, S. C.; Wang, W. B.; An, H. 

GC-FID 

1288 

Copper sulfide wire as a selective fiber in solid-phase microextraction. 


Djozan, D.; Amir-Zehni, M. 

GC-FID 

1303 

CE in a nonuniform capillary modulated by a cylindrical insert, and zonenarrowing 

effects during sample injection. 


Stoyanov, A. V.; Liu, Z.; Pawliszyn, J. * 

CE 

1304 

Styrene-butyl acrylate copolymer as solid-phase microextraction adsorbent and 

its applications. 

Sepu (2003) 21 (3), 285-287. 

Xue, H. Y.; Shen, S. C.*; Wang, W. B.; An, H. 

Styrene-butyl acrylate copolymer 

Anodized aluminium wire as a solid-phase microextraction fibre. 

Aliphatic alcohols, 

1353 BTEX Analytical Chemistry (2001) 73(16), 4054-4058. 

Djozan, D.; Assadi, Y.; Haddadi, S. H. 

GC 

Solid-phase microextraction using fused-silica fibers coated with sol-gel-derived 

hydroxy-crown ether. 

1393 Phenols Analytical Chemistry (2001) 73(11), 2429-2436. 

Zeng, Z. R.; Qiu, W. L.; Huang, Z. F. 

1433 GC tools 

Tools simplify GC analysis of trace components 

Research and Development (2001) 43(8), 36-39. 

Marsill, R. 

GC 

1492 

Field sampling with 


Solid-phase microextraction ( SPME ) for rapid field sampling and analysis by 

gas chromatography-mass spectrometry (GC-MS). 

Trends in Analytical Chemistry (2002) 21(8), 534-543 GC-MS 





Smith, Philip A.; Hall, Tara; Hook, Gary L.; Kimm, Gregory L. 


Headspace sampling: Critical part in evaluating true gas phase concentrations. 

1498 Headspace sampling Abstracts of Papers American Chemical Society (2002) 224(1-2), AGFD 72 

1515 

Zehentbauer, Gerhard N.; Eddy, Cindy L.; Pelfrey, Christa S.; Rodriguez, Pete 

A. 

Theoretical considerations on the use of solid-phase microextraction with 

complex environmental samples. 

Use of SPME with 

complex environmental Environmental Science & Technology (2002) 36(15), 3385-3392 

samples 

Zeng, Eddy Y.; Noblet, James A. 

Electrochemical control of solid phase micro-extraction: conducting polymer 

coated film material applicable for preconcentration/analysis of neutral species. 

Organometallic 

1051 arsenobetaine Talanta (2002) 58 (4), 739-745. 

Yates, B. J.; Temsamani, K. R.; Ceylan, O.; Oztemiz, S.; Gbatu, T. P.; LaRue, 

R. A.; Tamer, U.; Mark, H. B., Jr.* 

HPLC-ICP/MS 

1073 

Helical sorbent for fast sorption and desorption in solid-phase microextractiongas 

chromatographic analysis. 


Ciucanu, I. 

PDMS GC 

Systematic error in automated in-tube solid-phase microextraction 

1078 Journal of Chromatography A (2003) 995 (1-2), 1-10. 

Raghani, Anil R.; Schultz, Kristin N. 

Flow-sampling system for solid-phase microextraction in situ. 

1097 Fenxi Huaxue (2002) 30 (11), 1394-1398. 

Xu, D. Y.; Liu, M.; Liang, Y. L.; Liu, H. W.; Yin, B. Z.* 

Physico-chemical approach to study organotin sorption-desorption during solidphase 


1115 Organotin Journal of Chromatography A (2003) 999 (1-2), 61-70. 

Aguerre, Sandrine; Lespes, Gaetane; Potin-Gautier, Martine 

1124 

High extraction efficiency solid-phase microextraction fibers coated with open 

crown ether stationary phase using sol-gel technique 

Analytica Chimica Acta (2003) 486 (1), 63-72. 

Yun, Lei 

Various 

1125 

A gas sample pre-concentration device based on solid phase microextraction 

(SPME) and temperature programmed desorption (TPD) 

Instrumentation Science and Technology (2003) 31 (2), 155-164. 

Basile, Franco 

Various 

1136 Ehtylene oxide 

Determination of ethylene oxide by solid-phase microextraction device with onfiber 

derivatization. 


Tsai, S. W.; Wu, K. K. 

Carboxen/PDMS GC-MS 

1137 Amines 

Modified copper wire as solid-phase microextraction fibre, selective extraction of 

some amines. 


Djozan, D.; Assadi, Y.; Karim-Nezhad, G. 

GC 

1143 

Modified headspace-SPME-GC device for sampling volatile compounds in 

acidic medium 


Araujo, W.A.; Cappelaro, E.A.; Lacerda, C.A.; Lancas, Fernando M. 

GC-FPD 

Hydroxyfullerene as a novel coating for solid-phase microextraction fibre with solgel 

technology. 





1157 Journal of Chromatography, A (2002) 978 (1-2), 37-48. 

Yu, J. X.; Dong, L.; Wu, C. Y.*; Wu, L.; Xing, J. 

GC-ECD 

1212 

Novel benzo-15-crown-5 sol-gel coating for solid-phase microextraction 


Peng, Jiagang; Wang, Danhua; Wu, Caiying; Xing, Jun 

GC 

New high-performance cryofocalizer injector for in-tube solid-phase 

microextraction and headspace capillary gas chromatographic applications. 

1214 Journal of Chromatography, A (2003) 985 (1-2), 67-78. 

Nardi, L. 

Electrochemically assisted solid phase micro-extraction using L-dopa imprinted 

conducting polymer electrode fibers: Structural aspects. 

1247 Abstracts of Papers American Chemical Society (2003) 225 (1-2), anyl 98. 

Schmiesing, Carla S.; Brooks, Elwood E.; Galal, Ahmed; LaRue, Rebecca A.; 

Mark, Harry B., Jr.; Temsamani, Khalid R. 

1259 

Patterns in the precision of quantitative data from multicomponent gas 

chromatographic or gas chromatographic-mass spectrometric analysis 


Garcia, M.A.; Martinez-Castro, I.; Sanz, J.; Soria, A.C. 

GC-MS 

Solid-phase microextraction from small volumes of sample in a glass capillary. 

1270 Journal of Chromatography, A (2003) 988 (1), 25-32. 

Zhu, P. L.; Liu, C. L.; Liu, M. C. 

Hydroxycarbonyl products of the reactions of selected diols with the OH radical 

1281 Journal of Physical Chemistry A (2003) 107 (32), 6200-6205. 

Arey, Janet; Atkinson, Roger; Bethel, Heidi L. 

GC-FID 

1329 

A comparison of alkyl derivatization methods for speciation of mercury based on 

solid phase microextraction gas chromatography with furnace atomization 

plasma emission spectrometry detection 

Journal of Analytical Atomic Spectrometry (2003) 18 (8), 902-909. PDMS GC-FAPES 

Grinberg, P.; Campos, R. C.; Mester, Z.; Sturgeon, R. E.* 

Spectroscopic Studies of Sorbing Fibers Using Combined Elements with 

Multiple Attenuated Total Internal Reflection 

1332 Optics and Spectroscopy (2000) 89 (3), 413-417. 

Bobasheva, A.S.; Enikeeva, A.G.; Malinin, I.V.; Mamedov, R.K.; Stolyarov, 

B.V.; Volchek, B.Z. 

Negligible depletion solid-phase microextraction with radiolabeled analytes to 

study free concentrations and protein binding: An example with /sup3/H 

estradiol 

1337 Analytical Chemistry (2003) 74 (23), 5993-5997. 

Algra, Jon; Heringa, Minne B.; Hermenst, Joop L. M.; Pastor, Dolors; Vaes, 

Wouter H. J. 

1341 

Solid phase micro-extraction in a miniature ion-trap mass spectrometer. 

Analyst (2003) 128 (9), 1119-1122. PDMS 

Riter, L. S.; Meurer, E. C.; Cotte-Rodriguez, I.; Eberlin, M. N.; Cooks, R. G.* 


Solid-phase microextraction of monocyclic aromatic amines using novel fibres 

coated with crown ether. 

Journal of Chromatography, A (2001) 934(1-2), 51-57. 

Zeng, Z. R.; Qiu, W. L.; Yang, M.; Wei, X. A.; Huang, Z. F.; Li, F. 

Various GC 

2664 Nitrate esters 

Determination of nitrate esters in water samples: comparison of 

efficiency of solid-phase extraction and SPME 65µm PDMS/DVB HPLC-UV 

in water J Chromatogr A 1174, #1/2, 13-19 (2007) 





Jezova, V.; Skladal, J.; Eisner, A.; Bajerova, P.; Ventura, K. 

Pedersen-Bjergaard, S. 


Measurement of octanol-air partition coefficients using solid-phase 

microextraction ( SPME ): Application to hydroxy alkyl nitrates. 

1400 Hydroxy alkyl nitrates. Atmospheric Environment (2001) 35(33), 5843-5854. 

Rudich, Yinon; Shragina, Lea; Treves, Keren 

Application of low-temperature glassy carbon films in solid-phase 


1429 Aromatic hydrocarbons Anal. Chem. (2001) 73(24), 5841-5851. GC-FID 

Giardina, M.; Olesik, S.V. 

1430 

Atomic spectrometry update. Industrial analysis: Metals, chemicals and 

advanced materials 

J Anal At Spectrom (2001) 16(12), 1446-1469. 

Fairman, B.; Goodall, P.; Hinds, M.W.; Nelms, S.M.; Penny, D.M. 

ICP-MS 

1435 VOC's 

Application of the polysilicone fullerene coating for solid-phase microextraction 

in the determination of semi-volatile compounds 

Journal of Chromatography A (2001) 927(1-2), 121-130. 

Han, S.; Wang, Z.; Wu, C.; Xiao, C.; Xing, J. 

PDMS GC-FID 

1507 

Aliphatic carboxylic 

acids 

Solid-phase microextraction and on-line methylation gas chromatography for 

aliphatic carboxylic acids. 

Analytical and Bioanalytical Chemistry (2002) 373(1-2), 64-69 Various fibers compared GC-MS 

Danielson, Neil D.; Cho, Seong R.; Liu, Yaqian 

Effect of masking agents on the emission of VOCs from asphalt. 

1502 VOCs from asphalt Abstracts of Papers American Chemical Society (2002) 223(1-2), CHED 451 

Smith, Crystal; Hardee, John 

Determination of impurities in industrial caprolactam produced 

2213 Impurities in from toluene by SPME and GC-MS GC-MS 

caprolactam J. Appl. Polym. Sci.100 #4, 3141-3144 (2006) 

Li, Na; Zou, Jiankai 

Capillary extractors for left dbl quote negligible depletion right dbl quote 

sampling of benzene, toluene, ethylbenzene and xylenes by in-tube solid-phase 



Nardi, L. 

1099 

Method for determining chlorohydrocarbon residues in dry cleaning fabrics with 


Chlorohydrocarbon in 

dry cleaning fabrics. Sepu (2002) 20 (6), 573-576. 

Chen, J. 


1257 Formic acid 

Quantitation of formate by solid-phase microextraction and gas chromatography 

mass spectrometry utilizing a " 13 C"formate internal standard. 


Kim, J. K.; Shiraishi, T.; Fukusaki, E.; Kobayashi, A. * 

GC-EIMS 

Before the injection - Modern methods of sample preparation for separation 

Review 

techniques 

1119 Review article Journal of Chromatography A (2003) 1000 (1-2), 3-27. 

Smith, Roger M. 

Derivatization - solid-phase microextraction techniques and its application to 

analysis of organic compounds. 

1269 Review Fenxi Huaxue (2003) 31 (4), 496-500. 

Luan, T. G.; Zhang, Z. X. 





A field guide to instrumentation: modern sample preparation methodology. 1. 

Automated SPE. 

1371 Review Inside Laboratory Management (2001) 5(5), 14-18. 

Sherma, J.; Larkin, J. D.; Larkin, F. H. 

A new thermal desorption SPME system for hand-held 

2310 volatile organic ion mobility spectrometry headspace GC/MS 

Anal. Chim. Acta 559 #2, 159-165 (2006) 

Grigoriev, A.; Liu, Xinyu; Lynds, Paul; Nacson, S.; Pawliszyn, J. 

Thermal desorption SPME inlet for differential 

2124 BTX solvents mobility spectrometry differential mobility 

in water Appl Spectrosc, 59, #6, 754-762 spectrometry 

De Harrington, Peter B.; Rainsberg, Matthew R. 

A review on SPME-HPLC analysis of pesticides 

2125 pesticides Crit. Rev. Anal. Chem., 35, #1,71-85 in-tube HPLC 

various Aulakh, J.; Kaur, V; Malik, A.; Schmitt-Kopplin, P 

matrices 

Kinetic Calibration Using Dominant Pre-equilibrium Desorption for 

2399 PAH standards On-Site and in Vivo Sampling by Solid-Phase Microextractio 

in water Anal Chem 80. #2, 481-90 (2008 Jan 15) 

Zhou, Simon Ningsun; Zhao, Wennan; Pawliszyn, Janusz 

On-fiber standardization technique for solid-coated SPME 

2427 Carbamate Anal. Chem. 79, #3, 1221-1230 (2007-02-01) 50µm Carbowax/TPR, 

pesticide Zhou, S. N. S.; Zhang, X.; Ouyang, G. F.; Es-haghi, A.; Pawliszyn, J. 

2398 Pre-loaded 

Preparation and application of in-fibre internal standardization SPME 

Analyst (Cambridge, U. K.) 132, #3, 256-261 (2007-03-15) headspace GC 

standard on fiber Zhao, W. N.; Ouyang, G. F.; Pawliszyn, J. 

Flow-through system for the generation of standard aqueous solution 

2183 PAH standards of polycyclic aromatic hydrocarbons 

in water J. Chromatogr. A, 1105, #1-2,176-179 (2006) 

Chen, Yong; Ouyang, Gangfeng; Pawliszyn, Janusz 

System for the generation of standard gas mixtures 

2126 Volatiles & of volatile and semi-volatile organic compounds fo headspace GC 

seimivolatiles calibrations of SPME and other sampling devices 

in air J Chromatogr A, 1025, #1, 3-9 

Koziel, Jacek; Martos, Perry.; Pawliszyn, J 

Origin of carbons in sulfur-containing aroma compounds from the 

2191 Sulfur compd Maillard reaction of xylose, cysteine and thiamine headspace GC-MS 

from Mailard Food Sci. Technol. 40, #8, 1309-1315 (Oct. 2007) 

reaction Cerny, C. 

Small alpha -Mercaptoketone formation during the 

2127 Sulfur compd Maillard reaction of cysteine and C13 ribose headspace GC-MS 

from Mailard J Agrl Food Chem, 52, #4, 958-961 

reaction Cerny, C.; Davidek, T. * 

Role of the solvent glycerol in the Maillard reaction of D-fructose 

2163 Volatiles from and L-alanine headspace GC-MS 

D-fructose and J Ag Food Chem, 54, #2, 574-577 (2006) 130 C 

L-alanine Cerny, Christoph; Guntz-Dubini, Renee 

SPME based on polypyrrole films with different counter ions 

2128 Review Anal. Chim. Acta, 520, #1-2, 257-264 polypyrrole 

Pawliszyn, Janusz; Wu, Jingcun 

Coupling of dynamic headspace sampling and SPME 

2129 Review Chromatographia, 60, #11-12, 687-691 headspace GC 

Silva, R. C.; Aguiar, P. M. S.; Augusto, F. * 

Extraction techniques 

2130 organics from Anal. Bioanal. Chem., 372, #1, 39-40 comparison w/SFE, GC 

water Camel, Valerie microwave, pressure 

solvent 

Methyl benzoate as a marker for the detection of mold in indoor 





2188 Methyl benzoate building materials headspace GC-MS 

from J. Sep. Sci., 28, #18, 2517-2525 (2005) 

mold samples Wady, Loay; Parkinson, Don-Roger; Pawliszyn, Janusz 

Study on the method of SPME-GC-MS to quantify 

2131 Odors from organic gas component. GC/MS 

aging material Zhipu Xuebao, 25, Suppl, 97-98 

Yang, X. L.; Qin, J. Y.; Kang, B. 

Solid-phase microextraction field sampler 

2132 Review Anal. Chem., 76, #22, 6823-6828 field sampling 


Kinetics and the on-site application of standards in a 

2133 BTEX in solid-phase microextration fiber preloaded fiber GC 

water Anal. Chem., 76, #19, 5807-5815 


Modelling SPME data from kinetic measurements in 

2134 Review complex samples. GC 

Analyst (Cambridge, U. K.), 129, #11, 1137-1142 

van Eijkeren, J. C. H.; Heringa, M. B.; Hermens, J. L. M. 

Modern extraction techniques. 

2135 Review Analytical Chemistry, 76, #16, 4659-4664 GC 

Raynie, D. E. 

Derivatization and solid-phase microextraction 

2136 Polar analytes TrAC Trends Anal. Chem., 23, #8, 553-561 review article GC 

Martinez, Jairo R.; Stashenko, Elena E. 

The relationship between elimination rates and 

2137 Review partition coefficients GC 

Chemosphere, 57, #8, 745-753 

Jager, T.; Kooi, B.W.; Kooijman, S.A.L.M. 

SPME coupled to GC-MS for determining PAH-micelle 

2138 PAHs partition coefficients. GC-MS 

Anal Chem, 76, #15, 4572-4578 

Pino, V.; Ayala, J. H.; Gonzalez, V.; Afonso, A. 

Equilibrium in-fibre standardisation technique for SPME 

2139 Aromatic J. Chromatogr. A, 1072, #1, 13-17 headspace GC-FID 

standard on fiber Chen, Y; O'Reilly, J; Pawliszyn, Janusz; Wang, Y 

Coupling spme to liquid chromatography. A review 

2140 Review Anal. Bioanal. Chem., 375, #1,73-80 HPLC 

Zambonin, Carlo G. 

Approaches for coupling SPME to nanospray 

2141 Peptides from J. Chromatogr. A, 1067, #1-2, 197-205 Restrictive access MS-nanospray 

tryptic digests Dartiguenave, C; Gu, Yu; Lubda, D; Musteata, F; coated fibers 

Pawliszyn, Janusz; Waldron, Karen; Walles, Markus 

Experimental determination and calculation of 

2142 Terpene & distribution coefficients between air and fiber with PDMS PDMS fibers GC 

ketones in coating for some groups of organic compounds 

air J. Chromatogr. A, 1077, #2, 195-201 

Isidorov, Valery A.; Vinogorova, Vera T. 

A survey on high-concentration-capability headspace 

2143 Review of sampling techniques in the analysis of flavors headspace GC-MS 

extraction and fragrances. 

techniques J Chrom Sci, 42, #8, 402-409 

Bicchi, C.; Cordero, C.; Rubiolo, P. 


SPME Literature 

Literature 

No. Title 

Biochemical / Food and Beverage 

T195869 Solid Phase Microextraction: Solventless Sample Preparation for Monitoring Flavor Compounds 

by Capillary Gas Chromatography (AYM) 

T196901 Solid Phase Microextraction/Capillary GC Analysis of Drugs, Alcohols, and Organic Solvents in Biological Fluids (AYY) 

T396110 SPME Reduces Extraction Time in HPLC Analyses of Food Antioxidants and Preservatives 

T397140 Analysis of Fat Soluble Vitamins from Tablets, Using SPME/HPLC (BKK) 

T398147 

Pharmaceutical 

Solid Phase Microextraction of Odors in Drinking Water, for Analysis by GC-MS (BRG) 

T394062 

Forensic 

Monitor Organic Volatile Impurities (OVIs) in Pharmaceutical Products, Using Solid Phase Microextraction/Capillary GC (AQX) 

T196901 Solid Phase Microextraction/Capillary GC Analysis of Drugs, Alcohols, and Organic Solvents in Biological Fluids (AYY) 

T198922 SPME/GC for Forensic Applications: Explosives, Fire Debris, and Drugs of Abuse (BQS) 

T394061 Solid Phase Microextraction/Capillary GC: Rapid, Sensitive Detection of Gasoline in Fire Debris (AQW) 

T396098 

Environmental 

SPME / HPLC Interface Combines Fast Sample Extraction with Efficient Analysis for Explosives (ASE) 

T394006 Solid Phase Microextraction of Semivolatile Compounds in US EPA Method 625 (AOH) 

T394011 Solid Phase Microextraction of Volatile Compounds in US EPA Method 524.4 (AOM) 

T394017 Polyacrylate Film Fiber for Solid Phase Microextraction of Polar Semivolatiles from Water (AOS) 

T394056 Fast Analysis of Volatile Organic Compounds by Solid Phase Microextraction/Capillary GC (AQL) 

T394058 Fast Screening for Chlorinated Pesticides by Solid Phase Microextraction/Capillary GC (AQN) 

T395081 Monitor BTEX Compounds and Fuels in Water, Using Solid Phase Microextraction and Capillary GC (ARO) 

T395085 Solid Phase Microextraction/Capillary GC Analysis of Nitrogen-Containing Herbicides in Water (ARS) 

T396094 Solid Phase Microextraction of Organophosphate Insecticides and Analysis by Capillary GC/MS (ASB) 

T396099 SPME / HPLC: A Rapid and Sensitive Analysis of Polynuclear Aromatic Hydrocarbons in Water (ASF) 

T396106 Analysis of Surfactants in Water by SPME/HPLC 

T397121 Solid Phase Microextraction for HPLC Analysis of Carbamate and Urea Pesticides (BGU) 

T397141 Air Sampling of VOCs Using SPME for Analysis by Capillary GC (BKF) 

T397143 Field Sampling for Pesticides, Using Solid Phase Microextraction/Capillary GC (BJT) 

T398147 Solid Phase Microextraction of Odors in Drinking Water, for Analysis by GC/MS (BRG) 

Lab Hints and Selection Guides 

T101928 SPME Troubleshooting Guide (EDV) 

T101929 Guide to Quantitation with SPME (EDW) 

T198923 Solid Phase Microextraction: Theory and Optimization of Conditions (BQT) 

T396098 SPME / HPLC Interface Combines Fast Sample Extraction with Efficient Analysis for Explosives (ASE) 

T496037 Solid Phase Microextraction Sampling Stand (AWS) 

T496049 SPME / HPLC Interface (AWV) 

T497105 SPME Portable Field Sampler with Carboxen/PDMS Fiber (BIZ) 

T497174 SPME Portable Field Sampler with 100 µm PDMS Fiber (BKL) 

Free Supelco Literature 

To obtain any of the free literature listed above, to see a complete list of Supelco literature, or to see any new Supelco products, use one 

of the following methods. Some literature is available electronically only. 

● Download from Our World Wide Web Site 

sigma-aldrich.com/supelco 

● Contact Our Order Processing Department 

Phone 800-247-6628 (US only) or 814-359-3441 

Fax 800-447-3044 (US only) or 814-359-3044 

231

Ordering Information: 

Sampling and Analysis Mode 

Fiber Core/ Hub Manual Holder Autosampler 

Assembly Type Description (w/ spring) (w/o spring) 

23 Ga* 24 Ga* 23 Ga* 24 Ga* 

Carboxen/Polydimethylsiloxane 

75 µm Carboxen/PDMS Fused Silica/SS Black/plain 57344-U 57318 57343-U 57319 

85 µm Carboxen/PDMS Metal alloy/Metal alloy** Lt. Blue/plain 57906-U 

85 µm Carboxen/PDMS Stableflex/SS Lt. Blue/plain 57334-U 57295-U 57335-U 

Polydimethylsiloxane (PDMS) 

7 µm PDMS Metal alloy/Metal alloy** Green/plain 57919-U 

7 µm PDMS Fused Silica/SS Green/plain 57302 57291-U 57303 

30 µm PDMS Metal alloy/Metal alloy** Yellow/plain 57922-U 

30 µm PDMS Fused Silica/SS Yellow/plain 57308 57289-U 57309 

100 µm PDMS Metal alloy/Metal alloy** Red/plain 57298-U 

100 µm PDMS Fused Silica/SS Red/plain 57342-U 57300-U 57341-U 57301 

Polydimethylsiloxane/Divinylbenzene (PDMS/DVB) 

60 µm PDMS/DVB Stableflex/SS Brown/notched 57317 

65 µm PDMS/DVB Metal alloy/Metal alloy** Blue/plain 57902-U 

65 µm PDMS/DVB Fused Silica/SS Blue/plain 57346-U 57310-U 57345-U 57311 

65 µm PDMS/DVB Stableflex/SS Pink/plain 57326-U 57293-U 57327-U 

Polyacrylate 

85 µm Polyacrylate Fused Silica/SS White/plain 57304 57294-U 57305 

Divinylbenzene/Carboxen/Polydimethylsiloxane 

50/30 µm DVB/CAR/PDMS Metal alloy/Metal alloy (1 cm)** Gray/plain 57912-U 

50/30 µm DVB/CAR/PDMS Metal alloy/Metal alloy (2 cm)** Gray/notched 57914-U 

50/30 µm DVB/CAR/PDMS Stableflex/SS (1 cm) Gray/plain 57328-U 57298-U 57329-U 

50/30 µm DVB/CAR/PDMS Stableflex/SS (2 cm) Gray/notched 57348-U 57299-U 

Polyethylene Glycol (PEG) 

60 µm PEG 

* Ga - Needle gauge. 

Metal alloy/SS Purple/plain 57355-U 57354-U 

** Metal alloy fiber assemblies are provided 1/pk. 

Fiber Assortment Kits 

Automated/HPLC 

Name Description of Fiber Coatings (1 ea.) Recommended Use Manual Std. 23 Ga. 

Needle Needle 

Kit # 1 85 µm polyacrylate, 100 µm PDMS, 7 µm PDMS GC 57306 57307 57285-U 

Kit # 2 75 µm Carboxen/PDMS, 65 µm PDMS/DVB, 85 µm polyacrylate GC 57320-U 57321-U 57286-U 

Kit # 3 60 µm PDMS/DVB, 85 µm polyacrylate, 100 µm PDMS HPLC – 57323-U – 

Kit # 4 100 µm PDMS, 65 µm PDMS/DVB, 75 µm Carboxen/PDMS GC 57324-U 57325-U 57287-U 

StableFlex Kit 65 µm PDMS/DVB, 50/30 µm DVB/Carboxen/PDMS GC 57550-U 57551-U – 

Kit # 5 100 µm PDMS, 65 µm PDMS/DVB, 85 µm Carboxen/PDMS GC 57324-U 57325-U 57287-U 

50/30 µm DVB/Carboxen/PDMS GC 57362-U 

SPME Fiber Holders 

The holder protects the coated fiber, and controls exposure of the 

fiber during analyte adsorption and desorption. The holder is 

reusable indefinitely and accepts the replaceable fiber assembly. 

First time users must order both a holder and a fiber assembly. 

Fiber Holder for Manual Sampling 

An adjustable depth guide positions the fiber for sampling and for 

correct placement in the heated zone of the GC injection port. The 

fiber can be locked in the exposed position. 

Fiber Holder for Automated Sampling or HPLC Analysis 

Use this fiber holder with a Varian 8100/8200 AutoSampler or with 

our SPME/HPLC interface. An SPME upgrade kit is necessary for 

operation with the Varian AutoSampler – contact Varian Instrument 

Division for information concerning system requirements. 

232 

Automated or HPLC Holder 

Manual Holder 

995-0125 

Fiber Holder for CTC, Gerstel, and Thermo Autosamplers ▲▲▲▲▲ 

Use this holder with SPME fiber assemblies that are designed for 

automated sampling. 

Description Cat. No. 

Fiber Holder 

For Manual Sampling 57330-U 

For Varian Autosampler or HPLC Analysis 57331 

For CTC, Gerstel, and Thermo Autosamplers 57347-U 

▲ Autosamplers distributed by Varian, Leap, Gerstel, and Thermo.

World Headquarters 

3050 Spruce St., St. Louis, MO 63103 

(314) 771-5765 


Ordering/Customer Service 

To place an order or to inquire about an existing order. 24 hours a day, 7 days a week 

Phone ......................................................................................... 800-247-6628 

Phone ......................................................................................... 800-325-3010 

Fax ................................................................................................ 800-325-5052 

Address .................................................................. Sigma-Aldrich, PO Box 14508 

St. Loius, MO 63178 USA 

Technical Service 

To discuss applications or product-specific questions. 

Monday - Thursday, 8:00am - 8:00pm, EST; Friday, 8:00am - 6:00pm, EST 

Phone ......................................................................................... 800-359-3041 

Phone ......................................................................................... 814-359-3041 

Fax .............................................................................................. 800-359-3044 

Fax .............................................................................................. 814-359-5468 

E-mail ............................................................................ techservice@sial.com 

Custom Products/Quotations 

Gas chromatography, liquid chromatography, sample preparation, chemical standards, 

and reagents 

Phone ........................................................................................... 800-247-6628 

Phone ........................................................................................... 814-359-3441 

Fax ................................................................................................ 800-447-3044 

E-mail ............................................................................. techservice@sial.com 

Bid Requests/Quotations 

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Fax .............................................................................................. 800-554-6541 

Fax ................................................................................................ 314-771-5757 

General Business 

Monday - Friday, 8:00am - 5:00pm, EST 

Phone ......................................................................................... 814-359-3441 

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Fax .............................................................................................. 814-359-5459 

Remittance 

East of the Mississippi: Sigma-Aldrich Inc., C/O Wachovia Bank, N/A 

PO Box 932594, Altanta, GA 31193-2594 

West of the Mississippi: Sigma-Aldrich Inc., C/O Wachovia Bank, N/A 

PO Box 951524, Dallas, TX 75395-1524 

Order/Customer Service (800) 325-3010 Fax (800) 325-5052 

Technical Service (800) 325-5832 sigma-aldrich.com/techservice 

Development/Bulk Manufacturing Inquiries (800) 244-1173 

©2008 Sigma-Aldrich Co. All rights reserved. SIGMA, , SAFC, , SIGMA-ALDRICH, ALDRICH, , FLUKA, , and SUPELCO, are trademarks belonging to Sigma-Aldrich Co. 

and its affiliate Sigma-Aldrich Biotechnology, L.P. Sigma brand products are sold through Sigma-Aldrich, Inc. Sigma-Aldrich, Inc. warrants that its products conform to the information 

contained in this and other Sigma-Aldrich publications. Purchaser must determine the suitability of the product(s) for their particular use. Additional terms and conditions may apply. 

Please see reverse side of the invoice or packing slip. 

T199925F 

CJQ 

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Success through Leadership 

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SPME Applications Guide - Overbrook Scientific

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